The document describes an experiment using a bomb calorimeter to determine heats of combustion. Students measured the heat of combustion of naphthalene and used benzoic acid as a known standard. The sample was fused to a wire and suspended in the bomb, which was filled with oxygen and ignited. Temperature changes before and after combustion were measured and used to calculate the energy released and heat of combustion based on the apparatus' specific heat, determined from benzoic acid trials. Results are presented in tables and graphs.
This document appears to be an exam for an engineering thermodynamics course, consisting of 15 multi-part questions testing students' knowledge of key thermodynamics concepts. It begins with 10 short answer questions worth 2 marks each, followed by 5 longer form questions worth 16 marks each. The questions cover topics like the laws of thermodynamics, entropy, phase changes, psychrometrics, gas cycles, and thermodynamic processes and cycles. The exam is assessing students' understanding of fundamental thermodynamic principles as well as their ability to apply those principles to analyze thermodynamic systems and cycles.
The document describes the purpose, basic theory, tools, steps, and results of using a calorimeter to determine the specific heat of solid materials. The calorimeter is used to measure the heat involved in chemical reactions or changes in substances. The basic theory states that heat absorbed or released by a substance is directly proportional to its mass and temperature change, and depends on its type. The steps involve using the calorimeter to determine its heat capacity, then using it to find the specific heat of metal samples by measuring temperature changes when the hot metal is mixed with cold water. The results found the heat capacity of the calorimeter and specific heats of brass and iron samples.
Bomb calorimetry involves measuring the heat of combustion (calorific value) of fuels and other combustible materials. A bomb calorimeter consists of (1) a bomb vessel where combustion occurs, (2) a bucket containing water for absorbing heat, (3) an insulating jacket, and (4) a thermometer. The heat released by combusting a sample in oxygen is absorbed by water in the bucket, causing its temperature to rise. By comparing this rise to that of a standard material, the sample's calorific value can be calculated after applying corrections. Safety precautions must be followed when using high-pressure oxygen.
A fully inkjet printed wireless and chipless sensor for co2 and temperature d...ieeeprojectsbangalore
A fully inkjet-printed wireless chipless sensor is presented that uses split ring resonators printed with three different inks to independently detect CO2 and temperature through polarization responses. A polymer/carbon nanotube composite ink detects both CO2 and temperature, while an additional polymer coating is shown to reduce CO2 sensitivity without affecting temperature detection. Simulations and experiments validate the repeatability of the sensor's design and functionality.
The document describes different types of calorimeters used to measure heat changes in chemical reactions, including bomb calorimeters and coffee cup calorimeters. Bomb calorimeters allow measurement of combustion reactions under constant volume conditions, while coffee cup calorimeters measure heat changes under constant pressure. Examples are provided demonstrating how to use calorimetry data to determine the heat of reaction for a combustion reaction and a neutralization reaction. Both examples show the reactions are exothermic as heat is released.
Enthalpy of formation of magnesium oxidesreshtha95
This document describes an experiment to determine the enthalpy of formation of magnesium oxide (MgO) through calorimetry. Three chemical reactions are used: 1) Mg + 2HCl → MgCl2 + H2; 2) MgO + 2HCl → MgCl2 + H2; 3) H2 + 1/2O2 → H2O. The enthalpy of formation of MgO is calculated by adding the enthalpies of reactions 1 and 3 and subtracting the enthalpy of reaction 2. Data on temperature changes is collected when Mg and MgO are added to HCl solution. The enthalpy of formation is found to be 590 kJ/mol,
The document describes an experiment using a bomb calorimeter to determine heats of combustion. Students measured the heat of combustion of naphthalene and used benzoic acid as a known standard. The sample was fused to a wire and suspended in the bomb, which was filled with oxygen and ignited. Temperature changes before and after combustion were measured and used to calculate the energy released and heat of combustion based on the apparatus' specific heat, determined from benzoic acid trials. Results are presented in tables and graphs.
This document appears to be an exam for an engineering thermodynamics course, consisting of 15 multi-part questions testing students' knowledge of key thermodynamics concepts. It begins with 10 short answer questions worth 2 marks each, followed by 5 longer form questions worth 16 marks each. The questions cover topics like the laws of thermodynamics, entropy, phase changes, psychrometrics, gas cycles, and thermodynamic processes and cycles. The exam is assessing students' understanding of fundamental thermodynamic principles as well as their ability to apply those principles to analyze thermodynamic systems and cycles.
