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Surface Engineering

_tech

Surface Engineering
aintech@ain.es

_tech | _consulting | _legal
_tech | _consulting | _legal

Sesiones de Comunicación AIN_tech, 13 de Enero de 2012

1/20
1/18
Surface Engineering

_tech

SURFACE ENGINEERING AT AIN
Materials technology is a transversal research field
strategic for most of industrial sectors and activities.
The surface of a material is the most critical part:
- Is the frontier between the material and its environment.
- It is the key for ensuring its service life.

Anexos

- It allows to provide new functions to the materials
- It concentrates most of the added value of materials

_tech | _consulting | _legal

2/18
Surface Engineering

_tech

SURFACE ENGINEERING OVERVIEW

2000

2010

Nanoparticles &
nanocompounding lab
(2012)

Equipment for Plasma
treatments (2011)

Equipment for analysis
and electron
microscopy (2003)

ProjectCONSOLIDER
coordinated by AIN
(2008)

First CENIT project
coordinated by AIN
(2007)

First EUREKA project
leaded by AIN (2003)

Incorporation of PVD
treatments (2000)
First European Project
leaded by AIN (1992)

1980,s

1990

Creation of the
Tribologylab (1995)

_tech | _consulting | _legal

AIN - CIAS is created in
1989 as a pioneer
center in Spain on Ion
Implantation

Laboratories

First project within thel
Plan Nacional de I+D
leaded by AIN(1991)

Projects

Organization of the XII edition of
TRATERMAT (2010)

First participation in a scientific
conference in the USA (2004)

Anexos
First Course on Surface Engineering
(1998)
First European Symposium on Surfaces
in AIN (1994)

First participation on a scientific
European conference (1993)

Technological Difussion

3/18
Surface Engineering

_tech

SURFACE ENGINEERING OVERVIEW
THE BIG NUMBERS 1990 - 2012
- 21 RESEARCHERS (80% PhD or MSc).
- 19 GRANT HOLDERS TRAINED AT AIN.
- 500 CLIENTS IN NAVARRE, SPAIN AND EUROPE.
- 100 CONSOLIDATED PARTNERS ALL OVER EUROPE.
- PARTICIPATION IN10 NETWORKS OR PLATFORMS.
- PARTICIPATION IN MORE THAN 100 EUROPEAN AND NACIONAL PROJECTS.
- ORGANIZATION OF MORE THAN 50 COURSES, SYMPOSIUMS, etc.
- 4 NATIONAL & 1 EUROPEAN PATENTS.
- PUBLICATION OF 120 SCIENTIFIC ARTICLES.
- PARTICIPATION IN MORE THAN 100 CONFERENCES
- 350 APPEARANCES IN THE MEDIA.
- 2 M€ / YEAR ANNUAL TURNOVER.
_tech | _consulting | _legal

4/18
Surface Engineering

_tech

THE SURFACE ENGINEERING TEAM
EL GRUPO - ORGANIZACION

Laboratorios y support
Laboratories andapoyo

Proyectos projects
Applied R&D con empresas

Proyectos fundamentales
Basic R&D projects

_tech | _consulting | _legal

5/18
Surface Engineering

_tech

TECHNOLOGICAL OFFER
Surface Treatment Techniques:
Ion implantation:
- All species mass separation Ion Implanter
- Nitrogen ion implanter
- IBAD + LEHT
- Plasma Immersion PI3 implanter
PVD:
- PVD – Cathodic Arc
- PVD - Magnetron Sputtering
Others:
- Spin coating
- Plasma activation & Plasma polymerization

_tech | _consulting | _legal

Film

Substrate
Coatings
can
change
dimensions of components
and
have
an
abrupt
interlayer.

Implanted
zone

Anexos

Ion implanted surfaces have
not any interlayer and do
not change dimensions

6/18
Surface Engineering

_tech

TECHNOLOGICAL OFFER
Microscopy and analysis techniques:
Analysis:
- GD-OES (48 channels)
- XRF
- EDS
- EBSD
- XRD
- IR (FTIR) y UV (VISNIR)
Optical microscopy:
- 3 optical microscopes + image analysis
Electron and scan probe microscopy:
- FE-SEM
- AFM

At%

Anexos

_tech | _consulting | _legal

90
85
80
75
70
65
C
60
Cr
55
50
Fe
45
N
40
O
35
30
Ti
25
20
15
10
5
0
0,0 0,5 1,0 1,5 2,0 2,5 3,0 3,5 4,0
Profundidad (μm)

