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COMBINED GAIN-SCHEDULING AND MULTIMODEL CONTROL
OF A REACTIVE DISTILLATION COLUMN
Budi H. Bisowarno, Yu-Chu Tian, Moses O. Tadé
Department of Chemical Engineering,
Curtin University of Technology,
GPO Box U1987, Perth WA 6845, Australia
Abstract: Reactive distillation (RD) is a favourable alternative to conventional series of
reaction-separation processes. Control of RD is challenging due to its integrated
functionality and complex dynamics. Linear PID algorithm is not satisfactory and
needs because of the need for adequate retuning over a wide range of operating
conditions. Combined gain-scheduling and multimodel control scheme is proposed to
handle the nonlinearities of the process. Simulation results show the superior
performance of the proposed method to that of a standard PI control.
Copyright © 2003 IFAC
Keywords: reactive distillation, gain-scheduling, multimodel, switching, tuning.
1. INTRODUCTION
The RD column is gradually becoming an important
unit operation in chemical process industry. It offers
reduction in both investment as well as operational
costs. Tight control of product composition and
conversion is fundamental for an economically
optimal operation. Unfortunately, both composition
and conversion cannot be economically and reliably
measured on-line and in real time. Moreover, the
relationship between the product composition and the
potential manipulated variable (eg. reboiler duty)
may reveal multiplicity. Inferential control via stage
temperatures, which have monotonic relationship
with the manipulated variable, is commonly adopted.
Directionality of a chemical process means that a
vector of inputs (eg. manipulated variables) is
differently amplified according to its direction. It has
been known to create considerable complex problem
in control system design for multivariable processes
such as in conventional distillation (Sågfors and
Waller, 1995). Standard PID with fixed parameters is
not satisfactory because of the need for adequate
retuning over a wide range of operating conditions.
Inferential control of RD, which has directionality in
the process gain, is investigated in this study. Limited
number of reports has discussed control aspects of
RD. Control strategies of batch RD (Sorensen and
Skogestad, 1994) and its structure for optimisation
(Wajge and Reklaitis, 1999) have been investigated.
Recently, nonlinear control of batch RD has been
proposed (Balasubramhanya and Doyle III, 2000).
For continuous RD, a nonlinear input-output
linearizing controller and nonlinear controller have
been designed for ethylene glycol system (Kumar
and Daoutidis, 1999). A robust PI control scheme has
been proposed for the same system (Loperena et al.,
2000). Linear and nonlinear control strategies have
been applied for an ethyl acetate system (Vora and
Daoutidis, 2001). A variety of control structures have
also been explored for two product RD (Al-Arfaj and
Luyben, 2000).
For ethyl tert-butyl ether (ETBE) RD, which is the
focus of this study, general control considerations
have been presented (Sneesby et al., 1997).
Combined composition and conversion control have
been discussed (Sneesby et al., 1999). Control
performance of a variety of one-point control
schemes has been compared (Bisowarno and Tadé,
2002). Pattern-based predictive control has recently
been proposed for controlling the product
composition (Tian et al., 2003). Effectiveness of
control schemes has been compared for single and
double-feed RD (Al-Arfaj and Luyben, 2002).
Standard PI algorithms, which were employed for all
cases, indicated more advanced controller is required
to improve the control performance.
In this study, combined gain-scheduling and
multimodel control will be implemented on one-point
control of an ETBE RD. The models cover
directionality of the process gain and a switching
scheme will be employed to integrate them. Its
performance will be compared to that of a standard
PI controller.
2. REACTIVE DISTILLATION
A pilot scale packed RD column for ETBE
production serves as an example for a typical single-
feed two-products RD process. The column consists
of 1 rectifying stage, 3 reactive stages, 4 stripping
stages, a total condenser, and an electric partial
reboiler, respectively, as shown in Figure 1. The feed
is a mixture of isobutylene, ethanol, ETBE, and n-
butane, resulting from a pre-reactor, which converts
most of isobutylene to ETBE. Typical operating data
including the operating range are summarised in
Table 1. The primary and secondary manipulated
variables are reboiler duty (QR) and reflux rate (LR),
respectively. LV control scheme, which outperforms
other control schemes for this column (Bisowarno
and Tadé, 2002), is employed.
