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MIXING &
             STIRRING



Specialized in process installations
   for dry materials and liquids
Fields of application
 Liquid-liquid
 Solid-solid
 Solid-liquid (solid)
 Solid-liquid (liquid)
Liquid-liquid
                           Storage

                      LIQUID

                                  FI


                                       FI
                         Dosing



   LIQUID
   SOLID ADDITIVES        mixing

   LIQUID ADDITIVES
   WATER
   MIXTURE
Liquid-liquid
 Soap emulsions
 Food
 Polymerization
 Chemistry
Fields of application
 Liquid-liquid
 Solid-solid
 Solid-liquid (solid)
 Solid-liquid (liquid)
Solid-solid

                Storage
           Macrocomponenten
                              Storage Minor-   Storage Micro-
                              componenten      componenten

       M      M     M     M




     MACRO COMPONENTS
     MINOR COMPONENTS
     MICRO COMPONENTS
     PRODUCT
Solid-solid




 Construction materials
 Construction chemistry
 Food
 Feed / pet food
Fields of application
 Liquid-liquid
 Solid-solid
 Solid-liquid (solid)
 Solid-liquid (liquid)
Solid-liquid (solid)

                                     Storage


                           FILLING
                           AGENT


                                               FI

                           M


                                                    FI

                       Dosing

                                     Mixing

    FILLING AGENTS
    SOLID ADDITIVES
    LIQUID ADDITIVES
    LIQUID
    WATER
Solid-liquid (solid)




  Construction materials
  Food
  Waste processing / sludge processing
Fields of application
 Liquid-liquid
 Solid-solid
 Solid-liquid (solid)
 Solid-liquid (liquid)
Milk of lime

                        Storage


               LIME


                            Scrubber
           M

                                              FI



               Dosing
                                       `




               Preparing


        LIME                               Storage, dilution
        WATER                              & circulation
        MILK OF LIME
Milk of lime
 Water decarbonation
 Washing incineration gases
 Chemistry
Glue preparation
                          Storage



                  RAW
                  MATE-
                   RIAL                FI
                                                          Cooling &
                                              FI          viscosity
              M




                                       TI

                   Dosing




                   Preparing
                                                   Storage &
                                                   circulation
  RAW MATERIALS                     Cooking
  ADDITIVES
  STEAM
  WATER
  SUSPENSION
Glue preparation
 Paper & cardboard
 Pressed and glued wood
Paint
                            Storage

                  FILLING
                  AGENT

                                               Dosing
                  M



                                                                  MEDIUM

                                                        FI


                                                             FI




                            Transport
        FILLING AGENTS
        SOLID ADDITIVES
                                      Dissolving
        LIQUID ADDITIVES
        MEDIUM
        WATER
        PAINT
Paint
 Water based
 Solvent based
Compounds
                                     Storage


                        FILLING
                        AGENT
                                                         POLY
                                                         MER
                                               FI

                        M


                                                    FI



                   Dosing


                            Mixing
     FILLING AGENTS
     SOLID ADDITIVES
     LIQUID ADDITIVES
     POLYMER
     WATER
     COMPOUND
Compounds
 Carpets
 Finishing materials
 (leather, paper, metal)
Solid – liquid: suspensions
 Not a solution – contains solid particles
 Specific behavior
  •   Abrasive
  •   Rheology
 Precipitation
  •   Stabilizers (feed / pharmacy / consumables)
  •   Mechanical (processing)
 Stability equal to mixing quality
Thesis:
Mixing vs. stirring
 Stirring
  •   Similar behaving components
  •   Mostly at low agitating speed
 Mixing
  •   Non-similar behaving components
  •   Dispersing & suspending solid materials
  •   Slurries
  •   Mostly at quick agitating speed
Influence Rheology
                  Newtonian vs. rheopact                                                         Slurry vs. suspension
                                      Viscosity vs. capacity                                                  PRessure vs. capacity
                 1500
                 1400                                                                      17,50
                 1300

                 1200
                                                                                           15,00
                 1100
                                                                                           12,50
                 1000
Viscosity (Cp)




                  900
                                                                                           10,00



                                                                                      Pressure
                  800

                  700                                                                            7,50
                  600
                  500                                                                            5,00
                  400

                  300                                                                            2,50
                  200
                  100
                                                                                                 0,00
                   0                                                                                 0,00   10,00    20,00   30,00    40,00     50,00       60,00   70,00
                        0   10       20        30       40        50       60    70                                                  Capacity
                                             Capacity (m³/hr)
                                                                                                                    Water       Suspension              Slurry
                                 Newtonian                      Shear thinning
Influence viscosity
      400 Cp          1.500 Cp
In-line vs. mixing tank




