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ACKNOWLEDGEMENT 
With due respect, I express my deep sense of gratitude to the respected and learned 
guides of Indane Bottling Plant, Oil India Corporation Limited (marketing division) for 
providing their painstaking and untiring supervision. I am thankful to the training 
center for giving me the opportunity to learn deeper inside the basics of “study of 
operation of various mechanical units involved in the bottling of LPG cylinders”. 
I also express my sincere thanks to Mr. Hitesh Mehta, Assistant Manager 
(Engineering), Indane Bottling Plant, OIL (Marketing Division) for providing me with a 
conducive environment and necessary facilities, allowing me to reach the desired 
accomplishment. 
I am heartily thankful to all the Managers, Engineers and all Shift Operators 
working under them to give me direction and valuable inputs on each and every 
sections of study of operation of various mechanical units involved in the bottling of 
LPG cylinders. 
MOHIT DHULL 
B.Tech 5th semester 
Mechanical Engineering 
Guru Jambheshwar University of 
Science and Technology 
(GJU S&T)
INTRODUCTION 
Over 100 million LPG consumers in the domestic sector in India are serviced 
Through a network of 9365 LPG distributors who are getting supply from 181 LPG 
Bottling plants located across the country. In 2007-08, India consumed a total of 
About 1170 TMT of LPG which is around 10% of the consumption of total 
Petroleum products in the country. Out of the total LPG consumption during the 
Year 2007-08, almost 75% was used for cooking, 17% as auto LPG and the 
Remaining 8% for industrial use. Of the total supply of 11.7 Million Tonnes of LPG 
During 2007-08, the indigenous production was 8868 TMT from crude oil and 
Natural gas fractionation (3:1). Imports by PSUs and private entrepreneurs 
Accounted for 2156 TMT and 673 TMT respectively. 
LPG is transported from production installations i.e. Refineries, Fractionation 
Plants and Import terminals to the bottling plants through pipelines, Bulk LPG 
Wagons or Bulk LPG Tank Trucks. This LPG, subsequently, is bottled in 19 Kg, 
14.2 Kg and 5 Kg cylinders and is then delivered to commercial consumers and 
Individual households. Bottling operation of LPG is very critical, as LPG is a highly 
Inflammable product and the systems are required to be intrinsically safe. The 
Systems also require very comprehensive fire safety arrangements. 
A typical LPG bottling plant has the following major energy consuming 
Equipments:- 
1. LPG pumps 
2. LPG compressors 
3. Conveyors 
4. Blowers 
5. Cold repair facilities including painting 
6. Air compressors and air drying units. 
7. Transformer, MCC & DG sets 
8. Firefighting facilities 
9. Loading and unloading facilities 
Some of the LPG bottling plants use a comprehensive monitoring technique for 
Keeping track of energy / fuel Consumption on per tonne basis. PCRA's energy 
audit 
Studies in various LPG plants have found 20-25% energy saving potential in the 
LPG Plant operations. The following are major energy conservation opportunities 
In a LPG Plan
INTRODUCTION (OIL) 
Oil India Limited (OIL), an E & P company is a premier National Oil Company engaged in the 
business of Exploration, Production and Transportation of crude oil and natural gas. A Navratna 
Company under The Ministry of Petroleum and Natural Gas, Government of India, it is the 
second largest national oil and gas company in India as measured by total proved plus probable 
oil and natural gas reserves and production. Incorporated as a private company in 1959, OIL has 
been present in the Indian oil and gas exploration and production industry for over five decades. 
The company presently produces around 3.90MMTPA (Metric Million Ton Per Annum) of crude 
oil, around 7.93MMSCUMD (Metric Million) of natural gas and more than 45,010 tons of LPG 
annually. 
Main Producing Areas:- 
 Assam, Arunachal Pradesh and Rajasthan in India. 
 Customers: 
 Assam-AGCL, BVFCL, ASEB, NEEPCO, IOC and APL 
 Rajasthan-RRVUNL 
 The company operates a crude oil pipeline in the North-East for transportation of crude oil 
produced for both OIL and ONGCL in the region to feed Numaligarh, Guwahati, Bongaigaon and 
Barauni refineries and a branch line to feed Digboi refinery. 
 Moreover it has also extended its blocks overseas in Iran, Libya, Gabon, Nigeria, Sudan, Yemen, 
Egypt and Timor Leste. 
 A reservoir of hydrocarbons from where natural gas and oil are collected through a drilling in the 
earth is called a well. 
 Types- Oil and gas well 
 Oil well – crude oil + associated gas 
 Gas well – natural gas(unassociated gas) + condensate 
There are various departments in OIL a few are:- 
 Production (Oil & Gas) 
 Civil engineering 
 Chemical engineering 
 LPG 
 Geological 
 Electrical engineering 
 Instrumentation 
 IT 
 Fire and Safety 
 Transport 
 Field communication 
 Field engineering 
 Drilling 
 Well logging 
 Geophysics 
 Materials 
 Medical 
 Finance and maintenance 
 Training and development
OIL’S LPG PLANT 
The two major products of Oil India Limited are Crude Oil 
and Natural Gas, LPG (Liquified Petroleum Gas) being an 
important value addition to the natural gas produced. It 
is the first diversification of OIL active since the last 29 
years. 
LPG department has two installations:- 
(i) LPG Recovery Plant 
(ii) LPG Filling Plant 
The various sections at LPG department are:- 
(a) Recovery Plant Operation 
(b) Filling Plant Operation 
(c) Mechanical and General Maintenance 
(d) Electrical 
(e) Instrumentation 
(f) Quality control 
(g) Safety 
(h) Planning & Administration
LPG RECOVERY PLANT 
This plant indulges in production of LPG and a by-product 
i.e, Natural Gasoline (Condensate) from 
natural gas. 
Designed and commissioned in 1982 by The Randall 
Corporation, USA, it is the second plant in India 
where LPG is produced from natural gas. 
Maintenance of high productivity, quality and 
concern for safety, health and environment in a 
professional manner has always been the main 
motto of this department. 
The plant was originally designed to handle 2.215 
MMSCM/day of natural gas to produce 60,000 TPA 
of 50:50 (w/w) C3H8:C4H10 LPG and 12,000 TPA of 
condensate on 350 days working. But due to 
changes in the feed gas composition the plant 
design capacity has been re-rated as 55,000 TPA of 
49:51 (w/w) C3H8:C4H10 LPG and 25,000 TPA of 
condensate.
LPG is liquefied petroleum gas which is a mixture of 
certain light hydrocarbons, derived from petroleum, 
which are gaseous at ambient temperature and 
atmospheric pressure but may be condensed to liquid 
state at ambient temperature by the application of 
moderate pressure. Liquefaction is accompanied by a 
considerable decrease in the volume, thus the liquid 
formed requires much less storage space stored in the 
liquid phase in pressurized containers and systems, 
finally allowed to revert to the vapour phase at or 
near the point of eventual utilization. 
The feed gas, i.e ,natural gas is first drilled from 
oil well and gas well and then collected at the OCS 
from where it is sent via pipelines to the main plant 
area. 
In the process of LPG production, the plant also 
produces a high revenue-earning by-product, i.e, 
Natural Gasoline, which contains pentane and hexane 
and it is sold to solvent-manufacturing companies like 
EPC International, Sikkim Organics, etc.
Important Properties of LPG 
LPG is colourless, odourless, highly volatile and 
hazardous liquid that mixes quickly with air. It is 
heavier than air and one litre of LPG when expands 
produces about 250 litres of vapour. 
Max. Vapour pressure at 40 deg. C =1050 kPa, gauge 
Volatility i.e. evaporation temp. In deg. C for 95 % by 
volume at 760 mm of Hg pressure, Max = 2.0 
Hydrogen sulphide ======= pass, i.e. Hydrogen 
sulphide is not more than 5 ppm 
Free water content======= none 
Min. 20 ppm of ethyl mercaptan for odor. 
Auto-ignition temperature==410 to 580 degree Celsius 
Flash Point ============== -104.4 degree Celsius 
In a closed liquid filled vessel or pipe, for 1 degree rise 
in temperature, the pressure increases by 14 to 15 
kg/cm^2 
Explosive Limit =========== 1.85 to 9.5 % v/v in air
PROCESS 
The process comprises of broadly the following:- 
(a) Compression 
(b) Dehydration 
(c) Product extraction through: 
(i) On stream cooling by heat exchanger 
(ii) Turbo expansion 
(iii) Removal of non-condensable and undesired lighter 
fractions 
(d) Product fractionation 
 The different stages are as follows:- 
• Compression:- 
 1st stage -> Inlet Gas Compression Suction Scrubber 
 The inlet gas enters at 14kg/cm^2, is compressed to 
33.8kg/cm2 in a 4 stage centrifugal compressor driven by 
York Manufacturer’s 4500HP electric motor operating on 
11KV power supply. 
 The heat of compression is partly used in re-boiling the 
bottom liquid of de-ethanizer and then cooled to 37.8’c in 
water cooled heat exchanger.
2nd stage -> Booster Compression Suction Scrubber 
 The gas is then compressed to 41.9 kg/cm2 driven by the turbo 
expander and then cooled to 37.8’c. 
 It is then sent through an inlet filter separator wherein any water 
that may condense out is knocked out. 
• Dehydration:- 
 The gas is dried in one dehydrator while the other is being 
regenerated. 
 The pressure of compressed gas decreases to 39.6 kg/m2 as it 
reaches dehydrator. 
 Dehydrator consists of molecular sieve made of crystallized metal 
Aluminum Silicate of 4A’ size of approx. 11650kg weight in which 
water particles are retained. 
 This process is required as the temperature of the gas can go 
down up to minus 100’c where ice crystals form. 
 The dehydrated gas passes through a dust filter to remove sieve 
dust etc. 
• Product extraction:- 
 70% (by volume) of inlet gas is exchanged with cold residue from 
de-ethanizer and expander separator overhead, 30% (by volume) 
exchanges heat with the cold separator liquid in the gas-liquid 
exchanger and also with the expander separator liquid. 
 These two streams combine to enter the cold separator. 
 Liquid condensed is separated by cold separator and then the 
liquid is pressurised through the de-ethanizer reflux condenser.
 The inlet gas from the cold separator enters the expander where 
the pressure is lowered, following Joule-Thompson Effect. 
 The gas liquid mixture out of the expander of 1670 HP and 27000 
rpm speed reducing temperature to -84’c, is separated in the 
expander separator. 
 Liquid thus collected flows to the de-ethanizer feed pre-heater 
and then to the de-ethanizer. 
• Product Fractionations:- 
 A de-ethanizer column with three separate packed sections and 
a reboiler. 
 The liquid formed at the cold separator and the expander 
separator enter it, by maintaining proper bottom temperature 
with reboiler and reflux, the undesirable liquefied fraction 
methane, ethane and excess of propane are knocked out from the 
top. 
 The temperature of LPG is increased by exchanging heat with 
residue gas, whose refrigeration is in turn used in heat gas 
exchangers. 
 A de-butanizer column having 34 trays and reboiler provision 
through closed circuit hot oil systems with direct fired heater. 
 The bottom liquid flows on to de-butanizer tower where LPG and 
condensate are separated out. 
 LPG comes out at the top which is cooled to ambient temperature 
and sent for storage in bullets and Horton spheres. 
