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Weidong Zhanga*, Xuhui Guan, Maoyong Fu and Shouqiang Zhao
College of Petroleum Engineering, China University of Petroleum, China
*Corresponding author: Weidong Zhanga, College of Petroleum Engineering, China University of Petroleum, Qingdao 266580, China,
Email:
Submission: February 12, 2018; Published: February 20, 2018
Clay Migration in Proppant during Production
in Argillaceous Unconsolidated Reservoir
Abstract
Fine migration inevitably occurs during the process of fracturing production in argillaceous unconsolidated reservoirs. Using the API conductivity
cell simulate the process of the production of the reservoir. The damage to conductivity caused by fines migration in the pack and the factors affecting
such migration are analyzed. The result indicates that clay are likely to aggregate and be retained in the prop pant pack because of the adsorption and
deposition, thereby resulting in pore throat plugging, which causes serious damage to fracture conductivity. The mobility and retention of clay in the
prop pant pack are affected by flow rate, fracture closure stress and fines property. This research is important for the further research.
Keywords: Unconsolidated sand; Fine migration; Fracture conductivity; Argillaceous unconsolidated reservoir
Introduction
Figure 1: Another view of the newborn with Adams-Oliver
syndrome associated with the related disorders.
Fines migration and consequent permeability damage is one of
the widest spread physical mechanisms of formation damage in gas
andoilfields[1,2].Liftingofnaturalreservoirfinesathighinjection/
production rates with resulting migration and straining usually
yields a significant increase in the flow trajectory tortuosity and
resulting drastic permeability decline [2,3]. Numerous measures
focused on fixing the reservoir fines (against fines mobilization)
[4-6]. Figure 1 shows the sequential processes of fines detachment
from the pore surface, migration and straining in a thin pore throat.
Fines-sensitive technologies of oil and gas recovery are primarily
focused on enhancing or inhibiting the particle detachment
process [7]. However few are focused on the mechanism of the fine
migration in the field, fracture and prop pant. So understanding
the mechanics of particle migration and the decline degree of
permeability in the prop pant is important. The structure of the text
is as follows. Section 2 presents the methodology of the laboratory
study, including preparation of materials. Section 3present the
mechanism of the clay retention. Section 4 describes and analyses
the obtained results. Section 5 concludes the paper.
Figure 2: Schematic of fines migration model and conductivity
test apparatus.
The experimental apparatus used in this paper are mainly
based on a modified API standard fracture conductivity instrument
[8,9] that consists of an Automated hydraulic intensifier system, a
fluid injection system, and a hastelloy conductivity cell (Figure 2).
This instrument can simulate real reservoir conditions. However,
the provided flow rate is limited, and a constant-flux pump of
maximum flow rate up to 10mL/min is configured. The simulation
process of fines invasion into the prop pant pack is presented as
follows:
(1) The conductivity cell was paved with high-strength and
large-sized ceramsite (380–830µm) from the inlet to outlet.
Intermediate container provides mixed suspension which can
provide different fines concentrations to represent the formation
Research Article
Aspects in
Mining & Mineral ScienceC CRIMSON PUBLISHERS
Wings to the Research
1/4Copyright © All rights are reserved by Weidong Zhanga.
Volume 1 - Issue - 2
ISSN 2578-0255
Aspects Min Miner Sci Copyright © Weidong Zhanga
2/4
How to cite this article: Weidong Z, Xuhui G, Maoyong F, Shouqiang Z. Clay Migration in Proppant during Production in Argillaceous Unconsolidated
Reservoir. Aspects Min Miner Sci. 1(2). AMMS.000508. 2018. DOI: 10.31031/AMMS.2018.01.000508
Volume 1 - Issue - 2
supply capability. Fines consist of 60% quartz sand, 24% illite, 6%
montmorillonite, 10% Plagioclase. The clay size was measured
using intelligent laser particle analyzer, as shown in Figure 3.
Figure 3: Diameter distribution of clay fines.
