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Pressure oven
High pressure reactor
Pressure vessel
Isostatic press
Agitator(Magnedrive)
Nano disperser & Micro disperser
Supercritical carbon dioxide system
High shear mixer
( Homo mixer, Inline mixer, Ultra high shear nozzle )
Paste mixer
Three roll mill
Plant
Waterjet
www.suflux.com
Overview
High pressure reactor
Pressure oven
Isostatic press
Pressure vessel
Supercritical carbon dioxide system
Agitator(Magnedrive)
High shear mixer ( Homo mixer, Inline mixer, Ultra high shear nozzle )
Nano disperser & Micro disperser
Three roll mill
Paste mixer
Waterjet
Plant
Test Service
03
04 - 05
06 - 07
08 - 09
10 - 11
12 - 15
16
17 - 19
20 - 23
24 - 25
26 - 27
28
29
30 - 31
Contents
ISO9001 ISO14001 SELS STAMP STAMPU STAMPU2
History
Certification
ASME ASME ASME
03
Found ENGINEERING
Developed products Autoclave system
Magnedrive
Hot plate press
High temperature & pressure test loop system
Incorporated as ILSHIN AUTOCLAVE CO.,LTD, ISA/KSA9001, 14001
Established an annexed research institue
The building and factory were moved to Daeduck techno valley
Developed products
Nano Disperser (High pressure homogenizer)
Isostatic press ( CIP /WIP /HPP)
Supercritical water oxidization device for non-resolvable materials
Aerogel supercritical drying system
Supercritical degreasing system
Supercritical extraction system for mass production
Supplied commercial purpose of SC-CO2 extraction system
(to Otoogi foods Co., , Korea ginseng corp. )
1990’s
1993
1993~1999
2001
2002
2009
2001~2009
2000’s
2010’s
Won the grand prize in safety certification part from KOSHA and MOEL
ASME stamp 'S', 'U', 'U2' renewal, SEL certification ( China Special Equipment License )
Nano disperser awarded in "NANO KOREA 2013 AWARD", 'GOOD DESIGN", "IT INNOVATION"
iF DESIGN AWARD in Germany ( Nano Disperser)
Developed products
Pilot scale of supercritical water system (LG chem)
Industrial scale of supercritical extraction system (JNBC)
Waterjet
Nano disperser for high capacity
High shear mixer
3 roll mill / Paste mixer
2011
2012
2013
2014
2010~2014
SUFLUX means our brand for components produced by ourselves for high pressure and temperature control. It is a compound word of super and flux. SUFLUX
stands for "high value and continuous effort to make it changed", thus providing high quality and reliable performance. Our continuous effort to make innovative
products is included in SUFLUX.
Overview - ‘ILSHIN AUTOCLAVE's brand
ASME S STAMP ASME U STAMP ASME U2 STAMP SEL
Agitator
Seal type
(O-ring/gasket)
Port(Inlet/Outlet)
Thermocouple
Pressure Vessel
Liner
FEATURE CERTIFICATION
18 HIGH PRESSURE REACTOR04
It has diverse applications which are hydrothermal and decomposition, sublimation, extraction in laboratory by high
pressure and temperature with various optional device.
1
2
3
Bench top type Multi-purpose system Hydrothermal synthesis
Reaction system for polymerization
(Customized)
Reaction system for hydride
(Customize)
Reaction system with catalyst
(Customized)
t ith t l t
Temperature(℃
)
Pressure(㎏/㎠)
Volume(ℓ)
Pressure vessel based on ASME
Various size and pressure & temperature
Various optional device for easy maintenance
- Agitator, upload / lift system, etc..
Guide of option
PTFE or Stainless steel Liner Belt driven or Motor driven
(direct with magnetic coupling)
Adjustable speed 0~1700 rpm
Touch screen for control/monitor Heat insulated jacket on cover
Up&down of body by air cylinder Front&rear of body by air cylinder Front&rear of body by air cylinder Analog pressure gauge
Digital pressure transmitter
05
HIGH PRESSURE REACTOR
Reactor for Self-propagation
(Customized)
Reactor with rotation
(Customized)
Reaction system for thermal decomposiotion
(Customized)
Reaction system for blasting
(Customized)
Reaction system with ultra high temperature
& pressure (Customized)
Reaction system with continuous operation
(Customized)
Stirrer parts
Cover & Body
It has application for lamination and to remove voids both layers in industries of touch panel and LCD, PDP, semi conductor.
