Pipeline Drying
• Pipeline must be dried in order for the
  delivered product to meet the moisture
  specifications.
• Natural gas pipelines are generally dried to
  lesser extent to prevent hydrate formation.
• The natural gas industry specifies dryness in
  pounds of water per million standard cubic
  feet (mscf) of gas.
Dew Point
• Temperature at which water vapor begins to
  condense out of a gas at atmospheric pressure.
• A high relative humidity indicates that the dew
  point is closer to the current air temperature.
• Relative humidity of 100% indicates the dew
  point is equal to the current temperature and
  that the air is maximally saturated with water.
• When the dew point remains constant and
  temperature increases, relative humidity
  decreases.
Vacuum Drying
• Vacuum Drying is a process in which drying is
  carried out at reduced pressure, which lowers the
  heat required for rapid drying.
• Corrosion is generally inhibited at relative
  humidity(R.H.) levels below 30%, but in presence
  of hydroscopic dirt corrosion can occur at R.H.
  levels of 20%.
• Therefore, systems should be thoroughly drained
  and then vacuum dried to lower than 20% R.H.
• Vacuum Drying consists of 3 phases: Evacuation,
  Evaporation and Final Drying.
Pressure
Phase I- Evacuation
• Pressure in the pipeline is reduced to a level
  where evaporation of water starts at ambient
  temperature.
• This pressure is similar to the saturated vapor
  pressure of free water in pipeline, which depends
  upon the ambient temperature of pipeline.
• This pressure is calculated in advance but varies
  onsite ,which is noted from the plot of pressure
  against time.
• A leak test is performed by stopping the vacuum
  equipment for approximately 4 hours, to rectify
  any leaks on flanges, hoses or fittings.
Phase II-Evaporation
• Once Standard Vapor Pressure is achieved, evaporation starts.
• Pressure is kept constant ,using the vacuum equipment, until all
  free water evaporates.
• Evaporation may take several days depending on:
   – Amount of water to be evaporated
   – Ambient temperature of pipeline
   – Size of vacuum equipment
• End of evaporation will be indicated by a decrease in the pressure.
• To ensure if all the free water in the pipeline is evaporated, Soak
  Test is performed.
• Vacuum equipment is isolated for at least 12 hours, and any
  changes in the pressure are recorded.
• Pressure will remain constant , if all free water has evaporated.
Phase III- Final Drying
• To achieve required dryness level, water vapor
  must be removed.
• Further Reducing the pressure in the pipeline,
  which has a effect of drawing water vapor out
  of the pipeline through vacuum equipment.
• The slope of the final drying line must be
  observed , if it follows the calculated value.
• A shallower slope indicates the presence of
  free water still remaining in the pipeline.
Dryness?
• The dryness of a pipeline is measured in terms of dew point which is
  measured using an instrument called a mirror hygrometer.
• The water vapor is passed across a polished surface that is slowly cooled
  until dew forms.
• The temperature at which the dew forms is the dew point of the water
  vapor and is normally expressed in degrees centigrade.
• The drier the air, the lower the temperature at which dew will form.
• In terms of a pipeline being vacuum dried, the lower the pressure in the
  pipeline, the lower the dew point will be.
• For example, at a pressure level of 0.26 kPa, the equivalent dew point of
  the pipeline would be -10 degree C. If the pressure were further reduced
  to 0.104kPa, then the dew point would be -20 degree C.
• For gas pipelines a dew point level of -20 degree C is generally considered
  to be adequate and the 0.10 kPa pressure level required to achieve this
  dew point is readily attainable using the portable vacuum equipment
• To prove the dryness of the pipeline, a dry gas
  purge using atmospheric air or nitrogen is carried
  out.
• The air is allowed to enter the pipeline through a
  valve at the end remote from the vacuum
  equipment ,until the pressure has risen to the
  SVP equivalent of the target dew point.
• Once this pressure level has been reached, the
  vacuum equipment is started and that pressure
  level maintained.
• This has the effect of drawing gas through the
  pipeline under vacuum at a relatively constant
  dew point equal to the final dew point required.
Water Vapor Pressure Table
     T                      SVP(kPa)        Vapor Density
( Degrees C)              (mb x 10^-1)        (gm m^3)
    -50                 0.0039( .039 mb)       0.038
    -45                     0.0128             0.119
    -35                     0.0223             0.203
    -30                     0.0308             0.339
    -25                     0.0632             0.552
    -20                     0.1043             0.884
    -15                     0.1652             1.387
    -10                     0.2597             2.139
     -5                     0.4015             3.246
     0                      0.6108             4.847
     5                      0.8719             6.797
    10                      1.2270             9.399
    15                      1.7040             12.830
    20                      2.3370             17.300
    25                      3.1670             23.050
    30                      4.2430             30.380
• The purge gas, will reach the vacuum equipment and be pulled
  through it.
• The dew point at both ends of the pipeline is carefully monitored
  and compared.
• If there is no free water remaining in the pipeline then the dew
  point at the vacuum equipment end will be the same as the dew
  point at the remote end.
• If there is any free water present then the dry air passing through
  the pipeline under vacuum will absorb the water hygroscopically.
• The dry gas purge operation must then continue to remove the
  remaining free water until the dew points at both ends are equal, at
  which time purging is discounted.
• The pipeline has now been vacuum dried to the required dew point
  level, and the dryness proved.