 Constant capacities   Buffer for variations in
 Good mixable          capacity
 Dilution              Non-similar behaving
 Danger for plugging   components
Continuous vs. batch




 Preventing quality    Mixing time influences
 fluctuations          quality
 Short delay           Dosing accuracy
Slow vs. quick agitation




 Keeping in move         Mixing
 Remaining homogeneity   Including components
 (reaction)              Reducing particle size
Mixer design
                     90°

                       N6
                                      45°
           N1                    N3
   135°                                     30°




 180°                       N5         N7         0°



                N2
                                  N4
Agitator                              315°


                     270°

    Placement nozzles vs. agitator
Mixer design
 Flow profiles:
 •   Placement agitator
 •   Tank shape
 •   Helix type
 •   Influencing flow profile
 Preventing dead space
 •   Also regarding discharge
 Good agitating defines
 stability
Mixer design




 Eccentrically placed agitator vs. baffles
Mixer design




 Multiple agitators for high viscosities
 Scraper blades preventing polution
 Z-blade for dispersing
Process optimization
                                Batch-schema



    Weger FCD1


    Weger FCD2


    Weger FCD3


    Weger FCD4


    Zendvat 1


    Zendvat 2


    Zendvat 3


    Zendvat 4


    Recipiënt CW1


    Weger DW2


    HOB404


    Ketting TRL35


    Weger DW4


    Weger DW5


    TR06DW05S1


    Weger BSM12


    Vl PWP HOT


    Vl PWP COLD


    Tank HOT504


    Handstort BS1


    Menger BLM1


    TRM05


    TrBL1H12


    Tank HOT507


    Handstort BS2


    Menger BLM2


    TRN05


    TrBL1H34




                    0   a   b         c             d   e   f   g
                                          t (min)




 Parallel operations on different units
Process optimization
                                                                                                             Temps total max 30 min




                     Phase 1                                       Phase 2                                                                    Phase 3           Phase 4         Phase 5              Phase 6                Phase 7



     C CM40xL




                                                                                                                         Augmentation réel:
                                                                                                                            C CM40xX

                                                                                                      Poids réel:
                                                                                                      C CM40xN
                                                                                                                                                                             Agitation maxi


                                                                                      x
                                                                              e   chau                                                                                                                  Tête de lavage
                                                                        lait d                                                                                                                            P CM40xR
     C CM40xK                                                                                                                                                 C CM40xM

                                                                                                  ess
                                                                                          H2O proc



     P CM40xC                                   C CM40xG




                                     P CM40xB


     C CM40xF



                                                                                             (CaO)
                                                                                    Chaux
                                                                                                                                                                                 Arrêt ventilateur
                                                                                                     C CM40xH                                                                       scrubber
     C CM40xB
                                                                                                                                                                                                                         Eau de rinçage
                                                                                                                                                                                                                           P CM40xT

                                                                         P CM40xJ                    H2O scrubber
       40 are
         xO




                                                                                                                                                                                        ge
    CM ds t




                                                                                                                                                                                      an
       i
     Po




                                                                                                                                                                                  vi d
                                                                                                                                                                                de
     C




                                                                                                                                                                              an
                                                                                                                                                                             m
                                                                                                                                                                            m
                                                                                                                                                                          Co
                prédosage de l'eau                                                                                                             Ajustement
                                                                                                                                                                          Attendre et agiter
                                                                                                                                              concentration
                                                           dosage de la chaux et de l'eau de réaction                                                           Mélange                              Vidange              Rinçage
                                                                          P CM40xE                                                                             P CM40xH




 Parallel operations within a unit
Conclusion
 Design criteria dependent of application
 Suspensions can seem easy to handled, but
 a lot of attention on the details is necessary
 Need for a sparring partner with a lot of
 experience and a wide reference perspective
Your PROCESS is our PROJECT

  Consulting
  Engineering
  •   Mechanical
  •   Electrical
  Manufacturing
  Process control
  Erection
  Electrical installation
  Maintenance & service