(2) The desired closure pressure was applied to the steel plate
using the hydraulic pump. The constant-flux pumps then drew to
drive suspension to the prop pant pack in the conductivity cell. The
production process of the reservoir can be simulated using Steps
1-2.
Fines Retention Mechanisms
Filtration and straining are two distinct mechanisms that
cause fines retention in porous media [10]. Straining is a geometric
mechanism. Fines are retained by straining when they arrive in a
pore space that is too small to enable passage. However, the results
found in this paper suggest that anomalously small fines, which are
smaller than the smallest pore throats in the porous media, can be
strained as well. This finding is consistent with experimental results
reported by previous studies [8,11,12]. The conventional straining
model cannot explain this uncharacteristic behavior [11]. Filtration
is a physicochemical mechanism controlled by electrostatic,
chemical, and van der Waals forces that result in the attachment/
detachment of particles to the filter media. In addition to surface
deposition and pore throat binding, the surface properties of clay
were found to be greater influencing factors in causing coal fines
accumulation in the prop pant pack. The surface characteristics of
coal fines include surface area, pore volume and size distribution,
wettability, and electrical property [13]. The surface of fines has
very strong adsorption because of its greater surface area or pore
volume, surface roughness, and surface energy, which cause coal
fines to aggregate [14-18].
Results and Discussion
Experiment results show that clay invading into the prop pant
pack would plug the pore throat of the prop pant pack and would
cause a sharp decline in fracture conductivity [19-21]. There is a
linear relationship between closure pressure and conductivity.
This invasion could decrease the conductivity by 50% when the
concentration of coal fines is 3% and the closure pressure is 16MPa.
Moreover, the damage would rapidly worsen with increasing fines
concentration. When fines concentration reaches 5%, the pore
throat of the prop pant pack would be completely blocked, and
no conductivity would be available under 16MPa (Figure 4 & 5).
Different damage degree can be seen from Figure 6. This finding
indicates that when the qualities of fines retention in the prop pant
pack increase, propped fractures conductivity would decrease.
In order to mitigate conductivity damage, few fines should be
allowed to enter prop pant pack. The effects of flow rate and clay
concentration on conductivity damage are shown in Figure 5 &
6, respectively. The discharge of fluid at different rates and the
measurement of the corresponding conductivity are shown in
Figure 5. Under a 16MPa closure pressure, flow rate changed from
3 to 10mL/min much more clay are retained in the pore throat
at higher fluid rate because of their strong adsorption property,
thereby causing an inevitable decrease in conductivity, as shown
in Figure 5. The prop pant pack with higher clay concentration has
more retention (Figure 6). In addition, the formation of effective
flow path scan is seen during the experiments, which provide and
retain effective fracture conductivity as shown in the Figure7.
Figure 4: Effect of fracture close pressure on conductivity.
Figure 5: Effect of coal fines concentration on conductivity.
Figure 6: High-magnification view of proppant pack invaded
by fines. a: clean water; b: 3wt% clay; c: 4wt% clay; d: 5wt%
clay.
3/4
How to cite this article: Weidong Z, Xuhui G, Maoyong F, Shouqiang Z. Clay Migration in Proppant during Production in Argillaceous Unconsolidated
Reservoir. Aspects Min Miner Sci. 1(2). AMMS.000508. 2018. DOI: 10.31031/AMMS.2018.01.000508
Aspects Min Miner Sci Copyright © Weidong Zhanga
Volume 1 - Issue - 2
Figure 7: The formation of flow paths.
Conclusion
1. An effective experimental method that could simulate the
process of fine migration in the prop pant pack was proposed.
2. Fines retention seriously damages fracture conductivity. The
damage significantly worsens with increasing clay concentration
and fracture closure pressure. Only 3% clay can decrease
conductivity by 50%, whereas 5% fines can cause the fracture to
lose conductivity completely.
