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Build World-Class Food Factories
PMG Engineering Private Limited
The End-to-End Engineering Company in Food Industry
info@pmg.engineering |www.pmg.engineering
1
Quality Control & their CCPs
Milk processing
Build World-Class Food Factories
PMG Engineering Private Limited
The End-to-End Engineering Company in Food Industry
info@pmg.engineering |www.pmg.engineering
1 Introduction
2
CONTENTS
2
3
4
Quality and Safety Management System
5
6 References
Quality assessment at processing stage
Quality verification/ validation
CCPs in Milk Processing
X About PMG Engineering
Build World-Class Food Factories
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1. Introduction
3
Milk quality control involves processes to
measure quality of milk at various
processing stages.
ļƒ¼ Purpose: Ensure safety, healthfulness,
and adherence to required criteria for
milk and milk products.
ļƒ¼ Components of testing: Chemical
composition, purity, and the presence
of bacteria and other microorganisms.
ļƒ¼ Stakeholders involved: Milk collectors,
processors, and marketing
organizations.
ļƒ¼ Focus: Quality assurance through
proper procedures.
ļƒ¼ Key criteria: Safety, healthfulness,
chemical composition, purity, and
absence of harmful microorganisms.
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1.1 Milk Processing
ā€¢ Milk processing involves conversion of
raw milk into -
ļƒ¼ Pasteurized milk
ļƒ¼ Milk products like powder, cheese,
butter, and yogurt, etc.
ā€¢ Processing done using semi-automated
and automated machinery.
ā€¢ An excellent control over quality is
highly desirable, as milk is the only
product which is consumed by all from
infant/ children to senior citizens.
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2. Quality & Safety Management
Systems
For effective control over quality and safety of the milk products, the food
sector employs several quality and safety management systems, including.
Hazard Analysis and Critical
Control Point (HACCP)
ISO 9000, and others
Total Quality Management
(TQM)
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2.1 Benefits of quality control system
Farmers can
get fair prices
Milk Producers
Conformity of
milk quality
Milk
processors
Fair payment
as per quality
of milk
Consumers
Ensures
ā€¢Consumer
health
ā€¢Fair pricing
ā€¢Product safety
Government
bodies
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ā€¢Pleasant smell, White-
yellowish tint colour
1. Visual and
sensory tests
ā€¢< 0.5 mg (IS)
2. Sediment test
ā€¢Absence of Clots or
Flakes on boiling
3. Clot-on-
boiling (COB)
test
ā€¢Identifies aberrant
milk i.e., colostrum
4. Alcohol test
ā€¢Milk suitability for high
heat treatment
5. Alcoholā€“
alizarin test
7
3.1 Platform test for Raw Milk
ā€¢ Dairy Product Quality is influenced by -
ļƒ¼ Quality of raw milk used in manufacture, processing, and handling.
ļƒ¼ Poor socio-economic conditions in rural producers
3. Quality assessment
To check suitability/
acceptability for processing,
various quick quality tests
named ā€˜platform testā€™ are
done as mentioned in figure.
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3.2(a) Adulteration Test: Detection of preservatives
ā€¢ Done for both raw milk and processed milk
ā€¢ Any kind of preservative/neutralizing agents shouldnā€™t be present, but some of
additives can be present only if mentioned on label in various milk products
ā€¢ Hehner and
ā€¢ Lech tests
1. Formalin/
formaldehyde
ā€¢P-phenyl diamine
hydrochloride
2. Hydrogen
Peroxide
ā€¢Turmeric
paper
3. Boric acid/
borates
Rose red to
pink colour
Rose red to
pink colour
Rose red to
pink colour
3. Quality assessment
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ā€¢Rosalic acid
solution test
1. Neutralizer
ā€¢Resorcinol
sol test
2. Sugar
ā€¢ Iodine Test
3. Starch
ā€¢ DAMB test
4. Urea
ā€¢2% DPA
solution
5. Pond
water
Rose red to
pink colour
Red colour
Blue colour
Deep
yellow
colour
Blue
colour
3.2(b) Adulteration Test: Detection of other adulterants
3. Quality assessment
Additive
/adulterant
Result/
Indication
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3.3 Microbial Test
3. Quality assessment
ā€¢ Quality of milk and milk products
also lie on the microbial status
ā€¢ In case of milk,
ļƒ¼ presence of Coxiella Burnetii
indicates faults in
pasteurization
ļƒ¼ Presence of coliform
microorganism esp., E.coli
indicates ineffective CIP
As a results, products quality may
degrade before the general shelf
life of the products
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4. Quality verification/ validation
ā€¢ After quality assessment of milk, quality, verification and validation of
output as per the standard guidelines, is essential part of quality control.
