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Knowlegde required for
routine mode
Habilitation
1) Put the spinner onto the calibrator
2) Insert the sample through the
spinner until it touches the bottom
Sample Calibration
Connection to your laboratory
Double-click on the name of your
laboratory
Automatic mode analyses
Check in the « Option » tab that the
« Manual Lock/Shim » mode is not
crossed
Insertion of the sample
Click on the [ Inject/Eject ] icon
Insertion of the sample
Click on [ Insert New Sample ]
Insertion of the sample
1) Wait until the « Insert Sample » instruction is
displayed and then leave your sample on the
gaz flow
2) Click on [ OK ] as soon as your sample is left
Sample Identification
1) Write the name of your sample in the
field « name » (no space, + or * in
the sample name)
2) State the rank of the current
experiment in the field « N° »
3) Click on [ Continue ]
Description of the experiment
Choose your solvent from the
« solvent» list
Description of the experiment
1) Select experiment you want to run
from the « Experiment » list
2) Click on [ OK ] or [ Continue ]
Start experiment
Click on [ START ]
Steps of the analysis
You can be aware of the current task of the spectrometer by
looking up in the window: First ATMA, LOCK, SHIM, Receiver
gain calculation, then data acquisition, and finally data
processing
During acquisition
-Click on [ Spectrum ] to view the
spectrum of your sample after the
number of scans done so far
-Click on [ Halt ] if you wish to stop
the experiment and keep the data built
up until then
Run a second analysis
-Click on [ Use Same/Continue ] to run a
second analysis if you are satisfied by lock
and shim from the 1rst experiement
-In the case of a second sample to analyse
or of a problem with lock/shim process,
click on [ Insert New Sample ]
Sample recovery
1) Click on [ Eject + Terminate ] at the
end of your analyses
2) Wait for the authorization message
« Remove Sample » before taking it back
3) Click on [ OK ]

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Habilitation routine english

  • 1. Knowlegde required for routine mode Habilitation
  • 2. 1) Put the spinner onto the calibrator 2) Insert the sample through the spinner until it touches the bottom Sample Calibration
  • 3. Connection to your laboratory Double-click on the name of your laboratory
  • 4. Automatic mode analyses Check in the « Option » tab that the « Manual Lock/Shim » mode is not crossed
  • 5. Insertion of the sample Click on the [ Inject/Eject ] icon
  • 6. Insertion of the sample Click on [ Insert New Sample ]
  • 7. Insertion of the sample 1) Wait until the « Insert Sample » instruction is displayed and then leave your sample on the gaz flow 2) Click on [ OK ] as soon as your sample is left
  • 8. Sample Identification 1) Write the name of your sample in the field « name » (no space, + or * in the sample name) 2) State the rank of the current experiment in the field « N° » 3) Click on [ Continue ]
  • 9. Description of the experiment Choose your solvent from the « solvent» list
  • 10. Description of the experiment 1) Select experiment you want to run from the « Experiment » list 2) Click on [ OK ] or [ Continue ]
  • 12. Steps of the analysis You can be aware of the current task of the spectrometer by looking up in the window: First ATMA, LOCK, SHIM, Receiver gain calculation, then data acquisition, and finally data processing
  • 13. During acquisition -Click on [ Spectrum ] to view the spectrum of your sample after the number of scans done so far -Click on [ Halt ] if you wish to stop the experiment and keep the data built up until then
  • 14. Run a second analysis -Click on [ Use Same/Continue ] to run a second analysis if you are satisfied by lock and shim from the 1rst experiement -In the case of a second sample to analyse or of a problem with lock/shim process, click on [ Insert New Sample ]
  • 15. Sample recovery 1) Click on [ Eject + Terminate ] at the end of your analyses 2) Wait for the authorization message « Remove Sample » before taking it back 3) Click on [ OK ]