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TI355C/07/en/07.06
51512290
Technical Information
Stamolys CA71NO
Nitrite analyzer
Compact photometric analysis system for the nitrite measurement in
drinking water, wastewater and in mineral waters
Application
• Nitrite monitoring in drinking water
• Nitrite monitoring in sewage treatment plants
• Nitrite monitoring in the mineral water production
Your benefits
• Stainless steel or glass-fibre reinforced carbon housing
available
• Two channel version available
• Measured value storage using integrated data logger
• Automatic calibration and self-cleaning
• Free selectable measuring, cleaning and calibration intervals
Stamolys CA71NO
2 Endress+Hauser
Function and system design
Measuring principle
CA71NO-A/B/C
After sample conditioning, the analyzer sample pump conveys a part of the filtrate to a mixing vessel. The
reagent pump adds reagent at a specific ratio. As a result of the reaction, the sample turns a characteristic
colour. The photometer determines the sample’s absorption of an emitted light at a specific wavelength (s. Fig.,
Pos. 2). The wavelength is parameter specific. The absorbance is proportional to the concentration of the
specified parameter in the sample (Pos. 3). Additionally, the absorption of a reference light is determined to
receive a genuine measuring result. The reference signal is subtracted from the measuring signal to prevent any
effects due to turbidity, contamination and ageing of the LEDs.
The temperature in the photometer is controlled thermostatically so that the reaction is reproducible and takes
place within a short period of time.
Measuring principle
CA71NO-D
The LED sends light at a defined wavelength through the sample. The intensity of the received light is
measured by the detector and converted to an electrical signal. In the analyzer, the respective concentration is
calculated from the proportion of light absorbed by the sample.
Nitrite Nitrite is a metastable intermediate stage of bacterial oxidation: proteins, urea É ammonium É nitrite É
nitrate.
Thus nitrite serves as an indicator in sewage treatment plant processes or in discharge streams of incomplete
nitrification.
Nitrite is often added to process and cooling water as a corrosion inhibitor. The Food Industry uses it as a
preservative (e.g. pickling salt).
Nitrite occurs very rarely in surface waters since it easily oxidizes to nitrate in the presence of air. High nitrite
concentrations in water therefore indicate the presence of partially disintegrated, organic wastes.
There should be no nitrite present in drinking water due to its toxicity (limit value according to the German
Trinkwasserverordnung (drinking water ordinance): 0.1 mg/l (ppm)). Nitrite causes haemoglobin to convert
to methaemoglobin which suppresses take up of oxygen in the blood ("inner asphyxiation").
a0001612
Photometric principle
1
2
3
4
5
Reference LED
Emitter LED
Sample
Reference detector
Measuring detector
a0001613
Photometric measuring principle
1
2
3
LED
Detector
Sample
1 2
3
Stamolys CA71NO
Endress+Hauser 3
Photometric nitrite
determination
Naphthylamine method for nitrite determination acc. to DIN 38405-D10
Under acidic conditions, nitrite ions diazotices sulphonamido, which forms a red dye in conjunction with
N-(1-naphthyl)-ethylenediamine.
The absorption is determined at a wavelength of 565 nm. The absorption intensity is proportional to the nitrite
concentration in the sample.
The reference wavelength is 880 nm.
Interferences No interferences up to the given concentration:
Copper causes decreases in nitrite measured value.
Sample conditioning Micro/ultrafiltration (Stamoclean CAT430, optional)
A membrane filter element is suspended directly into the wastewater basin or channel. A hose pump is located
in a pump box on the basin rim.The pump creates a vacuum between the membrane and the carrier plate of
the filter element. This vacuum makes the filtrate pass through the filter membrane. Suspended materials,
particles, algae and bacteria are collected on the surface of the membrane.
Due to alternating pumping and pause, intervals of more than one month are achieved between cleaning
cycles. Parallel connection of two or four filter elements increases the sampling quantity up to approx. 1 l/h
(0.26 gal/hr).
The hose pump pressure transports the sample to a collecting vessel near the analyzer over a distance of 20 m
(66 ft). For distances up to 100 m (330 ft) the sample is transported to the collecting vessel by means of
compressed air. The analyzers suck the needed sample volume from the collecting vessel.
Membrane filtration (Stamoclean CAT411, optional)
A sample flow of 0.8 to 1.8 m3
/h (3.5 to 7.9 gal/min) is continuously conducted through the micro filter via
a pressure pipe. A part of the sample passes the filter membrane and is then conveyed to the measuring device
as filtrate.
Sampling is based on the cross flow filtration principle. The PTFE filter membrane separates particles with sizes
> 0.45 μm from the filtrate. These particles are collected in front of the membrane and are washed away with
the sample flow.
The medium is conducted in a meander-like channel through the filter element. This results in a constantly
high flow rate. The high flow rate generates the self cleaning effect. Therefore, mechanical drives for the
generation of a flow at the filter surface are not necessary.
Backwash filter (Stamoclean CAT221, optional)
A sample flow of 1 to 2.5 m3
/h (4.4 to 11 gal/min) is permanently conveyed through the backwash filter by
means of a sampling pump or compressed air or rinse water. The filtrate passes through the wedge wire sieve
and is then transported to the measuring device.
Clogging is minimized by the flow at the wedge wire sieve. Automatic backwashing results in a filter operating
time of several weeks.
The automatic backwashing and a small compressor or compressed air resp. rinse water supply guarantee
low-maintenance and low-energy operation.
Customer specific solution
Before analysis, the sample has to be conditioned and to be transported to an external or to the delivered
collecting vessel.
Concentration [mg/l (ppm)] Interference
1,000 Cl –, SO4
2–
700 Cd 2+
500 Na +
, K +
, Ca 2+
50 Pb 2+
, Zn 2+
, Ni 2+
, Fe 2+
, Fe 3+
, Co 2+
, Hg 2+
, Ag +
, NiO3
–
, CO3
2–
25 Sn 2+
10 Cr (VI)
Stamolys CA71NO
4 Endress+Hauser
Measuring system A complete measuring system comprises:
• An analyzer
• A sample conditioning system (optionally):
– Micro filtration / ultra filtration Stamoclean CAT430 or Stamoclean CAT411
– Backwash filter Stamoclean CAT221
– Customer specific solution
• Collecting vessel (see product structure)
Micro / ultra filtration
a0001616
Measuring system with Stamoclean CAT430
1
2
3
4
5
6
7
8
9
Control box
Pump
Control unit
Collecting unit (optional)
Collecting vessel
Overflow
Analyzer
Aeration basin
Membrane filter
a0001615
Measuring system with Stamoclean CAT411
1
2
3
4
5
6
7
8
9
Stamoclean CAT411
Inlet
Sample pump or hydraulic main
Filtrate line
Collecting vessel
Overflow
Analyzer
Analyzer sample line
Outlet
Backwash filter
a0001617
Measuring system with Stamoclean CAT221
1
2
3
4
5
6
7
Stamoclean CAT221
Compressor or compressed air
Sample pump or hydraulic main
Sample outlet
Collecting vessel
Overflow
Analyzer
1 2 3
8
6
5
4
9
7
1
2
3
7 5 4
6
Stamolys CA71NO
Endress+Hauser 5
Input
Measured variable • NO-A/B/C
NO2-N [mg/l (ppm)]
• NO-D
NO2 [mg/l (ppm)]
Measuring ranges • NO-A
10 ... 500 μg/l (ppb)
• NO-B
0.10 ... 1.00 mg/l (ppm)
• NO-C
0.20 ... 3.00 mg/l (ppm)
• NO-D
0.01 ... 250.00 μg/l (ppb)
Wavelength • NO-A/B/C
565 nm
• NO-D
555 nm
Reference wavelength 880 nm (NO-A/B/C only)
Output
Output signal 0/4 ... 20 mA
Signal on alarm Contacts: 2 limit contacts (per channel), 1 system alarm contact
optional: end of measurement (with two channel version display of channel no. available)
Load max. 500 Ω
Data interface RS 232 C
Data logger 1024 data pairs per channel with date, time and measured value
100 data pairs with date, time and measured value for calibration factor determination (diagnostic tool)
Load capacity 230 V / 115 V AC max. 2 A, 30 V DC max. 1 A
Stamolys CA71NO
6 Endress+Hauser
Power supply
Electrical connection
" Caution!