7/18
Surface Engineering

_tech

TECHNOLOGICAL OFFER
Surface caractherization techniques:

_tech | _consulting | _legal

Anexos

0,26

Referencia

0,24
0,22
0,20

Profundidad (µ m)

Hardness - Indentation:
- Durometer (Rockwell, Brinell, Vickers)
- Microdurometer (Vickers, Knoop)
- Ultramicrodurometer (Fischeroscope)
- Nanoindenter Hysitron
Tribology: Wear y Friction:
- Tribometer with humidity control
- High Temperature Tribometer
- Tribo-corrosion
Other surface properties:
- Optical profilometer
- Mechanical profilometer
- Scratch tester
- Contact angle goniometer
- Calotest
- Spectrophotometer
- Conductimeter

0,18
0,16
0,14
0,12
0,10

CrN

0,08
0,06
0,04
0,02
0,00
-0,02
0

2

4

6

8

10

Carga (mN)

8/18
Surface Engineering

_tech

TECHNOLOGICAL OFFER
Techniques for nanoparticles and nanocomposites:
Closed room:
- Prototype of compounding reactor (5 to 20 l)
- Laminar flow cabinet
- Sonicators
- Schlenk techniques
Auxiliary equipment:
- Z-sizer
- Viscosimeter
- Universal centrifuges
- Vacuum ovens

_tech | _consulting | _legal

Anexos

9/18
Surface Engineering

_tech
STRATEGIC AREAS

Smart
Materials

Advanced treatments and
coatings to solve friction, wear
and corrosion problems.

Tribology
Smart coatings for decorative
applications with optical,
electrical or biological
properties.

Energy

Bio

Biocompatible or biocide
surfaces for medical
applications.

New materials and surfaces for
renevable energy applications

Treatments, analysis and
characterisation of surfaces

_tech | _consulting | _legal

10/18
_tech

Surface Engineering

TRIBOLOGY
Was the traditional R+D field at AIN.
Now, this activity continues:
- Tribocorrosion.
- Tribology under extreme conditions.
- Micro / nano fabrication.
- Standarization.

Tribology

RECENT PROJECTS:
- 6FP MASMICRO.
- 7FP M32S.
- CENIT FORMA-0.
- MAT-NANOTRIBOCOR, MAT-Ni-TOOLS.
- IAP MICROCONTACT, IAP MULTICAPA.
- MANUNET EDS-CUT
- E! TRIBOSTAND.
- CVD DIAMANTE
_tech | _consulting | _legal

11/18
_tech

Surface Engineering

SMART COATING & MATERIALS
It is the answer to an increasing demand on:
- Eco-friendly coating technologies.
- Self-cleaning coatings.
- Active windows.
- Electric and magnetic properties.
- Customised displays.

Deco

RECENT PROJECTS:
- CONSOLIDER FUN-COAT.
- CENIT ART-DECO.
- EUROINNOVA NANOCONS.
- SURFALUX.
- NANOMAT.

_tech | _consulting | _legal

12/18
_tech

Surface Engineering

BIOMATERIALS
Bio

Due to a growing demand and a natural growth
of our activity in applications such us:
- Articular prostheses (wear, metallosis).
- Coronary prostheses (restenosis).
- Hypoallergenic coatings.
- Bacteriostatic and biocide coatings.
RECENT PROJECTS:
- 6FP NEWBONE.
- E! DUBIOP.
- GdN BIO-COAT.
- CONSOLIDER FUN-COAT.
- ADDISC.
- BIOSURF.
_tech | _consulting | _legal

13/18
_tech

Surface Engineering

NEW ENERGY SOURCES
Energy

New opportunities in materials for the
generation of new alternative energy
sources:
- Photovoltaic coatings.
- Coatings for Solar Thermal applications.
- Materials for fuel cells.

RECENT PROJECTS:
- 7FP DEPHOTEX.
- ENE-ODISEA.
- CONSOLIDER FUN-COAT.
- CCPC
- HITECO
_tech | _consulting | _legal

Energía

14/18
Surface Engineering

_tech

GEOGRAPHIC SEGMENTATION
5

20

10

140
15

250

25

30

130

145
60

15

5

5

Anexos
5

15
5

_tech | _consulting | _legal

15/18
_tech

Surface Engineering
MARKET SEGMENTATION

Anexos

Transversal technologies: Useful for all industrial sectors!
_tech | _consulting | _legal

16/18
Surface Engineering

_tech

National and European Projects

Anexos
- 20 P. National projects
- 3 CENIT projects
- 1 CONSOLIDER project
- 12 European Framework Programmes’ projects
- 4 EUREKA projects
- 8 INTERREG, A-N and CTP projects
- 5 ERA-NET projects
_tech | _consulting | _legal

17/18
_tech

Surface Engineering

THANKS FOR
YOUR KIND ATTENTION!

