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processengineeringcoursepresentation-181129070537.pdf
1.
Organic Synthesis Course-0456: Process Analysis
and Evaluation Advisor: Chaniago Yus Donald 1 Presented By
2.
2
3.
3
4.
4
5.
Organic Synthesis 5
6.
6
7.
History 7
8.
8 History
9.
Retrosynthetic Analysis 9
10.
Practice of Synthesis 10
11.
Analysis 11
12.
Design and Execution
of Synthesis 12
13.
Trouble Shooting 13
14.
Linear and Convergent
Synthesis 14
15.
Examples 15
16.
Examples 16
17.
Synthesis of Chlorobenzide 17
18.
Synthesis of Fenfluoramine 18
19.
Selectivity in Organic
Synthesis 19
20.
Chemoselectivity 20
21.
Examples 21
22.
Regioselectivity 22
23.
Examples 23
24.
Stereoselectivity 24
25.
25 RM RM RM
R R R Checking of Reaction Progress Through TLC Plates https://www.youtube.com/watch?v=kx9Ilfqp8RE Laboratory Synthesis Approach
26.
26 Running Solvent
27.
27 Isolation Of Desired
Product
28.
28 Evaporation of solvent
from Isolated Product through Column Chromatography on Rota Evaporator
29.
29 Vacuum Drying of
Isolated Product
30.
30 NMR Sample in
NMR Tube
31.
31 NMR Spectrum for
Isolated Product 1H-NMR 13C-NMR
32.
32
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