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Determination of Soil Reaction (pH)
with the help of a pH Meter
UG Geography Honours CBCS Syllabus
Part of GEO-A-CC-4-10-P: Soil and Bio-Geography Lab:
30 marks, 2 Credits
Study Material: Part II
Dr. Sarada Mandal
Associate professor in Geography
Prabhu Jagatbandhu College
Courtesy: Dr. Shrabani Som Majumdar, Former Scientist, IESWM
Implements required for Collection of Soil
Sample
Garden Spade Image from
IndiaMART Image from : https://www.stepsystems.de/247-1-
Edelman-augers.html
Auger
Courtesy: Priya Kolay (Student of Prabhu Jagatbandhu College)
Estimated Budget for establishing a New Laboratory
Sl. No Item Tentative Budget in Rupees
as on April 2019
1 OVEN (ELECTRICAL) with Digital Microprocessor
Temp. Controller including auto short circuits
protection
CHAMBER SIZE-15 x 15 x 18 inch
10000 to 15000/-
2 DIGITAL WEIGHING MACHINE 0.001 gm to 200
gm with imported semi magnetic lode cell
CROWN GLASS WIND SHILD, auto cutup Adaptor,
big display, S S PAN grade-304, leveling
arrangement with stabilized voltage circuits fitted
inside the Weighing machine.
Around 10000/-
3 PORTABLE DIGITAL PH METER WITH ELECTRODE
PH METER, Pocket Model*0 to 14 pH
*Display: LCD, 13mm digit size.
*Size: 131 x 70 x 25 mm
Around 6000/-
Market Price is
liable to Change
with time
Estimated Budget for a New Laboratory (Contd.)
Sl. No Item Tentative Budget in Rupees as
on April 2019
4 One packet of Whattman Filter paper, , 11cm
diameter
Around 1200
5, 6 Borosillicate Glass 250 ml Conical Flask, 250 ml Beaker Around 150, Around 100
7 Spatula (stainless Steel: 6 inches long: required for
putting 5gm soil on Digital balance)
Around 40
8, 9 Borosillicate Glass Measuring Cylinder 100ml, Same 50
ml
Around 200, Around 100
10, 11 Borosillicate Glass Petri Dish with 3 inches diameter
(Required for putting the soil in oven), Mortar and
pestle Porcelain or wood with 4 inches Diameter
Around 300
Around 100
12 Borosillicate Glass Funnel with 3 inches diameter
(fitted to conical flask)
Around 60
Market
Price is
liable to
Change
with time
Students have to write the following description during the experiment
Determination of Soil pH
With the help of a pH meter
Principle
• The soil pH reflects whether a soil is acidic, neutral,
basic or alkaline. The acidity, neutrality or alkalinity of a
soil is measured in terms of hydrogen ion activity of the
soil water system. The negative logarithm of the H ion
activity is called pH and thus pH of a soil is a measure of
only the intensity of activity and not the amount of the
acid present. The pH range normally found in soils
varies from 3 to 9. Mathematically pH is represented
as, log 1/H = - log H+
Apparatus:
• Sample solution
• pH Meter
• Physical Balance
• Oven
• Beaker
• Conical Flask
• Measuring Cylinder
• Petri dish
• Filter Paper
• Funnel
• Mortar and
pestle
• Glass Rod.
Procedure:
• The pH meter was calibrated using pH 7 buffer solution.
• Then the meter was adjusted with known pH of buffer
solutions 4.0 and 9.2.
• 5.0 g of soil was weighed and transferred into
100 ml beaker.
• 50 ml distilled water was added and stirred well with a
glass rod.
• This was allowed to stand for half an hour with
intermittent stirring.
• To the soil water suspension in the beaker, the electrode
was immersed and pH value was determined from the
automatic display of the pH meter.
Room Temperature should be noted down
by a Thermometer
Calculation
Sample
No.