Inferential control is adopted to control the ETBE
purity. The relationship between the purity and the
reboiler duty reveals input multiplicity phenomena as
shown in Figure 2. Based on the sensitivity analysis,
stage 7 temperature is found to be the most
appropriate measured variable to infer the ETBE
purity (Tian and Tadé, 2000). Figure 2 also shows the
relationship between the stage 7 temperature and the
UHERLOHU GXW 7KH QRQOLQHDU SURFHVV JDLQ  77 4r)
is large around the nominal operating condition and
becomes small outside this range.
PC
LC
Reflux Distillate
FC
Feed TC
LC
Reboiler
Bottoms
Fig. 1 ETBE Column with the controllers
0.6
0.65
0.7
0.75
0.8
0.85
0.9
0.95
1
0.45 0.5 0.55 0.6
Reboiler duty (MJ/min)
ETBEpurity(wt)
70
80
90
100
110
120
130
140
150
Stage7temp.(
o
C)
purity
temperature
Fig.2 Stage 7 temp./purity vs. QR (LR = 2.2 l/min)
Table 1 ETBE RD column characteristics and Inputs
Column Specifications:
Nre/Nrx/Nst 3/3/5
Feed stage 6
Overhead pressure 950 kPa
Feed Conditions: Range Nominal*
Temperature 30o
C 30o
C
Rate (l/min) 0.684-0.836 0.76
Comp. (mol) 70–80 mol%
conversion
in the pre-reactor
0.291 ETBE,
0.091 EtOH,
0.073 iBut,
0.545 nBut
Man. Variables: Range Nominal*
LR (l/min) 2.0 – 2.4 2.2
QR (MJ/min) 0.4825-0.555 0.520
* Nominal (optimum) operating condition for
designing the control system
3. CONTROL OBJECTIVES
The main objective of the control system is to keep
the controlled stage 7 temperature close to the set-
points despite the presence of disturbances. The most
significant disturbances are changes in the feed flow
rate and in the feed composition. The second
objective is a sufficiently fast set-point tracking.
These two objectives must be achieved for the entire
operating range of the reactive distillation column.
4. CONTROL DESIGN METHOD
Adaptive control with multimodel was introduced in
(Narendra and Balakrishnan, 1997). The basic idea is
to choose the best model for the column from an a
priori known set of models at every instant, and then
apply the output of the corresponding controller to
the column. Firstly, the process identification is
performed by rapidly choosing the smallest error
with respect to a criterion (switching). Unlike the
previous work, the controller parameters are then
adjusted using a parameter-adaptation algorithm in
this study (gain-scheduling).
4.1 Multimodel
Although a single highly nonlinear and/or adaptive
model may be used to represent the process
dynamics, several simple fixed multimodels are
employed. They are chosen to cope with nonlinear
and time varying characteristics of each operating
condition point. A proper switching scheme is
needed to integrate the models. As a result, process
identification and rapid control action can be
satisfied.
Simplified input-output dynamic models of the
manipulation and disturbance paths are identified
Table 2 Multimodels based on open-loop tests
LR (l/min) QR, min QR, nom QR, max
2.0 4709.5
238.4Ti s + 1
4679.5
78.5Ti s + 1
498
21 Ti s + 1
2.2 6442.75
197.4Ti s + 1
4675
73.2 Ti s + 1
493
23.2 Ti s + 1
2.4 960.5
122.4Ti s + 1
9043.5
126.1Ti s + 1
1472
54.9Ti s + 1
Disturbances at LR = 2.2 l/min
Feed rate 0.412
23.75Ti s + 1
Feed comp. 0.163
6.75Ti s + 1
around the optimum reboiler duty at constant reflux
rate. Referring to Figure 2, three simplified models
are derived to capture the nonlinearity of the process
gain for each constant reflux rate. At each of the
reboiler duty of 0.4825, 0.520, and 0.555 MJ/min,
respectively, the models are derived at the reflux rate
of 2.0, 2.2, and 2.4 l/min, respectively. The models of
disturbance patch are derived at the optimum reboiler
duty of 0.520 MJ/min. Table 2 shows the models
formulated as first order transfer functions.