The following figure (→ å 1) shows the connection department sticker as an example. Terminal assignment
and cable core colors can be different to the originals.
For connecting your analyzer only use the terminal assignment of the connection department sticker in the
device (→ å 2)!
a0001369
Fig. 1: Example of the connection sticker
a0001372
Fig. 2: Analyzer from top (open version resp. swung out)
1 Connection department sticker
2 Printed circuit board with terminal strip
3 Backside of the analyzer
Supply voltage 115 V AC / 230 V AC ±10%, 50/60 Hz
Power consumption approx. 50 VA
Current consumption approx. 0.2 A at 230 V
approx. 0.5 A at 115 V
Fuses 1 x time-lag 0.5 A for electronics
2 x medium time-lag 0.2 A for photometer
1 x time-lag 0.5 A for motors
80 75 70 63 57 39
27 21 15
64 58 40
28 22 16
65
79 74 69 62 56 38
26 20 14
78 73 68 61 55 37
25 19 13
77 72 67 60 54 36
24 18 12
76 71 66 59 53 35
23 17 11
RELAIS / Relay:
max. Last / load: 2A bei / at 115/230V AC, 1A bei / at 30V DC
RELAIS / Relay:
max. Last / load: 2A bei / at 115/230V AC, 1A bei / at 30V DC
OR
BK
RD
YE
V 3
V 3
V 2
V 2
V 1
V 1
0 V
0 V
keine Probe
No sample
keine Probe
No sample
0V
0V fx
fx
n.b.
n.c.
n.b.
n.c.
-17 V
-17 V
+17 V
+17 V
Schirm
Screen
Schirm
Screen
MP5 MP6
Schirm
Shield
Schirm
Shield
Reserve
Mess 2
Meas 2
Mess 2
Meas 2
+24V
I2 +
I2 +
I1 +
I1 +
I2 -
I2 -
I1 -
I1 -
Photometer
SCHRITTMOTOR
SCHRITTMOTOR
LECKF.
LECKF.
ALARM
2
ALARM
2
OPTION
STÖRUNG
ALARM
1
ALARM
1
F5
F4 M 0.2 A
M 0.2 A M 0.2 A
M 0.2 A
COM
NC
NO
COM
NC
NO
Kanal 1 Kanal 2
Channel 2
ALARM
2
ALARM
2
ALARM
1
ALARM
1
Photometer +17V
Photometer +17V Photometer -17V
Photometer -17V
n.b.
n.c.
n.b.
n.c.
BN
WH
YE
GY
BK
GN BK
YE
GN
BU
BN
Analog Out
0/4-20mA
STEP
MOTOR
LEAK
S.
LEAK
S.
0 V
0 V
WH
Channel 1
ERROR
7
6
5
4
L2
N
L1
PE
AC
MOTOR
AC
MOTOR
F2
F1
AC Motor
T 0.1A
AC Motor
T 0.1A
Elektronik
Electronics
T 0.5A
Elektronik
Electronics
T 0.5A
3
2
1
L
N
PE
NETZ
MAINS
NETZ
MAINS
Klemmen führen auch bei ausgeschaltetem Gerät Spannung !!!
Klemmen führen auch bei ausgeschaltetem Gerät Spannung !!!
Terminals voltage to ground even when the unit is switched off !!!
Terminals voltage to ground even when the unit is switched off !!!
V 4
V 4
31
30
29 0V
n.b.
n.c.
n.b.
n.c.
BU
YE
RD
GN/YE
Status
Schirm
Shield
Schirm
Shield
Schirm
Shield
Schirm
Shield
Schirm
Shield
Schirm
Shield
Schirm
Shield
Schirm
Shield
7
6
5
4
L2
N
L1
PE
AC
MOTOR
AC
MOTOR
F2
F1
AC Motor
T 0.1A
AC Motor
T 0.1A
Elektronik
Electronics
T 0.5A
Elektronik
Electronics
T 0.5A
3
2
1
L
N
PE
NETZ
MAINS
NETZ
MAINS
Klemmen führen auch bei ausgeschaltetem Gerät Spannung !!!
Klemmen führen auch bei ausgeschaltetem Gerät Spannung !!!
Terminals voltage to ground even when the unit is switched off !!!
Terminals voltage to ground even when the unit is switched off !!!
BU
YE
RD
GN/YE
GN/YE
80 75 70 63 57 39
27 21 15
64 58 40
28 22 16
65
79 74 69 62 56 38
26 20 14
78 73 68 61 55 37
25 19 13
77 72 67 60 54 36
24 18 12
76 71 66 59 53 35
23 17 11
RELAIS / Relay:
max. Last / load: 2A bei / at 115/230V AC, 1A bei / at 30V DC
RELAIS / Relay:
max. Last / load: 2A bei / at 115/230V AC, 1A bei / at 30V DC
OR
BK
RD
YE
V 3
V 3
V 2
V 2
V 1
V 1
0 V
0 V
keine Probe
No sample
keine Probe
No sample
0V
0V fx
fx
n.b.
n.c.
n.b.
n.c.
-17 V
-17 V
+17 V
+17 V
Schirm
Screen
Schirm
Screen
MP5 MP6
Schirm
Shield
Schirm
Shield
Reserve
Mess 2
Meas 2
Mess 2
Meas 2
+24V
I2 +
I2 +
I1 +
I1 +
I2 -
I2 -
I1 -
I1 -
Photometer
SCHRITTMOTOR
SCHRITTMOTOR
LECKF.
LECKF.
ALARM
2
ALARM
2
OPTION
OPTION
STÖRUNG
STÖRUNG
ALARM
1
ALARM
1
F5
F4 M 0.2 A
M 0.2 A M 0.2 A
M 0.2 A
COM
NC
NO
COM
NC
NO
Kanal 1 Kanal 2
Channel 2
ALARM
2
ALARM
2
ALARM
1
ALARM
1
Photometer +17V
Photometer +17V Photometer -17V
Photometer -17V
n.b.
n.c.
n.b.
n.c.
BN
WH
YE
GY
BK
GN BK
YE
GN
BU
BN
Analog Out
0/4-20mA
STEP
MOTOR
STEP
MOTOR
LEAK
S.