 The bottom condensate (Natural Gasoline) is similarly stored in 
separate storage tanks.
Fire Protection & Safety 
LPG is a colorless liquid which evaporates easily into a 
gas, and the leakage of even a small volume can expand 
into a large hazardous zone. Since it has no smell, a little 
mercaptan is added to help detect leaks. 
It can burn and explode when gets mixed with air and 
meets a source of ignition and it can also cause cold 
burns to skin. 
Therefore, Fire Protection & safety is of utmost 
importance in LPG plant. 
Safety in LPG plant includes:- 
 FIRE PROTECTION SYSTEM 
 ALARM AND SHUT DOWN SYSTEM 
 ESD DEVICE 
 SAFETY RELIEF VALVES 
 FIRE ALARM SYSTEM 
 GAS DETECTION SYSTEM 
 FIRE EXTINGUISHERS 
 FIRE DRILL 
 COMMUNICATION SYSTEM 
 REGULAR INSPECTION OF PLANT
Fire Protection System 
It comprises of:- 
1) A continuously pressurized water network of approximately 2 
km length, consisting of one 3000 kLs water reservoir, pumps, 
hydrant points, monitors (water and foam), hose reels, 
temperature sensing medium velocity water spray system. 
2) Portable fire extinguishers and sand buckets. 
3) Fire water pumps. 
4) Manual fire call points at different locations. 
One of the most important components of the safety system is the 
Deluge Valve, which is the controlling valve of the pressurized 
water network. 
It can be operated either on auto mode or manually. 
Auto Operation:- 
1) Water pressure is maintained in the hydrant system through a 
jockey pump. 
2) DV is kept closed by maintaining air pressure in the network. 
3) Due to rise in temperature, a heat detector bulb (Quartzoid bulb) 
in the air network bursts releasing air pressure. 
4) When air pressure drops, DV opens spraying water on the vessel. 
Manual Operation:- 
DV can be opened locally through a valve provided at the DV or by 
operation of a switch provided in the control room.
EQUIPMENT QUANTITY 
FIRE WATER PUMPS 
JOCKEY PUMPS 
HYDRANTS 
MONITORS 
FIRE ALARM POINTS 
GAS DETECTION SYSTEM 
Sr.No. 
1 
2 
3 
4 
5 
6 
06 (04+02) 
02 
28 (21+7) 
16 (9+7) +2 
21 (12+9) 
28 (20+8)
Pump Capacity Head Drive Auto start 
pressure M3/ Hr meter WC (on discharge line) 
Jockey 20 90 Electric Motor 4.6 kg/cm2 
Pump [Auto stop pressure = 8.4 kg/cm2] 
(02 Nos.) 
Sprinkler 275 88 Electric Motor 4.0 kg/cm2 
Pump 
Spray 410 88 Electric Motor 1.0 kg/cm2 
Pump 
‘B’ 
Spray 410 88 Electric Motor 2.0 kg/cm2 
Pump ‘A’ 
Hydrant 410 88 Electric Motor 3.0 kg/cm2 
Pump 
DEFP -1 410 88 Diesel Engine 
DEFP -2 410 88 Diesel Engine 2.5 kg/cm2
Alarm and Shutdown System 
The plant has got automatic in-built shutdown system to 
protect the vital equipment and the plant as a whole from 
any abnormal condition of operation. Audio-visual alarms 
and shutdown indications are displayed in LPG control 
room. 
 All the important equipment are provided with alarm 
and shutdown devices for critical operating 
parameters. 
 All the storage devices are provided with high level 
alarms. 
 Emergency shutdown switch is provided in control 
room to shut down the plant in any case of emergency. 
 Remote shutdown switches are provided in the local 
panels of two most important equipment- inlet gas 
compressor and expander compressor. 
Status monitoring is done round the clock through DCS work 
stations. Operation tested during running condition, 
planned and non-planned shutdown of the plant. 
Testing/calibration is done as and when required for smooth 
running of the plant and also during the annual 
maintenance of plant.
EMERGENCY SHUT-DOWN SYSTEM(ESD) 
The plant is equipped with ESD switches which calls for shut down in emergency 
situations. The plant has these emergency switches in three locations – (a) Top 
Control Room (b) Bottom Control Room (c) Expander Compressor Panel 
SAFETY RELIEVE VALVES 
SRVs are required to release the excess pressure build-up in the system due to 
process upset etc. so that they are protected from failure due to over- pressure. 
These valves are provided in the scrubbers, inlet filter separators, dehydrators, 
gas flow lines and in each of the process pressure vessels. 
FIRE ALARM SYSTEM 
The fire alarm system consists of alarm switch glass, which when broken will lead 
to an audio –visual alarm at the bottom control room indicating the location of 
emergency , and also hooting of sirens in LPG Recovery and Filling Plant areas. 
GAS DETECTION SYSTEM 
Gas Detectors, located at the vulnerable areas of the plant, detects the leakage of 
any explosive gas displaying the amount of leakage in terms of %LEL, together with 
hooting of an alarm in the DCS system of the control room.
FIRE EXTINGUISHERS 
Fire Extinguishers are classified into the following categories, as per the 
nature of associated fire- 
 Type A: for general fire out of wood, paper and other such stationary sort 
of stuffs. 
 Type B: for fire from liquid as diesel, petrol, diesel etc. utilizing dry 
chemical powder 
 Type C: for gaseous fire, as LPG gas, Natural Gasoline etc. utilizing 
carbon dioxide 
 Type D: for electrical and metallic source fire 
FIRE DRILL 
Fire drill is carried out forth nightly in LPG Recovery and also in LPG Filling 
Plant by the plant personnel from all sections along with personnel from 
Fire Service Section ( General Engineering Department ) to test the 
performance of the Fire Protection System of LPG Department and to take 
corrective action as necessary. 
COMMUNICATION SYSTEM 
Both LPG Recovery and Filling Plant are provided with 2 fire sirens (1 km and 5 
km region) incorporating the entire area. The smaller siren is operated in manual 
mode in normal fire drill, else the bigger siren is operated. The bigger siren is 
inter-locked with fire alarm switches which run in auto-operation mode.
Instrumentation 
The role of this section is to quantify all physical parameters such as 
pressure, temperature, flow rate and liquid level. It is an integral 
part of LPG department of OIL. 
 LPG implements PLC other than DCS dedicated to equipment 
control only, sequential start and stop of all devices and tripping of 
plants during emergency is done by PLC. Whereas DCS controls the 
entire process temperature, flow and level. 
=====Two types of control systems are===== 
• Distributed Control System (DCS):- is a digital control system based 
on distributed control philosophy. It means a control system which 
works on the principle of power delegation, for which there should 
be some connectivity to reach the data to all nodes i.e. Ethernet 
dual ring network called distributed communication network. 
• Programmable Logic Control (PLC):- is a digital computer used for 
automation of electromechanical processes, designed for multiple 
inputs and output arrangements, extended temperature ranges, 
immunity to electrical noise, and resistance to vibration and impact. 
• AC 460 is the heart of the system used to execute any function to 
maintain it, acts as interface and reads and writes over the I/O 
panel. 
• Ethernet connection is used to communicate or integrate all the 
nodes. 
• Graphics package are used to build plant objects. 
• Text package provides libraries through which the system is 
configured and started. 
• Database management might be there and uses oracle to send 
report. 
• Input devices- transmitter
The different devices used and maintained by this section are 
as follows: 
• Gas Chromatography: - used for analysing a mixture of 
a sample, a fully electronically controlled device. It consists 
of columns and detectors situated in the oven maintained 
at 80’c. 
• Moisture Analyzer: - If the temperature is less than - 
80’C, the moisture in the gas will become saturated and 
form ice crystals which blocks the pipelines and hence has 
to be prevented. This is done by placing a device at 
different locations for checking the amount of moisture 
present and creates an electrical signals. 
• TCD (Thermal conductivity detector):- uses the 
property of thermal conductivity of gases and converts 
into electrical signals unique for each and every gas 
imitating the same property which are received by the 
calibrated and programmed computers. 
• Thermocouple is used for sensing temperature. 
• Level transmitters work based on Archimedes Principle. 
=======the different types are======= 
 Magnetic level gauge 
 Radar level gauge 
 Servo level gauge 
 Floatation method on the basis of buoyancy force
Flow rate indicator: - 
• Mass flow meter: - senses both gravity and volume. It 
carries out a lot of algorithms considering the resonant 
frequency of the U wire which gives the inertia of the 
liquid and temperature for gravity calculation. 
• Orifice flow meter: - works on the Bernoulli’s principle and 
specifies only volume. 
Types of valves: - 
• Shutdown valve 
• Deluge valve 
• Solenoid valve: - is a logical valve and operated by 
solenoid coil which opens up at 110V of AC current or 
240V DC. 
• Safety relief valve: - are protection devices used in the 
worst conditions and are always maintained. 
• Remotely operated valve (ROV): - It is a logical valve 
which either closes or opens and requires 60-70psi. The 
feedback signal is received through PLC in control room 
and is used only for shutdown, can’t be controlled. 
• Control valves: - are the ultimate output devices. 
• Audio, visual, olfactory and vibration are the four types of 
alarms used.
Pressure gauges, based on the Hooke’s law relating stress 
and strain, consists of the following components: - 
• C-type tubes 
• Spiral type 
• Bello 
• Diaphragm 
• Dead weight tester 
• Manometer 
 DP (Differential Pressure) transmitter: - measures the 
difference in pressure through micro-controller. 
 LEL (Lower Explosive Limit): - calibrated optimum quantity 
of a combustible substance which can support a self-propagating 
flame when ignited. The device uses the 
infrared radiation emitted by the gas which is dependent 
on its concentration. The inner part is maintained at a 
higher temperature causing convection i.e. the hot air rises 
due to its lower density sucking in the air below which is at 
a lower temperature. 
• LELs of substances in terms of percentage present in the 
atmosphere are- 
• CH4- 5% 
• LPG- 1.2% 
• Condensate- 1.8% 
• If LEL exceeds 10% sparking is prohibited.
Process water: - 
• The pH must be maintained in the alkaline range i.e. more 
than 7 as acidic process water may cause scaling in the 
heat exchangers. This can be done by treating the water 
with NaOH and KOH. 
• The viscosity should not be very high. 
• This water cannot be released into the environment 
without being treated for its salinity, pH, minerals added 
and oil accumulated. 
The methods employed to dispose off this water without 
causing any damage are: - 
 Flocculent (gravity) and coagulant (sand) filters 
 Aerobic and anaerobic treatment 
 UV rays cleaning system 
 Bleaching(chlorine) 
 Demineralization: - is a series of anion and cation 
exchanger to maintain the pH around 7. 
 The minerals such as Ca, Mg, SO4-2, Cl-1 can be removed 
completely but the water cannot be polished off silica if its 
concentration is below 2ppm. 
 The water is heated in a high pressure water boiler. 
 If the toxic level of water is very high and cannot be 
treated it is injected back into the well.
Quality Control Laboratory 
It is a branch of the Chemical department of OIL, and being a service 
section its main role is to evaluate the quality of products, LPG and 
Residue Gas, along with the feed gas that is, Natural Gas. 
It mainly performs two types of tests, viz., compositional and physical. 