4.2 Switching scheme
The switching scheme involves firstly monitoring a
performance index based on the identification error
for each model and then switching to the model with
smallest index. A small identification error leads to a
small tracking error (Narendra and Balakrishnan,
1997). The performance index (IE) is formulated in
equation 1,
,( i
2
 ∫ -λ(t-τ)
i
2
GW ≥  DQG !
ZKHUH DQG DUH WKH ZHLJKWLQJ IDFWRUV RQ WKH
instantaneous measures and the long-term accuracy,
respectively. These two free design parameters
provide smooth transition between different process
PRGHOV i is the difference between the outputs of the
model and the real plant.
4.3 Gain Scheduling
Gain scheduling is based on linear time-invariance of
the process at a number of operating points. A linear
controller is then designed for each operating point.
Therefore, the parameters of the controller should be
interpolated or scheduled (Rugh and Shamma, 2000).
The controller gain is commonly scheduled due to
the process nonlinearity with constant dynamics.
Switching between local linear controllers is a
conventional way for gain scheduling. A function of
a scheduling variable can also be employed to
interpolate the gain. Measured ouput or set-point may
be used as a scheduling variable (Bequette, 2000).
set-point output
Fig. 3 Combined gain-scheduling and multimodel
control scheme
In this study, the scheduling controller gain (Kc) is
formulated in equation 2 (Ogunnaike and Ray, 1994),
Kc =
Kp
KpoKco
(2)
where Kco and Kpo are the reference values of the
controller gain and process gains, respectively. The
time varying process gain (Kp) is identified and
computed on-line from the inferred variable and the
manipulated variable.
The reference control parameters are tuned by using
Abbas method (Abbas, 1997). This method relates
the controller parameters to the characteristics of a
first-order plus time delay model and the desired
over-shoot of the closed loop system (Alexander and
Trahan, 2001). For a PI controller, the controller
parameters are formulated in equation 3,
Kc =
(Kpo
T
+
+
(3a)
Ti = T + (3b)
ZKHUH .SR 7 DQG DUH WKH RSHQ-loop process gain,
WLPH FRQVWDQW DQG WLPH GHOD UHVSHFWLYHO DQG LV
the desired closed-loop time constant.
The general structure of the combined gain-
scheduling and multimodel control scheme is shown
in Figure 3. G1, Gn, GS, and IE are the simplified
model 1, the simplified model n, the gain-scheduling
controller, and the performance index, respectively.
5. CONTROL PERFORMANCE
The control performance of the proposed method is
compared to that of a standard PI controller. The
desired closed-loop time constant is chosen to be 5
min. Applying the Abbas method, the controller gain
and time constant of the PI controller in the range of
operating conditions are 0.00622 o
C/(MJ/min) and
GS RD Plant
G1
Gn
IE
84.53 min, respectively. For the proposed method,
the time constant is kept constant at 84.53 min while
the controller gain is computed on-line as a function
of the scheduling variable.
Figures 4 and 5 show the dynamic responses when
the feed flow rates (Ff) increase or decrease steeply
by using either standard PI or the proposed method,
respectively. The Figure shows that the disturbance
rejection of the proposed method is superior to the
standard PI controller.
Figure 6 shows the dynamic response resulting from
step change in the feed composition (Fc). The
changes were represented by changes in the pre-
reacted feed from 80 to 70 mol% of the isobutylene
conversion. Figure 6 shows the proposed controller,
which can tightly control the stage 7 temperature,
does not keep the purity at the set-point value. This
results from the model mismatch. Although more
models can be employed to enhance the control
performance, the intrinsic problem remains. This
problem results from the difficulties to infer
composition from VLE temperature measurements in
multi-component mixture.
Figures 7 and 8 show the dynamic responses for step
changes in the set-point value (T7). The proposed
method clearly has better set-point tracking as shown
by shorter settling time.