Effect of removing voids by pressure and temperature
Effect of hardness by temperature
Effect of adhesive strength by pressure
Solderball
Top and Bottom Die Die Attach Film/Paste
Air
Bubbles
(기포)
Dieelectric
Before After Before After Before After
Mold Cap
FR-5 Substrate
Silicon ICEpoxy Undrfill
Air
Bubbles
Solder Ball (63Sn/37Pb)
Bubble
Pressure curing oven06
Completed lamination
and removed voids
TPVB or EVA film
Glass
1
2
3
Clutch Door
Chamber
Touch Screen
Pressure gauge (Seal / Inlet / Chamber)
Three color light
Glass
(GA)
Touch panel screen,
Film (FA)
ass
GA)
panel screen,
m (FA)
Semiconductor of package
process (HA)
Parts of system
FEATURE
CONSIDERATION TO ORDER
Main O-ring
To seal cover Heating & Cooling Internal air circulation To pressurize the vessel
Pressure curing oven
07
M/D
Air circulation
Cooling system
Heater
Main O-ring Heater and cooling coil Fan and motor Booster
Compacted size
Reasonable price
Durability
BoosterAward for safety
Internal air flow
Before sealed
cover
After sealed
cover
Uniformity : +/-3deg C
Size (A, B)1
1
2
3
Pressure2
Temperature3
Cooling4
Booster or compressed air5
Gas media (Air or gas )6
A
B
B
ISOSTATIC PRESS
The mold by
isodirectional
force
Lamination
The sterilization
by
high pressure
It has the technology of isodirectional force with solvent liquid inside pressure vessel by high pressure.
There are applications of lamination in electronic industry and sterilization in food industry, etc..
08
11
2
1
2
1
2
Customized system
(Size, operating process)
Design according to ASME, CSEL
Wire Wounding
Reasonable price
Rapid response
Easy operation
Easy maintenance
CIP (Cold Isostatic Press)
Laboratory
Laboratory
Production
Production
Laboratory Production
WIP (Warm Isostatic Press)
Engineering
FIP (Food Isostatic Press)
Technology Competitiveness Convenience
FEATURE
1
2
3
4
5
6
1
2
3
4
5
6
Pin Closing Type
It has many different high pressure depending on application of metal forming process, electrical parts, food.
CIP series
WIP series
FIP series
Custom
Custom
Custom
OIL / WATER
OIL / WATER
OIL / WATER
0 ~ 6000 bar
0 ~ 6000 bar
0 ~ 6000 bar
RT
50 - 120 ℃
RT - 80 ℃
COLD ISOSTATIC PRESS Macromolecule, Ceramic, Metal, Carbon, etc.
MLCC, LTCC, multi other chips
Fruit juice, Sea food, etc.
CIP series
WARM ISOSTATIC PRESSWIP series
FOOD ISOSTATIC PRESSFIP series
ISOSTATIC PRESS
09
Pressure : ~1000 bar
Temperature : RT ~80 ℃
Volume : ~ Custom
Air Driven Liquid Pump / Hydraulic Pump
O-ring /U-packing / Energizer seal
CIP /WIP
Pressure : ~4000 bar & Custom
Temperature: RT ~120 ℃
Volume : ~ 100L & Custom
Air Driven Liquid Pump / Hydraulic Pump
O-ring / U-packing
CIP / WIP / Laboratory FIP
Pressure : ~6000 bar
Temperature : ~RT
Volume : ~ 200L & Custom
Hydraulic Pump
O-ring Seal /U-packing / Energizer seal
CIP / FIP (Wire wounding)
Model PRESSURE INTERNAL DIAMETER WORKING MEDIA TEMPERATURE
Pin Clos
C-clamp Type
Press frame closing type
1
2
3
4
5
6
ng type
Pressure Vessel
Industrial scale & Customized pressure vessel
Reactor for reaction or special purpose
Wide rage of material and optional close method for the use of environment in industries of chemical and pharmaceuticals, others.