1. Physical Analysis: - 
It includes Volatility and Vapor Pressure tests as per IS 4576: 1999 
certification, depending on which one can decide whether the product 
is good or bad. 
a) Volatility: - It is measured by Weathering Test. In this test, the 
sample is taken in a tube called weathering tube and a 
thermometer is put in it. The temperature is noted at 25, 50, 90 
and 95 percent (by volume) evaporation and the temperature 
corresponding to 95% evaporation is called the Weathering 
Temperature and it should be in the range of +2 degree C and -2 
degree C. 
b) Vapor Pressure: - For this we take the sample in a sampler and 
put it in a temperature bath which is maintained at 40 degree C 
and we check the pressure building up at this temperature 
indicated by the pressure gauge. 
Apart from these tests, some other tests are also performed to measure the 
density of sample, moisture level and also the Ethyl Mercaptan (C2H5SH) 
level in LPG. A hydrometer is used to measure density. 
We use Doctor’s Test to check minimum value of Mercaptan added to LPG. 
For this, Sodium Plumbate solution is taken in a cylinder and LPG sample is 
added which mixes with it. A positive Doctor’s Test gives a yellow 
precipitate/solution indicating presence of Mercaptan.
Dew Point Test: - 
We have to check dew point at dehydrator inlet and outlet, gas 
inlet and air inlet. As the feed gas, after compression, needs to 
be dehydrated using dehydrator, hence we need to check 
whether the molecular sieves (which are made of alumina 
silicate) are working. 
2. Compositional Analysis: - 
It includes compositional analysis of the natural gas coming from 
production department, LPG and Residue gas, done by Gas 
Chromatography (GC), as explained below: - 
GC, a common type of chromatography performed in a Gas 
Chromatograph, is used in analytical chemistry for separating and 
analyzing compounds that can be vaporized without decomposition. It 
is based on different boiling points and retention time for different 
components. It is used for testing the purity of a particular substance, 
or separating the different components of a mixture. 
GC consists of two phases: - mobile phase and a stationary phase. 
Here the mobile phase is a carrier gas, usually an inert gas like Helium 
or a non-reactive gas like Nitrogen. 
The stationary phase is a microscopic layer of a liquid or a polymer on 
an inert solid support, inside a piece of glass or metal tubing called a 
column. 
The molecules move to the wall of the column, coated with different 
stationary phases, which causes each compound to elute at a different 
time, known as the Retention Time of the compound.
GC Analysis:- 
In a GC analysis, a known volume of gaseous or liquid analyte is 
injected into the column using a micro-syringe. As the carrier 
gas sweeps the analyte molecules through the column, this 
motion is inhibited by the adsorption of the analyte molecules 
either onto the column walls or onto packing materials in the 
column. The rate at which molecules progress along the column 
depends on the strength of adsorption, which in turn depends 
on the type of molecules and on the stationary phase materials. 
As each type of a molecule has a different rate of progression, 
the various components of the analyte mixture are separated 
as they progress along the column and reach the end of the 
column at different times (retention time). A detector is used to 
monitor the outlet stream from the column, hence the time at 
which each component reaches the outlet and the amount of 
that component can be determined. 
Generally substances are identified by the order in which they 
emerge from the column and by the retention time of the 
analyte in the column. The chromatographic data is presented 
as a chromatogram, which is a graph of detector response (y-axis) 
against retention time (x-axis). This provides a spectrum of 
peaks for a sample representing the analyte present in a 
sample eluting from the column at different times. The area 
under a peak is proportional to the amount of analyte present 
in the chromatogram, and by calculating it, the concentration 
of an analyte in the original sample can be determined.
Electrical maintenance 
• The power house of OIL generates 14.45 MW with the help of two gas 
turbines which are alternatively at running and standby modes. 
• The power house supplies 11KV to the substation in the LPG plant through 
two underground cables. 
• This incoming power is sent into the feeder from two different power 
houses, #1 and #2. These two sections are connected by a bus coupler 
which is used only when the maintenance job needs to be done. 
• From #1 the 11KV is supplied to the spare feeder, 4500HP motor starter 
panel and to a transformer1 of 1000KVA capacity which steps 11000V down 
to 415V. 
• There are 8 vacuum circuit breakers. It is monitored by protective relays 
such as VCB, ACB, SF6 of the circuits. 
• UPS system gives an uninterrupted power supply normally of AC current 
with a battery backup of 120KVA capacity. There are 2 types of UPS in 
which input is 415V but outputs are 415V and 110V. 
• A battery converts a voltage input of AC to DC. An 110V Ni-Cd battery set is 
used. 
• Another auto-transformer other than the two in the feeder circuits produce 
450V line. It is a part of motor starter panel. During starting of motor the 
load might reach seven times its full load and then drop back which can’t be 
allowed. To reduce this we use this auto-transformer starter for 20 seconds 
and then give back to the normal system. 
• Motor control center (MCC) is provided by the 415V bus. 
• Tripping is a condition when difference between the incoming and outgoing 
currents of the isolator is more than a given value and the on-off switch of 
the isolator turns off automatically.
AUTOTRANSFORMER: - 
• Auto-transformer is used for applying reduced voltage to stator during 
starting. Thereby the starting current is reduced. The auto-transformer is 
provided with change-over switch. As the motor comes to full speed, the 
change-over switch is thrown over to run position. 
CIRCUIT BREAKER AND ITS TYPES: - 
• Circuit Breaker is an automatic device capable of making and breaking an 
electric circuit under normal and abnormal conditions such as short circuits. 
The part of the circuit-breakers connected in one phase is called the pole. A 
circuit-breaker suitable for three phase system is called a triple pole circuit-breaker. 
• Each pole of the circuit-breaker comprises one or more interrupts or arc-extinguishing 
chambers. The interrupters are mounted on support 
insulators. The interrupter encloses a pair of fixed and moving contact. The 
moving contacts can be drawn apart by means of the operating links or the 
operating medium. The operating mechanism of the circuit-breaker gives 
the necessary energy for opening and closing of contacts of the circuit-breakers. 
• The arc produced by the separation of current carrying contacts is 
interrupted by a suitable medium and by adopting suitable techniques for 
extinction. 
• Circuit Breaker is used for opening and closing circuits for normal switching 
operations. During short circuits or abnormal conditions, relay operates and 
gives opening command to circuit-breaker and circuit is opened 
automatically. 
TYPES OF CIRCUIT BREAKERs IN LPG PLANT: - 
• Moulded Case Circuit Breaker (MCCB): 
• Air Circuit Breaker (ACB): It utilizes air at atmospheric pressure for arc- extinction. 
• Vacuum Circuit Breaker (VCB): The fixed and moving contacts are housed inside a 
permanently sealed vacuum interrupter. The arc is quenched as the contacts are 
separated in high vacuum.
POWER HOUSE 
Power House generates power for the entire plant using the concept of 
a Gas Turbine, which is based on the Bryton Cycle. 
The following components comprise a Gas Turbine: – 
(a) Axial Air Compressor 
(b) Combustor 
(c) Turbine 
(d) Auxiliaries 
Axial Air Compressor: - 
Air after passing through the filter enters the axial compressor and 
flows parallel to the axis .it consists of a stationary body called Casing 
and a moving part called Rotor, and Blades , some of which are 
attached to the casing and some to the rotor . A pair of stationary and 
moving blades is called a Stage and the compressor has got 15 such 
stages. Air gets compressed as it passes through the different stages. 
Combustor: - 
Air from the compressor enters the combustor which has 2 parts –a 
transition piece and a combustor, the latter being divided into 3 zones, 
viz, primary, secondary and tertiary, each consisting of a number of 
holes. 
Fuel is injected in the primary zone and ignited using spark from the 
spark plug, thereby creating a cyclone.
In the secondary zone, complete burning of fuel is 
ensured. As the temperature of air rises to a high value 
of 1200 degree C, it needs to be cooled down to 899 
degree C at least before entering the transition piece. For 
this more air is to be supplied to the tertiary zone. 
The transition piece has a nozzle which increases the 
velocity of air. 
Turbine: - 
Air from combustor enters the turbine where it expands 
and exits as exhaust gas. The rotating turbine then 
generates power via a generator. The exhaust gas is at a 
temperature of 370 degree C and this energy can be 
utilized to produce more electricity using the steam 
turbine. For this DM (De-Mineralized) plant is required 
but this is a costly process. This produces about 7 M watt 
power in addition to the actual power of 14.45 M watt. 
As the Gas Turbine is not self-starting, a starter diesel 
engine is required. 
A total of 14.45Mwatt electricity is the output from the 
generator. Out of this 10.4Mwatt is utilized to fulfill the 
electricity requirement of the different units of the 
industry.
Mechanical Maintenance 
The Maintenance Section of the LPG department is 
responsible for the following: - 
1)Maintaining the plant availability to achieve MOU target. 
2)Maintenance of all rotary and stationary equipment of the 
LPG plant to keep them in proper working conditions. 
3)Execution of various contract jobs under the department 
related to maintenance of the plant. 
4)Planning of maintenance activities for annual plant 
maintenance. 
5)Spare part management for maintenance of the plant. 
This section aims to achieve the following targets: - 
1)To reduce the cost of maintenance activities by 1 % of the 
previous year. 
2)To keep the minimum MTTR of critical equipment for 
achieving the MOU target. 
3)To keep good relations and understanding with the different 
sections of the LPG department. 
4)To keep good relations and understanding with the other 
departments of the company. 
5)To keep close watch on various activities so that there is no 
misuse of approved funds and that these are properly 
utilized.
The Mechanical Maintenance Section of the LPG department 
is responsible to perform the following duties: - 
1) Daily plant check up to ensure smooth operation of the plant and to 
check lube oil level and vibration & sound and other parameters. 
2) Monthly vibration measurement to ensure that vibration levels of 
critical equipment are within limits and take necessary corrective 
measurements. 
3) Periodical lube oil testing to test lube oil of three major equipment of 
LPG recovery section, namely, Inlet Gas Compressor, Gear Box and 
Expander-Compressor. 
4) Cleaning of cooling tower top chambers to ensure its proper 
functioning. 
5) Testing of SRV to ensure its correct functioning at its Set Pressure. 
6) Sound level measurement to measure the intensity of sound at 
specified locations and compare it with permissible limit. 
7) Replacement of damaged or worn out Vee-Belt (Endless belts used 
between driving pulleys to transfer power). 
8) Replacement of empty Mercaptan drum of LPG storage area. 
9) Top up lube oil into Expander Surge Tank to maintain a certain oil level 
in it. 
10) Air compressor lube oil top up to maintain the required level of oil. 
11) Materials inspection and suitability report for the acceptability of 
the materials received against direct charge Indents/purchase orders. 
12) Engaging staff on overtime to complete the repairing job within the 
day in view of urgent nature of work for operational as well as safety 
requirements.
13) Workshop job requisition to carry out emergency repair 
and fabrication jobs at general workshop. 
14) Breakdown maintenance of machines/ equipment. 
15) Preparation of tentative maintenance schedule of air 
compressor. 
16) Ultrasonic thickness measurement to gauge metal 
surfaces for the thickness. 
13) Handling/cleaning services and day-to-day maintenance 
in LPG recovery and filling plant. 
14) Servicing, Inspection and Testing of LPG storage vessels. 
15) To replace hot and cold insulation system of LPG 
recovery plant with new insulation system at a specified time 
interval. 
16) Major overhauling of Inlet Gas Compressor and Expander 
Compressor to ensure smooth and trouble free operation. 