The corresponding values of the integral absolute
error (IAE) and integral of time-weighted absolute
error (ITAE) criteria are shown in Table 3. The
criteria confirm the previous analysis that the control
performance can be improved by using the proposed
method.
Fig. 4 Dynamic responses due to +10% Feed rate
step change
Fig. 5 Dynamic responses due to –10% Feed rate step
change
Fig. 6 Dynamic responses due to feed concentration
step change
Fig. 7 Dynamic responses due to +5 set-point step
change
127
128
129
130
131
132
133
134
0 20 40 60 80 100 120
time (min)
stage7temp.(C)
0.969
0.9695
0.97
0.9705
0.971
0.9715
0.972
0.9725
0.973
0.9735 ETBEpurity(wt)
PI-Purity
MGS-Purity
PI-T7
MGS-T7
125
125.5
126
126.5
127
127.5
128
0 60 120 180 240 300 360
time (min)
stage7temp.(C)
0.9704
0.9706
0.9708
0.971
0.9712
0.9714
0.9716
0.9718
0.972
0.9722
0.9724
0.9726
ETBEpurity(wt)
MGS-Purity
PI-Purity
PI-T7
MGS-T7
127.5
128
128.5
129
129.5
130
130.5
0 60 120 180 240 300 360
time (min)
stage7temp.(C)
0.9708
0.971
0.9712
0.9714
0.9716
0.9718
0.972
0.9722
0.9724
0.9726
0.9728
ETBEpurity(wt)
MGS-T7
PI-T7
MGS-Purity
PI-Purity
127.5
127.6
127.7
127.8
127.9
128
128.1
128.2
128.3
128.4
128.5
128.6
0 60 120 180 240 300 360
time (min)
stage7temp.(C)
0.965
0.966
0.967
0.968
0.969
0.97
0.971
0.972
0.973
ETBEpurity(wt)
PI-T7
PI-Purity
MGS-T7
MGS-Purity

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4 combined gain scheduling and multimodel control of a reactive distillation column

  • 1. COMBINED GAIN-SCHEDULING AND MULTIMODEL CONTROL OF A REACTIVE DISTILLATION COLUMN Budi H. Bisowarno, Yu-Chu Tian, Moses O. Tadé Department of Chemical Engineering, Curtin University of Technology, GPO Box U1987, Perth WA 6845, Australia Abstract: Reactive distillation (RD) is a favourable alternative to conventional series of reaction-separation processes. Control of RD is challenging due to its integrated functionality and complex dynamics. Linear PID algorithm is not satisfactory and needs because of the need for adequate retuning over a wide range of operating conditions. Combined gain-scheduling and multimodel control scheme is proposed to handle the nonlinearities of the process. Simulation results show the superior performance of the proposed method to that of a standard PI control. Copyright © 2003 IFAC Keywords: reactive distillation, gain-scheduling, multimodel, switching, tuning. 1. INTRODUCTION The RD column is gradually becoming an important unit operation in chemical process industry. It offers reduction in both investment as well as operational costs. Tight control of product composition and conversion is fundamental for an economically optimal operation. Unfortunately, both composition and conversion cannot be economically and reliably measured on-line and in real time. Moreover, the relationship between the product composition and the potential manipulated variable (eg. reboiler duty) may reveal multiplicity. Inferential control via stage temperatures, which have monotonic relationship with the manipulated variable, is commonly adopted. Directionality of a chemical process means that a vector of inputs (eg. manipulated variables) is differently amplified according to its direction. It has been known to create considerable complex problem in control system design for multivariable processes such as in conventional distillation (Sågfors and Waller, 1995). Standard PID with fixed parameters is not satisfactory because of the need for adequate retuning over a wide range of operating conditions. Inferential control of RD, which has directionality in the process gain, is investigated in this study. Limited number of reports has discussed control aspects of RD. Control strategies of batch RD (Sorensen and Skogestad, 1994) and its structure for optimisation (Wajge and Reklaitis, 1999) have been investigated. Recently, nonlinear control of batch RD has been