The document describes the purpose, basic theory, tools, steps, and results of using a calorimeter to determine the specific heat of solid materials. The calorimeter is used to measure the heat involved in chemical reactions or changes in substances. The basic theory states that heat absorbed or released by a substance is directly proportional to its mass and temperature change, and depends on its type. The steps involve using the calorimeter to determine its heat capacity, then using it to find the specific heat of metal samples by measuring temperature changes when the hot metal is mixed with cold water. The results found the heat capacity of the calorimeter and specific heats of brass and iron samples.
Bomb calorimetry involves measuring the heat of combustion (calorific value) of fuels and other combustible materials. A bomb calorimeter consists of (1) a bomb vessel where combustion occurs, (2) a bucket containing water for absorbing heat, (3) an insulating jacket, and (4) a thermometer. The heat released by combusting a sample in oxygen is absorbed by water in the bucket, causing its temperature to rise. By comparing this rise to that of a standard material, the sample's calorific value can be calculated after applying corrections. Safety precautions must be followed when using high-pressure oxygen.
A fully inkjet printed wireless and chipless sensor for co2 and temperature d...ieeeprojectsbangalore
A fully inkjet-printed wireless chipless sensor is presented that uses split ring resonators printed with three different inks to independently detect CO2 and temperature through polarization responses. A polymer/carbon nanotube composite ink detects both CO2 and temperature, while an additional polymer coating is shown to reduce CO2 sensitivity without affecting temperature detection. Simulations and experiments validate the repeatability of the sensor's design and functionality.
The document describes different types of calorimeters used to measure heat changes in chemical reactions, including bomb calorimeters and coffee cup calorimeters. Bomb calorimeters allow measurement of combustion reactions under constant volume conditions, while coffee cup calorimeters measure heat changes under constant pressure. Examples are provided demonstrating how to use calorimetry data to determine the heat of reaction for a combustion reaction and a neutralization reaction. Both examples show the reactions are exothermic as heat is released.
Enthalpy of formation of magnesium oxidesreshtha95
This document describes an experiment to determine the enthalpy of formation of magnesium oxide (MgO) through calorimetry. Three chemical reactions are used: 1) Mg + 2HCl → MgCl2 + H2; 2) MgO + 2HCl → MgCl2 + H2; 3) H2 + 1/2O2 → H2O. The enthalpy of formation of MgO is calculated by adding the enthalpies of reactions 1 and 3 and subtracting the enthalpy of reaction 2. Data on temperature changes is collected when Mg and MgO are added to HCl solution. The enthalpy of formation is found to be 590 kJ/mol,
method to find calorific values of fuelsAWAISCHUDHARY
This document discusses calorific values, which measure the heating power or energy content of fuels and foods. It defines lower and higher calorific values, and explains that calorific value depends on a substance's composition. Junker's calorimeter is used to specifically measure the calorific value of gases. The document also provides the formula to calculate higher calorific value from experimental measurements of mass, temperatures, and heat capacities in a bomb calorimeter test.
The document discusses zirconia oxygen analyzers and their calibration. It provides details on:
- Zirconia oxygen analyzers measure oxygen concentration using air as a reference gas, but the oxygen concentration of air can vary with temperature and humidity, causing measurement errors.
- Zirconia oxygen analyzers use either a concentration cell system or limiting current type to generate a voltage corresponding to oxygen concentration based on the Nernst equation.
- Calibration of zirconia oxygen analyzers involves either a two-point calibration using zero and span gases or a one-point calibration using just a span gas or just a zero gas to establish the calibration curve.
1. The document describes an experiment to determine the heat capacity of aluminum, iron, and brass using a Cobra3 device. Metallic samples are boiled in water and then placed in a calorimeter filled with water at room temperature. The temperature increase of the calorimeter water is measured.
2. The specific heat capacities of the metals are calculated based on the temperature changes and the energy balance equation. The measured heat capacity values for aluminum, iron, and brass agree well with literature values.
3. The molar heat capacities determined from the experiment also agree with the theoretical Dulong-Petit value of 24.94 J/(mol·K), verifying Dulong-Petit's law.
The heating value, also known as the calorific value or energy value, is the amount of heat released during the combustion of a fuel. It is measured in units of energy per unit of the substance, such as kJ/kg. The higher heating value takes into account the latent heat of vaporization of water in the combustion products, while the lower heating value does not. Heating values are commonly determined through the use of a bomb calorimeter.