_tech | _consulting | _legal

18/18

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Surface engineering 2013-english

  • 1. Surface Engineering _tech Surface Engineering aintech@ain.es _tech | _consulting | _legal _tech | _consulting | _legal Sesiones de Comunicación AIN_tech, 13 de Enero de 2012 1/20 1/18
  • 2. Surface Engineering _tech SURFACE ENGINEERING AT AIN Materials technology is a transversal research field strategic for most of industrial sectors and activities. The surface of a material is the most critical part: - Is the frontier between the material and its environment. - It is the key for ensuring its service life. Anexos - It allows to provide new functions to the materials - It concentrates most of the added value of materials _tech | _consulting | _legal 2/18
  • 3. Surface Engineering _tech SURFACE ENGINEERING OVERVIEW 2000 2010 Nanoparticles & nanocompounding lab (2012) Equipment for Plasma treatments (2011) Equipment for analysis and electron microscopy (2003) ProjectCONSOLIDER coordinated by AIN (2008) First CENIT project coordinated by AIN (2007) First EUREKA project leaded by AIN (2003) Incorporation of PVD treatments (2000) First European Project leaded by AIN (1992) 1980,s 1990 Creation of the Tribologylab (1995) _tech | _consulting | _legal AIN - CIAS is created in 1989 as a pioneer center in Spain on Ion Implantation Laboratories First project within thel Plan Nacional de I+D leaded by AIN(1991) Projects Organization of the XII edition of TRATERMAT (2010) First participation in a scientific conference in the USA (2004) Anexos First Course on Surface Engineering (1998) First European Symposium on Surfaces in AIN (1994) First participation on a scientific European conference (1993) Technological Difussion 3/18
  • 4. Surface Engineering _tech SURFACE ENGINEERING OVERVIEW THE BIG NUMBERS 1990 - 2012 - 21 RESEARCHERS (80% PhD or MSc). - 19 GRANT HOLDERS TRAINED AT AIN. - 500 CLIENTS IN NAVARRE, SPAIN AND EUROPE. - 100 CONSOLIDATED PARTNERS ALL OVER EUROPE. - PARTICIPATION IN10 NETWORKS OR PLATFORMS. - PARTICIPATION IN MORE THAN 100 EUROPEAN AND NACIONAL PROJECTS. - ORGANIZATION OF MORE THAN 50 COURSES, SYMPOSIUMS, etc. - 4 NATIONAL & 1 EUROPEAN PATENTS. - PUBLICATION OF 120 SCIENTIFIC ARTICLES. - PARTICIPATION IN MORE THAN 100 CONFERENCES - 350 APPEARANCES IN THE MEDIA. - 2 M€ / YEAR ANNUAL TURNOVER. _tech | _consulting | _legal 4/18
  • 5. Surface Engineering _tech THE SURFACE ENGINEERING TEAM EL GRUPO - ORGANIZACION Laboratorios y support Laboratories andapoyo Proyectos projects Applied R&D con empresas Proyectos fundamentales Basic R&D projects _tech | _consulting | _legal 5/18
  • 6. Surface Engineering _tech TECHNOLOGICAL OFFER Surface Treatment Techniques: Ion implantation: - All species mass separation Ion Implanter - Nitrogen ion implanter - IBAD + LEHT - Plasma Immersion PI3 implanter PVD: - PVD – Cathodic Arc - PVD - Magnetron Sputtering Others: - Spin coating - Plasma activation & Plasma polymerization _tech | _consulting | _legal Film Substrate Coatings can change dimensions of components and have an abrupt interlayer. Implanted zone Anexos Ion implanted surfaces have not any interlayer and do not change dimensions 6/18
  • 7. Surface Engineering _tech TECHNOLOGICAL OFFER Microscopy and analysis techniques: Analysis: - GD-OES (48 channels) - XRF - EDS - EBSD - XRD - IR (FTIR) y UV (VISNIR) Optical microscopy: - 3 optical microscopes + image analysis Electron and scan probe microscopy: - FE-SEM - AFM At% Anexos _tech | _consulting | _legal 90 85 80 75 70 65 C 60 Cr 55 50 Fe 45 N 40 O 35 30 Ti 25 20 15 10 5 0 0,0 0,5 1,0 1,5 2,0 2,5 3,0 3,5 4,0 Profundidad (μm) 7/18