proposed (Balasubramhanya and Doyle III, 2000). For continuous RD, a nonlinear input-output linearizing controller and nonlinear controller have been designed for ethylene glycol system (Kumar and Daoutidis, 1999). A robust PI control scheme has been proposed for the same system (Loperena et al., 2000). Linear and nonlinear control strategies have been applied for an ethyl acetate system (Vora and Daoutidis, 2001). A variety of control structures have also been explored for two product RD (Al-Arfaj and Luyben, 2000). For ethyl tert-butyl ether (ETBE) RD, which is the focus of this study, general control considerations have been presented (Sneesby et al., 1997). Combined composition and conversion control have been discussed (Sneesby et al., 1999). Control performance of a variety of one-point control schemes has been compared (Bisowarno and Tadé, 2002). Pattern-based predictive control has recently been proposed for controlling the product composition (Tian et al., 2003). Effectiveness of control schemes has been compared for single and double-feed RD (Al-Arfaj and Luyben, 2002). Standard PI algorithms, which were employed for all cases, indicated more advanced controller is required to improve the control performance. In this study, combined gain-scheduling and multimodel control will be implemented on one-point control of an ETBE RD. The models cover directionality of the process gain and a switching scheme will be employed to integrate them. Its performance will be compared to that of a standard PI controller.
  • 2. 2. REACTIVE DISTILLATION A pilot scale packed RD column for ETBE production serves as an example for a typical single- feed two-products RD process. The column consists of 1 rectifying stage, 3 reactive stages, 4 stripping stages, a total condenser, and an electric partial reboiler, respectively, as shown in Figure 1. The feed is a mixture of isobutylene, ethanol, ETBE, and n- butane, resulting from a pre-reactor, which converts most of isobutylene to ETBE. Typical operating data including the operating range are summarised in Table 1. The primary and secondary manipulated variables are reboiler duty (QR) and reflux rate (LR), respectively. LV control scheme, which outperforms other control schemes for this column (Bisowarno and Tadé, 2002), is employed. Inferential control is adopted to control the ETBE purity. The relationship between the purity and the reboiler duty reveals input multiplicity phenomena as shown in Figure 2. Based on the sensitivity analysis, stage 7 temperature is found to be the most appropriate measured variable to infer the ETBE purity (Tian and Tadé, 2000). Figure 2 also shows the relationship between the stage 7 temperature and the UHERLOHU GXW 7KH QRQOLQHDU SURFHVV JDLQ 77 4r) is large around the nominal operating condition and becomes small outside this range. PC LC Reflux Distillate FC Feed TC LC Reboiler Bottoms Fig. 1 ETBE Column with the controllers 0.6 0.65 0.7 0.75 0.8 0.85 0.9 0.95 1 0.45 0.5 0.55 0.6 Reboiler duty (MJ/min) ETBEpurity(wt) 70 80 90 100 110 120 130 140 150 Stage7temp.( o C) purity temperature Fig.2 Stage 7 temp./purity vs. QR (LR = 2.2 l/min) Table 1 ETBE RD column characteristics and Inputs Column Specifications: Nre/Nrx/Nst 3/3/5 Feed stage 6 Overhead pressure 950 kPa Feed Conditions: Range Nominal* Temperature 30o C 30o C Rate (l/min) 0.684-0.836 0.76 Comp. (mol) 70–80 mol% conversion in the pre-reactor 0.291 ETBE, 0.091 EtOH, 0.073 iBut, 0.545 nBut Man. Variables: Range Nominal* LR (l/min) 2.0 – 2.4 2.2 QR (MJ/min) 0.4825-0.555 0.520 * Nominal (optimum) operating condition for designing the control system 3. CONTROL OBJECTIVES The main objective of the control system is to keep the controlled stage 7 temperature close to the set- points despite the presence of disturbances. The most significant disturbances are changes in the feed flow rate and in the feed composition. The second objective is a sufficiently fast set-point tracking. These two objectives must be achieved for the entire operating range of the reactive distillation column. 