This document compares indirect and direct gasification. Indirect gasification involves two coupled reactors that allow for complete carbon conversion at lower temperatures compared to direct gasification. The bed material in indirect gasification can transport oxygen from the combustor to the gasifier through chemical looping, providing energy for gasification and reducing tar formation. Studies show the bed material can supply up to 30% of the energy needed for gasification through this oxygen transport process. Indirect gasification provides more flexibility in operating conditions than direct gasification.
This document contains 4 problems regarding steam power plants and steam systems. Problem 1 calculates the heat supplied to a boiler and the power generated by a turbine. Problem 2 calculates turbine power and heat rejected from a condenser. Problem 3 calculates boiler heat input and mass flow rates of hot and cold water. Problem 4 determines the ratio of steam to water mass flow rates needed to produce hot water at a given temperature.
Calorific value refers to the total heat released when a fuel is completely burned. There are two types of calorific values for fuels containing hydrogen: higher (gross) calorific value and lower (net) calorific value. The higher calorific value includes the latent heat released from condensation of water vapor in the combustion products, while the lower calorific value does not include this latent heat as it escapes with the gases. The lower calorific value can be calculated by subtracting the latent heat of vaporization of hydrogen from the gross calorific value. Dulong's formula can also be used to theoretically calculate the calorific value based on the fuel's carbon, hydrogen, oxygen,
The document compares three common temperature scales: Fahrenheit, Celsius, and Kelvin. It lists the people who developed each scale, when they were developed, and how they were defined. Key temperatures are also listed in each scale, along with conversion formulas between the scales.
This document contains the questions from a Mechanical Engineering Thermodynamics exam. It covers topics like the first, second, and zeroth laws of thermodynamics, the Carnot cycle, psychrometrics, refrigeration, and steam power cycles. The exam has two sections - a short answer section with 10 two-mark questions, and a long answer section with 5 sixteen-mark questions covering applications of thermodynamic concepts to systems like air compressors, turbines, refrigerators and steam power plants.
This document contains 11 problems related to thermodynamics concepts like steam tables, properties of steam at different conditions, processes involving gases in closed systems. The problems involve determining states, properties, energies and sketching processes on p-v diagrams. The document provides the questions and expects the answers to be provided using concepts of thermodynamics.
Dry air and water vapor combine to form atmospheric air. The pressure of the dry air and water vapor pressure together make up the total pressure of the air mixture. Specific humidity is the ratio of mass of water vapor to total mass of air, while relative humidity is the ratio of actual water vapor pressure to saturation water vapor pressure. The enthalpy of atmospheric air depends on the enthalpies of dry air and water vapor as well as their relative quantities based on specific and relative humidity.
Convection Heat Transfer
Supervisor: Dr. Goharkhah
Presenter: Siavash Azizi
25 December 2017
Introduction
The importance of research
History of work
Application
Classified
Example
This document contains 6 problems involving calculations of heat and entropy changes for various thermodynamic processes involving steam and gases. Problem 1 involves heating steam at constant pressure. Problem 2 involves condensing steam at constant pressure. Problem 3 involves heating steam in a rigid vessel with changing pressure. Problem 4 involves heating nitrogen in a rigid cylinder. Problem 5 involves heating and cooling air in a constant pressure and constant volume process. Problem 6 involves expanding and compressing air while keeping temperature constant in one process and rejecting heat at constant pressure in another.
Oxygen analyzers measure the amount of oxygen a patient is receiving to ensure optimal levels. They work using either chemical or electrochemical methods. Chemical analyzers directly measure oxygen percentage but are not safe for operating rooms. Electrochemical analyzers use either a galvanic fuel cell or polarographic method using chemical reactions and electron flow to indirectly measure oxygen levels. Both require calibration to known oxygen percentages for accuracy.
The document describes procedures for using a bomb calorimeter to determine the heat of combustion of organic compounds. A bomb calorimeter consists of a combustion bomb surrounded by a water bucket and thermometer. Samples are burned in the bomb, warming the surrounding water. The temperature change is used to calculate the heat released from the sample. Fat has the highest energy per gram, providing over twice as much heat as carbohydrates and proteins when burned.
This document contains the solutions to 4 questions regarding thermodynamics. It involves calculations using the continuity equation, steady flow energy equation, and properties of water and steam at various conditions. Key steps and results are shown, including enthalpy values for water and steam at different pressures and temperatures. The questions involve calculations for energy transferred in various processes involving the mixing of steam and water.