LEAK
S.
0 V
0 V
WH
Channel 1
ERROR
ERROR
V 4
V 4
31
30
29 0V
n.b.
n.c.
n.b.
n.c.
Status
Schirm
Shield
Schirm
Shield
Schirm
Shield
Schirm
Shield
Schirm
Shield
Schirm
Shield
Schirm
Shield
Schirm
Shield
1
2 3
Stamolys CA71NO
Endress+Hauser 7
Performance characteristics
Time between two
measurements
tmes = reaction time + rinse time + waiting time + rinse again time + filling time + sampling time +
reagent refusal time (min. waiting time = 0 min)
Maximum measured error ±2 % of measuring range end
Repeatability • NO-A:
up to 100 μg/l: ± 5 μg/l (ppb)
> 100 μg/l: ± 0.1 μg/l (ppb)
• NO-B:
up to 0.25 mg/l: ± 0.01 mg/l (ppm)
> 0.25 mg/l: ± 0.02 mg/l (ppm)
• NO-C:
up to 0.50 mg/l: ± 0.03 mg/l (ppm)
> 0.50 mg/l: ± 0.06 mg/l (ppm)
• NO-D:
± 2 μg/l (ppb)
Measuring interval tmes to 120 min
Reaction time NO-A/B/C
2 minutes
NO-D
210 sec
Sample requirement NO-A/B/C
15 ml (0.51 fl.oz.) per measurement
NO-D
20 ml (0.68 fl.oz.) per measurement
Reagent requirement NO-A/B/C
1 x 0.21 ml (0.007 fl.oz.)
0.91 l (0.24 gal) per reagent per month with 10 minute measuring interval
NO-D
1 x 0.115 ml (0.004 fl.oz.)
0.5 l (0.13 gal) per reagent per month with 10 minute measuring interval
Calibration interval1)
0 to 720 h
Rinse interval 0 to 720 h
Rinse time selectable from 20 to 300 s (standard = 60 s)
Rinse again time 30 s
Filling time NO-A/B/C
22 s
NO-D
30 sec
1) standard solutions have a limited tenability because of biological activity
Stamolys CA71NO
8 Endress+Hauser
Maintenance interval 6 months (typical)
Servicing requirement 15 minutes per week (typical)
Environment
Ambient temperature 5 ... 40 °C (40... 100 °F), avoid strong fluctuations
Humidity below the condensation limit, installation in usual, clean rooms
outdoor installation only possible with protective devices (customer supplied)
Ingress protection IP 43
Process
Sample temperature 5 to 40 °C (40 to 100 °F)
Sample flow rate min. 5 ml (0.0013 US.gal.) per min
Consistence of the sample low solid content (< 50 ppm)
Sample inlet pressureless
Stamolys CA71NO
Endress+Hauser 9
Mechanical construction
Design, dimensions Stainless steel housing, NO-A/B/C/D
a0001361
Stainless steel version
A
Detail A
360 (14.2)
436 (17.2)
243
(9.57)
200 (7.87)
120(4.72)
326 (12.8)
15(0.59)
330 (13.0)
163(6.42)
110(4.33)
Ø
27(1.06)
60(2.36)
100(3.94)
140 (5.51)
160 (6.30)
250 (9.84)
524
(20.6)
555
(21.8)
125(4.92)
165
(6.50)
Ø
21(0.83)
Ø
26
(1.02)
Ø 26(1.02)
119(4.69)
78(3.07)
47(1.85)
207 (8.15)
580
(22.8)
648
(25.5)
15(0.59)
3(0.12)
15(0.59)
30(1.18)
9(0.35)
Ø
21(0.83)
mm(inch)
38(1.5)
Stamolys CA71NO
10 Endress+Hauser
GFR housing, NO-A/B/C
a0001354-en
GFR version
GFR housing, NO-D
a0001355
GFR version
60 (2.36)
100(3.94)
140 (5.51)
160 (6.30)
250 (9.84)
125
(4.92)
165
(6.50)
Ø
21(0.83)
Ø
26(1.02)
Ø
21
(0.83)
119/4.69
78(3.07)
47(1.85)
648
(25.5)
360 (14.2)
436 (17.2)
243
(9.57)
200 (7.87)
120
(4.72)
326 (12.8)
Ø 16 (0.63)
Ø 27 (1.06)
120(4.72)
555
(21.8)
465 (18.3)
500 (19.7)
7-11/
0.28 - 0.43
(M 6)
Ø 26 (1.02)
mm(inch)
330 (13.0)
163 (6.42)
Ø
26(1.02)
Ø
16(0.63)
120
(4.72)
60 (2.36)
100(3.94)
140 (5.51)
160 (6.30)
250 (9.84)
125(4.92)
165
(6.50)
Ø
21(0.83)
Ø
26/1.02
Ø
21
(0.83)
119(4.69)
78(3.07)
47(1.85)
648
(25.5)
360 (14.2)
436 (17.2)
243
(9.57)
200 (7.87)
120
(4.72)
326 (12.8)
330 (13.0)
110
(4.33)
Ø
27
(1.06)
Ø 16 (0.63)
Ø 27 (1.06)
120(4.72)
555
(21.8)
465 (18.3)
500 (19.7)
7-11/
0.28 - 0.43
(M 6)
Ø 26(1.02)
mm (inch)
38 (1.5)
Stamolys CA71NO
Endress+Hauser 11
Open version, NO-A/B/C/D
a0001356
Open version (without housing)
! Note!
With the open version, you need an additional platform for the reagents. Mount this platform max. 35 cm
(13.8 inch) below the pumps. The reagent bottels have the following dimensions: 90 x 90 x 215 mm (3.54 x
5.54 x 8.46 inch). The number of bottles varies from 2 to 5 depending on the analyzer version.
For some versions, the outlet pipe must be installed right of the analyzer. See the supplement to the Operating
Instructions.
The outlet pipe must be mounted to a wall so that the sample outlet hoses from the photometer have a gradient
of 5 to 10 %. If neccessary, extend the hoses.
RS 232
RS 232
381 (15.0)
351 (13.8)
325 (12.8)
8 (0.31)
9 (0.35)
540
(21.3)
562
(22.1)
19 (0.75) 197 (7.76)
192
(7.56)
175
(6.89)
mm (inch)
Ø6
(0.24)
Stamolys CA71NO
12 Endress+Hauser
Collecting vessel
Weight
Material
Connecting the sample line One channel version
Two channel version
• Depending on the ordered version, one or two collecting vessels (with or without level measurement) are
included in the scope of delivery.
• Level measurement is only possible for one channel.
