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Using A Wireless Sensor Network to
    monitor Fenton!s Reaction for Water
                Purification

Mid Term Presentation
Yuen, Wan-Choi Rainbow
Supervisor: Dr. Kim Lau
Overview of My project

! Topic:
  quot; Monitoring Fenton!s reaction by using a
    wireless sensor network
    ! Color of the solution changes from dark to clear

! Application:
  quot; In-house Water purification system
Fenton!s Reaction
! Chemicals used:
 ! Ferric Sulfate Heptahydrate (Catalyst) – Fe2SO4 +7H2O
 ! Hydrogen Peroxide (Reactant) – H2O2
 ! Aniline Blue (Dye – Pollutant)
! pH value should be around 3-4 to keep the reaction
   work
  ! Fe2+ + H2O2 # Fe(OH)3
! Reaction equation:
  ! Fe2+ + H2O2 # Fe3+ .OH + OH-
  ! Fe3+ + H2O2 # Fe2+ + OOH_ + H+
quot; Fe2+ is the catalyst, Fe3+ can be used as the catalyst
   too, therefore, no need to add extra Ferric Sulfate in
   2nd run
quot; .OH (Hydroxyl Radical) is the chemical which oxidizes
   any Pollutants in water
Experimental equipment set-up:
How the sensor senses the light?
 How the Internal sensor
    senses the light




                           How the external sensor senses the
                                         light?
                  !part
 LED     Fluid                                      Sitting
        Channel                                     Lamp



                                                     External
                                                     (upper)

                           External
                           (Lower)                  Beaker
Process


         Processing




Before
                       After
Result - µPart analysis




                            Ferric Sulfate    Hydrogen
                 chemical                                   Aniline Blue (g)
                            Heptaoxide (g)   peroxide (g)
Date
                                0.02            0.51             0.03
    21 Jun 07 (1st run)
                                  -              0.3             0.06
   21 Jun 07 (2nd run)
Work in progress




•Using solidwork to
draw the box

•Using 3D printer
to make the box

•Using milling
machine to mill the
                             Amount of chemical adjustment (optimizing)
hold in fluid
channel
                       Ferric Sulfate         Hydrogen
                                                                Aniline Blue (g)
                      Heptahydrate (g)       peroxide (g)
                            0.01                 0.26                 0.05
Future Work

! Investigate issues with a larger sensor
  network
  quot; Implement 7 sensor nodes
  quot; Radio interference
  quot; Node range (< 30m in-house)
! Apply to larger sample (fish tank)
! Transfer of the sensor network from the
  lab to real-life applications
Project                     Set Up
                          Experiment

Procedure
                            Optimize
      Adjust Suitable                       Collaboration of
                          the chemicals
       Environment                            equipment
                               used




                          Adding more
                            sensors




                        Adjust the sensor
                         network to work
                           Corporately




                            Apply the
                          process into
                           the real life
Experiment Procedure                        B
                          A
     Start
                                        Add Aniline
                                       blue (Dye) and
                   Place the sensor
    Weigh out                               start
                   holder and check
   appropriate                           monitoring
                    the LED light is
    amount of             on
    chemicals
                                        Add Ferric
                                         Sulfate
                    Check that the
 Place the water                       Heptahydrate
                      base station
  pump inside      receives signals
     Beaker         from all sensor
                                           Keep
                                       monitoring for
                                        at least 30
  Fill in 1500ml       Place the
                                         minutes
       water          camera on
                      appropriate
                     location and
                                       Add Hydrogen
 Adjust pH value    check that the
                                         Peroxide
     to “3”          base station
                   receives image
   Install upart                           Keep
 sensor nodes to                       monitoring the
                    Switch on the
   appropriate                         color change
                    sitting Lamp
     locations

                                            End
                         B
       A

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Using A Wireless Sensor Network to Monitor Fenton’s Reaction (midterm)

  • 1. Using A Wireless Sensor Network to monitor Fenton!s Reaction for Water Purification Mid Term Presentation Yuen, Wan-Choi Rainbow Supervisor: Dr. Kim Lau
  • 2. Overview of My project ! Topic: quot; Monitoring Fenton!s reaction by using a wireless sensor network ! Color of the solution changes from dark to clear ! Application: quot; In-house Water purification system
  • 3. Fenton!s Reaction ! Chemicals used: ! Ferric Sulfate Heptahydrate (Catalyst) – Fe2SO4 +7H2O ! Hydrogen Peroxide (Reactant) – H2O2 ! Aniline Blue (Dye – Pollutant) ! pH value should be around 3-4 to keep the reaction work ! Fe2+ + H2O2 # Fe(OH)3 ! Reaction equation: ! Fe2+ + H2O2 # Fe3+ .OH + OH- ! Fe3+ + H2O2 # Fe2+ + OOH_ + H+ quot; Fe2+ is the catalyst, Fe3+ can be used as the catalyst too, therefore, no need to add extra Ferric Sulfate in 2nd run quot; .OH (Hydroxyl Radical) is the chemical which oxidizes any Pollutants in water
  • 5. How the sensor senses the light? How the Internal sensor senses the light How the external sensor senses the light? !part LED Fluid Sitting Channel Lamp External (upper) External (Lower) Beaker
  • 6. Process Processing Before After
  • 7. Result - µPart analysis Ferric Sulfate Hydrogen chemical Aniline Blue (g) Heptaoxide (g) peroxide (g) Date 0.02 0.51 0.03 21 Jun 07 (1st run) - 0.3 0.06 21 Jun 07 (2nd run)
  • 8.
  • 9. Work in progress •Using solidwork to draw the box •Using 3D printer to make the box •Using milling machine to mill the Amount of chemical adjustment (optimizing) hold in fluid channel Ferric Sulfate Hydrogen Aniline Blue (g) Heptahydrate (g) peroxide (g) 0.01 0.26 0.05
  • 10. Future Work ! Investigate issues with a larger sensor network quot; Implement 7 sensor nodes quot; Radio interference quot; Node range (< 30m in-house) ! Apply to larger sample (fish tank) ! Transfer of the sensor network from the lab to real-life applications
  • 11. Project Set Up Experiment Procedure Optimize Adjust Suitable Collaboration of the chemicals Environment equipment used Adding more sensors Adjust the sensor network to work Corporately Apply the process into the real life
  • 12. Experiment Procedure B A Start Add Aniline blue (Dye) and Place the sensor Weigh out start holder and check appropriate monitoring the LED light is amount of on chemicals Add Ferric Sulfate Check that the Place the water Heptahydrate base station pump inside receives signals Beaker from all sensor Keep monitoring for at least 30 Fill in 1500ml Place the minutes water camera on appropriate location and Add Hydrogen Adjust pH value check that the Peroxide to “3” base station receives image Install upart Keep sensor nodes to monitoring the Switch on the appropriate color change sitting Lamp locations End B A