CH EN 3453 Heat Transfer 2014 Fall Utah Homework HW 01 Assignmentsemihypocrite
This document contains information about a heat transfer course including:
1) An assignment on explaining the basic laws of heat transfer and solving conductivity problems is due on August 29th.
2) Help sessions will be held on Wednesday, August 27th at 4:30pm to assist with the assignment.
3) An end of document survey asks students questions about their background and experience relevant to the course.
The Expander Gas and Ammonia Ratio Influence on the Calcium Cyanamide YieldYogeshIJTSRD
For the first time, thermodynamic calculations based on relatively new physicochemical constants clarified the onset temperature of thermal ammonia decomposition, as well as the side chemical reactions probability between ammonia and carbon dioxide. The influence of the main technological parameters on the calcium cyanamide synthesis is investigated. The exhaust gases composition from the reactor for the calcium cyanamide synthesis was studied depending on the temperature. Kinetic studies of the calcium cyanamide synthesis determined the chemical reaction orders with respect to ammonia and carbon dioxide, and it was proved that the limiting stage of calcium cyanamide synthesis is the initial gas components diffusion through the product layer. O. Kh. Panzhiev | A. Kh. Panzhiev | N. Umarov | O. Azimov "The Expander Gas and Ammonia Ratio Influence on the Calcium Cyanamide Yield" Published in International Journal of Trend in Scientific Research and Development (ijtsrd), ISSN: 2456-6470, Special Issue | International Research Development and Scientific Excellence in Academic Life , March 2021, URL: https://www.ijtsrd.com/papers/ijtsrd38440.pdf Paper Url: https://www.ijtsrd.com/engineering/other/38440/the-expander-gas-and-ammonia-ratio-influence-on-the-calcium-cyanamide-yield/o-kh-panzhiev
Importance of Micropore–Mesopore Interfaces in Carbon Dioxide Capture by Carb...Roxana-Alina Milescu
This study finds that mesoporous carbon materials called Starbons, derived from waste biomass, can adsorb more carbon dioxide than commercially available activated charcoal. While Starbons have lower microporosity than activated charcoal, they contain interconnected micropores and mesopores. This interconnected pore structure enhances CO2 adsorption by providing more accessible micropore surface area. Testing of various Starbon materials found that those carbonized at 800°C adsorbed the most CO2. Analysis showed that CO2 adsorption depends on both micropore volume and the product of micropore and mesopore volumes. Therefore, the interconnected micropore-mesopore structure enables superior CO2 capture compared to
method to find calorific values of fuelsAWAISCHUDHARY
This document discusses calorific values, which measure the heating power or energy content of fuels and foods. It defines lower and higher calorific values, and explains that calorific value depends on a substance's composition. Junker's calorimeter is used to specifically measure the calorific value of gases. The document also provides the formula to calculate higher calorific value from experimental measurements of mass, temperatures, and heat capacities in a bomb calorimeter test.
The document discusses zirconia oxygen analyzers and their calibration. It provides details on:
- Zirconia oxygen analyzers measure oxygen concentration using air as a reference gas, but the oxygen concentration of air can vary with temperature and humidity, causing measurement errors.
- Zirconia oxygen analyzers use either a concentration cell system or limiting current type to generate a voltage corresponding to oxygen concentration based on the Nernst equation.
- Calibration of zirconia oxygen analyzers involves either a two-point calibration using zero and span gases or a one-point calibration using just a span gas or just a zero gas to establish the calibration curve.
1. The document describes an experiment to determine the heat capacity of aluminum, iron, and brass using a Cobra3 device. Metallic samples are boiled in water and then placed in a calorimeter filled with water at room temperature. The temperature increase of the calorimeter water is measured.
2. The specific heat capacities of the metals are calculated based on the temperature changes and the energy balance equation. The measured heat capacity values for aluminum, iron, and brass agree well with literature values.
3. The molar heat capacities determined from the experiment also agree with the theoretical Dulong-Petit value of 24.94 J/(mol·K), verifying Dulong-Petit's law.
The heating value, also known as the calorific value or energy value, is the amount of heat released during the combustion of a fuel. It is measured in units of energy per unit of the substance, such as kJ/kg. The higher heating value takes into account the latent heat of vaporization of water in the combustion products, while the lower heating value does not. Heating values are commonly determined through the use of a bomb calorimeter.