17) De-coupling of various motor devices to carry out 
maintenance work on driver (motor) or driven side (pumps, 
compressors, fans, etc.). 
18) Hydro-testing of pressure vessels and storage vessels to 
check the condition/health of vessel. 
19) Periodical testing of lifting tools. 
20) Storage, handling and disposal of lube oil and other 
hazardous materials.
LPG Filling Plant 
• In LPG Filling Plant – 
(i) LPG is bottled into cylinders (packed form) in Carousel 
machine containing 24 number of filling points or guns. 
(ii) LPG is filled into road tankers (bulk form). These cylinders 
and road tankers are handed over to IOCL for marketing. 
• The LPG is pumped to LPG Filling Plant from LPG storage 
vessels at LPG Recovery Plant. 
• The incoming LPG pressure in the pipeline is about 14kg/cm2. 
The cylinder consists of a head ring, 3 fins, valve, high 
pressure seamed cylinder and a foot ring. 
• The inside of the valve is installed with an O-ring and a valve 
pin. The valve needs to be checked for any leak possible. 
• The bottling capacity of the plant is about 6000-7000 cylinders 
per day. 
• The empty cylinders are first marked by TARE WEIGHT 
MARKING and their marked weights are stored by a HMI 
(Human Machine Interface) device called pre-check scale. 
• The marked cylinders go to Carousel machine by chain 
conveyor, run by 14 motor driven Gear boxes. In Carousel 
machine the empty cylinders are first sensed by photo-electric 
sensors. 
• In each filling gun two sensors are linked which are placed at 
the top and at the bottom side of the cylinder.
• The bottom side sensor is called wheel arm sensor. The bottom 
photo-cell senses the position of the cylinder on the machine. The 
top photocell senses the cylinder and gives instruction to the gun. 
Then the respective gun shoots the respective cylinder. 
• The cylinder is filled in the course of one rotation of the carousel, 
the filling time is approximately 60 seconds. 
• When the regulator’s pin when pressed together with the valve 
pin, two holes are opened. 
• The LPG filled in the cylinder should be of weight 14.2 kg. If the 
gun is unable to fill the cylinder within one minute for delay error, 
the cylinder will again revolve for one minute. 
• In the outlet of the machine has a puller with sensor which 
allows only those cylinders filled up to the standard weight to go 
out of the machine, otherwise it will return back the cylinder to 
the machine again. 
• The cylinders are introduced through a check scale, which checks 
the over weighted cylinders and bypass them to another section 
called correction unit by pusher with photo-electric sensor. 
• The over weighted cylinders are manipulated up to the standard 
by manual filling. This over weighted range is considered as 
+200gm.Now the corrected cylinders are lined up with the other 
cylinders. 
• Now the cylinders are fed to Gas detector and O-ring detector 
unit to check the leakages and damages. In this unit the damaged 
cylinders are rejected. The tested cylinders are then fed to 
counting unit to count by a sensor and stored. In hot air sealing 
unit the cylinders are sealed and fed to transportation section.
• The evacuation unit takes care of the rejected 
cylinders which are found defective by applying 
suction pressure on the LPG cylinder and the 
valuable LPG is sent back in the form of vapor to the 
storage tanks. 
• In the sealing unit i.e. Hot air seal unit, a plastic cap 
is placed over the cylinder along with a thin PVC seal 
which then is exposed to 265’C of hot air. 
• Compressed air of 7.5kg/cm2 is required for the 
functioning of the plant, which is done by using V-type, 
screw-type and vertical air compressor which 
are manually checked after the working hours which 
can be done. 
• In bulk filling, LPG and condensate are filled into 
tankers following the same procedure as that of 
packed form. 
• The tanker is checked for a hydraulic testing 
certificate valid for a period of 5 years from the date 
of issue. 
• The tanker evacuation unit is utilized when excess is 
sent into the tanker. The liquefied form of LPG filled 
into the tank is 18% less than the total tanker 
capacity.
• 
CONCLUSION 
The vocational training enhanced my practical 
knowledge. Most importantly, I am oriented to the 
industrial scenario and its many challenges and 
subtleties. The smooth functioning of an industry 
depends to a large extent on the mutual co-operation 
among its different wings. 
Nevertheless, I did enjoy the training to the fullest 
and are very sure that this training will help me in 
my future endeavors. 
Thanking You
A REPORT ON INDUSTRIAL 
TRAINING 
AT 
OIL INDIA LIMITED 
BADSHAHPUR 
INDANE BOTTLING PLANT 
(MARKETING DIVISION) 
Submitted by: - 
MOHIT DHULL 
Bachelor of Technology 
5th Semester 
Department of Mechanical Engineering 
Guru Jambheshwar University of Science and Technology 
Hisar
A 
PRACTICAL TRAINING REPORT 
AT 
INDANE BOTTLING PLANT 
BADSHAHPUR, GURGAON 
INDIAN OIL CORPORATION LIMITED 
(MARKETING DIVISION) 
Submitted to: - Submitted by:- 
Mr. Kaushal Mohit Dhull 
Faculty of Mech. Deptt. 12162035 
GJUS&T BTECH. 3rd Year
PLANT LAYOUT 
SCOPE 
The general layout principles of LPG 
Storage, bottling and bulk handling facilities 
Have been detailed in this chapter. The various 
Facilities within LPG storage and bottling 
Premises shall be located based on Table-I and 
Table-II. 
TABLE – I 
INTERDISTANCES FOR LPG 
FACILITIES 
1 LPG STORAGE 
VESSEL 
2 T-11 T-11 15 T-11 
2 BOUNDARY NOT 
ASSOCIATED 
WITH LPG 
PLANTS 
T-11 - 15 15 - 
3 LPG SHED T-11 15 15 15 30 
4 TANK TRUCK 
GANTRY 
15 15 15 NA 30 
5 FIRE WATER 
PUMP HOUSE 
T-11 * 30 30 -
NOTES: - 1. ALL DIMENSIONS ARE IN MTS. 
2. NOTATION 
T-II: REFER TABLE II 
*: ANY DISTANCE FOR OPERATIONAL CONVENIENCE 
3. MAXIMUM PACKED STORAGE LIMITED TO 20000 KGS 
TABLE – II 
INTERDISTANCES BETWEEN LPG 
STORAGE VESSELS, FILLING SHED, 
STORAGE SHED 
AND BOUNDARY/PROPERTY LINE/GROUP 
OF BUILDINGS. 
CAPACITY OF EACH 
VESSEL 
(CU. MTS. OF WATER) 
DISTANCES 
(MTS.) 
10-20 15 
20-40 20 
41 – 235 Note 3 
30
LOCATION & SAFETY DISTANCES 
LOCATION 
While assessing the suitability of any site 
For location of LPG storage facilities, the 
Following aspects shall be considered: 
(a) In addition to the requirements for safety the 
Plant should be located in such a manner so 
As not to be contagious to any industry 
Having open flame. Property line of the 
Plant shall be away from the central line of 
The road/railways as per statutory 
Requirements and overhead high tension 
Wire shall not traverse through the battery 
Limit of the plant. 
(b) Adequate availability of water from a nearby 
Reliable source should be ensured.
(c) The topographical nature of the site wit 
Special reference to its effect on the disposal 
Of LPG, in the even of its escape, if any, 
Shall be considered. 
(d) The access for mobile fire fighting 
Equipment to the storage vessels under all 
Foreseen circumstances, preferably from two 
Sides and upward prevailing wind direction 
Is an important parameter. 
(e) For any expansion beyond the specified 
Limit, all provision under OISD-144 shall be 
Applicable. 
(f) Predominant direction of wind and velocity 
Shall be considered. 
(g) Longitudinal axis of horizontal vessels 
(Bullets) shall not point towards other 
Vessels, vital process equipment and other 
Facilities. 
(h) Storage vessels shall be located downward 
Of processing units, important buildings. 
(I) Storage vessels shall be laid out in single 
Row within a group. 
(j) Storage vessels shall not be located one 
Above the other.
SAFETY DISTANCES 
The safety distances as given in Table-I 
and Table-II are the distances in plane between 
the nearest point on a vessel other than the 
filling/discharge line and a specified feature, 
e.g. 
adjacent vessel, site boundary etc. 
TYPE OF STORAGE 
VESSELS 
HORIZONTAL CYLINDRICAL 
VESSELS 
Horizontal bullets with the total volumetric 
capacity upto 235 Cu. M. Note 3 shall be used 
for 
storing LPG.
LAYOUT 
The following aspects shall be considered while 
Establishing layout of LPG storage vessels. 
LPG STORAGE FACILITIES 
GRADING 
Area below the storage vessels 
(Bullets) shall be free from vegetation, property 
Graded with the slope of 1.100 (towards one 
Side) away from the pipeline manifold. 
PIPING 
(i) Piping manifold shall be away from the 
Shadow of the vessel. 
(ii)Spring loaded quick closing valve with 
fusible link or Rov to facilitate 
immediate closure in the event of 
emergency, if any, shall be provided in 
the LPG liquid line of each vessel 
between excess flow check valve 
(EFCV) and pipeline manifold.
SURFACE DRAINAGE 
In order to prevent the escape of spillage 
into the main drainage system, surface water 
from the storage area and from the manifold 
area shall be directed to the main drainage 
through a water seal designed to avoid the 
spread of hydrocarbon. 
GROUPING 
Vessels shall be arranged in a group and 
total volumetric capacity of the group shall 
be ,limited to 235 Cu. M. Note 3. Interdistances 
as specified in Table-I and Table- 
II shall be maintained. 
Top surfaces of all the vessels installed in a 
group shall be on the same plane so that the 
safety blowout from them do not affect each 
Other.
LPG BULK HANDLING FACILITIES 
1. LPG tank lorry loading/unloading gantry 
shall be located in a separate block and 
shall not be grouped with other petroleum 
products. 
2. Space for turning with a minimum radius 
of 20 meters for tank lorries shall be 
provided commensurate with the 
capacities of the tank trucks. 
3. LPG tank lorries upto the maximum of 2 
Nos, at a time should only be taken for 
unloading. 
4. Adequate permanent protection for TLD 
pipeline island shall be provided. The 
minimum width of such pipeline island 
shall be 1 metre.
LPG BOTTLIG FACILITIES 
(1) LPG Bottling facilities should be located a 
a safe distance from other facilities with 
minimum ingress of trucking traffic and 
downward wind direction with respect to 
bulk storage. 
There shall not be any deep ditches in the 
surrounding area to avoid settling of LPG. 
(2) Bottling section shedshall be of single story 
having asbestos roofing and open from all 
sides for adequate ventilation to ensure 
quick dessipation of LPG Vapour in the 
event of leakage, if any, RCC roofing 
shall not be used. Anti-static mastic 
flooring conforming to IS-8374 shall be 
provided in the LPG filling shed/cylinder 
storage shed to avoid frictional sparks. 
Anti-static mastic coating up to 1.5 meters 
Height from bottom of the supporting 
Columns in the shed shall be provided.
(3) Stacking area for empty and filled 
cylinders shall be marked specifically. 
Cylinders shall always be stacked 
vertically in two lines. For details of 
cylinders stacking pattern refer Annexure 
Plant should have one shed each for 
filling and storing of filled./empty 
cylinders. 
