The document discusses mixing and stirring processes for liquids and solids. It covers various applications and fields including liquid-liquid, solid-solid, and solid-liquid mixing. Key aspects addressed include storage, dosing, mixing techniques for different materials, mixer design considerations, and the differences between mixing and stirring. Process optimization is also mentioned as an important factor to consider.
This was my pharmaceutics presentation for mixing. Provides definitions, mechanism, types of mixers etc.
P.S: I am not the sole presenter. Ideas are from my two other colleagues as well.
5 November, 2015
This is a part of our assignment in which we are told to pick one of the pharmaceutical engineering topics and make a paperwork + presentation out of it.
Recorded presentation can be found in: https://youtu.be/O4QvWmW37YA
Paperwork can be found in:
http://www.slideshare.net/annisahayatunnufus/paperwork-mixing-pharmaceutical-engineering
Students of Bachelor of Pharmacy
Management & Science University
Mixing of Solid-Liquid Systems
0 INTRODUCTION/PURPOSE
1 SCOPE
2 FIELD OF APPLICATION
3 DEFINITIONS
4 TYPICAL APPLICATIONS
5 AGITATED VESSELS
5.1 Suspension of Heavier-than-Liquid Solids
5.1.1 Dispersion
5.1.2 Agitator Speed Correlation
5.2 Floating Solids
5.3 Mass Transfer
6 JET MIXING FOR SOLID LIQUID AGITATION
6.1 Flat Bottomed Vessel
6.2 Changes in the Shape of the Vessel Base
7 NOMENCLATURE
8 BIBLIOGRAPHY
APPENDICES
A WORKED EXAMPLE
TABLES
1 VALUES OF Po AND ZWIETERING CONSTANT "S"
FOR USE IN EQUATION 1
FIGURES
1 RECOMMENDED CONFIGURATION
2 RECOMMENDED CONFIGURATION FOR DRAW-DOWN OF FLOATING SOLIDS IN AGITATED VESSEL
3 ALTERNATIVE RECOMMENDED CONFIGURATION
FOR DRAW-DOWN OF FLOATING SOLIDS IN FOR
AGITATED VESSEL
4 JET MIXING FOR SOLIDS SUSPENSION
5 ESTIMATION OF S FROM KNOWN DATA
This was my pharmaceutics presentation for mixing. Provides definitions, mechanism, types of mixers etc.
P.S: I am not the sole presenter. Ideas are from my two other colleagues as well.
5 November, 2015
This is a part of our assignment in which we are told to pick one of the pharmaceutical engineering topics and make a paperwork + presentation out of it.
Recorded presentation can be found in: https://youtu.be/O4QvWmW37YA
Paperwork can be found in:
http://www.slideshare.net/annisahayatunnufus/paperwork-mixing-pharmaceutical-engineering
Students of Bachelor of Pharmacy
Management & Science University
Mixing of Solid-Liquid Systems
0 INTRODUCTION/PURPOSE
1 SCOPE
2 FIELD OF APPLICATION
3 DEFINITIONS
4 TYPICAL APPLICATIONS
5 AGITATED VESSELS
5.1 Suspension of Heavier-than-Liquid Solids
5.1.1 Dispersion
5.1.2 Agitator Speed Correlation
5.2 Floating Solids
5.3 Mass Transfer
6 JET MIXING FOR SOLID LIQUID AGITATION
6.1 Flat Bottomed Vessel
6.2 Changes in the Shape of the Vessel Base
7 NOMENCLATURE
8 BIBLIOGRAPHY
APPENDICES
A WORKED EXAMPLE
TABLES
1 VALUES OF Po AND ZWIETERING CONSTANT "S"
FOR USE IN EQUATION 1
FIGURES
1 RECOMMENDED CONFIGURATION
2 RECOMMENDED CONFIGURATION FOR DRAW-DOWN OF FLOATING SOLIDS IN AGITATED VESSEL
3 ALTERNATIVE RECOMMENDED CONFIGURATION
FOR DRAW-DOWN OF FLOATING SOLIDS IN FOR
AGITATED VESSEL
4 JET MIXING FOR SOLIDS SUSPENSION
5 ESTIMATION OF S FROM KNOWN DATA
5 November, 2015
This is a part of our assignment in which we are told to pick one of the pharmaceutical engineering topics and make a paperwork + presentation out of it.