This document compares indirect and direct gasification. Indirect gasification involves two coupled reactors that allow for complete carbon conversion at lower temperatures compared to direct gasification. The bed material in indirect gasification can transport oxygen from the combustor to the gasifier through chemical looping, providing energy for gasification and reducing tar formation. Studies show the bed material can supply up to 30% of the energy needed for gasification through this oxygen transport process. Indirect gasification provides more flexibility in operating conditions than direct gasification.
This document contains 4 problems regarding steam power plants and steam systems. Problem 1 calculates the heat supplied to a boiler and the power generated by a turbine. Problem 2 calculates turbine power and heat rejected from a condenser. Problem 3 calculates boiler heat input and mass flow rates of hot and cold water. Problem 4 determines the ratio of steam to water mass flow rates needed to produce hot water at a given temperature.
Calorific value refers to the total heat released when a fuel is completely burned. There are two types of calorific values for fuels containing hydrogen: higher (gross) calorific value and lower (net) calorific value. The higher calorific value includes the latent heat released from condensation of water vapor in the combustion products, while the lower calorific value does not include this latent heat as it escapes with the gases. The lower calorific value can be calculated by subtracting the latent heat of vaporization of hydrogen from the gross calorific value. Dulong's formula can also be used to theoretically calculate the calorific value based on the fuel's carbon, hydrogen, oxygen,
The document compares three common temperature scales: Fahrenheit, Celsius, and Kelvin. It lists the people who developed each scale, when they were developed, and how they were defined. Key temperatures are also listed in each scale, along with conversion formulas between the scales.
This document contains the questions from a Mechanical Engineering Thermodynamics exam. It covers topics like the first, second, and zeroth laws of thermodynamics, the Carnot cycle, psychrometrics, refrigeration, and steam power cycles. The exam has two sections - a short answer section with 10 two-mark questions, and a long answer section with 5 sixteen-mark questions covering applications of thermodynamic concepts to systems like air compressors, turbines, refrigerators and steam power plants.
This document contains 11 problems related to thermodynamics concepts like steam tables, properties of steam at different conditions, processes involving gases in closed systems. The problems involve determining states, properties, energies and sketching processes on p-v diagrams. The document provides the questions and expects the answers to be provided using concepts of thermodynamics.
Dry air and water vapor combine to form atmospheric air. The pressure of the dry air and water vapor pressure together make up the total pressure of the air mixture. Specific humidity is the ratio of mass of water vapor to total mass of air, while relative humidity is the ratio of actual water vapor pressure to saturation water vapor pressure. The enthalpy of atmospheric air depends on the enthalpies of dry air and water vapor as well as their relative quantities based on specific and relative humidity.
Convection Heat Transfer
Supervisor: Dr. Goharkhah
Presenter: Siavash Azizi
25 December 2017
Introduction
The importance of research
History of work
Application
Classified
Example
This document contains 6 problems involving calculations of heat and entropy changes for various thermodynamic processes involving steam and gases. Problem 1 involves heating steam at constant pressure. Problem 2 involves condensing steam at constant pressure. Problem 3 involves heating steam in a rigid vessel with changing pressure. Problem 4 involves heating nitrogen in a rigid cylinder. Problem 5 involves heating and cooling air in a constant pressure and constant volume process. Problem 6 involves expanding and compressing air while keeping temperature constant in one process and rejecting heat at constant pressure in another.
Oxygen analyzers measure the amount of oxygen a patient is receiving to ensure optimal levels. They work using either chemical or electrochemical methods. Chemical analyzers directly measure oxygen percentage but are not safe for operating rooms. Electrochemical analyzers use either a galvanic fuel cell or polarographic method using chemical reactions and electron flow to indirectly measure oxygen levels. Both require calibration to known oxygen percentages for accuracy.
The document describes procedures for using a bomb calorimeter to determine the heat of combustion of organic compounds. A bomb calorimeter consists of a combustion bomb surrounded by a water bucket and thermometer. Samples are burned in the bomb, warming the surrounding water. The temperature change is used to calculate the heat released from the sample. Fat has the highest energy per gram, providing over twice as much heat as carbohydrates and proteins when burned.
This document contains the solutions to 4 questions regarding thermodynamics. It involves calculations using the continuity equation, steady flow energy equation, and properties of water and steam at various conditions. Key steps and results are shown, including enthalpy values for water and steam at different pressures and temperatures. The questions involve calculations for energy transferred in various processes involving the mixing of steam and water.