3. Flow paths form in the flow of the plugging, which is the main
reason that keeps the permeability of the reservoir. Flow path can
keep a steady condition while a constant flow and concentration is
steady during a long period.
4. Formation clay should not be allowed to enter the prop pant
pack. Injecting non-fluids into reservoir should be suggested to take
into consideration.
Acknowledgment
This research is supported by the National Natural Science
Foundation of China (Project no.51374229).
References
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Academic Publishers, USA.
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migration by nanofluids injection, an experimental study. Notre Dame L
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characteristics to study utilization of nanoparticles to reduce fines
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8.	 Marlow HJ, Duston KL, Wiesner MR, Tomson MB, Wilson JT, et al. (1991)
Microbial transport through porous media: the effects of hydraulic
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(2007) Controlling formation fines at their sources to maintain well
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10.	Rodriguez E, Bryant S (2007) Straining of fine particles in gaps in porous
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11.	Gruesbeck C, Collins RE (1982) Entrainment and deposition of fine
particles in porous media. Soc Pet Eng AIME 6(6): 847-856.
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of permeability and spatial correlation in a real random sphere
packing. Transport in Porous Media 11(1): 53-70.
13.	Rong RX, Hitchins J (1995) Preliminary study of correlations between
fine coal characteristics and properties and their dewatering
behaviour. Minerals Engineering 8(3): 293-309.
14.	Baghdikian SY, Sharma MM, Handy LL (1989) Flow of clay suspensions
through porous media.  Society of Petroleum Engineers 4(2): SPE-
16257-PA.
15.	Blauch M, Weaver J, Parker M, Todd B, Glovor M (1999) New insights into
proppant-pack damage due to infiltration of formation fines. SPE Annual
Technical Conference and Exhibition, Houston, Texas, SPE 56833.
16.	El-Monier IA, Nasr-El-D HA (2011) Mitigation of fines migration using
a new clay stabilizer: a mechanistic study. SPE European Formation
Damage Conference, Noordwijk, The Netherlands, SPE 144180.
17.	Huang T, Crews JB, Willingham JR (2008) Nanoparticles for formation
fines fixation and improving performance of surfactant structure fluids.
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elevated temperature. J Energy Resour Technol 127(3): 171-180.
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saturatedsand columns: influence of physical and chemical surface
properties on deposition. Colloids Surf A Physicochem Eng Asp 316(1-
3): 142-150.
Aspects Min Miner Sci Copyright © Weidong Zhanga
4/4
How to cite this article: Weidong Z, Xuhui G, Maoyong F, Shouqiang Z. Clay Migration in Proppant during Production in Argillaceous Unconsolidated
Reservoir. Aspects Min Miner Sci. 1(2). AMMS.000508. 2018. DOI: 10.31031/AMMS.2018.01.000508
Volume 1 - Issue - 2
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Clay Migration in Proppant during Production in Argillaceous Unconsolidated Reservoir-Crimson Publishers

  • 1. Weidong Zhanga*, Xuhui Guan, Maoyong Fu and Shouqiang Zhao College of Petroleum Engineering, China University of Petroleum, China *Corresponding author: Weidong Zhanga, College of Petroleum Engineering, China University of Petroleum, Qingdao 266580, China, Email: Submission: February 12, 2018; Published: February 20, 2018 Clay Migration in Proppant during Production in Argillaceous Unconsolidated Reservoir Abstract Fine migration inevitably occurs during the process of fracturing production in argillaceous unconsolidated reservoirs. Using the API conductivity cell simulate the process of the production of the reservoir. The damage to conductivity caused by fines migration in the pack and the factors affecting such migration are analyzed. The result indicates that clay are likely to aggregate and be retained in the prop pant pack because of the adsorption and deposition, thereby resulting in pore throat plugging, which