4. CONTROL DESIGN METHOD Adaptive control with multimodel was introduced in (Narendra and Balakrishnan, 1997). The basic idea is to choose the best model for the column from an a priori known set of models at every instant, and then apply the output of the corresponding controller to the column. Firstly, the process identification is performed by rapidly choosing the smallest error with respect to a criterion (switching). Unlike the previous work, the controller parameters are then adjusted using a parameter-adaptation algorithm in this study (gain-scheduling). 4.1 Multimodel Although a single highly nonlinear and/or adaptive model may be used to represent the process dynamics, several simple fixed multimodels are employed. They are chosen to cope with nonlinear and time varying characteristics of each operating condition point. A proper switching scheme is needed to integrate the models. As a result, process identification and rapid control action can be satisfied. Simplified input-output dynamic models of the manipulation and disturbance paths are identified
  • 3. Table 2 Multimodels based on open-loop tests LR (l/min) QR, min QR, nom QR, max 2.0 4709.5 238.4Ti s + 1 4679.5 78.5Ti s + 1 498 21 Ti s + 1 2.2 6442.75 197.4Ti s + 1 4675 73.2 Ti s + 1 493 23.2 Ti s + 1 2.4 960.5 122.4Ti s + 1 9043.5 126.1Ti s + 1 1472 54.9Ti s + 1 Disturbances at LR = 2.2 l/min Feed rate 0.412 23.75Ti s + 1 Feed comp. 0.163 6.75Ti s + 1 around the optimum reboiler duty at constant reflux rate. Referring to Figure 2, three simplified models are derived to capture the nonlinearity of the process gain for each constant reflux rate. At each of the reboiler duty of 0.4825, 0.520, and 0.555 MJ/min, respectively, the models are derived at the reflux rate of 2.0, 2.2, and 2.4 l/min, respectively. The models of disturbance patch are derived at the optimum reboiler duty of 0.520 MJ/min. Table 2 shows the models formulated as first order transfer functions. 4.2 Switching scheme The switching scheme involves firstly monitoring a performance index based on the identification error for each model and then switching to the model with smallest index. A small identification error leads to a small tracking error (Narendra and Balakrishnan, 1997). The performance index (IE) is formulated in equation 1, ,( i 2 ∫ -λ(t-τ) i 2 GW ≥ DQG !
  • 4. ZKHUH DQG DUH WKH ZHLJKWLQJ IDFWRUV RQ WKH instantaneous measures and the long-term accuracy, respectively. These two free design parameters provide smooth transition between different process PRGHOV i is the difference between the outputs of the model and the real plant. 4.3 Gain Scheduling Gain scheduling is based on linear time-invariance of the process at a number of operating points. A linear controller is then designed for each operating point. Therefore, the parameters of the controller should be interpolated or scheduled (Rugh and Shamma, 2000). The controller gain is commonly scheduled due to the process nonlinearity with constant dynamics. Switching between local linear controllers is a conventional way for gain scheduling. A function of a scheduling variable can also be employed to interpolate the gain. Measured ouput or set-point may be used as a scheduling variable (Bequette, 2000). set-point output Fig. 3 Combined gain-scheduling and multimodel control scheme In this study, the scheduling controller gain (Kc) is formulated in equation 2 (Ogunnaike and Ray, 1994), Kc = Kp KpoKco (2) where Kco and Kpo are the reference values of the controller gain and process gains, respectively. The time varying process gain (Kp) is identified and computed on-line from the inferred variable and the manipulated variable. The reference control parameters are tuned by using Abbas method (Abbas, 1997). This method relates the controller parameters to the characteristics of a first-order plus time delay model and the desired over-shoot of the closed loop system (Alexander and Trahan, 2001). For a PI controller, the controller parameters are formulated in equation 3, Kc =