CH EN 3453 Heat Transfer 2014 Fall Utah Homework HW 01 Assignmentsemihypocrite
This document contains information about a heat transfer course including:
1) An assignment on explaining the basic laws of heat transfer and solving conductivity problems is due on August 29th.
2) Help sessions will be held on Wednesday, August 27th at 4:30pm to assist with the assignment.
3) An end of document survey asks students questions about their background and experience relevant to the course.
The Expander Gas and Ammonia Ratio Influence on the Calcium Cyanamide YieldYogeshIJTSRD
For the first time, thermodynamic calculations based on relatively new physicochemical constants clarified the onset temperature of thermal ammonia decomposition, as well as the side chemical reactions probability between ammonia and carbon dioxide. The influence of the main technological parameters on the calcium cyanamide synthesis is investigated. The exhaust gases composition from the reactor for the calcium cyanamide synthesis was studied depending on the temperature. Kinetic studies of the calcium cyanamide synthesis determined the chemical reaction orders with respect to ammonia and carbon dioxide, and it was proved that the limiting stage of calcium cyanamide synthesis is the initial gas components diffusion through the product layer. O. Kh. Panzhiev | A. Kh. Panzhiev | N. Umarov | O. Azimov "The Expander Gas and Ammonia Ratio Influence on the Calcium Cyanamide Yield" Published in International Journal of Trend in Scientific Research and Development (ijtsrd), ISSN: 2456-6470, Special Issue | International Research Development and Scientific Excellence in Academic Life , March 2021, URL: https://www.ijtsrd.com/papers/ijtsrd38440.pdf Paper Url: https://www.ijtsrd.com/engineering/other/38440/the-expander-gas-and-ammonia-ratio-influence-on-the-calcium-cyanamide-yield/o-kh-panzhiev
Importance of Micropore–Mesopore Interfaces in Carbon Dioxide Capture by Carb...Roxana-Alina Milescu
This study finds that mesoporous carbon materials called Starbons, derived from waste biomass, can adsorb more carbon dioxide than commercially available activated charcoal. While Starbons have lower microporosity than activated charcoal, they contain interconnected micropores and mesopores. This interconnected pore structure enhances CO2 adsorption by providing more accessible micropore surface area. Testing of various Starbon materials found that those carbonized at 800°C adsorbed the most CO2. Analysis showed that CO2 adsorption depends on both micropore volume and the product of micropore and mesopore volumes. Therefore, the interconnected micropore-mesopore structure enables superior CO2 capture compared to
The Mintek process is a large-scale batch silicothermic process for extracting magnesium that operates at atmospheric pressure. It aims to overcome issues with an earlier Magnetherm process. In the Mintek process, the furnace must operate above 1600°C, potentially as high as 1800°C, to achieve an economically acceptable rate of magnesium extraction while maintaining low energy consumption. Several factors like temperature, feed recipe, slag depth relative to furnace diameter, and reactions in the arc attachment zone influence the process.
This document summarizes a research article about a novel hydrogen storage system using carbon sorbents and heat pipes. It begins by introducing the need for alternative fuel sources and discusses the challenges with hydrogen storage. It then describes a new design using microporous carbon materials for adsorption storage and heat pipes for thermal control. The document outlines the mathematical model used to analyze heat and mass transfer during the sorption processes in the storage cylinder. In conclusion, it presents the goals of developing and optimizing an onboard hydrogen storage system using carbon sorbents and thermal regulation.
The document summarizes research on the electrocatalytic reduction of CO2 to produce ethylene using copper-based nanoparticles supported on carbon. Key points:
1. Copper oxide nanoparticles with an initial size of 20 nm were synthesized on carbon and fragmented into smaller 2-4 nm nanoparticles during CO2 electroreduction, improving ethylene selectivity.
2. Operando transmission electron microscopy showed the nanoparticles distort and break apart over time, correlated with increasing ethylene production.
3. In situ X-ray absorption spectroscopy indicated the copper oxidation state decreases to metallic copper during electrolysis, the active state for CO2 reduction.
4. The fragmented nanoparticle morphology, combining small particles and compact
ICR NOx Optimised reburn staging and SNCRTom Lowes
This document discusses methods for controlling NOx emissions from cement plants, including reburn, staging, and selective non-catalytic reduction (SNCR). It provides three key points:
1) Hot reburn involves combusting fuel volatiles sub-stoichiometrically at 1300°C for 0.15s or 1200°C for 1.2s to promote the conversion of NO to N2 before allowing air to mix. This can reduce NOx levels below 500 mg/Nm3 without SNCR.