• Only one collecting vessel can be mounted at the housing. The second is to be placed nearby the analyzer.
a0001363
Collecting vessel at analyzer (optional)
1 Ventilation
2 Sample inlet from sampling
3 Collecting vessel
4 Electrical connections
5 Analyzer sample inlet
a0001346
Collecting vessel dimensions
* variable, freely adjustable dimensions
6 Sampling for analyzer
7 Analyzer outlet
8 Sample overflow
1
2
3
4
5
6
7
8
*
*
*
130
(5.12)
17
(0.67)
10 (0.39)
145 (5.71)
79
(3.11)
120
(4.72)
140
(5.51)
115 (4.53)
Ø 34/25 (1.34/0.98)
3 x Ø 28/20 (1.1/0.79)
4 x Ø 6.6 (0.26)
27 (1.06) 60 (2.36)
4 x Ø 5.5/10.4 (0.22/0.41)
Ø 56 (2.2)
Ø 50H7 (1.97H0.28)
M20x1.5
Ø 24 (0.94)
70 (2.76)
100
(3.9)
80(3.15)
mm (inch)
48(1.89)
42(1.65)
70(2.76)
60(2.36)
GFR housing
Stainless steel housing
Without housing
approx. 28 kg (62 lbs)
approx. 33 kg (73 lbs)
approx. 25 kg (55 lbs)
Housing:
Front windows:
Endless hose:
Pump hose:
Valves:
Stainless steel 1.4301 (AISI 304) or
glass-fibre reinforced carbon(GFR)
Polycarbonate®
C-Flex®, Norprene®
Tygon®, Viton®
Tygon®
, silicone
Collecting vessel (at analyzer, with or without level measurement)
Connection hose ID 3.2 mm (0.13 inch)
Customer collecting vessel
Connection hose ID 1.6 mm (0.06 inch)
Max. distance from collecting vessel to analyzer 1 m (3.3 ft)
Max. height difference from collecting vessel to analyzer 0.5 m (1.6 ft)
Stamolys CA71NO
Endress+Hauser 13
Sample outlet NO-A/B/C
NO-D
Human Interface
Display and
operating elements
a0001679
Display and operating elements
1 LED (measured value)
2 LC display (measured value and status)
3 Serial interface RS 232
4 Operating keys and control LEDs
Certificates and approvals
4 approval Declaration of conformity
The product meets the legal requirements of the harmonized European standards.
The manufacturer confirms compliance with the standards by affixing the 4 symbol.
Test reports Quality certificate
Depending on the order code, you receive a quality certificate.
With the certificate the manufacturer confirms compliance with all technical regulations and the successful
individual testing of your product.
Connection Hose ID 6.4 mm (0.25 inch)
– Max. length of closed loop: 1 m (3.28 ft)
– Open outlet downgrade installed
– No combination of several devices to a closed-loop system
Min. volume per measurement 20 ml (0.68 fl.oz.)
Connection Hose ID 16 mm (0.63 inch)
– Max. length of closed loop: 1 m (3.3 ft)
– Open outlet downgrade installed
– No combination of several devices to a closed-loop system
Min. volume per measurement 20 ml (0.68 fl.oz.)
RS 232
M CE E K
1 2
4 3
Stamolys CA71NO
14 Endress+Hauser
Ordering information
Product structure
Scope of delivery NO-A/B/C
The scope of delivery comprises:
• an analyzer with mains plug
• a cleaning injector
• a tin of silicone spray
• a Norprene hose, length 2.5 m (8.2 ft), ID 1.6 mm (0.06 inch)
• a C-flex hose, length 2.5 m (8.2 ft), ID 6.4 mm (0.25 inch)
• a C-flex hose, length 2.5 m (8.2 ft), ID 3.2 mm (0.13 inch)
• two hose fittings of each size:
– 1.6 mm x 1.6 mm (0.06 inch x 0.06 inch)
– 1.6 mm x 3.2 mm (0.06 inch x 0.13 inch)
– 6.4 mm x 3.2 mm (0.25 inch x 0.13 inch)
• two T-hose fittings of each size:
– 1.6 mm x 1.6 mm x 1.6 mm (0.06 inch x 0.06 inch x 0.06 inch)
– 3.2 mm x 3.2 mm x 3.2 mm (0.13 inch x 0.13 inch x 0.13 inch)
• an interference suppressor for the current output
• 4 edge covers
• a quality certificate
• Operating Instructions (English).
Measuring range
A 10 ... 500 μg/l (ppb) NO2-N
B 0.1 ... 1 mg/l (ppm) NO2-N
C 0.2 ... 3 mg/l (ppm) NO2-N
D 0.01 ... 250 μg/l (ppb) NO2
Y Special version acc. to customer’s specification
Sample transfer
1 From one measuring point (one channel version)
2 From two measuring points (two channel version)
Power supply
0 230 V AC / 50 Hz
1 115 V AC / 60 Hz
2 115 V AC / 50 Hz
3 230 V AC / 60 Hz
Collecting vessel (for up to 3 analyzers)
A Not selected (without collecting vessel)
B Collecting vessel without level measurement
C Collecting vessel with level measurement (one-channel version only)
D Two collecting vessels without level measurement (two-channel version)
Housing
1 Open design
2 GFR housing
3 Stainless steel (1.4301 / AISI 304) + purge
8 Stainless steel (1.4301 / AISI 304) + without purge
Output
A 0/4 ... 20 mA, RS 232
B Profibus DP
Reagents
1 To order separately
2 One set, inactive
3 Three sets, inactive
CA71NO - complete order code
Stamolys CA71NO
Endress+Hauser 15
NO-D
The scope of delivery comprises:
• an analyzer with mains plug
• a cleaning injector
• a tin of silicone spray
• a Norprene hose, length 2.5 m (8.2 ft), ID 1.6 mm (0.06 inch)
• a Grifflex hose, length 2.0 m (6.6 ft), ID 19 mm (0.75 inch)
• a C-flex hose, length 2.5 m (8.2 ft), ID 3.2 mm (0.13 inch)
• two hose fittings of each size:
– 1.6 mm x 1.6 mm (0.06 inch x 0.06 inch)
– 1.6 mm x 3.2 mm (0.06 inch x 0.13 inch)
• two T-hose fittings of each size:
– 1.6 mm x 1.6 mm x 1.6 mm (0.06 inch x 0.06 inch x 0.06 inch)
– 3.2 mm x 3.2 mm x 3.2 mm (0.13 inch x 0.13 inch x 0.13 inch)
• an interference suppressor for the current output
• a screwed socket for the outlet pipe
• 4 edge covers
• a quality certificate
• Operating Instructions (English).
! Note!
Please, order reagents separately with analyzer version CA71XX-XXXXXX1.
With all other versions, inactive reagents are included in the scope of delivery. You have to mix the reagents
before using them. Please, read the instructions attached to the reagents.
Accessories
Reagents and
standard solutions
• Reagent NO1 active, 1 l (0.26 gal); order no. CAY343-V10AAE
• Reagent NO1 inactive, 1 l (0.26 gal); order no. CAY343-V10AAE
• Cleaning agent R; order no. CAY344-V10AAE
• Standard (stock solution) 250 mg/l (ppm) NO2 - N; order no. CAY345-V05C25AAE2)
Cleaner for hoses • Cleaning agent, alkaline, 100 ml (3.4 fl.oz.); order no. CAY746-V01AAE
• Cleaning agent, acidic, 100 ml (3.4 fl.oz.); order no. CAY747-V01AAE
Collecting vessel – for sampling from pressurised systems
– results in an unpressurised continuous sample stream
• Collecting vessel without level measurement; order no. 51512088
• Collecting vessel with level measurement (conductive); order no. 51512089
Maintenance kit • Maintenance kit CAV 740:
– 1 set pump hoses yellow/blue
– 1 set pump hoses black/black
– 1 set hose connectors per hose set
order no. CAV 740-1A
Additional accessories • Interference suppressor for control, power and signal lines
order no. 51512800
• Silicon spray
order no. 51504155
• Valve set, 2 pieces, for two-channel version
order no. 51512234
• Upgrade kit for upgrading from one-channel to two-channel version
order no. 51512640
2) The stock solution is highly concentrated due to its tenability. Mix your own standard solutions according to the package insert information.