ā€¢ In India, FSSAI rules and regulation, & CODEX guidelines are
recommended by government for result validations.
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1.Definition
ā€¢ Specific
stage where
safety
precautions
are taken to
avoid, remove,
or lessen any
risks.
1.Effect
ā€¢ Crucial point
to ensure milk
product
quality &
safety
ā€¢Common CCPs
ā€¢ CCPs include
Pasteurization,
Fermentation
and,
Packaging
ā€¢Identifying and
Monitoring
ā€¢ Maintaining
quality,
ā€¢ Preventing
contamination,
ā€¢ Guaranteeing
safe,
ā€¢ wholesome
milk production
12
5. CCPs in Milk Processing
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Receiving of
Milk
Filtration
Chilling &
Storage of
raw milk
Preheating at
regen. 1 & 2
Clarification/B
actofugation
Pasteurization
(HTST/LTLT/Fl
ash) or UHT
Cooling at <
4oC
Homo-
genization
Storage in
PMST at < 4oC
Packaging
(Pouch filling/
bottling)
Transportation/
distribution
5.1 Process flow chart of Milk Processing with CCPs
critical control points critical points
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Processing
Step/
Stage
CCPs
Issues (If CCPs
not meet)
Monitoring &
correction
measure
Critical Limit
Receiving
of
Milk
CCP 1: Raw
Milk
a. pH
b. Specific
gravity
c. Temp.
d. Freezing
Point
e. Microbial
load
a. Milk clotting
on boiling
b. Quality
degradation
c. Shorter shelf
life
d. Chances of
adulteration
e. Higher
processing
condition
required
ā€¢ Checked by
pH meter,
lactometer,
thermometer,
freezing test,
milko scan
ā€¢ Rejection of
lot, accept if
all condition
meets.
a. pH: 6.6-6.8
b. s. g: 1.028 -1.032
c. Temp: < 4oC
d. F.pt: -0.53 to
0.575oC
e. Microbial load:-
ā€¢ Total bacteria:
30,000/mL
ā€¢ Somatic cell count:
< 750,000/mL
5.2 CCPs in Milk Processing with critical limit
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Processing
Step/ Stage
CCPs
Issues (If
CCPs not
meet)
Monitoring and
correction measure
Critical Limit
Clarification
&
Bactofugation
CCP 2:
Filtered raw
milk
a. Filter pore
size
b. Microbial
load
a. Pump
clogging
b. Shorter
shelf life
1. Checked by
Sampling, testing
(including
adulteration test,
microbial test),
2. Faults corrected by
re-processing etc.)
a) Filter pore size: 100
ā€“ 200 Āµm
b) TPC: 1.81 Ā± 0.72
log cfu/mL or 95.3
ā€“ 99% reduction.