2) Air staging, where fuel is injected below tertiary air ducts at 70% sub-stoichiometry for 1s, can also achieve NOx levels under 500 mg/Nm
Monitoring and interpreting of insitu combustionGowtham Dada
This document discusses using carbon isotope analysis to monitor and interpret in situ combustion processes. It provides background on in situ combustion, carbon isotopes, and carbon isotope analysis. Different carbon isotope values are expected from various combustion reactions. Field data and combustion tube experiments can be interpreted using carbon isotope signatures to understand the temperature of reactions and identify communication between injectors and producers. Carbon isotope analysis is a useful tool when combined with gas analysis to distinguish reaction sources and burning characteristics during in situ combustion.
Thermal regeneration of activated carbon saturated with nitrate ions from an ...IJAEMSJORNAL
The present study was initiated to help the simple and less expensive regeneration of activated carbons after saturation in rural area. In order to determine a regeneration time and the number of regeneration cycles, an adsorption test was necessary. Thus, 3h and 4 cycles of carbon regeneration are obtained after evaluation of the performance, percentage and adsorption capacity after each cycle. Regeneration percentages of 71.29, 54.05, 40.40, 28.06 % and 72.6, 69.84, 64.33, 34.98 %for respective concentrations of 30± 1.2 mg/L and 55 ± 1.6 mg/L are observed. Also, the performances of activated carbon 8.5, 10, 12, 20 g/L and capacities 24.04, 19.93, 14.9 and 10.35mg/g 35.7, 34.12, 31.43 and 17.09 mg/g respectively for dry season and rainy season were necessary to fix the number of cycles. The artisanal furnace with its ease of installation and its maximum temperature of 500±2°C is suitable for the regeneration of saturated activated carbon.
This document summarizes research on carbon nanotubes conducted by Vaneet Kumar Sharma at the University of Connecticut. It discusses the synthesis of single-walled carbon nanotubes using chemical vapor deposition, oxidation of the nanotubes using acid, and their application as probes for atomic force microscopy. The synthesis is optimized using small metal nanoparticle catalysts well dispersed on supports like MgO. Methane and hydrogen are used as the carbon source to minimize impurities. Acidic oxidation introduces functional groups to the nanotubes, making them suitable for use as ultra-sharp AFM probes fabricated using dielectrophoresis.
This document summarizes a study investigating the simultaneous removal of NO and CO2 using coconut shell char and calcined limestone in a calcium looping process. Coconut shell char and calcined limestone were added to a carbonator where they effectively removed NO and CO2 from flue gases. Oxygen played an important role in NO removal by the char, while the calcined limestone showed a strong catalytic effect on NO reduction by carbon monoxide generated from the char reacting with oxygen. High temperatures, carbon monoxide concentrations, and carbonation temperatures positively impacted NO reduction rates. The system was able to achieve over 97% NO removal and 80% CO2 capture efficiency.
Modification of CWZ-22 with KOH to enhance CO2 adsorptionumut mutlu
This document summarizes a study on modifying a commercial activated carbon, CWZ-22, with potassium hydroxide (KOH) to enhance its carbon dioxide (CO2) adsorption capacity. Various ratios of KOH to CWZ-22 were tested. Characterization of the modified samples found that specific surface area and pore volume increased with higher KOH ratios from 1 to 2, but then increased only slightly with further increases in KOH ratio. CO2 adsorption capacity was also evaluated at different temperatures.
This document provides information about gas welding and cutting. It discusses oxy-fuel welding, which uses oxygen and acetylene gases to produce a flame over 5700°F that can melt metals. Cutting uses the flame to preheat and then pure oxygen to burn away metal. The document describes the equipment used, including oxygen and acetylene cylinders, regulators, hoses, and torches. It explains the chemical reactions that produce the high temperature flame and discusses properties of acetylene such as its heat output. Advantages and limitations of oxy-fuel welding are also outlined.
This document discusses stable carbon isotopes and their applications. It begins by introducing stable isotopes and focusing on the two stable isotopes of carbon: 12C and 13C. It then discusses how the ratio of these isotopes varies in different materials and can be used to determine organic vs inorganic origins of carbon and distinguish marine vs nonmarine deposits. Applications include determining the source and maturity of fossil fuels, identifying evidence of early life in Precambrian sediments, and studying the deep earth carbon cycle via analyses of carbonatites and diamonds.
