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Photocalorimetry - Progress in Solid State Analysis Techniques Development   Andy C Morris Medway Sciences, University of Greenwich, UK GlaxoSmithKline, Harlow, UK
Background  2 ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],May affect the stability behaviour and cause both physical and chemical changes
Current Problems  3 Current storage & analysis: ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Current Photostability Work  4 ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Previous Work  5 ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Planned Work  6 ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
The TAM  7 ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
The TAM  8 ,[object Object],[object Object]
Triacetin Test Reaction  9 ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Fill Volume Study  10 ,[object Object],[object Object],[object Object],[object Object],[object Object],H   =   -91.7    3.0 kJ mol -1 k  = 2.80    0.10 x 10 -6  dm 3 mol -1 s -1 100% 75% 50% 25% 0%
11
Specialist Equipment  12 ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],2.  Glass 20ml Ampoule 3.  Stainless Steel 20ml Ampoule
Objectives 13 ,[object Object],5)  To examine the causative wavelengths hypothesis 4)  To apply these tests to unknown pharmaceutical materials supplied by GSK ,[object Object],[object Object],[object Object],[object Object],[object Object]
1)  Ampoule Comparison 14 ,[object Object]
Expected Difficulties 15 ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],Light  Optical  Fibre Ampoule Sample “arms”
Summary 16 ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Acknowledgments 17 ,[object Object],[object Object],[object Object]

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NC 2004

  • 1. Photocalorimetry - Progress in Solid State Analysis Techniques Development Andy C Morris Medway Sciences, University of Greenwich, UK GlaxoSmithKline, Harlow, UK
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