Presentation slide can be found in: http://www.slideshare.net/annisahayatunnufus/power-point-mixing-pharmaceutical-engineering
Recorded presentation can be found in: https://youtu.be/O4QvWmW37YA
Students of Bachelor of Pharmacy
Management & Science University
Agitation and Mixing are two important unit operations used in industries such as Impellers agitators are widely used to circulate the liquid through the vessel in which the dispersion of liquids and gases into other liquids like mixing of stiff paste, elastomers and dry solids powders takes place.
Frequently Asked Questions about Rotational MouldingFrancis Ward Ltd
At Francis Ward, we are often asked a variety of questions relating to rotomoulding, our processes, products and capabilities, so we have put together a list of the most frequently asked for your information.
However if you cannot find the answer you require please get in touch.
Questions include:
- What thicknesses of plastic can be moulded using rotomoulding?
- What plastics or other materials can be rotomoulded?
- How are plastics coloured?
- What radiuses can be used on rotomoulded products?
- Why are rotomoulded plastic products more expensive than blowmoulded?
- How much do moulds for rotomoulding cost?
- How many products can I make off one mould?
- Can I have flat surfaces on my products?
- How can I make my rotomoulded product stronger?
- What are the minimum and maximum size of moulds?
- What accreditations should a rotomoulder have?
- How is rotomoulding more environmentally friendly than other plastic moulding processes?
- How do I go about creating a design for rotomoulding?
- What are the advantages of using a rotomoulded tank for the storage or transportation of liquids?
- What are the maximum temperatures that a rotomoulded product can stand?
- How long can I expect a rotomoulded product to last?
The second lecture in the module Particle Technology, delivered to second year students who have already studied basic fluid mechanics.
Dilute particle systems is mainly about sedimentation of single particles and dilute suspensions. The Particle Reynolds number determines the degree of turbulence in the fluid and techniques are provided for settling in laminar and turbulent systems. Industrial clarification is included.
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In questo evento online gratuito, organizzato dalla Community Italiana di UiPath, potrai esplorare le nuove funzionalità di Autopilot, il tool che integra l'Intelligenza Artificiale nei processi di sviluppo e utilizzo delle Automazioni.
📕 Vedremo insieme alcuni esempi dell'utilizzo di Autopilot in diversi tool della Suite UiPath:
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Welcome to UiPath Test Automation using UiPath Test Suite series part 4. In this session, we will cover Test Manager overview along with SAP heatmap.
The UiPath Test Manager overview with SAP heatmap webinar offers a concise yet comprehensive exploration of the role of a Test Manager within SAP environments, coupled with the utilization of heatmaps for effective testing strategies.
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What will you get from this session?
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2. Heatmap utilization for testing
3. Optimization of testing processes
4. Demo
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Execution from the test manager
Orchestrator execution result
Defect reporting
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ESnet has led the way in helping national facilities—and many other institutions in the research community—configure Science DMZs and troubleshoot network issues to maximize data transfer performance. In this talk we will present a summary of approaches and tips for getting the most out of your network infrastructure using Globus Connect Server.
5 November, 2015
This is a part of our assignment in which we are told to pick one of the pharmaceutical engineering topics and make a paperwork + presentation out of it.
Presentation slide can be found in: http://www.slideshare.net/annisahayatunnufus/power-point-mixing-pharmaceutical-engineering
Recorded presentation can be found in: https://youtu.be/O4QvWmW37YA
Students of Bachelor of Pharmacy
Management & Science University
Agitation and Mixing are two important unit operations used in industries such as Impellers agitators are widely used to circulate the liquid through the vessel in which the dispersion of liquids and gases into other liquids like mixing of stiff paste, elastomers and dry solids powders takes place.
Frequently Asked Questions about Rotational MouldingFrancis Ward Ltd
At Francis Ward, we are often asked a variety of questions relating to rotomoulding, our processes, products and capabilities, so we have put together a list of the most frequently asked for your information.
However if you cannot find the answer you require please get in touch.
Questions include:
- What thicknesses of plastic can be moulded using rotomoulding?
- What plastics or other materials can be rotomoulded?
- How are plastics coloured?
- What radiuses can be used on rotomoulded products?
- Why are rotomoulded plastic products more expensive than blowmoulded?