(4) Valve changing operation should be 
carried out in a demarcated place within 
the filling shed itself. 
(5) Cylinder storage shall be kept on or above 
grade and never below grade in celler or 
basement. 
(6) Filled cylinders shall not be stored in the 
vicinity of cylinders containing other 
gasses or hazardous substances. 
(7) Escape routes shall be specified in LPG 
sheds for evacuation of employees in 
emergency.
(8) There shall not be any trapping of 
personnel in LPG sheds by conveyours, 
cylinders and other facilities. If such 
trapping cannot be eliminated, it should be 
kept to the minimum. In such places 
sufficient arrangements for escape routes 
to be provided. 
(9) Adequate lighting shall be provided in the 
cylinder filling area. 
(10)Water drains from cylinder filling areas to 
out side drainage system shall be provided 
with water seals (near the plant boundary) 
PROTECTION OF FACILITIES 
(1) There shall be road all around the various 
facilities within the bottling plant areas for 
accessibility of fire fighting operations. 
(2) There shall be proper industry type 
boundary wall all around the Bottling 
Plant.
UTILITIES 
Utilities consisting of Fire Water Pumps, 
Admin. Building, Motor Control Center, DG 
Room, Air Compressors, Dryers etc. shall be 
separated from other LPG facilities and to 
be located as per the area classification as 
specified in Table-I.
CONTENTS
FACULTY CERTIFICATE 
Forwarded here with a summer internship report on “STUDY OF VARIOS 
MECHANICAL UNITS INVOLVED IN THE BOTTLING OF LPG CYLINDERS” of Indian 
Oil Corporation Limited submitted by Mohit Dhull, Enrollment No- 12162035 
student of Bachelor of Technology 5th Semester (2014-15). 
This project work is partial fulfillment of the requirement for the degree of Bachelor 
of Technology from Guru Jambheshwar University of Science and Technology 
Hisar, Haryana. 
-------------------------------- 
Mr. Kaushal 
Deptt. Of Mechanical Engg. 
Guru Jambheshwar University of Science and Technology
WORD FORMAT PROJECT REPORT ON VARIOUS MECHANICAL UNITS INVOLVED IN THE BOTTLING OF LPG CYLINDERS BY MOHIT DHULL

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WORD FORMAT PROJECT REPORT ON VARIOUS MECHANICAL UNITS INVOLVED IN THE BOTTLING OF LPG CYLINDERS BY MOHIT DHULL

  • 1. ACKNOWLEDGEMENT With due respect, I express my deep sense of gratitude to the respected and learned guides of Indane Bottling Plant, Oil India Corporation Limited (marketing division) for providing their painstaking and untiring supervision. I am thankful to the training center for giving me the opportunity to learn deeper inside the basics of “study of operation of various mechanical units involved in the bottling of LPG cylinders”. I also express my sincere thanks to Mr. Hitesh Mehta, Assistant Manager (Engineering), Indane Bottling Plant, OIL (Marketing Division) for providing me with a conducive environment and necessary facilities, allowing me to reach the desired accomplishment. I am heartily thankful to all the Managers, Engineers and all Shift Operators working under them to give me direction and valuable inputs on each and every sections of study of operation of various mechanical units involved in the bottling of LPG cylinders. MOHIT DHULL B.Tech 5th semester Mechanical Engineering Guru Jambheshwar University of Science and Technology (GJU S&T)
  • 2. INTRODUCTION Over 100 million LPG consumers in the domestic sector in India are serviced Through a network of 9365 LPG distributors who are getting supply from 181 LPG Bottling plants located across the country. In 2007-08, India consumed a total of About 1170 TMT of LPG which is around 10% of the consumption of total Petroleum products in the country. Out of the total LPG consumption during the Year 2007-08, almost 75% was used for cooking, 17% as auto LPG and the Remaining 8% for industrial use. Of the total supply of 11.7 Million Tonnes of LPG During 2007-08, the indigenous production was 8868 TMT from crude oil and Natural gas fractionation (3:1). Imports by PSUs and private entrepreneurs Accounted for 2156 TMT and 673 TMT respectively. LPG is transported from production installations i.e. Refineries, Fractionation Plants and Import terminals to the bottling plants through pipelines, Bulk LPG Wagons or Bulk LPG Tank Trucks. This LPG, subsequently, is bottled in 19 Kg, 14.2 Kg and 5 Kg cylinders and is then delivered to commercial consumers and Individual households. Bottling operation of LPG is very critical, as LPG is a highly Inflammable product and the systems are required to be intrinsically safe. The Systems also require very comprehensive fire safety arrangements. A typical LPG bottling plant has the following major energy consuming Equipments:- 1. LPG pumps 2. LPG compressors 3. Conveyors 4. Blowers 5. Cold repair facilities including painting 6. Air compressors and air drying units. 7. Transformer, MCC & DG sets 8. Firefighting facilities 9. Loading and unloading facilities Some of the LPG bottling plants use a comprehensive monitoring technique for Keeping track of energy / fuel Consumption on per tonne basis. PCRA's energy audit Studies in various LPG plants have found 20-25% energy saving potential in the LPG Plant operations. The following are major energy conservation opportunities In a LPG Plan
  • 3. INTRODUCTION (OIL) Oil India Limited (OIL), an E & P company is a premier National Oil Company engaged in the business of Exploration, Production and Transportation of crude oil and natural gas. A Navratna Company under The Ministry of Petroleum and Natural Gas, Government of India, it is the second largest national oil and gas company in India as measured by total proved plus probable oil and natural gas reserves and production. Incorporated as a private company in 1959, OIL has been present in the Indian oil and gas exploration and production industry for over five decades. The company presently produces around 3.90MMTPA (Metric Million Ton Per Annum) of crude oil, around 7.93MMSCUMD (Metric Million) of natural gas and more than 45,010 tons of LPG annually. Main Producing Areas:-  Assam, Arunachal Pradesh and Rajasthan in India.  Customers:  Assam-AGCL, BVFCL, ASEB, NEEPCO, IOC and APL  Rajasthan-RRVUNL  The company operates a crude oil pipeline in the North-East for transportation of crude oil produced for both OIL and ONGCL in the region to feed Numaligarh, Guwahati, Bongaigaon and Barauni refineries and a branch line to feed Digboi refinery.  Moreover it has also extended its blocks overseas in Iran, Libya, Gabon, Nigeria, Sudan, Yemen, Egypt and Timor Leste.  A reservoir of hydrocarbons from where natural gas and oil are collected through a drilling in the earth is called a well.  Types- Oil and gas well  Oil well – crude oil + associated gas  Gas well – natural gas(unassociated gas) + condensate There are various departments in OIL a few are:-  Production (Oil & Gas)  Civil engineering  Chemical engineering  LPG  Geological  Electrical engineering  Instrumentation  IT  Fire and Safety  Transport  Field communication  Field engineering  Drilling  Well logging  Geophysics  Materials  Medical  Finance and maintenance  Training and development
  • 4. OIL’S LPG PLANT The two major products of Oil India Limited are Crude Oil and Natural Gas, LPG (Liquified Petroleum Gas) being an important value addition to the natural gas produced. It is the first diversification of OIL active since the last 29 years. LPG department has two installations:- (i) LPG Recovery Plant (ii) LPG Filling Plant The various sections at LPG department are:- (a) Recovery Plant Operation (b) Filling Plant Operation (c) Mechanical and General Maintenance (d) Electrical (e) Instrumentation (f) Quality control (g) Safety (h) Planning & Administration
  • 5. LPG RECOVERY PLANT This plant indulges in production of LPG and a by-product i.e, Natural Gasoline (Condensate) from natural gas. Designed and commissioned in 1982 by The Randall Corporation, USA, it is the second plant in India where LPG is produced from natural gas. Maintenance of high productivity, quality and concern for safety, health and environment in a professional manner has always been the main motto of this department. The plant was originally designed to handle 2.215 MMSCM/day of natural gas to produce 60,000 TPA of 50:50 (w/w) C3H8:C4H10 LPG and 12,000 TPA of condensate on 350 days working. But due to changes in the feed gas composition the plant design capacity has been re-rated as 55,000 TPA of 49:51 (w/w) C3H8:C4H10 LPG and 25,000 TPA of condensate.
  • 6. LPG is liquefied petroleum gas which is a mixture of certain light hydrocarbons, derived from petroleum, which are gaseous at ambient temperature and atmospheric pressure but may be condensed to liquid state at ambient temperature by the application of moderate pressure. Liquefaction is accompanied by a considerable decrease in the volume, thus the liquid formed requires much less storage space stored in the liquid phase in pressurized containers and systems, finally allowed to revert to the vapour phase at or near the point of eventual utilization. The feed gas, i.e ,natural gas is first drilled from oil well and gas well and then collected at the OCS from where it is sent via pipelines to the main plant area. In the process of LPG production, the plant also produces a high revenue-earning by-product, i.e, Natural Gasoline, which contains pentane and hexane and it is sold to solvent-manufacturing companies like EPC International, Sikkim Organics, etc.
  • 7. Important Properties of LPG LPG is colourless, odourless, highly volatile and hazardous liquid that mixes quickly with air. It is heavier than air and one litre of LPG when expands produces about 250 litres of vapour. Max. Vapour pressure at 40 deg. C =1050 kPa, gauge Volatility i.e. evaporation temp. In deg. C for 95 % by volume at 760 mm of Hg pressure, Max = 2.0 Hydrogen sulphide ======= pass, i.e. Hydrogen sulphide is not more than 5 ppm Free water content======= none Min. 20 ppm of ethyl mercaptan for odor. Auto-ignition temperature==410 to 580 degree Celsius Flash Point ============== -104.4 degree Celsius In a closed liquid filled vessel or pipe, for 1 degree rise in temperature, the pressure increases by 14 to 15 kg/cm^2 Explosive Limit =========== 1.85 to 9.5 % v/v in air
  • 8. PROCESS The process comprises of broadly the following:- (a) Compression (b) Dehydration (c) Product extraction through: (i) On stream cooling by heat exchanger (ii) Turbo expansion (iii) Removal of non-condensable and undesired lighter fractions (d) Product fractionation  The different stages are as follows:- • Compression:-  1st stage -> Inlet Gas Compression Suction Scrubber  The inlet gas enters at 14kg/cm^2, is compressed to 33.8kg/cm2 in a 4 stage centrifugal compressor driven by York Manufacturer’s 4500HP electric motor operating on 11KV power supply.  The heat of compression is partly used in re-boiling the bottom liquid of de-ethanizer and then cooled to 37.8’c in water cooled heat exchanger.
  • 9. 2nd stage -> Booster Compression Suction Scrubber  The gas is then compressed to 41.9 kg/cm2 driven by the turbo expander and then cooled to 37.8’c.  It is then sent through an inlet filter separator wherein any water that may condense out is knocked out. • Dehydration:-  The gas is dried in one dehydrator while the other is being regenerated.  The pressure of compressed gas decreases to 39.6 kg/m2 as it reaches dehydrator.  Dehydrator consists of molecular sieve made of crystallized metal Aluminum Silicate of 4A’ size of approx. 11650kg weight in which water particles are retained.  This process is required as the temperature of the gas can go down up to minus 100’c where ice crystals form.  The dehydrated gas passes through a dust filter to remove sieve dust etc. • Product extraction:-  70% (by volume) of inlet gas is exchanged with cold residue from de-ethanizer and expander separator overhead, 30% (by volume) exchanges heat with the cold separator liquid in the gas-liquid exchanger and also with the expander separator liquid.  These two streams combine to enter the cold separator.  Liquid condensed is separated by cold separator and then the liquid is pressurised through the de-ethanizer reflux condenser.