The industry of ultrafine and nanopowder materials requires new methods for their production and hardware equipment for engineering processes. Among them there is plasmachemical synthesis of powder materials with the use of electric arc generators of low-temperature plasma. Plasma heating of initial inputs allows evaporation of almost any material and performance of the required chemical reactions in the gas phase with following vapor condensation to the nanodisperse solid phase. Considering the capacities of plasma generators and plasmachemical reactors achieved for today (many hundreds of kilowatts), we can expect that productivity by the desired product can be hundreds of kilograms per hour. Moreover, the plasma equipment demonstrates high universality relative to the initial materials, possible synthesis of complex powders and continuous conditions of operatingprocedure. The developed electric-arc plasmatrons and reactors allow different high-temperature processes, including powder processing in plasma flows . Now the most common constructions ofplasma reactors are the direct-flow ones with co-axial plasmatron and the three-jet ones with three plasmatrons tilted at 30–45° relative to the reactor axis and located in 120° intervals on the water-cooled upper lid. The plasmatron with sectioned inter-electrode insertion and shaped outlet nozzle-electrode ensure diffuse glow of the anode region of the arc discharge, what leads to the uniform temperature field and flow velocity at the nozzle edge. These parameters of the plasma jet have a good impact on reproducibility of powder processing, high coefficient of initial material use and production of powder with the given physical-chemical properties. Application of the three-jet plasmachemical reactor ensures the uniform temperature field along the reaction zone, allows easy control of productivity due
Some fact about Ammonia Production by Prem Baboo.pdfPremBaboo4
Operation of the plant is mainly supervised by the operators in the control room, who monitor the various instruments and adjust operating conditions in order to obtain satisfactory operation. They should also react when an alarm is activated. In some cases they can re-establish normal conditions by adjusting the controls in the control room; in other cases they give instructions to a field operator to make the necessary adjustments at various locations in the plant. Field operators work in regular shifts in the plant, especially in the reforming section, in order to supervise the firing of the reformer and the temperature of the tubes in the reformer, to record local instrument readings, and to notice any irregularities such as leaks. Every change of temperature of the reformer a little change can bring big change resulting energy losses, e.g. temperature of the primary reformer and CO slip losses in methanation etc.
This document describes the development of a lean NOx trap (LNT) catalyst that does not require precious metals. It proposes using ultrasmall nanoparticles of iron, vanadium, and cerium oxides as the active catalytic components, supported on a porous barium oxide substrate. During lean exhaust conditions, NOx would be oxidized and stored as nitrates in the barium oxide. Under brief rich conditions, the stored NOx would be reduced to N2 via reactions with hydrocarbons facilitated by the redox activity of the iron, vanadium, and cerium oxides. Laboratory testing of prototypes made with this design could evaluate the catalyst's performance versus EPA emissions standards at reducing temperatures compared to conventional precious metal-based
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Mixed oxide capacitor of cu o—batio3 as a new type co2 gas sensor
1. Mixed Oxide Capacitor of CuO—BaTiO3 as a New Type CO2 Gas Sensor | ISweek -
Industry sourcing
An oxide capacitor consisting of BaTiO3 and an oxide is studied as a new type CO2
sensor based on capacitance change. Sensitivity to CO2, as well as the optimum
operating temperature, was strongly dependent on the particular oxide mixed with
BaTiO3.
Among the elements investigated in this study, CuO–BaTiO3 exhibited the highest
sensitivity to CO2. In particular, the CuO–BaTiO3 mixed oxide at the equimolar
composition is highly sensitive to CO2. The optimum operating temperature and
frequency for CuO–BaTiO3 are 729 K and 100 Hz, respectively, and the 80% response
time to 2% CO2 is within 25 s. The equimolar mixture of CuO and BaTiO3 can measure
the CO2 concentration from 100 to 60 000 ppm. Carbonation of oxide seems to play a
key role for the detection of CO2 on these mixed oxide capacitors.
The optimum operating temperature of these mixed oxide capacitors for CO2 detection,
therefore, correlates with the decomposition temperature of the carbonate corresponding
to the oxide mixed with BaTiO3. The capacitance increase of CuO–BaTiO3 upon exposure
to CO2 seems to result from the elevated height of the potential barrier at the grain
boundary between CuO and BaTiO3. Carbonation of CuO in the element seems to bring
about the elevation in the height of the potential barrier.
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