- How much do moulds for rotomoulding cost?
- How many products can I make off one mould?
- Can I have flat surfaces on my products?
- How can I make my rotomoulded product stronger?
- What are the minimum and maximum size of moulds?
- What accreditations should a rotomoulder have?
- How is rotomoulding more environmentally friendly than other plastic moulding processes?
- How do I go about creating a design for rotomoulding?
- What are the advantages of using a rotomoulded tank for the storage or transportation of liquids?
- What are the maximum temperatures that a rotomoulded product can stand?
- How long can I expect a rotomoulded product to last?
The second lecture in the module Particle Technology, delivered to second year students who have already studied basic fluid mechanics.
Dilute particle systems is mainly about sedimentation of single particles and dilute suspensions. The Particle Reynolds number determines the degree of turbulence in the fluid and techniques are provided for settling in laminar and turbulent systems. Industrial clarification is included.
Le nuove frontiere dell'AI nell'RPA con UiPath Autopilot™UiPathCommunity
In questo evento online gratuito, organizzato dalla Community Italiana di UiPath, potrai esplorare le nuove funzionalità di Autopilot, il tool che integra l'Intelligenza Artificiale nei processi di sviluppo e utilizzo delle Automazioni.
📕 Vedremo insieme alcuni esempi dell'utilizzo di Autopilot in diversi tool della Suite UiPath:
Autopilot per Studio Web
Autopilot per Studio
Autopilot per Apps
Clipboard AI
GenAI applicata alla Document Understanding
👨🏫👨💻 Speakers:
Stefano Negro, UiPath MVPx3, RPA Tech Lead @ BSP Consultant
Flavio Martinelli, UiPath MVP 2023, Technical Account Manager @UiPath
Andrei Tasca, RPA Solutions Team Lead @NTT Data
UiPath Test Automation using UiPath Test Suite series, part 4DianaGray10
Welcome to UiPath Test Automation using UiPath Test Suite series part 4. In this session, we will cover Test Manager overview along with SAP heatmap.
The UiPath Test Manager overview with SAP heatmap webinar offers a concise yet comprehensive exploration of the role of a Test Manager within SAP environments, coupled with the utilization of heatmaps for effective testing strategies.
Participants will gain insights into the responsibilities, challenges, and best practices associated with test management in SAP projects. Additionally, the webinar delves into the significance of heatmaps as a visual aid for identifying testing priorities, areas of risk, and resource allocation within SAP landscapes. Through this session, attendees can expect to enhance their understanding of test management principles while learning practical approaches to optimize testing processes in SAP environments using heatmap visualization techniques
What will you get from this session?
1. Insights into SAP testing best practices
2. Heatmap utilization for testing
3. Optimization of testing processes
4. Demo
Topics covered:
Execution from the test manager
Orchestrator execution result
Defect reporting
SAP heatmap example with demo
Speaker:
Deepak Rai, Automation Practice Lead, Boundaryless Group and UiPath MVP
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ESnet has led the way in helping national facilities—and many other institutions in the research community—configure Science DMZs and troubleshoot network issues to maximize data transfer performance. In this talk we will present a summary of approaches and tips for getting the most out of your network infrastructure using Globus Connect Server.
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One such alternative that has garnered significant attention and acclaim is Nitrux Linux 3.5.0, a sleek, powerful, and user-friendly Linux distribution that promises to redefine the way we interact with our devices. With its focus on performance, security, and customization, Nitrux Linux presents a compelling case for those seeking to break free from the constraints of proprietary software and embrace the freedom and flexibility of open-source computing.
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The modern software delivery process (or the CI/CD process) includes many tools, distributed teams, open-source code, and cloud platforms. Constant focus on speed to release software to market, along with the traditional slow and manual security checks has caused gaps in continuous security as an important piece in the software supply chain. Today organizations feel more susceptible to external and internal cyber threats due to the vast attack surface in their applications supply chain and the lack of end-to-end governance and risk management.
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Bob Boule
Robert Boule is a technology enthusiast with PASSION for technology and making things work along with a knack for helping others understand how things work. He comes with around 20 years of solution engineering experience in application security, software continuous delivery, and SaaS platforms. He is known for his dynamic presentations in CI/CD and application security integrated in software delivery lifecycle.
