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ON THE REPRESENTATIVENESS OF MEASUREMENTS
Markku Ohenoja
Control Engineering group
University of Oulu
1
10/28/2015Faculty of Technology / Control Engineering / Markku Ohenoja
BACKGROUND
• All measurements retain some amount of uncertainty, but also
sampling errors may affect on the result
• It is difficult to compare the information content of different
measurements, collected with very different sampling rates
• Online measurements
• Laboratory samples
• MOFI features
• MMEA/WP2
• Literature review à variogram
• Methods demonstrated with WWTP data
28.10.2015
2
Faculty of Technology / Control Engineering / Markku Ohenoja
markku.ohenoja@oulu.fi
VARIOGRAM
• Tool for empirical estimation of sampling errors incl. analytical
error
• Enables optimizing the sampling strategy with respect to
variance of the sampling error and number of samples taken
• Provides an estimate of the standard error of the lot mean and
the minimum possible error (MPE) of sampling
28.10.2015
3
Faculty of Technology / Control Engineering / Markku Ohenoja
markku.ohenoja@oulu.fi
Semi-variogram
Chrono-variogram
Variographical
analysis
Geostatistics
Kriging
Variography Chronostatistics
EXAMPLES WITH WWTP DATA
• Error evaluation for MOFI
• Illustration of the benefits of dense data
• Monitoring of relation between sampling error and process
variation
• Model variable selection based on the latter one
28.10.2015Faculty of Technology / Control Engineering / Markku Ohenoja
markku.ohenoja@oulu.fi
4
ERROR EVALUATION FOR MOFI
Strong periodicity in the
data -> potentially biased
samples with systematic
sampling
28.10.2015Faculty of Technology / Control Engineering / Markku Ohenoja
markku.ohenoja@oulu.fi
5
Equivalent diameter with 52 data
points and sampling interval of 1h
0 5 10 15 20 25 30
0.4
0.6
0.8
1
1.2
1.4
1.6
1.8
2
Lag / Time between samples, h
Relativestandarddeviation,%
ERROR EVALUATION FOR MOFI
28.10.2015Faculty of Technology / Control Engineering / Markku Ohenoja
markku.ohenoja@oulu.fi
6
Equivalent diameter with 52 data
points and sampling interval of 1h
0 5 10 15 20 25 30
0.4
0.6
0.8
1
1.2
1.4
1.6
1.8
2
Lag / Time between samples, h
Relativestandarddeviation,%
Strong periodicity in the
data -> potentially biased
samples with systematic
sampling
Linear trend in data -> non-
stationary process
0 5 10 15 20 25 30
0.4
0.6
0.8
1
1.2
1.4
1.6
1.8
2
Lag / Time between samples, h
Relativestandarddeviation,%
Variogram
Random
ERROR EVALUATION FOR MOFI
28.10.2015Faculty of Technology / Control Engineering / Markku Ohenoja
markku.ohenoja@oulu.fi
7
Equivalent diameter with 52 data
points and sampling interval of 1h
Strong periodicity in the
data -> potentially biased
samples with systematic
sampling
Linear trend in data -> non-
stationary process
0 5 10 15 20 25 30
0.4
0.6
0.8
1
1.2
1.4
1.6
1.8
2
Lag / Time between samples, h
Relativestandarddeviation,%
Variogram
Random
Systematic
ERROR EVALUATION FOR MOFI
28.10.2015Faculty of Technology / Control Engineering / Markku Ohenoja
markku.ohenoja@oulu.fi
8
Equivalent diameter with 52 data
points and sampling interval of 1h
Strong periodicity in the
data -> potentially biased
samples with systematic
sampling
Linear trend in data -> non-
stationary process
0 5 10 15 20 25 30
0.4
0.6
0.8
1
1.2
1.4
1.6
1.8
2
Lag / Time between samples, h
Relativestandarddeviation,%
Variogram
Random
Systematic
ERROR EVALUATION FOR MOFI
2 = 2 = 1.45
2 ̅ = 2 = 0.78
Random sampling:
2 ̅ = 2
.
= 1.45%
Systematic sampling (lag=6):
2 ̅ = 2
.