350 ℃
250 ℃
350 ℃
250 ℃
300 bar
50 bar
700 bar
200 bar
BV series
CV series
PV series
VCV series
Bolt Closure type
Cap Closure type
Plug & Cap Closure type
View Cell
O-ring/Teflon/Metal
O-ring
O-ring/Teflon
Urethane/O-ring/Teflon
O / X
X
O / X
O / X
Steam generator
Reactor for external pressure test
Reactor for micro-organisms
Heater exchanger
MODEL METHOD OF CONTRACT TEMPERATURE PRESSURE SEAL TYPE AGITATION
FEATURE
Pressure vessel based on ASME
Optional gas line depending on required gas.
Customized service
ASME S STAMP ASME U STAMP ASME U2 STAMP SEL
CERTIFICATION
10
1
2
3
ILSHIIN AUTOCALVE is providing many different size of pressure vessel. Depending on application
and customer's requirement, it's available many different size with high pressure and temperature, optional diveces.
Pressure vessel
11
BV TYPE (BOLT CLOSURE PRESSURE VESSEL)
Basic type
Sealed by bolts(Screws)
Easy to make tubing and ports.
1
2
3
CV TYPE (CAP CLOSURE PRESSURE VESSEL)
Easy to open and close cover
PTFE liner
PV TYPE (PLUG TYPE PRESSURE VESSEL)
1
2
Easy to open and close cover
Sealed for high pressure and temperature
1
2
VCV TYPE (VIEW CELL PRESSURE VESSEL)
Quick to open and close1
QCQ TYPE (QUICK CLAMP CLOSURE PRESSURE VESSEL)
Quick to open and close
For high pressure maximum 6000bar
1
2
QCP TYPE (PIN CLOSURE PRESSURE VESSEL)
Quick to open and close
For high pressure maximum 6000bar
1
2
QCY TYPE (YOKE FLAME CLOSURE PRESSURE VESSEL)
Easy to open and close
For high pressure maximum 6000bar
1
2
SUPERCRITICAL CARBON DIOXIDE FLUID SYSTEM12
It has application of extraction and drying system by technology of supercritical point with carbon dioxide.
Supercritical making nano-particle system
Supercritical degreasing system
Supercritical extraction system
Supercritical expansion system
Supercritical drying system
Critical Point
Pressure
Temperature
Supercritical Fluid
Solid Phase
Liquid Phase
Gaseous Phase
Liquid and
gas Increasing
Supercrtical
condition
Density of
gas & liquid
Supercritical CO2 + Oil
Liquid CO2
Gas CO2 Gas CO2
Supercritical CO2
Extractor
Chiller
CO2 Reservoir
PumpHeater
Control valve Control Valve
Seperator
Extract yield
Pressure vessel based on ASME
Eco-friendly
For high quality production
Supercritical
Fluid
GAS LIQID
High diffusion coefficient
Low viscosity
Low surface tension
High density
High solubility
FEATURE
[C-Clamp type] [Yoke frame type]
BPR
(Back Pressure Regulator)
Extractor
Extractor
Reservoir
Reservoir
Heater
Separator
Separator
Pump for co-solvent
Touch Screen
CO2 Pump
CO2 Pump
Chiller
Hydraulic
unity
Extractor : Yoke frame / C-clamp type Reservoir
Condenser High pressure pump Pre heater
SUPERCRITICAL CARBON DIOXIDE FLUID SYSTEM
SUPERCRITICAL CARBON DIOXIDE FLUID SYSTEM
13
Pressure Gauge
Separator
[Cover type] [Open type]
Main pressure vessel for extraction with supercritical
condition
Yoke, clamp close/open type
Operated by hydraulic unit
Process to break supercritical condition.