• Once the dryness has been attained and proved, the pipeline is
  ready for commissioning.
• It is possible to introduce the gas directly into the vacuum or to
  relieve the vacuum using dry nitrogen

Vacuum drying

  • 1.
    Pipeline Drying • Pipelinemust be dried in order for the delivered product to meet the moisture specifications. • Natural gas pipelines are generally dried to lesser extent to prevent hydrate formation. • The natural gas industry specifies dryness in pounds of water per million standard cubic feet (mscf) of gas.
  • 2.
    Dew Point • Temperatureat which water vapor begins to condense out of a gas at atmospheric pressure. • A high relative humidity indicates that the dew point is closer to the current air temperature. • Relative humidity of 100% indicates the dew point is equal to the current temperature and that the air is maximally saturated with water. • When the dew point remains constant and temperature increases, relative humidity decreases.
  • 3.
    Vacuum Drying • VacuumDrying is a process in which drying is carried out at reduced pressure, which lowers the heat required for rapid drying. • Corrosion is generally inhibited at relative humidity(R.H.) levels below 30%, but in presence of hydroscopic dirt corrosion can occur at R.H. levels of 20%. • Therefore, systems should be thoroughly drained and then vacuum dried to lower than 20% R.H. • Vacuum Drying consists of 3 phases: Evacuation, Evaporation and Final Drying.
  • 4.
  • 5.
    Phase I- Evacuation •Pressure in the pipeline is reduced to a level where evaporation of water starts at ambient temperature. • This pressure is similar to the saturated vapor pressure of free water in pipeline, which depends upon the ambient temperature of pipeline. • This pressure is calculated in advance but varies onsite ,which is noted from the plot of pressure against time. • A leak test is performed by stopping the vacuum equipment for approximately 4 hours, to rectify any leaks on flanges, hoses or fittings.
  • 6.
    Phase II-Evaporation • OnceStandard Vapor Pressure is achieved, evaporation starts. • Pressure is kept constant ,using the vacuum equipment, until all free water evaporates. • Evaporation may take several days depending on: – Amount of water to be evaporated – Ambient temperature of pipeline – Size of vacuum equipment • End of evaporation will be indicated by a decrease in the pressure. • To ensure if all the free water in the pipeline is evaporated, Soak Test is performed. • Vacuum equipment is isolated for at least 12 hours, and any changes in the pressure are recorded. • Pressure will remain constant , if all free water has evaporated.
  • 7.
    Phase III- FinalDrying • To achieve required dryness level, water vapor must be removed. • Further Reducing the pressure in the pipeline, which has a effect of drawing water vapor out of the pipeline through vacuum equipment. • The slope of the final drying line must be observed , if it follows the calculated value. • A shallower slope indicates the presence of free water still remaining in the pipeline.
  • 8.
    Dryness? • The drynessof a pipeline is measured in terms of dew point which is measured using an instrument called a mirror hygrometer. • The water vapor is passed across a polished surface that is slowly cooled until dew forms. • The temperature at which the dew forms is the dew point of the water vapor and is normally expressed in degrees centigrade. • The drier the air, the lower the temperature at which dew will form. • In terms of a pipeline being vacuum dried, the lower the pressure in the pipeline, the lower the dew point will be. • For example, at a pressure level of 0.26 kPa, the equivalent dew point of the pipeline would be -10 degree C. If the pressure were further reduced to 0.104kPa, then the dew point would be -20 degree C. • For gas pipelines a dew point level of -20 degree C is generally considered to be adequate and the 0.10 kPa pressure level required to achieve this dew point is readily attainable using the portable vacuum equipment
  • 10.
    • To provethe dryness of the pipeline, a dry gas purge using atmospheric air or nitrogen is carried out. • The air is allowed to enter the pipeline through a valve at the end remote from the vacuum equipment ,until the pressure has risen to the SVP equivalent of the target dew point. • Once this pressure level has been reached, the vacuum equipment is started and that pressure level maintained. • This has the effect of drawing gas through the pipeline under vacuum at a relatively constant dew point equal to the final dew point required.
  • 11.
    Water Vapor PressureTable T SVP(kPa) Vapor Density ( Degrees C) (mb x 10^-1) (gm m^3) -50 0.0039( .039 mb) 0.038 -45 0.0128 0.119 -35 0.0223 0.203 -30 0.0308 0.339 -25 0.0632 0.552 -20 0.1043 0.884 -15 0.1652 1.387 -10 0.2597 2.139 -5 0.4015 3.246 0 0.6108 4.847 5 0.8719 6.797 10 1.2270 9.399 15 1.7040 12.830 20 2.3370 17.300 25 3.1670 23.050 30 4.2430 30.380
  • 12.
    • The purgegas, will reach the vacuum equipment and be pulled through it. • The dew point at both ends of the pipeline is carefully monitored and compared. • If there is no free water remaining in the pipeline then the dew point at the vacuum equipment end will be the same as the dew point at the remote end. • If there is any free water present then the dry air passing through the pipeline under vacuum will absorb the water hygroscopically. • The dry gas purge operation must then continue to remove the remaining free water until the dew points at both ends are equal, at which time purging is discounted. • The pipeline has now been vacuum dried to the required dew point level, and the dryness proved. • Once the dryness has been attained and proved, the pipeline is ready for commissioning. • It is possible to introduce the gas directly into the vacuum or to relieve the vacuum using dry nitrogen