Pasteurization
CCP 3:
Pasteurized
milk
a. Process
condition
b. Target
microbe
a. Shorter
shelf life
b. Food
borne
illnesses
1. Checked by Sensor
based thermo-meter
& sampling and
testing,
2. Corrected by re-
pasteurization
a) Conditions: -
ā€¢ 63oC/30min,
ā€¢ 72oC/15 sec,
ā€¢ 135oC/2- 3 sec
b) Coxiella burnetti:
absent
5.2 CCPs in Milk Processing with critical limit (cont.)
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Processing
Step/ Stage
CCPs Issues (If CCPs
not meet)
Monitoring/ correction
measure
Critical Limit
Homogenization
CCP 4:
Homogenize
d milk
ā€¢Fat globule
size
ā€¢ Non
uniformity in
milk
constituent,
ā€¢ cream may
separate out
from milk
1. Monitoring done by
sampling and testing
fat globule size
2. Correction done by re-
homogenization
Fat size: 0.2 ā€“ 2
Āµm
Packaging
CCP: 5
Packed milk
ā€¢Packaging
material
ā€¢ Process
contaminati
on,
ā€¢ Shorter
shelf life
1. Monitoring whole
process of sterilization
of packaging material
and their processing
environment,
2. Usage of food grade
packaging material
1. Food grade
packaging
material
2. Food grade
sterilizing
components
5.2 CCPs in Milk Processing with critical limit (cont.)
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6. Reference
ā€¢ Griep-Moyer, E. R., Trmčić, A., Qian, C., & Moraru, C. I. (2022). Monte
Carlo simulation model predicts bactofugation can extend shelf-life of
pasteurized fluid milk, even when raw milk with low spore counts is
used as the incoming ingredient. Journal of Dairy Science, 105(12),
9439-9449.
ā€¢ FAO. 1998. Milk Testing and Quality Control. Milk Processing Guide
Series. Volume 2. FAO/TCP/KEN/6611 Project. Training Programme for
Small Scale Dairy Sector and Dairy Training Institute ā€“ Naivasha.
Kenya
ā€¢ Dairy production and products: Quality and testing (fao.org)
ā€¢ https://www.scielo.br/j/sa/a/tLWrMkgCycV3hSSFmhMp8fy/#
ā€¢ https://www.researchgate.net/figure/Flow-chart-indicating-the-
presumptive-Critical-Control-Points-CCPs-for-microbial-
hazard_fig1_342838484
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We deliver End-to-End Engineering Design and Construction Management
Projects in Food and Beverage Industry.
Meeting Global Benchmarks
In ENGINEERING DESIGN and PROJECT MANAGEMENT
for FOOD and BEVERAGE Industry with SINGLE POINT ACCOUNTABILITY
Process Engineering | Project Management | Mechanical | Electrical | Automation | Food Safety
Key Clients
We deliver End-to-End Engineering Design and Construction Management
Projects in Food and Beverage Industry.
Meeting Global Benchmarks
In ENGINEERING DESIGN and PROJECT MANAGEMENT
for FOOD and BEVERAGE Industry with SINGLE POINT ACCOUNTABILITY
Process Engineering | Project Management | Mechanical | Electrical | Automation | Food Safety
Key Clients
We deliver End-to-End Engineering Design and Construction Management
Projects in Food and Beverage Industry.
Meeting Global Benchmarks
In ENGINEERING DESIGN and PROJECT MANAGEMENT
for FOOD and BEVERAGE Industry with SINGLE POINT ACCOUNTABILITY
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QC and its CCPs_Milk processing.pptx....

  • 1. Build World-Class Food Factories PMG Engineering Private Limited The End-to-End Engineering Company in Food Industry info@pmg.engineering |www.pmg.engineering 1 Quality Control & their CCPs Milk processing
  • 2. Build World-Class Food Factories PMG Engineering Private Limited The End-to-End Engineering Company in Food Industry info@pmg.engineering |www.pmg.engineering 1 Introduction 2 CONTENTS 2 3 4 Quality and Safety Management System 5 6 References Quality assessment at processing stage Quality verification/ validation CCPs in Milk Processing X About PMG Engineering
  • 3. Build World-Class Food Factories PMG Engineering Private Limited The End-to-End Engineering Company in Food Industry info@pmg.engineering |www.pmg.engineering 1. Introduction 3 Milk quality control involves processes to measure quality of milk at various processing stages. ļƒ¼ Purpose: Ensure safety, healthfulness, and adherence to required criteria for milk and milk products. ļƒ¼ Components of testing: Chemical composition, purity, and the presence of bacteria and other microorganisms. ļƒ¼ Stakeholders involved: Milk collectors, processors, and marketing organizations. ļƒ¼ Focus: Quality assurance through proper procedures. ļƒ¼ Key criteria: Safety, healthfulness, chemical composition, purity, and absence of harmful microorganisms.