causes serious damage to fracture conductivity. The mobility and retention of clay in the prop pant pack are affected by flow rate, fracture closure stress and fines property. This research is important for the further research. Keywords: Unconsolidated sand; Fine migration; Fracture conductivity; Argillaceous unconsolidated reservoir Introduction Figure 1: Another view of the newborn with Adams-Oliver syndrome associated with the related disorders. Fines migration and consequent permeability damage is one of the widest spread physical mechanisms of formation damage in gas andoilfields[1,2].Liftingofnaturalreservoirfinesathighinjection/ production rates with resulting migration and straining usually yields a significant increase in the flow trajectory tortuosity and resulting drastic permeability decline [2,3]. Numerous measures focused on fixing the reservoir fines (against fines mobilization) [4-6]. Figure 1 shows the sequential processes of fines detachment from the pore surface, migration and straining in a thin pore throat. Fines-sensitive technologies of oil and gas recovery are primarily focused on enhancing or inhibiting the particle detachment process [7]. However few are focused on the mechanism of the fine migration in the field, fracture and prop pant. So understanding the mechanics of particle migration and the decline degree of permeability in the prop pant is important. The structure of the text is as follows. Section 2 presents the methodology of the laboratory study, including preparation of materials. Section 3present the mechanism of the clay retention. Section 4 describes and analyses the obtained results. Section 5 concludes the paper. Figure 2: Schematic of fines migration model and conductivity test apparatus. The experimental apparatus used in this paper are mainly based on a modified API standard fracture conductivity instrument [8,9] that consists of an Automated hydraulic intensifier system, a fluid injection system, and a hastelloy conductivity cell (Figure 2). This instrument can simulate real reservoir conditions. However, the provided flow rate is limited, and a constant-flux pump of maximum flow rate up to 10mL/min is configured. The simulation process of fines invasion into the prop pant pack is presented as follows: (1) The conductivity cell was paved with high-strength and large-sized ceramsite (380–830µm) from the inlet to outlet. Intermediate container provides mixed suspension which can provide different fines concentrations to represent the formation Research Article Aspects in Mining & Mineral ScienceC CRIMSON PUBLISHERS Wings to the Research 1/4Copyright © All rights are reserved by Weidong Zhanga. Volume 1 - Issue - 2 ISSN 2578-0255
  • 2. Aspects Min Miner Sci Copyright © Weidong Zhanga 2/4 How to cite this article: Weidong Z, Xuhui G, Maoyong F, Shouqiang Z. Clay Migration in Proppant during Production in Argillaceous Unconsolidated Reservoir. Aspects Min Miner Sci. 1(2). AMMS.000508. 2018. DOI: 10.31031/AMMS.2018.01.000508 Volume 1 - Issue - 2 supply capability. Fines consist of 60% quartz sand, 24% illite, 6% montmorillonite, 10% Plagioclase. The clay size was measured using intelligent laser particle analyzer, as shown in Figure 3. Figure 3: Diameter distribution of clay fines. (2) The desired closure pressure was applied to the steel plate using the hydraulic pump. The constant-flux pumps then drew to drive suspension to the prop pant pack in the conductivity cell. The production process of the reservoir can be simulated using Steps 1-2. Fines Retention Mechanisms Filtration and straining are two distinct mechanisms that cause fines retention in porous media [10]. Straining is a geometric mechanism. Fines are retained by straining when they arrive in a pore space that is too small to enable passage. However, the results found in this paper suggest that anomalously small fines, which are smaller than the smallest pore throats in the porous media, can be strained as well. This finding is consistent with experimental results reported by previous studies [8,11,12]. The conventional straining model cannot explain this uncharacteristic behavior [11]. Filtration is a physicochemical mechanism controlled by electrostatic, chemical, and