To get extract yield
For storage/recycle of CO2 in liquid
Cooling device to make CO2 to liquid High pressure pump system of intensifier type by
hydraulic unit
Heating device to make temperature for supercritical
condition
Lab. Scale
Pilot Scale
Product Scale
30 - 80 ℃
30 - 80 ℃
30 - 80 ℃
Custom
Custom
Custom
0.3 ~ 2 ℓ
5 ~ 50 ℓ
Custom
Solid & liquid
Solid & liquid
Solid & liquid
14
SUPERCRITICAL CARBON DIOXIDE FLUID SYSTEM
SUPERCRITICAL EXTRACTION
SERIES VOLUME MAX. PRESSURE MAX.TEMPERATURE RAW MATERIAL PHASE
Debinding system Debinding system
EXTRACTOR : 100 ℓ X 2 uints
WORKING PRESSURE : 250 bar
EXTRACTOR : 100 ℓ X 2 uints
WORKING PRESSURE : 700bar
To extract the sesame oil To de-grease the pernicious ingredients
EXTRACTOR : 2300 ℓ X 3 uints
WORKING PRESSURE : 450 bar
EXTRACTOR : 600 ℓ X 2 uints
WORKING PRESSURE : 460bar
Available custom size and specification
The graph of density depending on pressure and temperature The graph of extract time depending on pressure.
X100
TO EXTRACT OIL
TO EXTRACT OIL
SUPERCRITICAL CARBON DIOXIDE FLUID SYSTEM
15
TEST SERVICE
Product
Extract
yield
Condition
Pressure (㎏/㎠) Temperature (℃)
300~500 bar
300~500 bar
300~450 bar
300~450 bar
300~450 bar
200~400 bar
400~500 bar
300~500 bar
400~500 bar
200~350 bar
200~350 bar
100~300 bar
200~350 bar
400~500 bar
300~400 bar
350~400 bar
200~350 bar
300~400 bar
150~200 bar
200~300 bar
300~500 bar
sesame
corn germ seed
soybean
rape blossoms seeds
sunflower seeds
paprika
castor
grape seeds
red pepper seed
coffee
green tea
iris
medicinal herbs
rice bran
raspberry
turmeric
citron
yolk
fish oil
camellia oil
Bija
40~60 ℃
40~60 ℃
40~60 ℃
40~60 ℃
40~60 ℃
40~50 ℃
40~60 ℃
40~60 ℃
50~60 ℃
40~60 ℃
40~60 ℃
40~50 ℃
40~60 ℃
55~60 ℃
50~60 ℃
55~60 ℃
45~50 ℃
40~60 ℃
40~60 ℃
40~60 ℃
50~60 ℃
40 %
35 %
15 %
25 %
34 %
6 %
25 %
8 %
20 %
7 %
Cosolvents
6 %
Cosolvents
10 %
15 %
10 %
Incense component
30 %
Deodorization
Deodorization
20 %
AGITATOR16
The graph of extract time depending on pressure.
MDB - Thread Type MDD - Thread Type
MDD - Flange Type
MDB - Flange Type
MDB series
MDD series
1000~8000 psi
1000~8000 psi
Thread/ Flange Type
Thread/ Flange Type
Φ 5~50
Φ 5~50
MDB series MDD series
SERIES SHAFT DIAPRESSURE TYPE
HIGH SHEAR MIXER
17
We're providing a solution for dispersion and mixing by using high shear system which are Homo mixer, Inline mixer, Ultra high shear nozzle
High pressure homogenizer (NLM100, NH series)
less than 10,000 cp
High shear mixer ( homo mixer, inline mixer )
less than 70,000 cp
3RollMill, Paste mixer
less than 200,000 cp
To save time and To reduce cost
원료
The existing process
Heating & Mixing
Pre Mixing In-line Mixing Packing
PackingCooling & Mixing
High shear mixer process
Difference 9 hours
6hr 6hr 12hr
1hr 2hr 3hr
Water
1 cp
15,000 cp
30,000 cp 45,000 cp 200,000 cp70,000 cp
Milk Kerosene Honey Glue Mayo Ink/Paint Mustard Paste
RANGE OF VISCOSITY (EXAMPLE)
Pre mixer (Agitator)
less than 100,000 cp
18
FLOW DIRECTION
FLOW DIRECTION
HIGH SHEAR MIXER
High shear homo-mixer is driven by high speed motor (max. 8,000rpm) and it's a specially designed nozzle and this precision machined nozzle
offers great versatility by allowing any machine to perform a wide range of mixing operation.