= 0.78%
28.10.2015Faculty of Technology / Control Engineering / Markku Ohenoja
markku.ohenoja@oulu.fi
9
Equivalent diameter with 52 data
points and sampling interval of 1h
Strong periodicity in the
data -> potentially biased
samples with systematic
sampling
Linear trend in data -> non-
stationary process
DENSE VS. SPARSE DATA
28.10.2015
10
Faculty of Technology / Control Engineering / Markku Ohenoja
markku.ohenoja@oulu.fi
0 10 20 30
0
5
10
15
20
25
30
Variogram of 24h averaged online data
Sampling interval (days)
Relativestandarddeviationofthesamplingerror(%)
0 10 20 30
0
5
10
15
20
25
30
Variogram of daily sample
Sampling interval (days)
Relativestandarddeviationofthesamplingerror(%)
Variogram
Systematic sampling
Random sampling
Variogram
Systematic sampling
Random sampling
3x
28.10.2015Faculty of Technology / Control Engineering / Markku Ohenoja
markku.ohenoja@oulu.fi
11
26-May-2013 05-Jul-2013 14-Aug-2013 23-Sep-2013 02-Nov-2013 12-Dec-2013
0
10
20
30
40
Meas.
Time series
Dense meas.
Sparse meas.
26-May-2013 05-Jul-2013 14-Aug-2013 23-Sep-2013 02-Nov-2013 12-Dec-2013
0
0.5
1
1.5
e
s
/s
P
Index
Dense meas.
Sparse meas.
26-May-2013 05-Jul-2013 14-Aug-2013 23-Sep-2013 02-Nov-2013 12-Dec-2013
-1
-0.5
0
0.5
1
Substracted index
Index
MONITORING
MODELING
28.10.2015Faculty of Technology / Control Engineering / Markku Ohenoja
markku.ohenoja@oulu.fi
12
• Variable selection for WWTP model
• 71 variables with 48 samples -> model with 5 variables
• Model uses scaled values, scaling after variable selection
• Variable selection based on MPE/σ -ratio
MODELING
28.10.2015Faculty of Technology / Control Engineering / Markku Ohenoja
Markku.ohenoja@oulu.fi
13
• Variable selection for WWTP model
• 71 variables with 48 samples -> model with 5 variables
• Model uses scaled values, scaling after variable selection
• Variable selection based on MPE/σ -ratio
• First 5 variables
à model r2 = 0.65
• First 5 MOFI-features
à model r2 = 0.76
• Expert knowledge to reject some
variables à r2 = 0.76
• Tomperi et al. 2015,
à model r2 = 0.80
Variable name MPE/σP Matrix index
'Fe B0'
'Mean aspectr for objs > th'
'Mean roundness of objs > th'
'Cl T1'
'Fe L0'
'Cl L0'
'7. linjan lämpötila'
'Mean equiv.d for objs > th'
'Mean. area of objs > th'
'Median. area of objs > th'
'Number of all objects'
'Total fil length'
'Number of objs > th'
'Fil length/floc area'
'Number of small objs'
'Fe Mk'
'SO4 T1'
'PO4-P L0'
'Sähkönjohtavuus L0'
'Nitraattityppi Mk'
0.1871
0.2496
0.2505
0.2755
0.2764
0.2887
0.3140
0.3277
0.3483
0.3593
0.3756
0.3798
0.3886
0.4295
0.4732
0.4816
0.5208
0.5460
0.5562
0.5674
64
6
5
60
65
61
68
7
10
11
12
1
13
2
14
63
58
35
57
45
Tomperi J., Koivuranta E., Kuokkanen A., Juuso E., Leiviskä K. (2015)
Real-time optical monitoring of the wastewater treatment process,
Environmental Technology, DOI: 10.1080/09593330.2015.1069898
SUMMARY
28.10.2015Faculty of Technology / Control Engineering / Markku Ohenoja
markku.ohenoja@oulu.fi
14
Variogram
Sampling optimization
Empirically and recursively
evaluated
Monitoring Decision making
Information content
Comparison of measurements
Modeling Filtering
Moving average and confidence
intervals
Representativeness of measurements

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On the representativeness of measurements