Temper
ature in
Degree
Celsius
Determin
ed Value
of pH
Result
Thus the pH of the
given soil sample
was ____________
and the given soil
sample is
__________ in nature

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Measurement of soil pH part ii

  • 1. Determination of Soil Reaction (pH) with the help of a pH Meter UG Geography Honours CBCS Syllabus Part of GEO-A-CC-4-10-P: Soil and Bio-Geography Lab: 30 marks, 2 Credits Study Material: Part II Dr. Sarada Mandal Associate professor in Geography Prabhu Jagatbandhu College Courtesy: Dr. Shrabani Som Majumdar, Former Scientist, IESWM
  • 2. Implements required for Collection of Soil Sample Garden Spade Image from IndiaMART Image from : https://www.stepsystems.de/247-1- Edelman-augers.html Auger
  • 3. Courtesy: Priya Kolay (Student of Prabhu Jagatbandhu College)
  • 4. Estimated Budget for establishing a New Laboratory Sl. No Item Tentative Budget in Rupees as on April 2019 1 OVEN (ELECTRICAL) with Digital Microprocessor Temp. Controller including auto short circuits protection CHAMBER SIZE-15 x 15 x 18 inch 10000 to 15000/- 2 DIGITAL WEIGHING MACHINE 0.001 gm to 200 gm with imported semi magnetic lode cell CROWN GLASS WIND SHILD, auto cutup Adaptor, big display, S S PAN grade-304, leveling arrangement with stabilized voltage circuits fitted inside the Weighing machine. Around 10000/- 3 PORTABLE DIGITAL PH METER WITH ELECTRODE PH METER, Pocket Model*0 to 14 pH *Display: LCD, 13mm digit size. *Size: 131 x 70 x 25 mm Around 6000/- Market Price is liable to Change with time
  • 5. Estimated Budget for a New Laboratory (Contd.) Sl. No Item Tentative Budget in Rupees as on April 2019 4 One packet of Whattman Filter paper, , 11cm diameter Around 1200 5, 6 Borosillicate Glass 250 ml Conical Flask, 250 ml Beaker Around 150, Around 100 7 Spatula (stainless Steel: 6 inches long: required for putting 5gm soil on Digital balance) Around 40 8, 9 Borosillicate Glass Measuring Cylinder 100ml, Same 50 ml Around 200, Around 100 10, 11 Borosillicate Glass Petri Dish with 3 inches diameter (Required for putting the soil in oven), Mortar and pestle Porcelain or wood with 4 inches Diameter Around 300 Around 100 12 Borosillicate Glass Funnel with 3 inches diameter (fitted to conical flask) Around 60 Market Price is liable to Change with time
  • 6. Students have to write the following description during the experiment Determination of Soil pH With the help of a pH meter Principle • The soil pH reflects whether a soil is acidic, neutral, basic or alkaline. The acidity, neutrality or alkalinity of a soil is measured in terms of hydrogen ion activity of the soil water system. The negative logarithm of the H ion activity is called pH and thus pH of a soil is a measure of only the intensity of activity and not the amount of the acid present. The pH range normally found in soils varies from 3 to 9. Mathematically pH is represented as, log 1/H = - log H+
  • 7. Apparatus: • Sample solution • pH Meter • Physical Balance • Oven • Beaker • Conical Flask • Measuring Cylinder • Petri dish • Filter Paper • Funnel • Mortar and pestle • Glass Rod.
  • 8. Procedure: • The pH meter was calibrated using pH 7 buffer solution. • Then the meter was adjusted with known pH of buffer solutions 4.0 and 9.2. • 5.0 g of soil was weighed and transferred into 100 ml beaker. • 50 ml distilled water was added and stirred well with a glass rod. • This was allowed to stand for half an hour with intermittent stirring. • To the soil water suspension in the beaker, the electrode was immersed and pH value was determined from the automatic display of the pH meter.
  • 9. Room Temperature should be noted down by a Thermometer Calculation Sample No. Temper ature in Degree Celsius Determin ed Value of pH Result Thus the pH of the given soil sample was ____________ and the given soil sample is __________ in nature