van der Waals forces that result in the attachment/ detachment of particles to the filter media. In addition to surface deposition and pore throat binding, the surface properties of clay were found to be greater influencing factors in causing coal fines accumulation in the prop pant pack. The surface characteristics of coal fines include surface area, pore volume and size distribution, wettability, and electrical property [13]. The surface of fines has very strong adsorption because of its greater surface area or pore volume, surface roughness, and surface energy, which cause coal fines to aggregate [14-18]. Results and Discussion Experiment results show that clay invading into the prop pant pack would plug the pore throat of the prop pant pack and would cause a sharp decline in fracture conductivity [19-21]. There is a linear relationship between closure pressure and conductivity. This invasion could decrease the conductivity by 50% when the concentration of coal fines is 3% and the closure pressure is 16MPa. Moreover, the damage would rapidly worsen with increasing fines concentration. When fines concentration reaches 5%, the pore throat of the prop pant pack would be completely blocked, and no conductivity would be available under 16MPa (Figure 4 & 5). Different damage degree can be seen from Figure 6. This finding indicates that when the qualities of fines retention in the prop pant pack increase, propped fractures conductivity would decrease. In order to mitigate conductivity damage, few fines should be allowed to enter prop pant pack. The effects of flow rate and clay concentration on conductivity damage are shown in Figure 5 & 6, respectively. The discharge of fluid at different rates and the measurement of the corresponding conductivity are shown in Figure 5. Under a 16MPa closure pressure, flow rate changed from 3 to 10mL/min much more clay are retained in the pore throat at higher fluid rate because of their strong adsorption property, thereby causing an inevitable decrease in conductivity, as shown in Figure 5. The prop pant pack with higher clay concentration has more retention (Figure 6). In addition, the formation of effective flow path scan is seen during the experiments, which provide and retain effective fracture conductivity as shown in the Figure7. Figure 4: Effect of fracture close pressure on conductivity. Figure 5: Effect of coal fines concentration on conductivity. Figure 6: High-magnification view of proppant pack invaded by fines. a: clean water; b: 3wt% clay; c: 4wt% clay; d: 5wt% clay.
  • 3. 3/4 How to cite this article: Weidong Z, Xuhui G, Maoyong F, Shouqiang Z. Clay Migration in Proppant during Production in Argillaceous Unconsolidated Reservoir. Aspects Min Miner Sci. 1(2). AMMS.000508. 2018. DOI: 10.31031/AMMS.2018.01.000508 Aspects Min Miner Sci Copyright © Weidong Zhanga Volume 1 - Issue - 2 Figure 7: The formation of flow paths. Conclusion 1. An effective experimental method that could simulate the process of fine migration in the prop pant pack was proposed. 2. Fines retention seriously damages fracture conductivity. The damage significantly worsens with increasing clay concentration and fracture closure pressure. Only 3% clay can decrease conductivity by 50%, whereas 5% fines can cause the fracture to lose conductivity completely. 3. Flow paths form in the flow of the plugging, which is the main reason that keeps the permeability of the reservoir. Flow path can keep a steady condition while a constant flow and concentration is steady during a long period. 4. Formation clay should not be allowed to enter the prop pant pack. Injecting non-fluids into reservoir should be suggested to take into consideration. Acknowledgment This research is supported by the National Natural Science Foundation of China (Project no.51374229). References 1. Khilar KC, Fogler HS (1998) Migration of fines in porous media. Kluwer Academic Publishers, USA. 2. Byrne M, Waggoner S (2009) Fines migration in a high temperature gas reservoir-laboratory simulation and implications for completion design. Society of Petroleum Engineers. 3. Zeinijahromi A, Farajzadeh R, Bruining J, Bedrikovetsky P (2016) Effect of fines migration on oil–water relative permeability during two-phase flow in porous media. Fuel 176: 222-236. 