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Mixing and stirring

  • 1. MIXING & STIRRING Specialized in process installations for dry materials and liquids
  • 2. Fields of application Liquid-liquid Solid-solid Solid-liquid (solid) Solid-liquid (liquid)
  • 3. Liquid-liquid Storage LIQUID FI FI Dosing LIQUID SOLID ADDITIVES mixing LIQUID ADDITIVES WATER MIXTURE
  • 4. Liquid-liquid Soap emulsions Food Polymerization Chemistry
  • 5. Fields of application Liquid-liquid Solid-solid Solid-liquid (solid) Solid-liquid (liquid)
  • 6. Solid-solid Storage Macrocomponenten Storage Minor- Storage Micro- componenten componenten M M M M MACRO COMPONENTS MINOR COMPONENTS MICRO COMPONENTS PRODUCT
  • 7. Solid-solid Construction materials Construction chemistry Food Feed / pet food
  • 8. Fields of application Liquid-liquid Solid-solid Solid-liquid (solid) Solid-liquid (liquid)
  • 9. Solid-liquid (solid) Storage FILLING AGENT FI M FI Dosing Mixing FILLING AGENTS SOLID ADDITIVES LIQUID ADDITIVES LIQUID WATER
  • 10. Solid-liquid (solid) Construction materials Food Waste processing / sludge processing
  • 11. Fields of application Liquid-liquid Solid-solid Solid-liquid (solid) Solid-liquid (liquid)
  • 12. Milk of lime Storage LIME Scrubber M FI Dosing ` Preparing LIME Storage, dilution WATER & circulation MILK OF LIME
  • 13. Milk of lime Water decarbonation Washing incineration gases Chemistry
  • 14. Glue preparation Storage RAW MATE- RIAL FI Cooling & FI viscosity M TI Dosing Preparing Storage & circulation RAW MATERIALS Cooking ADDITIVES STEAM WATER SUSPENSION
  • 15. Glue preparation Paper & cardboard Pressed and glued wood
  • 16. Paint Storage FILLING AGENT Dosing M MEDIUM FI FI Transport FILLING AGENTS SOLID ADDITIVES Dissolving LIQUID ADDITIVES MEDIUM WATER PAINT
  • 17. Paint Water based Solvent based
  • 18. Compounds Storage FILLING AGENT POLY MER FI M FI Dosing Mixing FILLING AGENTS SOLID ADDITIVES LIQUID ADDITIVES POLYMER WATER COMPOUND
  • 19. Compounds Carpets Finishing materials (leather, paper, metal)
  • 20. Solid – liquid: suspensions Not a solution – contains solid particles Specific behavior • Abrasive • Rheology Precipitation • Stabilizers (feed / pharmacy / consumables) • Mechanical (processing) Stability equal to mixing quality
  • 22. Mixing vs. stirring Stirring • Similar behaving components • Mostly at low agitating speed Mixing • Non-similar behaving components • Dispersing & suspending solid materials • Slurries • Mostly at quick agitating speed
  • 23. Influence Rheology Newtonian vs. rheopact Slurry vs. suspension Viscosity vs. capacity PRessure vs. capacity 1500 1400 17,50 1300 1200 15,00 1100 12,50 1000 Viscosity (Cp) 900 10,00 Pressure 800 700 7,50 600 500 5,00 400 300 2,50 200 100 0,00 0 0,00 10,00 20,00 30,00 40,00 50,00 60,00 70,00 0 10 20 30 40 50 60 70 Capacity Capacity (m³/hr) Water Suspension Slurry Newtonian Shear thinning
  • 24. Influence viscosity 400 Cp 1.500 Cp
  • 25. In-line vs. mixing tank Constant capacities Buffer for variations in Good mixable capacity Dilution Non-similar behaving Danger for plugging components
  • 26. Continuous vs. batch Preventing quality Mixing time influences fluctuations quality Short delay Dosing accuracy
  • 27. Slow vs. quick agitation Keeping in move Mixing Remaining homogeneity Including components (reaction) Reducing particle size
  • 28. Mixer design 90° N6 45° N1 N3 135° 30° 180° N5 N7 0° N2 N4 Agitator 315° 270° Placement nozzles vs. agitator
  • 29. Mixer design Flow profiles: • Placement agitator • Tank shape • Helix type • Influencing flow profile Preventing dead space • Also regarding discharge Good agitating defines stability
  • 30. Mixer design Eccentrically placed agitator vs. baffles
  • 31. Mixer design Multiple agitators for high viscosities Scraper blades preventing polution Z-blade for dispersing
  • 32. Process optimization Batch-schema Weger FCD1 Weger FCD2 Weger FCD3 Weger FCD4 Zendvat 1 Zendvat 2 Zendvat 3 Zendvat 4 Recipiënt CW1 Weger DW2 HOB404 Ketting TRL35 Weger DW4 Weger DW5 TR06DW05S1 Weger BSM12 Vl PWP HOT Vl PWP COLD Tank HOT504 Handstort BS1 Menger BLM1 TRM05 TrBL1H12 Tank HOT507 Handstort BS2 Menger BLM2 TRN05 TrBL1H34 0 a b c d e f g t (min) Parallel operations on different units
  • 33. Process optimization Temps total max 30 min Phase 1 Phase 2 Phase 3 Phase 4 Phase 5 Phase 6 Phase 7 C CM40xL Augmentation réel: C CM40xX Poids réel: C CM40xN Agitation maxi x e chau Tête de lavage lait d P CM40xR C CM40xK C CM40xM ess H2O proc P CM40xC C CM40xG P CM40xB C CM40xF (CaO) Chaux Arrêt ventilateur C CM40xH scrubber C CM40xB Eau de rinçage P CM40xT P CM40xJ H2O scrubber 40 are xO ge CM ds t an i Po vi d de C an m m Co prédosage de l'eau Ajustement Attendre et agiter concentration dosage de la chaux et de l'eau de réaction Mélange Vidange Rinçage P CM40xE P CM40xH Parallel operations within a unit
  • 34. Conclusion Design criteria dependent of application Suspensions can seem easy to handled, but a lot of attention on the details is necessary Need for a sparring partner with a lot of experience and a wide reference perspective
  • 35. Your PROCESS is our PROJECT Consulting Engineering • Mechanical • Electrical Manufacturing Process control Erection Electrical installation Maintenance & service