HIGH SHEAR HOMO-MIXER
Depending on customer's application, it's providing diverse system.
HIGH SHEAR INLINE MIXER
Blade shaft
Stator
guide
Stator
Rotor
Stator
Rotor
OUTLET
INLET PORT
MOTOR
ROTATOR
SHAFT
ROTOR
BLADE HOUSING
19
Ultra high shear nozzle makes highest shear force and highest cavitation by consisting multi-stage nozzle.
Precise stator as fineness holes
Suitable for emulsion application
TYPE
SYSTEM TYPE
Combination type
HIGH SHEAR MIXER
SUPER HIGH SHEAR INLINE MIXER
Chamber type
Nozzle type
Cone type
Arched rotator and stator
Suitable for emulsion/homogenization/dispersion
Precise stator as fineness holes
Suitable for emulsion application
Cylindrical shape of rotator
Suitable for emulsion/homogenization/dispersion
Liquid + Additive
Next Process
Next Process
Liquid + AdditiveAdded hopper
Next Process
Liquid + Additive
Basic
Optional
agitator
Optional
added
hopper
Pressure
GaugeHigh
Pressure
Pump
Inlet
Before After
Outlet
Heat
Exchanger
SHEAR FORCECAVITATION IMPACT
Particle Size Reduction
Emulsions
Suspensions
Liposomes
Cell Disruption
E-coil
Yeast
Nano-Encapsulation
Polymers
Liposomes
Emulsions
Nano Disperser make dispersion of particle passing through the nozzle chamber with ultra high pressure and
there are force of impact, cavitation and share stress in the nozzle chamber.
It used in applications of chemical, food, cosmetics, petroleum and paints.
HIGH PRESSURE HOMOGENIZER20
NANO DISPERSER VS MICRO DISPERSER
NANO DISPERSER Dia chamber
Adjustable valve
Dispersion
Emulsion
Chemical,
Electronic parts
Food, Cosmetic
Ultra high pressure
High pressure
Nozzle Chamber
MICRO DISPERSER
NOZZLE MAIN APPLICATION MAIN INDUSTRY PRESSURE
Motor driven and single piston Air vent valve
One Stage Valve Two Stage Valve Adjustable pressure b
y motor speed
Motor driven and single piston
Adjustable pressure
by motor speed
Cooling tank after process
HIGH PRESSURE HOMOGENIZER
21
MICRO DISPERSER(MLM100)
NANO DISPERSER (NLM100)
Operating Pressure
Flow rate
Pump system
Inlet reservoir
Dimension
Weight
Max. 1,500bar
Max. 100ml/min
Motor driven type [ 220VAC, 1PH, 60Hz, 1HP ]
300ml
490(D) x 580(W) x 445(H)mm
Approx. 40kg
NLM100-Z75
NLM100-Y75
100 ml / min
100 ml / min
1500 bar
1500 bar
75 um
75 um
Z type
Y type
Max Pressure
Size
Interaction Chamber
Type
Flow RateFlow Rate
Operating Pressure
Flow rate
Pump system
Inlet reservoir
Dimension
Weight
Max. 2,000bar
Max. 100ml/min
Motor driven type [ 220VAC, 1PH, 60Hz, 1HP ]
300ml
490(D) x 450(W) x 300(H)mm
Approx. 35kg
100 ml / min 1500 bar Variation 2 Stage vlave
Max Pressure
Size
Interaction Chamber
Type
Flow Rate
Back flushing system Cooling tank after process Protective case Adjustable pressure by hydraulic unit
HIGH PRESSURE HOMOGENIZER
22
NANO DISPERSER (NH 500)
NANO DISPERSER (NH 4000)
Operating Pressure
Flow rate
Pump system
Inlet reservoir
Dimension
Weight
Max. 2,000bar
Max. 500ml/min
Hydraulic unit system
2000ml
800(D) x 850(W) x 1500(H)mm
Approx. 300kg