  • 5. (Kpo T + + (3a) Ti = T + (3b) ZKHUH .SR 7 DQG DUH WKH RSHQ-loop process gain, WLPH FRQVWDQW DQG WLPH GHOD UHVSHFWLYHO DQG LV the desired closed-loop time constant. The general structure of the combined gain- scheduling and multimodel control scheme is shown in Figure 3. G1, Gn, GS, and IE are the simplified model 1, the simplified model n, the gain-scheduling controller, and the performance index, respectively. 5. CONTROL PERFORMANCE The control performance of the proposed method is compared to that of a standard PI controller. The desired closed-loop time constant is chosen to be 5 min. Applying the Abbas method, the controller gain and time constant of the PI controller in the range of operating conditions are 0.00622 o C/(MJ/min) and GS RD Plant G1 Gn IE
  • 6. 84.53 min, respectively. For the proposed method, the time constant is kept constant at 84.53 min while the controller gain is computed on-line as a function of the scheduling variable. Figures 4 and 5 show the dynamic responses when the feed flow rates (Ff) increase or decrease steeply by using either standard PI or the proposed method, respectively. The Figure shows that the disturbance rejection of the proposed method is superior to the standard PI controller. Figure 6 shows the dynamic response resulting from step change in the feed composition (Fc). The changes were represented by changes in the pre- reacted feed from 80 to 70 mol% of the isobutylene conversion. Figure 6 shows the proposed controller, which can tightly control the stage 7 temperature, does not keep the purity at the set-point value. This results from the model mismatch. Although more models can be employed to enhance the control performance, the intrinsic problem remains. This problem results from the difficulties to infer composition from VLE temperature measurements in multi-component mixture. Figures 7 and 8 show the dynamic responses for step changes in the set-point value (T7). The proposed method clearly has better set-point tracking as shown by shorter settling time. The corresponding values of the integral absolute error (IAE) and integral of time-weighted absolute error (ITAE) criteria are shown in Table 3. The criteria confirm the previous analysis that the control performance can be improved by using the proposed method. Fig. 4 Dynamic responses due to +10% Feed rate step change Fig. 5 Dynamic responses due to –10% Feed rate step change Fig. 6 Dynamic responses due to feed concentration step change Fig. 7 Dynamic responses due to +5 set-point step change 127 128 129 130 131 132 133 134 0 20 40 60 80 100 120 time (min) stage7temp.(C) 0.969 0.9695 0.97 0.9705 0.971 0.9715 0.972 0.9725 0.973 0.9735 ETBEpurity(wt) PI-Purity MGS-Purity PI-T7 MGS-T7 125 125.5 126 126.5 127 127.5 128 0 60 120 180 240 300 360 time (min) stage7temp.(C) 0.9704 0.9706 0.9708 0.971 0.9712 0.9714 0.9716 0.9718 0.972 0.9722 0.9724 0.9726 ETBEpurity(wt) MGS-Purity PI-Purity PI-T7 MGS-T7 127.5 128 128.5 129 129.5 130 130.5 0 60 120 180 240 300 360 time (min) stage7temp.(C) 0.9708 0.971 0.9712 0.9714 0.9716 0.9718 0.972 0.9722 0.9724 0.9726 0.9728 ETBEpurity(wt) MGS-T7 PI-T7 MGS-Purity PI-Purity 127.5 127.6 127.7 127.8 127.9 128 128.1 128.2 128.3 128.4 128.5 128.6 0 60 120 180 240 300 360 time (min) stage7temp.(C) 0.965 0.966 0.967 0.968 0.969 0.97 0.971 0.972 0.973 ETBEpurity(wt) PI-T7 PI-Purity MGS-T7 MGS-Purity