Editor's Notes

  1. Toepassingen kunnen we alle vier ondersteunen Werkgebied met name de laatste 2, vooral op het gebied van het maken van suspensies.
  2. Gedispergeerd latex, polyurethaan, polyacrylaat etc. met vulstoffen en additieven
  3. Polymeerproduktie: Vloeibaar-vloeibaar, veelal niet in een “gewone” mengtank en indien wel vaak agressieve milieu’s of hoge drukken noodzakelijk. Veel polymerisaties in (stripper) reaktoren met katalysatoren of inhibitoren.
  4. Macro 10-100 % van de batchgrootte Minor 1 -10 % van de batchgrootte Micro 0,01-1% van de batchgrootte
  5. Bekende mengers zijn Nautamengers, ploegschaar menger, paddle menger, lintmenger, etc.
  6. Vast kan zijn poeder of kluiten
  7. Basis is polyvinylalcohol met kaolinietklei en additieven
  8. Wordt binnen chemie/polymeerchemie gebruik als commodity
  9. Basis is polyvinylalcohol met kaolinietklei en additieven, zetmeel (inhibitor temperatuur of chemisch), “bio-resin” (cellulose, gemodificeerde cellulose)
  10. Koken met kooktank of jet-cooker. PVA en jet-cooker gaan slecht samen. Zetmeel kan wel. Cellulose veelal bij 60°C met glycol Toeslagstoffen glycol, boorzuur, fumaarzuur, loog, ABS etc.
  11. Inmengen van Latex en vulstoffen als titaniumdioxide, kalk (PCC), metaaloxides, pigmenten
  12. Moeilijkheid vaak inmengen/dispergeren van vaste stoffen.
  13. Gedispergeerd latex, polyurethaan, polyacrylaat etc. met vulstoffen en additieven Inmengen van o.a. roet, kalk/krijt, zwavel etc.
  14. Op de foto een “hoge” druk compound reactor en voorts wat opslagtanken. Grote en liggende opslag mogelijk omdat suspensies erg stabiel zijn
  15. Suspensies zijn veelal Newtoniaans. Polymeersuspensies zakken in de curve vrij snel in viscositeit, maar dit stabiliseert ook heel vroeg. De viscositeit is begrenst omdat in stroming de ketens langs elkaar gaan liggen, als dit gebeurd is is de viscositeit minimaal
  16. Verschil is duidelijk: vortex minder stabiel en meer golfjes bij lagere viscositeit
  17. Hoe hoger viscositeit, hoe meer laminair bij de wand en des te meer energie benodigd t.b.v. inmengen
  18. Vooral de hoek met poeders is erg belangrijk. Zorgvuldigheid nodig indien meerdere poeders gebruikt worden
  19. Baffles leveren grotere vervuiling door stilstaande vloeistof. Bij excentrisch roerwerk blijft de wand beduidend schoner
  20. Hoe hoger viscositeit, hoe meer laminair bij de wand en des te meer energie benodigd t.b.v. inmengen
  21. Door gelijktijdige processen (bijvoorbeeld wegen in aparte weger) batchtijdenverkorting
  22. Gelijktijdig doseren van verschillende grondstoffen kan kwaliteit en kwantiteit menger verbeteren