This document presents a thesis on new methods for triangulation-based 3D shape acquisition using laser scanners. It begins with an introduction to 3D metrology and laser scanners. The objectives of the thesis are then stated as developing new techniques for laser peak detection and scanner calibration. The remainder of the document describes existing approaches and the author's proposed new methods in detail across multiple chapters. Experimental results demonstrating the effectiveness of the new peak detection and calibration methods are also provided.