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Alt. GDG Cloud Southlake #33: Boule & Rebala: Effective AppSec in SDLC using ...James Anderson
Effective Application Security in Software Delivery lifecycle using Deployment Firewall and DBOM
The modern software delivery process (or the CI/CD process) includes many tools, distributed teams, open-source code, and cloud platforms. Constant focus on speed to release software to market, along with the traditional slow and manual security checks has caused gaps in continuous security as an important piece in the software supply chain. Today organizations feel more susceptible to external and internal cyber threats due to the vast attack surface in their applications supply chain and the lack of end-to-end governance and risk management.
The software team must secure its software delivery process to avoid vulnerability and security breaches. This needs to be achieved with existing tool chains and without extensive rework of the delivery processes. This talk will present strategies and techniques for providing visibility into the true risk of the existing vulnerabilities, preventing the introduction of security issues in the software, resolving vulnerabilities in production environments quickly, and capturing the deployment bill of materials (DBOM).
Speakers:
Bob Boule
Robert Boule is a technology enthusiast with PASSION for technology and making things work along with a knack for helping others understand how things work. He comes with around 20 years of solution engineering experience in application security, software continuous delivery, and SaaS platforms. He is known for his dynamic presentations in CI/CD and application security integrated in software delivery lifecycle.
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In this work, we equipped AFL, a popular fuzzer, with DIAR and examined two critical Linux libraries -- Libxml's xmllint, a tool for parsing xml documents, and Binutil's readelf, an essential debugging and security analysis command-line tool used to display detailed information about ELF (Executable and Linkable Format). Our preliminary results show that AFL+DIAR does not only discover new paths more quickly but also achieves higher coverage overall. This work thus showcases how starting with lean and optimized seeds can lead to faster, more comprehensive fuzzing campaigns -- and DIAR helps you find such seeds.
- These are slides of the talk given at IEEE International Conference on Software Testing Verification and Validation Workshop, ICSTW 2022.
5. Fields of application
Liquid-liquid
Solid-solid
Solid-liquid (solid)
Solid-liquid (liquid)
6. Solid-solid
Storage
Macrocomponenten
Storage Minor- Storage Micro-
componenten componenten
M M M M
MACRO COMPONENTS
MINOR COMPONENTS
MICRO COMPONENTS
PRODUCT
11. Fields of application
Liquid-liquid
Solid-solid
Solid-liquid (solid)
Solid-liquid (liquid)
12. Milk of lime
Storage
LIME
Scrubber
M
FI
Dosing
`
Preparing
LIME Storage, dilution
WATER & circulation
MILK OF LIME
13. Milk of lime
Water decarbonation
Washing incineration gases
Chemistry
14. Glue preparation
Storage
RAW
MATE-
RIAL FI
Cooling &
FI viscosity
M
TI
Dosing
Preparing
Storage &
circulation
RAW MATERIALS Cooking
ADDITIVES
STEAM
WATER
SUSPENSION
25. In-line vs. mixing tank
Constant capacities Buffer for variations in
Good mixable capacity
Dilution Non-similar behaving
Danger for plugging components
26. Continuous vs. batch
Preventing quality Mixing time influences
fluctuations quality
Short delay Dosing accuracy
27. Slow vs. quick agitation
Keeping in move Mixing
Remaining homogeneity Including components
(reaction) Reducing particle size
29. Mixer design
Flow profiles:
• Placement agitator
• Tank shape
• Helix type
• Influencing flow profile
Preventing dead space
• Also regarding discharge
Good agitating defines
stability
31. Mixer design
Multiple agitators for high viscosities
Scraper blades preventing polution