  • 10.  The inlet gas from the cold separator enters the expander where the pressure is lowered, following Joule-Thompson Effect.  The gas liquid mixture out of the expander of 1670 HP and 27000 rpm speed reducing temperature to -84’c, is separated in the expander separator.  Liquid thus collected flows to the de-ethanizer feed pre-heater and then to the de-ethanizer. • Product Fractionations:-  A de-ethanizer column with three separate packed sections and a reboiler.  The liquid formed at the cold separator and the expander separator enter it, by maintaining proper bottom temperature with reboiler and reflux, the undesirable liquefied fraction methane, ethane and excess of propane are knocked out from the top.  The temperature of LPG is increased by exchanging heat with residue gas, whose refrigeration is in turn used in heat gas exchangers.  A de-butanizer column having 34 trays and reboiler provision through closed circuit hot oil systems with direct fired heater.  The bottom liquid flows on to de-butanizer tower where LPG and condensate are separated out.  LPG comes out at the top which is cooled to ambient temperature and sent for storage in bullets and Horton spheres.  The bottom condensate (Natural Gasoline) is similarly stored in separate storage tanks.
  • 11. Fire Protection & Safety LPG is a colorless liquid which evaporates easily into a gas, and the leakage of even a small volume can expand into a large hazardous zone. Since it has no smell, a little mercaptan is added to help detect leaks. It can burn and explode when gets mixed with air and meets a source of ignition and it can also cause cold burns to skin. Therefore, Fire Protection & safety is of utmost importance in LPG plant. Safety in LPG plant includes:-  FIRE PROTECTION SYSTEM  ALARM AND SHUT DOWN SYSTEM  ESD DEVICE  SAFETY RELIEF VALVES  FIRE ALARM SYSTEM  GAS DETECTION SYSTEM  FIRE EXTINGUISHERS  FIRE DRILL  COMMUNICATION SYSTEM  REGULAR INSPECTION OF PLANT
  • 12. Fire Protection System It comprises of:- 1) A continuously pressurized water network of approximately 2 km length, consisting of one 3000 kLs water reservoir, pumps, hydrant points, monitors (water and foam), hose reels, temperature sensing medium velocity water spray system. 2) Portable fire extinguishers and sand buckets. 3) Fire water pumps. 4) Manual fire call points at different locations. One of the most important components of the safety system is the Deluge Valve, which is the controlling valve of the pressurized water network. It can be operated either on auto mode or manually. Auto Operation:- 1) Water pressure is maintained in the hydrant system through a jockey pump. 2) DV is kept closed by maintaining air pressure in the network. 3) Due to rise in temperature, a heat detector bulb (Quartzoid bulb) in the air network bursts releasing air pressure. 4) When air pressure drops, DV opens spraying water on the vessel. Manual Operation:- DV can be opened locally through a valve provided at the DV or by operation of a switch provided in the control room.
  • 13. EQUIPMENT QUANTITY FIRE WATER PUMPS JOCKEY PUMPS HYDRANTS MONITORS FIRE ALARM POINTS GAS DETECTION SYSTEM Sr.No. 1 2 3 4 5 6 06 (04+02) 02 28 (21+7) 16 (9+7) +2 21 (12+9) 28 (20+8)
  • 14. Pump Capacity Head Drive Auto start pressure M3/ Hr meter WC (on discharge line) Jockey 20 90 Electric Motor 4.6 kg/cm2 Pump [Auto stop pressure = 8.4 kg/cm2] (02 Nos.) Sprinkler 275 88 Electric Motor 4.0 kg/cm2 Pump Spray 410 88 Electric Motor 1.0 kg/cm2 Pump ‘B’ Spray 410 88 Electric Motor 2.0 kg/cm2 Pump ‘A’ Hydrant 410 88 Electric Motor 3.0 kg/cm2 Pump DEFP -1 410 88 Diesel Engine DEFP -2 410 88 Diesel Engine 2.5 kg/cm2
  • 15. Alarm and Shutdown System The plant has got automatic in-built shutdown system to protect the vital equipment and the plant as a whole from any abnormal condition of operation. Audio-visual alarms and shutdown indications are displayed in LPG control room.  All the important equipment are provided with alarm and shutdown devices for critical operating parameters.  All the storage devices are provided with high level alarms.  Emergency shutdown switch is provided in control room to shut down the plant in any case of emergency.  Remote shutdown switches are provided in the local panels of two most important equipment- inlet gas compressor and expander compressor. Status monitoring is done round the clock through DCS work stations. Operation tested during running condition, planned and non-planned shutdown of the plant. Testing/calibration is done as and when required for smooth running of the plant and also during the annual maintenance of plant.
  • 16. EMERGENCY SHUT-DOWN SYSTEM(ESD) The plant is equipped with ESD switches which calls for shut down in emergency situations. The plant has these emergency switches in three locations – (a) Top Control Room (b) Bottom Control Room (c) Expander Compressor Panel SAFETY RELIEVE VALVES SRVs are required to release the excess pressure build-up in the system due to process upset etc. so that they are protected from failure due to over- pressure. These valves are provided in the scrubbers, inlet filter separators, dehydrators, gas flow lines and in each of the process pressure vessels. FIRE ALARM SYSTEM The fire alarm system consists of alarm switch glass, which when broken will lead to an audio –visual alarm at the bottom control room indicating the location of emergency , and also hooting of sirens in LPG Recovery and Filling Plant areas. GAS DETECTION SYSTEM Gas Detectors, located at the vulnerable areas of the plant, detects the leakage of any explosive gas displaying the amount of leakage in terms of %LEL, together with hooting of an alarm in the DCS system of the control room.
  • 17. FIRE EXTINGUISHERS Fire Extinguishers are classified into the following categories, as per the nature of associated fire-  Type A: for general fire out of wood, paper and other such stationary sort of stuffs.  Type B: for fire from liquid as diesel, petrol, diesel etc. utilizing dry chemical powder  Type C: for gaseous fire, as LPG gas, Natural Gasoline etc. utilizing carbon dioxide  Type D: for electrical and metallic source fire FIRE DRILL Fire drill is carried out forth nightly in LPG Recovery and also in LPG Filling Plant by the plant personnel from all sections along with personnel from Fire Service Section ( General Engineering Department ) to test the performance of the Fire Protection System of LPG Department and to take corrective action as necessary. COMMUNICATION SYSTEM Both LPG Recovery and Filling Plant are provided with 2 fire sirens (1 km and 5 km region) incorporating the entire area. The smaller siren is operated in manual mode in normal fire drill, else the bigger siren is operated. The bigger siren is inter-locked with fire alarm switches which run in auto-operation mode.
  • 18. Instrumentation The role of this section is to quantify all physical parameters such as pressure, temperature, flow rate and liquid level. It is an integral part of LPG department of OIL.  LPG implements PLC other than DCS dedicated to equipment control only, sequential start and stop of all devices and tripping of plants during emergency is done by PLC. Whereas DCS controls the entire process temperature, flow and level. =====Two types of control systems are===== • Distributed Control System (DCS):- is a digital control system based on distributed control philosophy. It means a control system which works on the principle of power delegation, for which there should be some connectivity to reach the data to all nodes i.e. Ethernet dual ring network called distributed communication network. • Programmable Logic Control (PLC):- is a digital computer used for automation of electromechanical processes, designed for multiple inputs and output arrangements, extended temperature ranges, immunity to electrical noise, and resistance to vibration and impact. • AC 460 is the heart of the system used to execute any function to maintain it, acts as interface and reads and writes over the I/O panel. • Ethernet connection is used to communicate or integrate all the nodes. • Graphics package are used to build plant objects. • Text package provides libraries through which the system is configured and started. • Database management might be there and uses oracle to send report. • Input devices- transmitter
  • 19. The different devices used and maintained by this section are as follows: • Gas Chromatography: - used for analysing a mixture of a sample, a fully electronically controlled device. It consists of columns and detectors situated in the oven maintained at 80’c. • Moisture Analyzer: - If the temperature is less than - 80’C, the moisture in the gas will become saturated and form ice crystals which blocks the pipelines and hence has to be prevented. This is done by placing a device at different locations for checking the amount of moisture present and creates an electrical signals. • TCD (Thermal conductivity detector):- uses the property of thermal conductivity of gases and converts into electrical signals unique for each and every gas imitating the same property which are received by the calibrated and programmed computers. • Thermocouple is used for sensing temperature. • Level transmitters work based on Archimedes Principle. =======the different types are=======  Magnetic level gauge  Radar level gauge  Servo level gauge  Floatation method on the basis of buoyancy force
  • 20. Flow rate indicator: - • Mass flow meter: - senses both gravity and volume. It carries out a lot of algorithms considering the resonant frequency of the U wire which gives the inertia of the liquid and temperature for gravity calculation. • Orifice flow meter: - works on the Bernoulli’s principle and specifies only volume. Types of valves: - • Shutdown valve • Deluge valve • Solenoid valve: - is a logical valve and operated by solenoid coil which opens up at 110V of AC current or 240V DC. • Safety relief valve: - are protection devices used in the worst conditions and are always maintained. • Remotely operated valve (ROV): - It is a logical valve which either closes or opens and requires 60-70psi. The feedback signal is received through PLC in control room and is used only for shutdown, can’t be controlled. • Control valves: - are the ultimate output devices. • Audio, visual, olfactory and vibration are the four types of alarms used.
  • 21. Pressure gauges, based on the Hooke’s law relating stress and strain, consists of the following components: - • C-type tubes • Spiral type • Bello • Diaphragm • Dead weight tester • Manometer  DP (Differential Pressure) transmitter: - measures the difference in pressure through micro-controller.  LEL (Lower Explosive Limit): - calibrated optimum quantity of a combustible substance which can support a self-propagating flame when ignited. The device uses the infrared radiation emitted by the gas which is dependent on its concentration. The inner part is maintained at a higher temperature causing convection i.e. the hot air rises due to its lower density sucking in the air below which is at a lower temperature. • LELs of substances in terms of percentage present in the atmosphere are- • CH4- 5% • LPG- 1.2% • Condensate- 1.8% • If LEL exceeds 10% sparking is prohibited.
  • 22. Process water: - • The pH must be maintained in the alkaline range i.e. more than 7 as acidic process water may cause scaling in the heat exchangers. This can be done by treating the water with NaOH and KOH. • The viscosity should not be very high. • This water cannot be released into the environment without being treated for its salinity, pH, minerals added and oil accumulated. The methods employed to dispose off this water without causing any damage are: -  Flocculent (gravity) and coagulant (sand) filters  Aerobic and anaerobic treatment  UV rays cleaning system  Bleaching(chlorine)  Demineralization: - is a series of anion and cation exchanger to maintain the pH around 7.  The minerals such as Ca, Mg, SO4-2, Cl-1 can be removed completely but the water cannot be polished off silica if its concentration is below 2ppm.  The water is heated in a high pressure water boiler.  If the toxic level of water is very high and cannot be treated it is injected back into the well.