Documentation
• Technical Information Stamoclean CAT430, TI 338C/07/en
• Technical Information Stamoclean CAT411, TI 349C/07/en
• Technical Information Stamoclean CAT221, TI 384C/07/en
TI355C/07/en/07.06
51512290
Printed in Germany / FM+SGML 6.0 / DT

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Stamolys ca71 no endress+hauser datasheet-nitrite analyzer

  • 1. TI355C/07/en/07.06 51512290 Technical Information Stamolys CA71NO Nitrite analyzer Compact photometric analysis system for the nitrite measurement in drinking water, wastewater and in mineral waters Application • Nitrite monitoring in drinking water • Nitrite monitoring in sewage treatment plants • Nitrite monitoring in the mineral water production Your benefits • Stainless steel or glass-fibre reinforced carbon housing available • Two channel version available • Measured value storage using integrated data logger • Automatic calibration and self-cleaning • Free selectable measuring, cleaning and calibration intervals
  • 2. Stamolys CA71NO 2 Endress+Hauser Function and system design Measuring principle CA71NO-A/B/C After sample conditioning, the analyzer sample pump conveys a part of the filtrate to a mixing vessel. The reagent pump adds reagent at a specific ratio. As a result of the reaction, the sample turns a characteristic colour. The photometer determines the sample’s absorption of an emitted light at a specific wavelength (s. Fig., Pos. 2). The wavelength is parameter specific. The absorbance is proportional to the concentration of the specified parameter in the sample (Pos. 3). Additionally, the absorption of a reference light is determined to receive a genuine measuring result. The reference signal is subtracted from the measuring signal to prevent any effects due to turbidity, contamination and ageing of the LEDs. The temperature in the photometer is controlled thermostatically so that the reaction is reproducible and takes place within a short period of time. Measuring principle CA71NO-D The LED sends light at a defined wavelength through the sample. The intensity of the received light is measured by the detector and converted to an electrical signal. In the analyzer, the respective concentration is calculated from the proportion of light absorbed by the sample. Nitrite Nitrite is a metastable intermediate stage of bacterial oxidation: proteins, urea É ammonium É nitrite É nitrate. Thus nitrite serves as an indicator in sewage treatment plant processes or in discharge streams of incomplete nitrification. Nitrite is often added to process and cooling water as a corrosion inhibitor. The Food Industry uses it as a preservative (e.g. pickling salt). Nitrite occurs very rarely in surface waters since it easily oxidizes to nitrate in the presence of air. High nitrite concentrations in water therefore indicate the presence of partially disintegrated, organic wastes. There should be no nitrite present in drinking water due to its toxicity (limit value according to the German Trinkwasserverordnung (drinking water ordinance): 0.1 mg/l (ppm)). Nitrite causes haemoglobin to convert to methaemoglobin which suppresses take up of oxygen in the blood ("inner asphyxiation"). a0001612 Photometric principle 1 2 3 4 5 Reference LED Emitter LED Sample Reference detector Measuring detector a0001613 Photometric measuring principle 1 2 3 LED Detector Sample 1 2 3
  • 3. Stamolys CA71NO Endress+Hauser 3 Photometric nitrite determination Naphthylamine method for nitrite determination acc. to DIN 38405-D10 Under acidic conditions, nitrite ions diazotices sulphonamido, which forms a red dye in conjunction with N-(1-naphthyl)-ethylenediamine. The absorption is determined at a wavelength of 565 nm. The absorption intensity is proportional to the nitrite concentration in the sample. The reference wavelength is 880 nm. Interferences No interferences up to the given concentration: Copper causes decreases in nitrite measured value. Sample conditioning Micro/ultrafiltration (Stamoclean CAT430, optional) A membrane filter element is suspended directly into the wastewater basin or channel. A hose pump is located in a pump box on the basin rim.The pump creates a vacuum between the membrane and the carrier plate of the filter element. This vacuum makes the filtrate pass through the filter membrane. Suspended materials, particles, algae and bacteria are collected on the surface of the membrane. Due to alternating pumping and pause, intervals of more than one month are achieved between cleaning cycles. Parallel connection of two or four filter elements increases the sampling quantity up to approx. 1 l/h (0.26 gal/hr). The hose pump pressure transports the sample to a collecting vessel near the analyzer over a distance of 20 m (66 ft). For distances up to 100 m (330 ft) the sample is transported to the collecting vessel by means of compressed air. The analyzers suck the needed sample volume from the collecting vessel. Membrane filtration (Stamoclean CAT411, optional) A sample flow of 0.8 to 1.8 m3 /h (3.5 to 7.9 gal/min) is continuously conducted through the micro filter via a pressure pipe. A part of the sample passes the filter membrane and is then conveyed to the measuring device as filtrate. Sampling is based on the cross flow filtration principle. The PTFE filter membrane separates particles with sizes > 0.45 μm from the filtrate. These particles are collected in front of the membrane and are washed away with the sample flow. The medium is conducted in a meander-like channel through the filter element. This results in a constantly high flow rate. The high flow rate generates the self cleaning effect. Therefore, mechanical drives for the generation of a flow at the filter surface are not necessary. Backwash filter (Stamoclean CAT221, optional) A sample flow of 1 to 2.5 m3 /h (4.4 to 11 gal/min) is permanently conveyed through the backwash filter by means of a sampling pump or compressed air or rinse water. The filtrate passes through the wedge wire sieve and is then transported to the measuring device. Clogging is minimized by the flow at the wedge wire sieve. Automatic backwashing results in a filter operating time of several weeks. The automatic backwashing and a small compressor or compressed air resp. rinse water supply guarantee low-maintenance and low-energy operation. Customer specific solution Before analysis, the sample has to be conditioned and to be transported to an external or to the delivered collecting vessel. Concentration [mg/l (ppm)] Interference 1,000 Cl –, SO4 2– 700 Cd 2+ 500 Na + , K + , Ca 2+ 50 Pb 2+ , Zn 2+ , Ni 2+ , Fe 2+ , Fe 3+ , Co 2+ , Hg 2+ , Ag + , NiO3 – , CO3 2– 25 Sn 2+ 10 Cr (VI)