Z-blade for dispersing
32. Process optimization
Batch-schema
Weger FCD1
Weger FCD2
Weger FCD3
Weger FCD4
Zendvat 1
Zendvat 2
Zendvat 3
Zendvat 4
Recipiënt CW1
Weger DW2
HOB404
Ketting TRL35
Weger DW4
Weger DW5
TR06DW05S1
Weger BSM12
Vl PWP HOT
Vl PWP COLD
Tank HOT504
Handstort BS1
Menger BLM1
TRM05
TrBL1H12
Tank HOT507
Handstort BS2
Menger BLM2
TRN05
TrBL1H34
0 a b c d e f g
t (min)
Parallel operations on different units
33. Process optimization
Temps total max 30 min
Phase 1 Phase 2 Phase 3 Phase 4 Phase 5 Phase 6 Phase 7
C CM40xL
Augmentation réel:
C CM40xX
Poids réel:
C CM40xN
Agitation maxi
x
e chau Tête de lavage
lait d P CM40xR
C CM40xK C CM40xM
ess
H2O proc
P CM40xC C CM40xG
P CM40xB
C CM40xF
(CaO)
Chaux
Arrêt ventilateur
C CM40xH scrubber
C CM40xB
Eau de rinçage
P CM40xT
P CM40xJ H2O scrubber
40 are
xO
ge
CM ds t
an
i
Po
vi d
de
C
an
m
m
Co
prédosage de l'eau Ajustement
Attendre et agiter
concentration
dosage de la chaux et de l'eau de réaction Mélange Vidange Rinçage
P CM40xE P CM40xH
Parallel operations within a unit
34. Conclusion
Design criteria dependent of application
Suspensions can seem easy to handled, but
a lot of attention on the details is necessary
Need for a sparring partner with a lot of
experience and a wide reference perspective
35. Your PROCESS is our PROJECT
Consulting
Engineering
• Mechanical
• Electrical
Manufacturing
Process control
Erection
Electrical installation
Maintenance & service
Editor's Notes
Toepassingen kunnen we alle vier ondersteunen Werkgebied met name de laatste 2, vooral op het gebied van het maken van suspensies.
Gedispergeerd latex, polyurethaan, polyacrylaat etc. met vulstoffen en additieven
Polymeerproduktie: Vloeibaar-vloeibaar, veelal niet in een “gewone” mengtank en indien wel vaak agressieve milieu’s of hoge drukken noodzakelijk. Veel polymerisaties in (stripper) reaktoren met katalysatoren of inhibitoren.
Macro 10-100 % van de batchgrootte Minor 1 -10 % van de batchgrootte Micro 0,01-1% van de batchgrootte
Bekende mengers zijn Nautamengers, ploegschaar menger, paddle menger, lintmenger, etc.
Vast kan zijn poeder of kluiten
Basis is polyvinylalcohol met kaolinietklei en additieven
Wordt binnen chemie/polymeerchemie gebruik als commodity
Basis is polyvinylalcohol met kaolinietklei en additieven, zetmeel (inhibitor temperatuur of chemisch), “bio-resin” (cellulose, gemodificeerde cellulose)
Koken met kooktank of jet-cooker. PVA en jet-cooker gaan slecht samen. Zetmeel kan wel. Cellulose veelal bij 60°C met glycol Toeslagstoffen glycol, boorzuur, fumaarzuur, loog, ABS etc.
Inmengen van Latex en vulstoffen als titaniumdioxide, kalk (PCC), metaaloxides, pigmenten
Moeilijkheid vaak inmengen/dispergeren van vaste stoffen.
Gedispergeerd latex, polyurethaan, polyacrylaat etc. met vulstoffen en additieven Inmengen van o.a. roet, kalk/krijt, zwavel etc.
Op de foto een “hoge” druk compound reactor en voorts wat opslagtanken. Grote en liggende opslag mogelijk omdat suspensies erg stabiel zijn
Suspensies zijn veelal Newtoniaans. Polymeersuspensies zakken in de curve vrij snel in viscositeit, maar dit stabiliseert ook heel vroeg. De viscositeit is begrenst omdat in stroming de ketens langs elkaar gaan liggen, als dit gebeurd is is de viscositeit minimaal
Verschil is duidelijk: vortex minder stabiel en meer golfjes bij lagere viscositeit
Hoe hoger viscositeit, hoe meer laminair bij de wand en des te meer energie benodigd t.b.v. inmengen
Vooral de hoek met poeders is erg belangrijk. Zorgvuldigheid nodig indien meerdere poeders gebruikt worden
Baffles leveren grotere vervuiling door stilstaande vloeistof. Bij excentrisch roerwerk blijft de wand beduidend schoner
Hoe hoger viscositeit, hoe meer laminair bij de wand en des te meer energie benodigd t.b.v. inmengen
Door gelijktijdige processen (bijvoorbeeld wegen in aparte weger) batchtijdenverkorting
Gelijktijdig doseren van verschillende grondstoffen kan kwaliteit en kwantiteit menger verbeteren