  • 4. Build World-Class Food Factories PMG Engineering Private Limited The End-to-End Engineering Company in Food Industry info@pmg.engineering |www.pmg.engineering 4 1.1 Milk Processing ā€¢ Milk processing involves conversion of raw milk into - ļƒ¼ Pasteurized milk ļƒ¼ Milk products like powder, cheese, butter, and yogurt, etc. ā€¢ Processing done using semi-automated and automated machinery. ā€¢ An excellent control over quality is highly desirable, as milk is the only product which is consumed by all from infant/ children to senior citizens.
  • 5. Build World-Class Food Factories PMG Engineering Private Limited The End-to-End Engineering Company in Food Industry info@pmg.engineering |www.pmg.engineering Build World-Class Food Factories 5 2. Quality & Safety Management Systems For effective control over quality and safety of the milk products, the food sector employs several quality and safety management systems, including. Hazard Analysis and Critical Control Point (HACCP) ISO 9000, and others Total Quality Management (TQM)
  • 6. Build World-Class Food Factories PMG Engineering Private Limited The End-to-End Engineering Company in Food Industry info@pmg.engineering |www.pmg.engineering 6 2.1 Benefits of quality control system Farmers can get fair prices Milk Producers Conformity of milk quality Milk processors Fair payment as per quality of milk Consumers Ensures ā€¢Consumer health ā€¢Fair pricing ā€¢Product safety Government bodies
  • 7. Build World-Class Food Factories PMG Engineering Private Limited The End-to-End Engineering Company in Food Industry info@pmg.engineering |www.pmg.engineering Build World-Class Food Factories ā€¢Pleasant smell, White- yellowish tint colour 1. Visual and sensory tests ā€¢< 0.5 mg (IS) 2. Sediment test ā€¢Absence of Clots or Flakes on boiling 3. Clot-on- boiling (COB) test ā€¢Identifies aberrant milk i.e., colostrum 4. Alcohol test ā€¢Milk suitability for high heat treatment 5. Alcoholā€“ alizarin test 7 3.1 Platform test for Raw Milk ā€¢ Dairy Product Quality is influenced by - ļƒ¼ Quality of raw milk used in manufacture, processing, and handling. ļƒ¼ Poor socio-economic conditions in rural producers 3. Quality assessment To check suitability/ acceptability for processing, various quick quality tests named ā€˜platform testā€™ are done as mentioned in figure.
  • 8. Build World-Class Food Factories PMG Engineering Private Limited The End-to-End Engineering Company in Food Industry info@pmg.engineering |www.pmg.engineering 8 3.2(a) Adulteration Test: Detection of preservatives ā€¢ Done for both raw milk and processed milk ā€¢ Any kind of preservative/neutralizing agents shouldnā€™t be present, but some of additives can be present only if mentioned on label in various milk products ā€¢ Hehner and ā€¢ Lech tests 1. Formalin/ formaldehyde ā€¢P-phenyl diamine hydrochloride 2. Hydrogen Peroxide ā€¢Turmeric paper 3. Boric acid/ borates Rose red to pink colour Rose red to pink colour Rose red to pink colour 3. Quality assessment
  • 9. Build World-Class Food Factories PMG Engineering Private Limited The End-to-End Engineering Company in Food Industry info@pmg.engineering |www.pmg.engineering 9 ā€¢Rosalic acid solution test 1. Neutralizer ā€¢Resorcinol sol test 2. Sugar ā€¢ Iodine Test 3. Starch ā€¢ DAMB test 4. Urea ā€¢2% DPA solution 5. Pond water Rose red to pink colour Red colour Blue colour Deep yellow colour Blue colour 3.2(b) Adulteration Test: Detection of other adulterants 3. Quality assessment Additive /adulterant Result/ Indication
  • 10. Build World-Class Food Factories PMG Engineering Private Limited The End-to-End Engineering Company in Food Industry info@pmg.engineering |www.pmg.engineering 10 3.3 Microbial Test 3. Quality assessment ā€¢ Quality of milk and milk products also lie on the microbial status ā€¢ In case of milk, ļƒ¼ presence of Coxiella Burnetii indicates faults in pasteurization ļƒ¼ Presence of coliform microorganism esp., E.coli indicates ineffective CIP As a results, products quality may degrade before the general shelf life of the products
  • 11. Build World-Class Food Factories PMG Engineering Private Limited The End-to-End Engineering Company in Food Industry info@pmg.engineering |www.pmg.engineering 11 4. Quality verification/ validation ā€¢ After quality assessment of milk, quality, verification and validation of output as per the standard guidelines, is essential part of quality control. ā€¢ In India, FSSAI rules and regulation, & CODEX guidelines are recommended by government for result validations.