  • 4. Stamolys CA71NO 4 Endress+Hauser Measuring system A complete measuring system comprises: • An analyzer • A sample conditioning system (optionally): – Micro filtration / ultra filtration Stamoclean CAT430 or Stamoclean CAT411 – Backwash filter Stamoclean CAT221 – Customer specific solution • Collecting vessel (see product structure) Micro / ultra filtration a0001616 Measuring system with Stamoclean CAT430 1 2 3 4 5 6 7 8 9 Control box Pump Control unit Collecting unit (optional) Collecting vessel Overflow Analyzer Aeration basin Membrane filter a0001615 Measuring system with Stamoclean CAT411 1 2 3 4 5 6 7 8 9 Stamoclean CAT411 Inlet Sample pump or hydraulic main Filtrate line Collecting vessel Overflow Analyzer Analyzer sample line Outlet Backwash filter a0001617 Measuring system with Stamoclean CAT221 1 2 3 4 5 6 7 Stamoclean CAT221 Compressor or compressed air Sample pump or hydraulic main Sample outlet Collecting vessel Overflow Analyzer 1 2 3 8 6 5 4 9 7 1 2 3 7 5 4 6
  • 5. Stamolys CA71NO Endress+Hauser 5 Input Measured variable • NO-A/B/C NO2-N [mg/l (ppm)] • NO-D NO2 [mg/l (ppm)] Measuring ranges • NO-A 10 ... 500 μg/l (ppb) • NO-B 0.10 ... 1.00 mg/l (ppm) • NO-C 0.20 ... 3.00 mg/l (ppm) • NO-D 0.01 ... 250.00 μg/l (ppb) Wavelength • NO-A/B/C 565 nm • NO-D 555 nm Reference wavelength 880 nm (NO-A/B/C only) Output Output signal 0/4 ... 20 mA Signal on alarm Contacts: 2 limit contacts (per channel), 1 system alarm contact optional: end of measurement (with two channel version display of channel no. available) Load max. 500 Ω Data interface RS 232 C Data logger 1024 data pairs per channel with date, time and measured value 100 data pairs with date, time and measured value for calibration factor determination (diagnostic tool) Load capacity 230 V / 115 V AC max. 2 A, 30 V DC max. 1 A
  • 6. Stamolys CA71NO 6 Endress+Hauser Power supply Electrical connection " Caution! The following figure (→ å 1) shows the connection department sticker as an example. Terminal assignment and cable core colors can be different to the originals. For connecting your analyzer only use the terminal assignment of the connection department sticker in the device (→ å 2)! a0001369 Fig. 1: Example of the connection sticker a0001372 Fig. 2: Analyzer from top (open version resp. swung out) 1 Connection department sticker 2 Printed circuit board with terminal strip 3 Backside of the analyzer Supply voltage 115 V AC / 230 V AC ±10%, 50/60 Hz Power consumption approx. 50 VA Current consumption approx. 0.2 A at 230 V approx. 0.5 A at 115 V Fuses 1 x time-lag 0.5 A for electronics 2 x medium time-lag 0.2 A for photometer 1 x time-lag 0.5 A for motors 80 75 70 63 57 39 27 21 15 64 58 40 28 22 16 65 79 74 69 62 56 38 26 20 14 78 73 68 61 55 37 25 19 13 77 72 67 60 54 36 24 18 12 76 71 66 59 53 35 23 17 11 RELAIS / Relay: max. Last / load: 2A bei / at 115/230V AC, 1A bei / at 30V DC RELAIS / Relay: max. Last / load: 2A bei / at 115/230V AC, 1A bei / at 30V DC OR BK RD YE V 3 V 3 V 2 V 2 V 1 V 1 0 V 0 V keine Probe No sample keine Probe No sample 0V 0V fx fx n.b. n.c. n.b. n.c. -17 V -17 V +17 V +17 V Schirm Screen Schirm Screen MP5 MP6 Schirm Shield Schirm Shield Reserve Mess 2 Meas 2 Mess 2 Meas 2 +24V I2 + I2 + I1 + I1 + I2 - I2 - I1 - I1 - Photometer SCHRITTMOTOR SCHRITTMOTOR LECKF. LECKF. ALARM 2 ALARM 2 OPTION STÖRUNG ALARM 1 ALARM 1 F5 F4 M 0.2 A M 0.2 A M 0.2 A M 0.2 A COM NC NO COM NC NO Kanal 1 Kanal 2 Channel 2 ALARM 2 ALARM 2 ALARM 1 ALARM 1 Photometer +17V Photometer +17V Photometer -17V Photometer -17V n.b. n.c. n.b. n.c. BN WH YE GY BK GN BK YE GN BU BN Analog Out 0/4-20mA STEP MOTOR LEAK S. LEAK S. 0 V 0 V WH Channel 1 ERROR 7 6 5 4 L2 N L1 PE AC MOTOR AC MOTOR F2 F1 AC Motor T 0.1A AC Motor T 0.1A Elektronik Electronics T 0.5A Elektronik Electronics T 0.5A 3 2 1 L N PE NETZ MAINS NETZ MAINS Klemmen führen auch bei ausgeschaltetem Gerät Spannung !!! Klemmen führen auch bei ausgeschaltetem Gerät Spannung !!! Terminals voltage to ground even when the unit is switched off !!! Terminals voltage to ground even when the unit is switched off !!! V 4 V 4 31 30 29 0V n.b. n.c. n.b. n.c. BU YE RD GN/YE Status Schirm Shield Schirm Shield Schirm Shield Schirm Shield Schirm Shield Schirm Shield Schirm Shield Schirm Shield 7 6 5 4 L2 N L1 PE AC MOTOR AC MOTOR F2 F1 AC Motor T 0.1A AC Motor T 0.1A Elektronik Electronics T 0.5A Elektronik Electronics T 0.5A 3 2 1 L N PE NETZ MAINS NETZ MAINS Klemmen führen auch bei ausgeschaltetem Gerät Spannung !!! Klemmen führen auch bei ausgeschaltetem Gerät Spannung !!! Terminals voltage to ground even when the unit is switched off !!! Terminals voltage to ground even when the unit is switched off !!! BU YE RD GN/YE GN/YE 80 75 70 63 57 39 27 21 15 64 58 40 28 22 16 65 79 74 69 62 56 38 26 20 14 78 73 68 61 55 37 25 19 13 77 72 67 60 54 36 24 18 12 76 71 66 59 53 35 23 17 11 RELAIS / Relay: max. Last / load: 2A bei / at 115/230V AC, 1A bei / at 30V DC RELAIS / Relay: max. Last / load: 2A bei / at 115/230V AC, 1A bei / at 30V DC OR BK RD YE V 3 V 3 V 2 V 2 V 1 V 1 0 V 0 V keine Probe No sample keine Probe No sample 0V 0V fx fx n.b. n.c. n.b. n.c. -17 V -17 V +17 V +17 V Schirm Screen Schirm Screen MP5 MP6 Schirm Shield Schirm Shield Reserve Mess 2 Meas 2 Mess 2 Meas 2 +24V I2 + I2 + I1 + I1 + I2 - I2 - I1 - I1 - Photometer SCHRITTMOTOR SCHRITTMOTOR LECKF. LECKF. ALARM 2 ALARM 2 OPTION OPTION STÖRUNG STÖRUNG ALARM 1 ALARM 1 F5 F4 M 0.2 A M 0.2 A M 0.2 A M 0.2 A COM NC NO COM NC NO Kanal 1 Kanal 2 Channel 2 ALARM 2 ALARM 2 ALARM 1 ALARM 1 Photometer +17V Photometer +17V Photometer -17V Photometer -17V n.b. n.c. n.b. n.c. BN WH YE GY BK GN BK YE GN BU BN Analog Out 0/4-20mA STEP MOTOR STEP MOTOR LEAK S. LEAK S. 0 V 0 V WH Channel 1 ERROR ERROR V 4 V 4 31 30 29 0V n.b. n.c. n.b. n.c. Status Schirm Shield Schirm Shield Schirm Shield Schirm Shield Schirm Shield Schirm Shield Schirm Shield Schirm Shield 1 2 3