  • 23. Quality Control Laboratory It is a branch of the Chemical department of OIL, and being a service section its main role is to evaluate the quality of products, LPG and Residue Gas, along with the feed gas that is, Natural Gas. It mainly performs two types of tests, viz., compositional and physical. 1. Physical Analysis: - It includes Volatility and Vapor Pressure tests as per IS 4576: 1999 certification, depending on which one can decide whether the product is good or bad. a) Volatility: - It is measured by Weathering Test. In this test, the sample is taken in a tube called weathering tube and a thermometer is put in it. The temperature is noted at 25, 50, 90 and 95 percent (by volume) evaporation and the temperature corresponding to 95% evaporation is called the Weathering Temperature and it should be in the range of +2 degree C and -2 degree C. b) Vapor Pressure: - For this we take the sample in a sampler and put it in a temperature bath which is maintained at 40 degree C and we check the pressure building up at this temperature indicated by the pressure gauge. Apart from these tests, some other tests are also performed to measure the density of sample, moisture level and also the Ethyl Mercaptan (C2H5SH) level in LPG. A hydrometer is used to measure density. We use Doctor’s Test to check minimum value of Mercaptan added to LPG. For this, Sodium Plumbate solution is taken in a cylinder and LPG sample is added which mixes with it. A positive Doctor’s Test gives a yellow precipitate/solution indicating presence of Mercaptan.
  • 24. Dew Point Test: - We have to check dew point at dehydrator inlet and outlet, gas inlet and air inlet. As the feed gas, after compression, needs to be dehydrated using dehydrator, hence we need to check whether the molecular sieves (which are made of alumina silicate) are working. 2. Compositional Analysis: - It includes compositional analysis of the natural gas coming from production department, LPG and Residue gas, done by Gas Chromatography (GC), as explained below: - GC, a common type of chromatography performed in a Gas Chromatograph, is used in analytical chemistry for separating and analyzing compounds that can be vaporized without decomposition. It is based on different boiling points and retention time for different components. It is used for testing the purity of a particular substance, or separating the different components of a mixture. GC consists of two phases: - mobile phase and a stationary phase. Here the mobile phase is a carrier gas, usually an inert gas like Helium or a non-reactive gas like Nitrogen. The stationary phase is a microscopic layer of a liquid or a polymer on an inert solid support, inside a piece of glass or metal tubing called a column. The molecules move to the wall of the column, coated with different stationary phases, which causes each compound to elute at a different time, known as the Retention Time of the compound.
  • 25. GC Analysis:- In a GC analysis, a known volume of gaseous or liquid analyte is injected into the column using a micro-syringe. As the carrier gas sweeps the analyte molecules through the column, this motion is inhibited by the adsorption of the analyte molecules either onto the column walls or onto packing materials in the column. The rate at which molecules progress along the column depends on the strength of adsorption, which in turn depends on the type of molecules and on the stationary phase materials. As each type of a molecule has a different rate of progression, the various components of the analyte mixture are separated as they progress along the column and reach the end of the column at different times (retention time). A detector is used to monitor the outlet stream from the column, hence the time at which each component reaches the outlet and the amount of that component can be determined. Generally substances are identified by the order in which they emerge from the column and by the retention time of the analyte in the column. The chromatographic data is presented as a chromatogram, which is a graph of detector response (y-axis) against retention time (x-axis). This provides a spectrum of peaks for a sample representing the analyte present in a sample eluting from the column at different times. The area under a peak is proportional to the amount of analyte present in the chromatogram, and by calculating it, the concentration of an analyte in the original sample can be determined.
  • 26. Electrical maintenance • The power house of OIL generates 14.45 MW with the help of two gas turbines which are alternatively at running and standby modes. • The power house supplies 11KV to the substation in the LPG plant through two underground cables. • This incoming power is sent into the feeder from two different power houses, #1 and #2. These two sections are connected by a bus coupler which is used only when the maintenance job needs to be done. • From #1 the 11KV is supplied to the spare feeder, 4500HP motor starter panel and to a transformer1 of 1000KVA capacity which steps 11000V down to 415V. • There are 8 vacuum circuit breakers. It is monitored by protective relays such as VCB, ACB, SF6 of the circuits. • UPS system gives an uninterrupted power supply normally of AC current with a battery backup of 120KVA capacity. There are 2 types of UPS in which input is 415V but outputs are 415V and 110V. • A battery converts a voltage input of AC to DC. An 110V Ni-Cd battery set is used. • Another auto-transformer other than the two in the feeder circuits produce 450V line. It is a part of motor starter panel. During starting of motor the load might reach seven times its full load and then drop back which can’t be allowed. To reduce this we use this auto-transformer starter for 20 seconds and then give back to the normal system. • Motor control center (MCC) is provided by the 415V bus. • Tripping is a condition when difference between the incoming and outgoing currents of the isolator is more than a given value and the on-off switch of the isolator turns off automatically.
  • 27. AUTOTRANSFORMER: - • Auto-transformer is used for applying reduced voltage to stator during starting. Thereby the starting current is reduced. The auto-transformer is provided with change-over switch. As the motor comes to full speed, the change-over switch is thrown over to run position. CIRCUIT BREAKER AND ITS TYPES: - • Circuit Breaker is an automatic device capable of making and breaking an electric circuit under normal and abnormal conditions such as short circuits. The part of the circuit-breakers connected in one phase is called the pole. A circuit-breaker suitable for three phase system is called a triple pole circuit-breaker. • Each pole of the circuit-breaker comprises one or more interrupts or arc-extinguishing chambers. The interrupters are mounted on support insulators. The interrupter encloses a pair of fixed and moving contact. The moving contacts can be drawn apart by means of the operating links or the operating medium. The operating mechanism of the circuit-breaker gives the necessary energy for opening and closing of contacts of the circuit-breakers. • The arc produced by the separation of current carrying contacts is interrupted by a suitable medium and by adopting suitable techniques for extinction. • Circuit Breaker is used for opening and closing circuits for normal switching operations. During short circuits or abnormal conditions, relay operates and gives opening command to circuit-breaker and circuit is opened automatically. TYPES OF CIRCUIT BREAKERs IN LPG PLANT: - • Moulded Case Circuit Breaker (MCCB): • Air Circuit Breaker (ACB): It utilizes air at atmospheric pressure for arc- extinction. • Vacuum Circuit Breaker (VCB): The fixed and moving contacts are housed inside a permanently sealed vacuum interrupter. The arc is quenched as the contacts are separated in high vacuum.
  • 28. POWER HOUSE Power House generates power for the entire plant using the concept of a Gas Turbine, which is based on the Bryton Cycle. The following components comprise a Gas Turbine: – (a) Axial Air Compressor (b) Combustor (c) Turbine (d) Auxiliaries Axial Air Compressor: - Air after passing through the filter enters the axial compressor and flows parallel to the axis .it consists of a stationary body called Casing and a moving part called Rotor, and Blades , some of which are attached to the casing and some to the rotor . A pair of stationary and moving blades is called a Stage and the compressor has got 15 such stages. Air gets compressed as it passes through the different stages. Combustor: - Air from the compressor enters the combustor which has 2 parts –a transition piece and a combustor, the latter being divided into 3 zones, viz, primary, secondary and tertiary, each consisting of a number of holes. Fuel is injected in the primary zone and ignited using spark from the spark plug, thereby creating a cyclone.
  • 29. In the secondary zone, complete burning of fuel is ensured. As the temperature of air rises to a high value of 1200 degree C, it needs to be cooled down to 899 degree C at least before entering the transition piece. For this more air is to be supplied to the tertiary zone. The transition piece has a nozzle which increases the velocity of air. Turbine: - Air from combustor enters the turbine where it expands and exits as exhaust gas. The rotating turbine then generates power via a generator. The exhaust gas is at a temperature of 370 degree C and this energy can be utilized to produce more electricity using the steam turbine. For this DM (De-Mineralized) plant is required but this is a costly process. This produces about 7 M watt power in addition to the actual power of 14.45 M watt. As the Gas Turbine is not self-starting, a starter diesel engine is required. A total of 14.45Mwatt electricity is the output from the generator. Out of this 10.4Mwatt is utilized to fulfill the electricity requirement of the different units of the industry.
  • 30. Mechanical Maintenance The Maintenance Section of the LPG department is responsible for the following: - 1)Maintaining the plant availability to achieve MOU target. 2)Maintenance of all rotary and stationary equipment of the LPG plant to keep them in proper working conditions. 3)Execution of various contract jobs under the department related to maintenance of the plant. 4)Planning of maintenance activities for annual plant maintenance. 5)Spare part management for maintenance of the plant. This section aims to achieve the following targets: - 1)To reduce the cost of maintenance activities by 1 % of the previous year. 2)To keep the minimum MTTR of critical equipment for achieving the MOU target. 3)To keep good relations and understanding with the different sections of the LPG department. 4)To keep good relations and understanding with the other departments of the company. 5)To keep close watch on various activities so that there is no misuse of approved funds and that these are properly utilized.
  • 31. The Mechanical Maintenance Section of the LPG department is responsible to perform the following duties: - 1) Daily plant check up to ensure smooth operation of the plant and to check lube oil level and vibration & sound and other parameters. 2) Monthly vibration measurement to ensure that vibration levels of critical equipment are within limits and take necessary corrective measurements. 3) Periodical lube oil testing to test lube oil of three major equipment of LPG recovery section, namely, Inlet Gas Compressor, Gear Box and Expander-Compressor. 4) Cleaning of cooling tower top chambers to ensure its proper functioning. 5) Testing of SRV to ensure its correct functioning at its Set Pressure. 6) Sound level measurement to measure the intensity of sound at specified locations and compare it with permissible limit. 7) Replacement of damaged or worn out Vee-Belt (Endless belts used between driving pulleys to transfer power). 8) Replacement of empty Mercaptan drum of LPG storage area. 9) Top up lube oil into Expander Surge Tank to maintain a certain oil level in it. 10) Air compressor lube oil top up to maintain the required level of oil. 11) Materials inspection and suitability report for the acceptability of the materials received against direct charge Indents/purchase orders. 12) Engaging staff on overtime to complete the repairing job within the day in view of urgent nature of work for operational as well as safety requirements.
  • 32. 13) Workshop job requisition to carry out emergency repair and fabrication jobs at general workshop. 14) Breakdown maintenance of machines/ equipment. 15) Preparation of tentative maintenance schedule of air compressor. 16) Ultrasonic thickness measurement to gauge metal surfaces for the thickness. 13) Handling/cleaning services and day-to-day maintenance in LPG recovery and filling plant. 14) Servicing, Inspection and Testing of LPG storage vessels. 15) To replace hot and cold insulation system of LPG recovery plant with new insulation system at a specified time interval. 16) Major overhauling of Inlet Gas Compressor and Expander Compressor to ensure smooth and trouble free operation. 17) De-coupling of various motor devices to carry out maintenance work on driver (motor) or driven side (pumps, compressors, fans, etc.). 18) Hydro-testing of pressure vessels and storage vessels to check the condition/health of vessel. 19) Periodical testing of lifting tools. 20) Storage, handling and disposal of lube oil and other hazardous materials.