  • 7. Fig. 8 Dynamic responses due to –5% set-point step change Table 3 Comparison of IAE and ITAE indices Magnitude IAE ITAE PI GS* PI GS* +10% Ff 219 8.3 19990 1120 -10% Ff 218 8.3 19877 1113 80-70%conv. (Fc) 81 8.3 7741 1117 +5o C T7 19 4.1 389 288 -5o C T7 15 4.3 334 294 * The proposed method using gain-scheduling and multimodel control scheme 6. CONCLUSIONS The combined gain-scheduling and multimodel control has been applied to a RD column for ETBE production having nonlinearity in the process gain. Several input-output first order models were derived. Gain-scheduling control was then implemented employing the multimodel for model identification and scheduling the controller gain. The proposed controller is superior to standard PI control with fixed parameters for RD columns. However, the effectiveness is reduced for feed composition disturbances. This work clearly demonstrates that nonlinear processes can be controlled successfully with a linear multimodel concept. REFERENCES Abbas, A. (1997). A new set of controller tuning relations. ISA Transactions 36(3): 183-187. Al-Arfaj, M. A. and W. L. Luyben (2000). Comparison of alternative control structures for two- product reactive distillation column. Ind. Eng. Chem. Res. 39: 3298-3307. Al-Arfaj, M. A. and W. L. Luyben (2002). Control Study of Ethyl tert-Butyl Ether Reactive Distillation. Ind. Eng. Chem. Res. 41: 3784-3796. Alexander, C. A. and R. E. Trahan (2001). A comparison of traditional and adaptive control strategies for systems with time delay. ISA Transactions 40: 353-368. Balasubramhanya, L. S. and F. J. Doyle III (2000). Nonlinear model-based control of a batch reactive distillation column. J. Process Control 10: 209-218. Bequette, B. W. (2000). Practical Approaches to Nonlinear Control: A Review of Process Application. Bisowarno, B. H. and M. O. Tadé (2002). The Comparison of Disturbance Rejection Properties of One-Point Control Schemes for ETBE Reactive Distillation. Chem. Eng. Comm. 189(1): 85-100. Kumar, A. and P. Daoutidis (1999). Modeling, Analysis and Control of Ethylene Glycol Reactive Distillation Column. AIChE Journal 45(1): 51-68. Loperena, R. M., E. P. Cisneros, et al. (2000). A robust PI control configuration for a high-purity ethylene glycol reactive distillation column. Chem. Eng. Sci. 55: 4925-4937. Narendra, K. S. and J. Balakrishnan (1997). Adaptive Control Using Multiple Models. IEEE Transactions on Automatic Control 42(2): 171-187. Ogunnaike, B. and W. Ray (1994). Process Dynamics, Modelling and Control. Oxford, Oxford University Press. Rugh, W. J. and J. S. Shamma (2000). A Survey of Research on Gain Scheduling. Automatica: 1401- 1425. Sågfors, M. F. and K. V. Waller (1995). Dynamic Low-Order Models for Capturing Directionality in Nonideal Distillation. Ind. Eng. Chem. Res. 34: 2038- 2050. Sneesby, M. G., M. O. Tadé, et al. (1997). ETBE Synthesis via Reactive Distillation: 2. Dynamic Simulation and Control Aspects. Ind. Eng. Chem. Res. 36: 1870-1881. Sneesby, M. G., M. O. Tadé, et al. (1999). Two-Point Control of a Reactive Distillation Column for Composition and Conversion. J. Process Control 9: 19-31. Sorensen, S. and S. Skogestad (1994). Control strategies for reactive batch distillation. J. Process Control 4: 205-217. 122 123 124 125 126 127 128 129 0 20 40 60 80 100 120 time (min) stage7temp.(C) 0.9698 0.97 0.9702 0.9704 0.9706 0.9708 0.971 0.9712 0.9714 0.9716 0.9718 0.972 ETBEpurity(wt) PI-Purity MGS-Purity PI-T7 MGS-T7
  • 8. Tian, Y. C. and M. O. Tadé (2000). Inference of Conversion and Purity for ETBE Reactive Distillation. Brazilian J. of Chem. Eng. 17(4-7): 617- 625. Tian, Y.-C., F. Zhao, et al. (2003). Pattern-based predictive control for ETBE reactive distillation. J. Process Control 13(1): 57-67. Vora, N. and P. Daoutidis (2001). Dynamic and Control of an Ethyl Acetate Reactive Distillation Column. Ind. Eng. Chem. Res. 40: 833-846. Wajge, R. M. and G. V. Reklaitis (1999). RBDOPT: a general-purpose object-oriented module for distributed campaign optimization of reactive batch distillation. Chem. Eng. Journal 75: 57-68.