  • 12. Build World-Class Food Factories PMG Engineering Private Limited The End-to-End Engineering Company in Food Industry info@pmg.engineering |www.pmg.engineering 1.Definition ā€¢ Specific stage where safety precautions are taken to avoid, remove, or lessen any risks. 1.Effect ā€¢ Crucial point to ensure milk product quality & safety ā€¢Common CCPs ā€¢ CCPs include Pasteurization, Fermentation and, Packaging ā€¢Identifying and Monitoring ā€¢ Maintaining quality, ā€¢ Preventing contamination, ā€¢ Guaranteeing safe, ā€¢ wholesome milk production 12 5. CCPs in Milk Processing
  • 13. Build World-Class Food Factories PMG Engineering Private Limited The End-to-End Engineering Company in Food Industry info@pmg.engineering |www.pmg.engineering 13 Receiving of Milk Filtration Chilling & Storage of raw milk Preheating at regen. 1 & 2 Clarification/B actofugation Pasteurization (HTST/LTLT/Fl ash) or UHT Cooling at < 4oC Homo- genization Storage in PMST at < 4oC Packaging (Pouch filling/ bottling) Transportation/ distribution 5.1 Process flow chart of Milk Processing with CCPs critical control points critical points
  • 14. Build World-Class Food Factories PMG Engineering Private Limited The End-to-End Engineering Company in Food Industry info@pmg.engineering |www.pmg.engineering 14 Processing Step/ Stage CCPs Issues (If CCPs not meet) Monitoring & correction measure Critical Limit Receiving of Milk CCP 1: Raw Milk a. pH b. Specific gravity c. Temp. d. Freezing Point e. Microbial load a. Milk clotting on boiling b. Quality degradation c. Shorter shelf life d. Chances of adulteration e. Higher processing condition required ā€¢ Checked by pH meter, lactometer, thermometer, freezing test, milko scan ā€¢ Rejection of lot, accept if all condition meets. a. pH: 6.6-6.8 b. s. g: 1.028 -1.032 c. Temp: < 4oC d. F.pt: -0.53 to 0.575oC e. Microbial load:- ā€¢ Total bacteria: 30,000/mL ā€¢ Somatic cell count: < 750,000/mL 5.2 CCPs in Milk Processing with critical limit
  • 15. Build World-Class Food Factories PMG Engineering Private Limited The End-to-End Engineering Company in Food Industry info@pmg.engineering |www.pmg.engineering 15 Processing Step/ Stage CCPs Issues (If CCPs not meet) Monitoring and correction measure Critical Limit Clarification & Bactofugation CCP 2: Filtered raw milk a. Filter pore size b. Microbial load a. Pump clogging b. Shorter shelf life 1. Checked by Sampling, testing (including adulteration test, microbial test), 2. Faults corrected by re-processing etc.) a) Filter pore size: 100 ā€“ 200 Āµm b) TPC: 1.81 Ā± 0.72 log cfu/mL or 95.3 ā€“ 99% reduction. Pasteurization CCP 3: Pasteurized milk a. Process condition b. Target microbe a. Shorter shelf life b. Food borne illnesses 1. Checked by Sensor based thermo-meter & sampling and testing, 2. Corrected by re- pasteurization a) Conditions: - ā€¢ 63oC/30min, ā€¢ 72oC/15 sec, ā€¢ 135oC/2- 3 sec b) Coxiella burnetti: absent 5.2 CCPs in Milk Processing with critical limit (cont.)