  • 33. LPG Filling Plant • In LPG Filling Plant – (i) LPG is bottled into cylinders (packed form) in Carousel machine containing 24 number of filling points or guns. (ii) LPG is filled into road tankers (bulk form). These cylinders and road tankers are handed over to IOCL for marketing. • The LPG is pumped to LPG Filling Plant from LPG storage vessels at LPG Recovery Plant. • The incoming LPG pressure in the pipeline is about 14kg/cm2. The cylinder consists of a head ring, 3 fins, valve, high pressure seamed cylinder and a foot ring. • The inside of the valve is installed with an O-ring and a valve pin. The valve needs to be checked for any leak possible. • The bottling capacity of the plant is about 6000-7000 cylinders per day. • The empty cylinders are first marked by TARE WEIGHT MARKING and their marked weights are stored by a HMI (Human Machine Interface) device called pre-check scale. • The marked cylinders go to Carousel machine by chain conveyor, run by 14 motor driven Gear boxes. In Carousel machine the empty cylinders are first sensed by photo-electric sensors. • In each filling gun two sensors are linked which are placed at the top and at the bottom side of the cylinder.
  • 34. • The bottom side sensor is called wheel arm sensor. The bottom photo-cell senses the position of the cylinder on the machine. The top photocell senses the cylinder and gives instruction to the gun. Then the respective gun shoots the respective cylinder. • The cylinder is filled in the course of one rotation of the carousel, the filling time is approximately 60 seconds. • When the regulator’s pin when pressed together with the valve pin, two holes are opened. • The LPG filled in the cylinder should be of weight 14.2 kg. If the gun is unable to fill the cylinder within one minute for delay error, the cylinder will again revolve for one minute. • In the outlet of the machine has a puller with sensor which allows only those cylinders filled up to the standard weight to go out of the machine, otherwise it will return back the cylinder to the machine again. • The cylinders are introduced through a check scale, which checks the over weighted cylinders and bypass them to another section called correction unit by pusher with photo-electric sensor. • The over weighted cylinders are manipulated up to the standard by manual filling. This over weighted range is considered as +200gm.Now the corrected cylinders are lined up with the other cylinders. • Now the cylinders are fed to Gas detector and O-ring detector unit to check the leakages and damages. In this unit the damaged cylinders are rejected. The tested cylinders are then fed to counting unit to count by a sensor and stored. In hot air sealing unit the cylinders are sealed and fed to transportation section.
  • 35. • The evacuation unit takes care of the rejected cylinders which are found defective by applying suction pressure on the LPG cylinder and the valuable LPG is sent back in the form of vapor to the storage tanks. • In the sealing unit i.e. Hot air seal unit, a plastic cap is placed over the cylinder along with a thin PVC seal which then is exposed to 265’C of hot air. • Compressed air of 7.5kg/cm2 is required for the functioning of the plant, which is done by using V-type, screw-type and vertical air compressor which are manually checked after the working hours which can be done. • In bulk filling, LPG and condensate are filled into tankers following the same procedure as that of packed form. • The tanker is checked for a hydraulic testing certificate valid for a period of 5 years from the date of issue. • The tanker evacuation unit is utilized when excess is sent into the tanker. The liquefied form of LPG filled into the tank is 18% less than the total tanker capacity.
  • 36. • CONCLUSION The vocational training enhanced my practical knowledge. Most importantly, I am oriented to the industrial scenario and its many challenges and subtleties. The smooth functioning of an industry depends to a large extent on the mutual co-operation among its different wings. Nevertheless, I did enjoy the training to the fullest and are very sure that this training will help me in my future endeavors. Thanking You
  • 37. A REPORT ON INDUSTRIAL TRAINING AT OIL INDIA LIMITED BADSHAHPUR INDANE BOTTLING PLANT (MARKETING DIVISION) Submitted by: - MOHIT DHULL Bachelor of Technology 5th Semester Department of Mechanical Engineering Guru Jambheshwar University of Science and Technology Hisar
  • 38. A PRACTICAL TRAINING REPORT AT INDANE BOTTLING PLANT BADSHAHPUR, GURGAON INDIAN OIL CORPORATION LIMITED (MARKETING DIVISION) Submitted to: - Submitted by:- Mr. Kaushal Mohit Dhull Faculty of Mech. Deptt. 12162035 GJUS&T BTECH. 3rd Year
  • 39. PLANT LAYOUT SCOPE The general layout principles of LPG Storage, bottling and bulk handling facilities Have been detailed in this chapter. The various Facilities within LPG storage and bottling Premises shall be located based on Table-I and Table-II. TABLE – I INTERDISTANCES FOR LPG FACILITIES 1 LPG STORAGE VESSEL 2 T-11 T-11 15 T-11 2 BOUNDARY NOT ASSOCIATED WITH LPG PLANTS T-11 - 15 15 - 3 LPG SHED T-11 15 15 15 30 4 TANK TRUCK GANTRY 15 15 15 NA 30 5 FIRE WATER PUMP HOUSE T-11 * 30 30 -
  • 40. NOTES: - 1. ALL DIMENSIONS ARE IN MTS. 2. NOTATION T-II: REFER TABLE II *: ANY DISTANCE FOR OPERATIONAL CONVENIENCE 3. MAXIMUM PACKED STORAGE LIMITED TO 20000 KGS TABLE – II INTERDISTANCES BETWEEN LPG STORAGE VESSELS, FILLING SHED, STORAGE SHED AND BOUNDARY/PROPERTY LINE/GROUP OF BUILDINGS. CAPACITY OF EACH VESSEL (CU. MTS. OF WATER) DISTANCES (MTS.) 10-20 15 20-40 20 41 – 235 Note 3 30
  • 41. LOCATION & SAFETY DISTANCES LOCATION While assessing the suitability of any site For location of LPG storage facilities, the Following aspects shall be considered: (a) In addition to the requirements for safety the Plant should be located in such a manner so As not to be contagious to any industry Having open flame. Property line of the Plant shall be away from the central line of The road/railways as per statutory Requirements and overhead high tension Wire shall not traverse through the battery Limit of the plant. (b) Adequate availability of water from a nearby Reliable source should be ensured.
  • 42. (c) The topographical nature of the site wit Special reference to its effect on the disposal Of LPG, in the even of its escape, if any, Shall be considered. (d) The access for mobile fire fighting Equipment to the storage vessels under all Foreseen circumstances, preferably from two Sides and upward prevailing wind direction Is an important parameter. (e) For any expansion beyond the specified Limit, all provision under OISD-144 shall be Applicable. (f) Predominant direction of wind and velocity Shall be considered. (g) Longitudinal axis of horizontal vessels (Bullets) shall not point towards other Vessels, vital process equipment and other Facilities. (h) Storage vessels shall be located downward Of processing units, important buildings. (I) Storage vessels shall be laid out in single Row within a group. (j) Storage vessels shall not be located one Above the other.
  • 43. SAFETY DISTANCES The safety distances as given in Table-I and Table-II are the distances in plane between the nearest point on a vessel other than the filling/discharge line and a specified feature, e.g. adjacent vessel, site boundary etc. TYPE OF STORAGE VESSELS HORIZONTAL CYLINDRICAL VESSELS Horizontal bullets with the total volumetric capacity upto 235 Cu. M. Note 3 shall be used for storing LPG.
  • 44. LAYOUT The following aspects shall be considered while Establishing layout of LPG storage vessels. LPG STORAGE FACILITIES GRADING Area below the storage vessels (Bullets) shall be free from vegetation, property Graded with the slope of 1.100 (towards one Side) away from the pipeline manifold. PIPING (i) Piping manifold shall be away from the Shadow of the vessel. (ii)Spring loaded quick closing valve with fusible link or Rov to facilitate immediate closure in the event of emergency, if any, shall be provided in the LPG liquid line of each vessel between excess flow check valve (EFCV) and pipeline manifold.
  • 45. SURFACE DRAINAGE In order to prevent the escape of spillage into the main drainage system, surface water from the storage area and from the manifold area shall be directed to the main drainage through a water seal designed to avoid the spread of hydrocarbon. GROUPING Vessels shall be arranged in a group and total volumetric capacity of the group shall be ,limited to 235 Cu. M. Note 3. Interdistances as specified in Table-I and Table- II shall be maintained. Top surfaces of all the vessels installed in a group shall be on the same plane so that the safety blowout from them do not affect each Other.
  • 46. LPG BULK HANDLING FACILITIES 1. LPG tank lorry loading/unloading gantry shall be located in a separate block and shall not be grouped with other petroleum products. 2. Space for turning with a minimum radius of 20 meters for tank lorries shall be provided commensurate with the capacities of the tank trucks. 3. LPG tank lorries upto the maximum of 2 Nos, at a time should only be taken for unloading. 4. Adequate permanent protection for TLD pipeline island shall be provided. The minimum width of such pipeline island shall be 1 metre.
  • 47. LPG BOTTLIG FACILITIES (1) LPG Bottling facilities should be located a a safe distance from other facilities with minimum ingress of trucking traffic and downward wind direction with respect to bulk storage. There shall not be any deep ditches in the surrounding area to avoid settling of LPG. (2) Bottling section shedshall be of single story having asbestos roofing and open from all sides for adequate ventilation to ensure quick dessipation of LPG Vapour in the event of leakage, if any, RCC roofing shall not be used. Anti-static mastic flooring conforming to IS-8374 shall be provided in the LPG filling shed/cylinder storage shed to avoid frictional sparks. Anti-static mastic coating up to 1.5 meters Height from bottom of the supporting Columns in the shed shall be provided.
  • 48. (3) Stacking area for empty and filled cylinders shall be marked specifically. Cylinders shall always be stacked vertically in two lines. For details of cylinders stacking pattern refer Annexure Plant should have one shed each for filling and storing of filled./empty cylinders. (4) Valve changing operation should be carried out in a demarcated place within the filling shed itself. (5) Cylinder storage shall be kept on or above grade and never below grade in celler or basement. (6) Filled cylinders shall not be stored in the vicinity of cylinders containing other gasses or hazardous substances. (7) Escape routes shall be specified in LPG sheds for evacuation of employees in emergency.
  • 49. (8) There shall not be any trapping of personnel in LPG sheds by conveyours, cylinders and other facilities. If such trapping cannot be eliminated, it should be kept to the minimum. In such places sufficient arrangements for escape routes to be provided. (9) Adequate lighting shall be provided in the cylinder filling area. (10)Water drains from cylinder filling areas to out side drainage system shall be provided with water seals (near the plant boundary) PROTECTION OF FACILITIES (1) There shall be road all around the various facilities within the bottling plant areas for accessibility of fire fighting operations. (2) There shall be proper industry type boundary wall all around the Bottling Plant.
  • 50. UTILITIES Utilities consisting of Fire Water Pumps, Admin. Building, Motor Control Center, DG Room, Air Compressors, Dryers etc. shall be separated from other LPG facilities and to be located as per the area classification as specified in Table-I.
  • 52. FACULTY CERTIFICATE Forwarded here with a summer internship report on “STUDY OF VARIOS MECHANICAL UNITS INVOLVED IN THE BOTTLING OF LPG CYLINDERS” of Indian Oil Corporation Limited submitted by Mohit Dhull, Enrollment No- 12162035 student of Bachelor of Technology 5th Semester (2014-15). This project work is partial fulfillment of the requirement for the degree of Bachelor of Technology from Guru Jambheshwar University of Science and Technology Hisar, Haryana. -------------------------------- Mr. Kaushal Deptt. Of Mechanical Engg. Guru Jambheshwar University of Science and Technology