500ml/min 2000 bar 100um Z type / Y type
Max Pressure
Size
Interaction Chamber
Type
Flow Rate
Operating Pressure
Flow rate
Pump system
Inlet reservoir
Dimension
Weight
Max. 2,000bar
Max. 100ml/min
Motor driven type [ 220VAC, 1PH, 60Hz, 1HP ]
300ml
490(D) x 580(W) x 445(H)mm
Approx. 40kg
Solution tank to prevent the solidification Monitor and Alarm system Cooling line on high pressure part Back flushing system
NH8000
NH2000
NH2000
NH4000
NH8000
2l / min
4l / min
8l / min
2000 bar
2000 bar
2000 bar
200, 400um
200, 400um
200, 400um
Z / Y type
Z / Y type
Z / Y type
Max Pressure
Size
Interaction Chamber
Type
Flow RateSeries
HIGH PRESSURE HOMOGENIZER
23
Emulsion
Rupture
Dispersion
AFTERBEFORE
Product Number of pass Effect
Milk
Soybean milk,
CNT
Water + Oil
CERAMIC(Si)
TiO3
Graphite(Carbon)
CeO2
raw materials for cosmetics
Pigment
a high molecular substance
Al2O3
Dispersion
Homogenization
Dispersion
Suavity
Dispersion
Crushed
Crushed
Dispersion
Suavity
Dispersion
Crushed
Dispersion
1800 bar
[1 pass]
2000 bar
[5 pass]
2000 bar
[3 pass]
2500 bar
[5 pass]
2000 bar
[5 pass]
2500 bar
[3 pass]
2000 bar
[3 pass]
2500 bar
[3 pass]
1000 bar
[3 pass]
2500 bar
[3 pass]
2500 bar
[3 pass]
2000 bar
[3 pass]
Three roll mill is a machine that uses shear force created by three horizontally positioned rolls rotating in opposite directions and
different speeds relative to each other, in order to mix, refine, disperse, or homogenize viscous materials fed into it.
FEATURE
Precise roll
Materials of roll
Heating/Cooling system
Adjustable micro gap
Adjustable speed
Minimized noise and vibration
Stainless steel / Ceramic / Alloy steel
THREE ROLL MILL24
1
2
3
4
5
MICRO GAP SHEAR FORCE & PRESSURE Transmission ration
After
Scraper
Before
Shear gap 1
V 1 << V2 << V3
Shear gap 2
Specimen
Draw-in roll Middle roll Scrapper roll
Draw in roll Middle roll Scraper roll
1 : 3
1 : 3
1 : 9
1 : 3 : 9
Shear Gap(Elinination size)
V1
V1 < V2
V2 V1 V2
1
1
3
3
2
2
THREE ROLL MILL
25
Alarm
Gap control knob
End plate
Draw-in roll
Middle roll
Scraper roll
Control part
Roll size (mm)
Roll speed (RPM)
Roll ratio
Throughput (LPH)
Gap (micron)
Size (W x D x H)
Weight (Kg)
Electrical power
TRM 50
Model
Lab scale Product scale
TRM 80 TRM 145 TRM 230
φ 50 * 150
533 : 213 : 85
1 : 2.5 : 6.25
0.2 ~ 6
2 ~ 50
340 x 290 x 300
20
220V, 200W
φ 80 * 250
600 : 200 : 67
1 : 3 : 9
0.5 ~ 12
2 ~ 20
550 x 450 x 600
65
220V, 750W
φ 145 * 360
350 : 210 : 105
1 : 1.6 : 2.5
5.1 ~ 20
5 ~ 20
810 x 690 x 900
650
220/380V, 3φ, 3.7KW
φ 230 * 600
350 : 210 : 105
1 : 1.6 : 2.5
13.6 ~ 54.6
5 ~ 20
1100 x 1200 x 1300
1200
220/380V, 3φ, 7.5KW
Lab scale Product scale
PASTE MIXER26
FEATURE
Wide range of viscosity
No agitator
Compacted size
Easy control system and operation
Mounted electronic scale(optional)
1
2
3
4
5
Paste mixer is used for mixing wide range of viscosity without agitator and it has high speed of rotation and orbital as same time which it make
good a result of homogenization and mixing.