4. Habibi A, Pourafshari P, Ahmadi M, Ayatollahi S (2013) Reduction of fine migration by nanofluids injection, an experimental study. Notre Dame L rev 18(2): 374-384. 5. Assef Y, Arab D, Pourafshary P (2014) Application of nanofluid to control fines migration to improve the performance of low salinity water flooding andalkaline flooding. J Petrol Sci Eng 124: 331-340. 6. Yuan B, Moghanloo RG, Pattamasingh P (2015) Applying method of characteristics to study utilization of nanoparticles to reduce fines migration in deepwater reservoirs. SPE European Formation Damage Conference and Exhibition, SPE 174192. 7. Yuan B, Moghanloo R, Zheng D (2016) Analytical evaluation of Nanoparticle application to mitigate fines migration in porous media. SPE Journal. 8. Marlow HJ, Duston KL, Wiesner MR, Tomson MB, Wilson JT, et al. (1991) Microbial transport through porous media: the effects of hydraulic conductivity and injection velocity.  Journal of Hazardous Materials 28(1): 65-74. 9. Nguyen PD, Weaver JD, Rickman RD, Dusterhoft RG, Parker MA (2007) Controlling formation fines at their sources to maintain well productivity. Spe Production & Operations 22(2): 202-215. 10. Rodriguez E, Bryant S (2007) Straining of fine particles in gaps in porous media. Society of Petroleum Engineers. 11. Gruesbeck C, Collins RE (1982) Entrainment and deposition of fine particles in porous media. Soc Pet Eng AIME 6(6): 847-856. 12. Bryant SL, King PR, Mellor DW (1993) Network model evaluation of permeability and spatial correlation in a real random sphere packing. Transport in Porous Media 11(1): 53-70. 13. Rong RX, Hitchins J (1995) Preliminary study of correlations between fine coal characteristics and properties and their dewatering behaviour. Minerals Engineering 8(3): 293-309. 14. Baghdikian SY, Sharma MM, Handy LL (1989) Flow of clay suspensions through porous media.  Society of Petroleum Engineers 4(2): SPE- 16257-PA. 15. Blauch M, Weaver J, Parker M, Todd B, Glovor M (1999) New insights into proppant-pack damage due to infiltration of formation fines. SPE Annual Technical Conference and Exhibition, Houston, Texas, SPE 56833. 16. El-Monier IA, Nasr-El-D HA (2011) Mitigation of fines migration using a new clay stabilizer: a mechanistic study. SPE European Formation Damage Conference, Noordwijk, The Netherlands, SPE 144180. 17. Huang T, Crews JB, Willingham JR (2008) Nanoparticles for formation fines fixation and improving performance of surfactant structure fluids. International Petroleum Technology Conference, Malaysia, IPTC 12414. 18. Haug MD, Wong LC (1992) Impact of molding water content on hydraulic conductivity of compacted sand-bentonite. Can Geotech J 29(2): 253- 262. 19. Ruckenstein E, Prieve DC (1976) Adsorption and desorption of particles and their chromatographic separation. Am Inst Chem Eng J 22 (2): 276- 283. 20. Schembre KM, Kovscek AR (2005) Mechanism of formation damage at elevated temperature. J Energy Resour Technol 127(3): 171-180. 21. Shani C, Weisbrod N, Yakirevich A (1998) Colloid transport through saturatedsand columns: influence of physical and chemical surface properties on deposition. Colloids Surf A Physicochem Eng Asp 316(1- 3): 142-150.
  • 4. Aspects Min Miner Sci Copyright © Weidong Zhanga 4/4 How to cite this article: Weidong Z, Xuhui G, Maoyong F, Shouqiang Z. Clay Migration in Proppant during Production in Argillaceous Unconsolidated Reservoir. Aspects Min Miner Sci. 1(2). AMMS.000508. 2018. DOI: 10.31031/AMMS.2018.01.000508 Volume 1 - Issue - 2 Your subsequent submission with Crimson Publishers will attain the below benefits • High-level peer review and editorial services • Freely accessible online immediately upon publication • Authors retain the copyright to their work • Licensing it under a Creative Commons license • Visibility through different online platforms • Global attainment for your research • Article availability in different formats (Pdf, E-pub, Full Text) • Endless customer service • Reasonable Membership services • Reprints availability upon request • One step article tracking system For possible submissions Click Here Submit Article Creative Commons Attribution 4.0 International License