  • 16. Build World-Class Food Factories PMG Engineering Private Limited The End-to-End Engineering Company in Food Industry info@pmg.engineering |www.pmg.engineering 16 Processing Step/ Stage CCPs Issues (If CCPs not meet) Monitoring/ correction measure Critical Limit Homogenization CCP 4: Homogenize d milk ā€¢Fat globule size ā€¢ Non uniformity in milk constituent, ā€¢ cream may separate out from milk 1. Monitoring done by sampling and testing fat globule size 2. Correction done by re- homogenization Fat size: 0.2 ā€“ 2 Āµm Packaging CCP: 5 Packed milk ā€¢Packaging material ā€¢ Process contaminati on, ā€¢ Shorter shelf life 1. Monitoring whole process of sterilization of packaging material and their processing environment, 2. Usage of food grade packaging material 1. Food grade packaging material 2. Food grade sterilizing components 5.2 CCPs in Milk Processing with critical limit (cont.)
  • 17. Build World-Class Food Factories PMG Engineering Private Limited The End-to-End Engineering Company in Food Industry info@pmg.engineering |www.pmg.engineering Build World-Class Food Factories 17 6. Reference ā€¢ Griep-Moyer, E. R., Trmčić, A., Qian, C., & Moraru, C. I. (2022). Monte Carlo simulation model predicts bactofugation can extend shelf-life of pasteurized fluid milk, even when raw milk with low spore counts is used as the incoming ingredient. Journal of Dairy Science, 105(12), 9439-9449. ā€¢ FAO. 1998. Milk Testing and Quality Control. Milk Processing Guide Series. Volume 2. FAO/TCP/KEN/6611 Project. Training Programme for Small Scale Dairy Sector and Dairy Training Institute ā€“ Naivasha. Kenya ā€¢ Dairy production and products: Quality and testing (fao.org) ā€¢ https://www.scielo.br/j/sa/a/tLWrMkgCycV3hSSFmhMp8fy/# ā€¢ https://www.researchgate.net/figure/Flow-chart-indicating-the- presumptive-Critical-Control-Points-CCPs-for-microbial- hazard_fig1_342838484
  • 18. Build World-Class Food Factories PMG Engineering Private Limited The End-to-End Engineering Company in Food Industry info@pmg.engineering |www.pmg.engineering Build World-Class Food Factories # We deliver End-to-End Engineering Design and Construction Management Projects in Food and Beverage Industry. Meeting Global Benchmarks In ENGINEERING DESIGN and PROJECT MANAGEMENT for FOOD and BEVERAGE Industry with SINGLE POINT ACCOUNTABILITY Process Engineering | Project Management | Mechanical | Electrical | Automation | Food Safety Key Clients We deliver End-to-End Engineering Design and Construction Management Projects in Food and Beverage Industry. Meeting Global Benchmarks In ENGINEERING DESIGN and PROJECT MANAGEMENT for FOOD and BEVERAGE Industry with SINGLE POINT ACCOUNTABILITY Process Engineering | Project Management | Mechanical | Electrical | Automation | Food Safety Key Clients We deliver End-to-End Engineering Design and Construction Management Projects in Food and Beverage Industry. Meeting Global Benchmarks In ENGINEERING DESIGN and PROJECT MANAGEMENT for FOOD and BEVERAGE Industry with SINGLE POINT ACCOUNTABILITY Process Engineering | Project Management | Mechanical | Electrical | Automation | Food Safety Key Clients Our Clients