High speed of rotation and orbital makes high acceleration of gravity and it make good result of mixing in a short time.
PASTE MIXER
27
COMPARING WITH AGITATOR AND PASTE MIXER
SAMPLE TEST
Mixing Volume
Acceleration of gravity (G)
Orbital speed (rpm)
Rotation speed(rpm)
Time setting
Weight(kg)
Demension (W x D x H)
Operating conditions
Power supply
Safety interlocks
Vauum
PM-150D PM-150DV PM-370D PM-370V PM-500D
150 ml x 2 bottles
420
~1000
200~2000
24
351 x 412 x 432
28
421 x 471 x 487
65
-
70
-
35
-
150 ml x 2 bottles
420
~1000
200~2000
500 ml x 2 bottles
300
~ 400
200~1000
370 ml x 2 bottles
400
~1000
200~2000
370 ml x 2 bottles
420
~1000
200~2000
5 ~ 35℃, 35 ~ 85% RH (without condensationals)
220V AC, 1-Phase, 50/60Hz
Door / Vibration / Rotation sensor, Emergency stop switch
EPOXY RESIN + CaCO3 particle
AGITATOR PASTE MIXER
AGITATOR PASTE MIXER
1000rpm
30sec
1000rpm
60sec
AGITATOR PASTE MIXER
1000rpm
30sec
GREASE 49G : PAINT 1G
AGITATOR PASTE MIXER
1000rpm
30sec
EPOXY RESIN + CALCIUM CARBONATE
0 sec ~ 99 min
V -- V -
FlimGlass Acrylic
Recycle system: filtering used abrasive substance and fill into the pressure vessel.
High pressure pump: To generate high pressure to make abrasive and water into jet stream.
3axis stage system: To cut products into required form.
Abrasive Suspension Water-jet28
Cutting Zig
High Pressure Pump
Abrasive Recycle
Cutting Stage
Impact
Nozzle
Material
Abrasive Water
Hoper Unit
High pressure valve
High pressure pump
PumpPump
Filtering
Unit
Nozzle
High pressure valve
Pressure Vessel Catch Tank
Drain
SAMPLE TEST
PRINCIPLE
SD CARDSD CARD PCB GLASS, ACRYLIC
Router Waterjet
Year/Month : 2006/06
Client : OTTUGI
Purpose : sesame oil extraction
Spec : 400bar, 80℃
Supercritical CO2 extraction system
Year/Month : 2009/10
Client : LG CHEMICAL
Purpose : Nano powder production
Spec : 400bar, 450 ℃
Supercritical Hydrothermal Synthesis system
Pressure Vessel
Year/Month : 2012/10
Client : KIMM
Purpose : Steam Generator & Stroage
Spec : 200bar, 365 ℃
Control Element Drive Mechanism (CEDM)
Year/Month : 2008/10
Client : DOOSAN
Purpose : Performance test loop system
Spec : 160bar, 345 ℃
Hydrogenation Catalyst Process System
Year/Month : 2013/01
Client : NEUROPID
Purpose : High added-value powder production
Spec : 200bar, 80 ℃
Hydrothermal Carbonization Process System
Year/Month : 2014/5
Client : S 화학회사
Purpose : High Temperature Cabonization
Spec : 100bar at 260°C
Hydrothermal Synthesis synthetic resins System
Year/Month : 2015/1
Client : SOGANG UNIVERSITY
Purpose : Synthesis Synthetic resin
Spec : 100bar at 260°C
PLANT 29
Extraction
Drying
Others
Forming
Lamination
Sterilization for food
Hydrothermal synthesis
Reaction
SUPERCRITICAL CARBON DIOXIDE EXTRACTION SYSTEM
Extractor
Seperator 1,2
CO2 Flow rate
Co-Solvent flow rate
500bar / 80℃ (300ml)
100bar / 80℃
70ml/min
Max. 24ml/min
ISOSTATIC PRESS
Max. Operating Pressure
Temperature
Max. Flow rate
Volume
6000bar
RT ~ 80℃
I,D 50mm X I.L 200mm
300ml
HIGH PRESSURE REACTOR
Max. Operating Pressure
Temperature
Size(Volume)
Type
200bar
230℃
I.D 60mm X I.L 170mm
Stirred type
In order to make requirement and satisfaction to customers, engineers in R&D team are providing the test service always.