  • 7. Stamolys CA71NO Endress+Hauser 7 Performance characteristics Time between two measurements tmes = reaction time + rinse time + waiting time + rinse again time + filling time + sampling time + reagent refusal time (min. waiting time = 0 min) Maximum measured error ±2 % of measuring range end Repeatability • NO-A: up to 100 μg/l: ± 5 μg/l (ppb) > 100 μg/l: ± 0.1 μg/l (ppb) • NO-B: up to 0.25 mg/l: ± 0.01 mg/l (ppm) > 0.25 mg/l: ± 0.02 mg/l (ppm) • NO-C: up to 0.50 mg/l: ± 0.03 mg/l (ppm) > 0.50 mg/l: ± 0.06 mg/l (ppm) • NO-D: ± 2 μg/l (ppb) Measuring interval tmes to 120 min Reaction time NO-A/B/C 2 minutes NO-D 210 sec Sample requirement NO-A/B/C 15 ml (0.51 fl.oz.) per measurement NO-D 20 ml (0.68 fl.oz.) per measurement Reagent requirement NO-A/B/C 1 x 0.21 ml (0.007 fl.oz.) 0.91 l (0.24 gal) per reagent per month with 10 minute measuring interval NO-D 1 x 0.115 ml (0.004 fl.oz.) 0.5 l (0.13 gal) per reagent per month with 10 minute measuring interval Calibration interval1) 0 to 720 h Rinse interval 0 to 720 h Rinse time selectable from 20 to 300 s (standard = 60 s) Rinse again time 30 s Filling time NO-A/B/C 22 s NO-D 30 sec 1) standard solutions have a limited tenability because of biological activity
  • 8. Stamolys CA71NO 8 Endress+Hauser Maintenance interval 6 months (typical) Servicing requirement 15 minutes per week (typical) Environment Ambient temperature 5 ... 40 °C (40... 100 °F), avoid strong fluctuations Humidity below the condensation limit, installation in usual, clean rooms outdoor installation only possible with protective devices (customer supplied) Ingress protection IP 43 Process Sample temperature 5 to 40 °C (40 to 100 °F) Sample flow rate min. 5 ml (0.0013 US.gal.) per min Consistence of the sample low solid content (< 50 ppm) Sample inlet pressureless
  • 9. Stamolys CA71NO Endress+Hauser 9 Mechanical construction Design, dimensions Stainless steel housing, NO-A/B/C/D a0001361 Stainless steel version A Detail A 360 (14.2) 436 (17.2) 243 (9.57) 200 (7.87) 120(4.72) 326 (12.8) 15(0.59) 330 (13.0) 163(6.42) 110(4.33) Ø 27(1.06) 60(2.36) 100(3.94) 140 (5.51) 160 (6.30) 250 (9.84) 524 (20.6) 555 (21.8) 125(4.92) 165 (6.50) Ø 21(0.83) Ø 26 (1.02) Ø 26(1.02) 119(4.69) 78(3.07) 47(1.85) 207 (8.15) 580 (22.8) 648 (25.5) 15(0.59) 3(0.12) 15(0.59) 30(1.18) 9(0.35) Ø 21(0.83) mm(inch) 38(1.5)
  • 10. Stamolys CA71NO 10 Endress+Hauser GFR housing, NO-A/B/C a0001354-en GFR version GFR housing, NO-D a0001355 GFR version 60 (2.36) 100(3.94) 140 (5.51) 160 (6.30) 250 (9.84) 125 (4.92) 165 (6.50) Ø 21(0.83) Ø 26(1.02) Ø 21 (0.83) 119/4.69 78(3.07) 47(1.85) 648 (25.5) 360 (14.2) 436 (17.2) 243 (9.57) 200 (7.87) 120 (4.72) 326 (12.8) Ø 16 (0.63) Ø 27 (1.06) 120(4.72) 555 (21.8) 465 (18.3) 500 (19.7) 7-11/ 0.28 - 0.43 (M 6) Ø 26 (1.02) mm(inch) 330 (13.0) 163 (6.42) Ø 26(1.02) Ø 16(0.63) 120 (4.72) 60 (2.36) 100(3.94) 140 (5.51) 160 (6.30) 250 (9.84) 125(4.92) 165 (6.50) Ø 21(0.83) Ø 26/1.02 Ø 21 (0.83) 119(4.69) 78(3.07) 47(1.85) 648 (25.5) 360 (14.2) 436 (17.2) 243 (9.57) 200 (7.87) 120 (4.72) 326 (12.8) 330 (13.0) 110 (4.33) Ø 27 (1.06) Ø 16 (0.63) Ø 27 (1.06) 120(4.72) 555 (21.8) 465 (18.3) 500 (19.7) 7-11/ 0.28 - 0.43 (M 6) Ø 26(1.02) mm (inch) 38 (1.5)
  • 11. Stamolys CA71NO Endress+Hauser 11 Open version, NO-A/B/C/D a0001356 Open version (without housing) ! Note! With the open version, you need an additional platform for the reagents. Mount this platform max. 35 cm (13.8 inch) below the pumps. The reagent bottels have the following dimensions: 90 x 90 x 215 mm (3.54 x 5.54 x 8.46 inch). The number of bottles varies from 2 to 5 depending on the analyzer version. For some versions, the outlet pipe must be installed right of the analyzer. See the supplement to the Operating Instructions. The outlet pipe must be mounted to a wall so that the sample outlet hoses from the photometer have a gradient of 5 to 10 %. If neccessary, extend the hoses. RS 232 RS 232 381 (15.0) 351 (13.8) 325 (12.8) 8 (0.31) 9 (0.35) 540 (21.3) 562 (22.1) 19 (0.75) 197 (7.76) 192 (7.56) 175 (6.89) mm (inch) Ø6 (0.24)
  • 12. Stamolys CA71NO 12 Endress+Hauser Collecting vessel Weight Material Connecting the sample line One channel version Two channel version • Depending on the ordered version, one or two collecting vessels (with or without level measurement) are included in the scope of delivery. • Level measurement is only possible for one channel. • Only one collecting vessel can be mounted at the housing. The second is to be placed nearby the analyzer. a0001363 Collecting vessel at analyzer (optional) 1 Ventilation 2 Sample inlet from sampling 3 Collecting vessel 4 Electrical connections 5 Analyzer sample inlet a0001346 Collecting vessel dimensions * variable, freely adjustable dimensions 6 Sampling for analyzer 7 Analyzer outlet 8 Sample overflow 1 2 3 4 5 6 7 8 * * * 130 (5.12) 17 (0.67) 10 (0.39) 145 (5.71) 79 (3.11) 120 (4.72) 140 (5.51) 115 (4.53) Ø 34/25 (1.34/0.98) 3 x Ø 28/20 (1.1/0.79) 4 x Ø 6.6 (0.26) 27 (1.06) 60 (2.36) 4 x Ø 5.5/10.4 (0.22/0.41) Ø 56 (2.2) Ø 50H7 (1.97H0.28) M20x1.5 Ø 24 (0.94) 70 (2.76) 100 (3.9) 80(3.15) mm (inch) 48(1.89) 42(1.65) 70(2.76) 60(2.36) GFR housing Stainless steel housing Without housing approx. 28 kg (62 lbs) approx. 33 kg (73 lbs) approx. 25 kg (55 lbs) Housing: Front windows: Endless hose: Pump hose: Valves: Stainless steel 1.4301 (AISI 304) or glass-fibre reinforced carbon(GFR) Polycarbonate® C-Flex®, Norprene® Tygon®, Viton® Tygon® , silicone Collecting vessel (at analyzer, with or without level measurement) Connection hose ID 3.2 mm (0.13 inch) Customer collecting vessel Connection hose ID 1.6 mm (0.06 inch) Max. distance from collecting vessel to analyzer 1 m (3.3 ft) Max. height difference from collecting vessel to analyzer 0.5 m (1.6 ft)