  • 1. ON THE REPRESENTATIVENESS OF MEASUREMENTS Markku Ohenoja Control Engineering group University of Oulu 1 10/28/2015Faculty of Technology / Control Engineering / Markku Ohenoja
  • 2. BACKGROUND • All measurements retain some amount of uncertainty, but also sampling errors may affect on the result • It is difficult to compare the information content of different measurements, collected with very different sampling rates • Online measurements • Laboratory samples • MOFI features • MMEA/WP2 • Literature review à variogram • Methods demonstrated with WWTP data 28.10.2015 2 Faculty of Technology / Control Engineering / Markku Ohenoja markku.ohenoja@oulu.fi
  • 3. VARIOGRAM • Tool for empirical estimation of sampling errors incl. analytical error • Enables optimizing the sampling strategy with respect to variance of the sampling error and number of samples taken • Provides an estimate of the standard error of the lot mean and the minimum possible error (MPE) of sampling 28.10.2015 3 Faculty of Technology / Control Engineering / Markku Ohenoja markku.ohenoja@oulu.fi Semi-variogram Chrono-variogram Variographical analysis Geostatistics Kriging Variography Chronostatistics
  • 4. EXAMPLES WITH WWTP DATA • Error evaluation for MOFI • Illustration of the benefits of dense data • Monitoring of relation between sampling error and process variation • Model variable selection based on the latter one 28.10.2015Faculty of Technology / Control Engineering / Markku Ohenoja markku.ohenoja@oulu.fi 4
  • 5. ERROR EVALUATION FOR MOFI Strong periodicity in the data -> potentially biased samples with systematic sampling 28.10.2015Faculty of Technology / Control Engineering / Markku Ohenoja markku.ohenoja@oulu.fi 5 Equivalent diameter with 52 data points and sampling interval of 1h 0 5 10 15 20 25 30 0.4 0.6 0.8 1 1.2 1.4 1.6 1.8 2 Lag / Time between samples, h Relativestandarddeviation,%
  • 6. ERROR EVALUATION FOR MOFI 28.10.2015Faculty of Technology / Control Engineering / Markku Ohenoja markku.ohenoja@oulu.fi 6 Equivalent diameter with 52 data points and sampling interval of 1h 0 5 10 15 20 25 30 0.4 0.6 0.8 1 1.2 1.4 1.6 1.8 2 Lag / Time between samples, h Relativestandarddeviation,% Strong periodicity in the data -> potentially biased samples with systematic sampling Linear trend in data -> non- stationary process
  • 7. 0 5 10 15 20 25 30 0.4 0.6 0.8 1 1.2 1.4 1.6 1.8 2 Lag / Time between samples, h Relativestandarddeviation,% Variogram Random ERROR EVALUATION FOR MOFI 28.10.2015Faculty of Technology / Control Engineering / Markku Ohenoja markku.ohenoja@oulu.fi 7 Equivalent diameter with 52 data points and sampling interval of 1h Strong periodicity in the data -> potentially biased samples with systematic sampling Linear trend in data -> non- stationary process
  • 8. 0 5 10 15 20 25 30 0.4 0.6 0.8 1 1.2 1.4 1.6 1.8 2 Lag / Time between samples, h Relativestandarddeviation,% Variogram Random Systematic ERROR EVALUATION FOR MOFI 28.10.2015Faculty of Technology / Control Engineering / Markku Ohenoja markku.ohenoja@oulu.fi 8 Equivalent diameter with 52 data points and sampling interval of 1h Strong periodicity in the data -> potentially biased samples with systematic sampling Linear trend in data -> non- stationary process