  • 8. Surface Engineering _tech TECHNOLOGICAL OFFER Surface caractherization techniques: _tech | _consulting | _legal Anexos 0,26 Referencia 0,24 0,22 0,20 Profundidad (µ m) Hardness - Indentation: - Durometer (Rockwell, Brinell, Vickers) - Microdurometer (Vickers, Knoop) - Ultramicrodurometer (Fischeroscope) - Nanoindenter Hysitron Tribology: Wear y Friction: - Tribometer with humidity control - High Temperature Tribometer - Tribo-corrosion Other surface properties: - Optical profilometer - Mechanical profilometer - Scratch tester - Contact angle goniometer - Calotest - Spectrophotometer - Conductimeter 0,18 0,16 0,14 0,12 0,10 CrN 0,08 0,06 0,04 0,02 0,00 -0,02 0 2 4 6 8 10 Carga (mN) 8/18
  • 9. Surface Engineering _tech TECHNOLOGICAL OFFER Techniques for nanoparticles and nanocomposites: Closed room: - Prototype of compounding reactor (5 to 20 l) - Laminar flow cabinet - Sonicators - Schlenk techniques Auxiliary equipment: - Z-sizer - Viscosimeter - Universal centrifuges - Vacuum ovens _tech | _consulting | _legal Anexos 9/18
  • 10. Surface Engineering _tech STRATEGIC AREAS Smart Materials Advanced treatments and coatings to solve friction, wear and corrosion problems. Tribology Smart coatings for decorative applications with optical, electrical or biological properties. Energy Bio Biocompatible or biocide surfaces for medical applications. New materials and surfaces for renevable energy applications Treatments, analysis and characterisation of surfaces _tech | _consulting | _legal 10/18
  • 11. _tech Surface Engineering TRIBOLOGY Was the traditional R+D field at AIN. Now, this activity continues: - Tribocorrosion. - Tribology under extreme conditions. - Micro / nano fabrication. - Standarization. Tribology RECENT PROJECTS: - 6FP MASMICRO. - 7FP M32S. - CENIT FORMA-0. - MAT-NANOTRIBOCOR, MAT-Ni-TOOLS. - IAP MICROCONTACT, IAP MULTICAPA. - MANUNET EDS-CUT - E! TRIBOSTAND. - CVD DIAMANTE _tech | _consulting | _legal 11/18
  • 12. _tech Surface Engineering SMART COATING & MATERIALS It is the answer to an increasing demand on: - Eco-friendly coating technologies. - Self-cleaning coatings. - Active windows. - Electric and magnetic properties. - Customised displays. Deco RECENT PROJECTS: - CONSOLIDER FUN-COAT. - CENIT ART-DECO. - EUROINNOVA NANOCONS. - SURFALUX. - NANOMAT. _tech | _consulting | _legal 12/18
  • 13. _tech Surface Engineering BIOMATERIALS Bio Due to a growing demand and a natural growth of our activity in applications such us: - Articular prostheses (wear, metallosis). - Coronary prostheses (restenosis). - Hypoallergenic coatings. - Bacteriostatic and biocide coatings. RECENT PROJECTS: - 6FP NEWBONE. - E! DUBIOP. - GdN BIO-COAT. - CONSOLIDER FUN-COAT. - ADDISC. - BIOSURF. _tech | _consulting | _legal 13/18
  • 14. _tech Surface Engineering NEW ENERGY SOURCES Energy New opportunities in materials for the generation of new alternative energy sources: - Photovoltaic coatings. - Coatings for Solar Thermal applications. - Materials for fuel cells. RECENT PROJECTS: - 7FP DEPHOTEX. - ENE-ODISEA. - CONSOLIDER FUN-COAT. - CCPC - HITECO _tech | _consulting | _legal Energía 14/18
  • 16. _tech Surface Engineering MARKET SEGMENTATION Anexos Transversal technologies: Useful for all industrial sectors! _tech | _consulting | _legal 16/18
  • 17. Surface Engineering _tech National and European Projects Anexos - 20 P. National projects - 3 CENIT projects - 1 CONSOLIDER project - 12 European Framework Programmes’ projects - 4 EUREKA projects - 8 INTERREG, A-N and CTP projects - 5 ERA-NET projects _tech | _consulting | _legal 17/18
  • 18. _tech Surface Engineering THANKS FOR YOUR KIND ATTENTION! _tech | _consulting | _legal 18/18