  • 13. Stamolys CA71NO Endress+Hauser 13 Sample outlet NO-A/B/C NO-D Human Interface Display and operating elements a0001679 Display and operating elements 1 LED (measured value) 2 LC display (measured value and status) 3 Serial interface RS 232 4 Operating keys and control LEDs Certificates and approvals 4 approval Declaration of conformity The product meets the legal requirements of the harmonized European standards. The manufacturer confirms compliance with the standards by affixing the 4 symbol. Test reports Quality certificate Depending on the order code, you receive a quality certificate. With the certificate the manufacturer confirms compliance with all technical regulations and the successful individual testing of your product. Connection Hose ID 6.4 mm (0.25 inch) – Max. length of closed loop: 1 m (3.28 ft) – Open outlet downgrade installed – No combination of several devices to a closed-loop system Min. volume per measurement 20 ml (0.68 fl.oz.) Connection Hose ID 16 mm (0.63 inch) – Max. length of closed loop: 1 m (3.3 ft) – Open outlet downgrade installed – No combination of several devices to a closed-loop system Min. volume per measurement 20 ml (0.68 fl.oz.) RS 232 M CE E K 1 2 4 3
  • 14. Stamolys CA71NO 14 Endress+Hauser Ordering information Product structure Scope of delivery NO-A/B/C The scope of delivery comprises: • an analyzer with mains plug • a cleaning injector • a tin of silicone spray • a Norprene hose, length 2.5 m (8.2 ft), ID 1.6 mm (0.06 inch) • a C-flex hose, length 2.5 m (8.2 ft), ID 6.4 mm (0.25 inch) • a C-flex hose, length 2.5 m (8.2 ft), ID 3.2 mm (0.13 inch) • two hose fittings of each size: – 1.6 mm x 1.6 mm (0.06 inch x 0.06 inch) – 1.6 mm x 3.2 mm (0.06 inch x 0.13 inch) – 6.4 mm x 3.2 mm (0.25 inch x 0.13 inch) • two T-hose fittings of each size: – 1.6 mm x 1.6 mm x 1.6 mm (0.06 inch x 0.06 inch x 0.06 inch) – 3.2 mm x 3.2 mm x 3.2 mm (0.13 inch x 0.13 inch x 0.13 inch) • an interference suppressor for the current output • 4 edge covers • a quality certificate • Operating Instructions (English). Measuring range A 10 ... 500 μg/l (ppb) NO2-N B 0.1 ... 1 mg/l (ppm) NO2-N C 0.2 ... 3 mg/l (ppm) NO2-N D 0.01 ... 250 μg/l (ppb) NO2 Y Special version acc. to customer’s specification Sample transfer 1 From one measuring point (one channel version) 2 From two measuring points (two channel version) Power supply 0 230 V AC / 50 Hz 1 115 V AC / 60 Hz 2 115 V AC / 50 Hz 3 230 V AC / 60 Hz Collecting vessel (for up to 3 analyzers) A Not selected (without collecting vessel) B Collecting vessel without level measurement C Collecting vessel with level measurement (one-channel version only) D Two collecting vessels without level measurement (two-channel version) Housing 1 Open design 2 GFR housing 3 Stainless steel (1.4301 / AISI 304) + purge 8 Stainless steel (1.4301 / AISI 304) + without purge Output A 0/4 ... 20 mA, RS 232 B Profibus DP Reagents 1 To order separately 2 One set, inactive 3 Three sets, inactive CA71NO - complete order code
  • 15. Stamolys CA71NO Endress+Hauser 15 NO-D The scope of delivery comprises: • an analyzer with mains plug • a cleaning injector • a tin of silicone spray • a Norprene hose, length 2.5 m (8.2 ft), ID 1.6 mm (0.06 inch) • a Grifflex hose, length 2.0 m (6.6 ft), ID 19 mm (0.75 inch) • a C-flex hose, length 2.5 m (8.2 ft), ID 3.2 mm (0.13 inch) • two hose fittings of each size: – 1.6 mm x 1.6 mm (0.06 inch x 0.06 inch) – 1.6 mm x 3.2 mm (0.06 inch x 0.13 inch) • two T-hose fittings of each size: – 1.6 mm x 1.6 mm x 1.6 mm (0.06 inch x 0.06 inch x 0.06 inch) – 3.2 mm x 3.2 mm x 3.2 mm (0.13 inch x 0.13 inch x 0.13 inch) • an interference suppressor for the current output • a screwed socket for the outlet pipe • 4 edge covers • a quality certificate • Operating Instructions (English). ! Note! Please, order reagents separately with analyzer version CA71XX-XXXXXX1. With all other versions, inactive reagents are included in the scope of delivery. You have to mix the reagents before using them. Please, read the instructions attached to the reagents. Accessories Reagents and standard solutions • Reagent NO1 active, 1 l (0.26 gal); order no. CAY343-V10AAE • Reagent NO1 inactive, 1 l (0.26 gal); order no. CAY343-V10AAE • Cleaning agent R; order no. CAY344-V10AAE • Standard (stock solution) 250 mg/l (ppm) NO2 - N; order no. CAY345-V05C25AAE2) Cleaner for hoses • Cleaning agent, alkaline, 100 ml (3.4 fl.oz.); order no. CAY746-V01AAE • Cleaning agent, acidic, 100 ml (3.4 fl.oz.); order no. CAY747-V01AAE Collecting vessel – for sampling from pressurised systems – results in an unpressurised continuous sample stream • Collecting vessel without level measurement; order no. 51512088 • Collecting vessel with level measurement (conductive); order no. 51512089 Maintenance kit • Maintenance kit CAV 740: – 1 set pump hoses yellow/blue – 1 set pump hoses black/black – 1 set hose connectors per hose set order no. CAV 740-1A Additional accessories • Interference suppressor for control, power and signal lines order no. 51512800 • Silicon spray order no. 51504155 • Valve set, 2 pieces, for two-channel version order no. 51512234 • Upgrade kit for upgrading from one-channel to two-channel version order no. 51512640 2) The stock solution is highly concentrated due to its tenability. Mix your own standard solutions according to the package insert information.
  • 16. Documentation • Technical Information Stamoclean CAT430, TI 338C/07/en • Technical Information Stamoclean CAT411, TI 349C/07/en • Technical Information Stamoclean CAT221, TI 384C/07/en TI355C/07/en/07.06 51512290 Printed in Germany / FM+SGML 6.0 / DT