  • 9. 0 5 10 15 20 25 30 0.4 0.6 0.8 1 1.2 1.4 1.6 1.8 2 Lag / Time between samples, h Relativestandarddeviation,% Variogram Random Systematic ERROR EVALUATION FOR MOFI 2 = 2 = 1.45 2 ̅ = 2 = 0.78 Random sampling: 2 ̅ = 2 . = 1.45% Systematic sampling (lag=6): 2 ̅ = 2 . = 0.78% 28.10.2015Faculty of Technology / Control Engineering / Markku Ohenoja markku.ohenoja@oulu.fi 9 Equivalent diameter with 52 data points and sampling interval of 1h Strong periodicity in the data -> potentially biased samples with systematic sampling Linear trend in data -> non- stationary process
  • 10. DENSE VS. SPARSE DATA 28.10.2015 10 Faculty of Technology / Control Engineering / Markku Ohenoja markku.ohenoja@oulu.fi 0 10 20 30 0 5 10 15 20 25 30 Variogram of 24h averaged online data Sampling interval (days) Relativestandarddeviationofthesamplingerror(%) 0 10 20 30 0 5 10 15 20 25 30 Variogram of daily sample Sampling interval (days) Relativestandarddeviationofthesamplingerror(%) Variogram Systematic sampling Random sampling Variogram Systematic sampling Random sampling 3x
  • 11. 28.10.2015Faculty of Technology / Control Engineering / Markku Ohenoja markku.ohenoja@oulu.fi 11 26-May-2013 05-Jul-2013 14-Aug-2013 23-Sep-2013 02-Nov-2013 12-Dec-2013 0 10 20 30 40 Meas. Time series Dense meas. Sparse meas. 26-May-2013 05-Jul-2013 14-Aug-2013 23-Sep-2013 02-Nov-2013 12-Dec-2013 0 0.5 1 1.5 e s /s P Index Dense meas. Sparse meas. 26-May-2013 05-Jul-2013 14-Aug-2013 23-Sep-2013 02-Nov-2013 12-Dec-2013 -1 -0.5 0 0.5 1 Substracted index Index MONITORING
  • 12. MODELING 28.10.2015Faculty of Technology / Control Engineering / Markku Ohenoja markku.ohenoja@oulu.fi 12 • Variable selection for WWTP model • 71 variables with 48 samples -> model with 5 variables • Model uses scaled values, scaling after variable selection • Variable selection based on MPE/σ -ratio
  • 13. MODELING 28.10.2015Faculty of Technology / Control Engineering / Markku Ohenoja Markku.ohenoja@oulu.fi 13 • Variable selection for WWTP model • 71 variables with 48 samples -> model with 5 variables • Model uses scaled values, scaling after variable selection • Variable selection based on MPE/σ -ratio • First 5 variables à model r2 = 0.65 • First 5 MOFI-features à model r2 = 0.76 • Expert knowledge to reject some variables à r2 = 0.76 • Tomperi et al. 2015, à model r2 = 0.80 Variable name MPE/σP Matrix index 'Fe B0' 'Mean aspectr for objs > th' 'Mean roundness of objs > th' 'Cl T1' 'Fe L0' 'Cl L0' '7. linjan lämpötila' 'Mean equiv.d for objs > th' 'Mean. area of objs > th' 'Median. area of objs > th' 'Number of all objects' 'Total fil length' 'Number of objs > th' 'Fil length/floc area' 'Number of small objs' 'Fe Mk' 'SO4 T1' 'PO4-P L0' 'Sähkönjohtavuus L0' 'Nitraattityppi Mk' 0.1871 0.2496 0.2505 0.2755 0.2764 0.2887 0.3140 0.3277 0.3483 0.3593 0.3756 0.3798 0.3886 0.4295 0.4732 0.4816 0.5208 0.5460 0.5562 0.5674 64 6 5 60 65 61 68 7 10 11 12 1 13 2 14 63 58 35 57 45 Tomperi J., Koivuranta E., Kuokkanen A., Juuso E., Leiviskä K. (2015) Real-time optical monitoring of the wastewater treatment process, Environmental Technology, DOI: 10.1080/09593330.2015.1069898
  • 14. SUMMARY 28.10.2015Faculty of Technology / Control Engineering / Markku Ohenoja markku.ohenoja@oulu.fi 14 Variogram Sampling optimization Empirically and recursively evaluated Monitoring Decision making Information content Comparison of measurements Modeling Filtering Moving average and confidence intervals Representativeness of measurements