TEST SERVICE30
1
2
3
1
2
3
1
2
Inquiry Schedule Test Report
with data
TEST SERVICE
31
Dispersion
Emulsion
Disruption
HIGH PRESSURE HOMOGENIZER
Max. Operating Pressure
Max. Flow rate
Pump system
1500bar
100ml/min
Motor driven type
1
2
3
Dispersion
Emulsion
Rupture
HIGH PRESSURE HOMOGENIZER
Max. Operating Pressure
Max. Flow rate
Pump system
1500bar
100ml/min
Motor driven type
1
2
3
Disruption
Dispersion and mixing
THREE ROLL MILL
Dimension
Roller
Power
Roller materials
Ratio
310(W) X 450(D) X 300(H)
Φ50 * 150l
220VAC
Alumina, Stainless steel
3.6:1.8:1
1
2
Dimension
Capacity
Rotation
Cup volume
Power
330(W) X 410(D) X 430(H)
700g * 2cup
Rotation 2,000rpm / Revolution 1000rpm
500ml
220VAC, 300W
Disruption
Dispersion and mixing
Homogenization
PASTE MIXER
1
2
3
Dimension
Hopper capacity
Flow rate
Motor
1400(W) X 650(D) X 1000(H)
40 L
4,000L/hr (@3500rpm)
5HP (Max. 3500rpm)
Disruption
Dispersion and mixing
Homogenization
INLINE MIXER
1
2
3
1503-Total Cat.- EN -Ver.3-01
We make your idea possible
ILSHIN AUTOCLAVE CO.,LTD
255,Techno 2-ro,Yuseong-gu, Daejeon, Korea (Daedeok techno valley)
Tel: +82-42-931-6100 Fax: +82-42-935-6103 Homepage: www.suflux.com E-mail: webmaster@suflux.com

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Pressure vessel and reactor solutions

  • 1. Pressure oven High pressure reactor Pressure vessel Isostatic press Agitator(Magnedrive) Nano disperser & Micro disperser Supercritical carbon dioxide system High shear mixer ( Homo mixer, Inline mixer, Ultra high shear nozzle ) Paste mixer Three roll mill Plant Waterjet www.suflux.com
  • 2. Overview High pressure reactor Pressure oven Isostatic press Pressure vessel Supercritical carbon dioxide system Agitator(Magnedrive) High shear mixer ( Homo mixer, Inline mixer, Ultra high shear nozzle ) Nano disperser & Micro disperser Three roll mill Paste mixer Waterjet Plant Test Service 03 04 - 05 06 - 07 08 - 09 10 - 11 12 - 15 16 17 - 19 20 - 23 24 - 25 26 - 27 28 29 30 - 31 Contents
  • 3. ISO9001 ISO14001 SELS STAMP STAMPU STAMPU2 History Certification ASME ASME ASME 03 Found ENGINEERING Developed products Autoclave system Magnedrive Hot plate press High temperature & pressure test loop system Incorporated as ILSHIN AUTOCLAVE CO.,LTD, ISA/KSA9001, 14001 Established an annexed research institue The building and factory were moved to Daeduck techno valley Developed products Nano Disperser (High pressure homogenizer) Isostatic press ( CIP /WIP /HPP) Supercritical water oxidization device for non-resolvable materials Aerogel supercritical drying system Supercritical degreasing system Supercritical extraction system for mass production Supplied commercial purpose of SC-CO2 extraction system (to Otoogi foods Co., , Korea ginseng corp. ) 1990’s 1993 1993~1999 2001 2002 2009 2001~2009 2000’s 2010’s Won the grand prize in safety certification part from KOSHA and MOEL ASME stamp 'S', 'U', 'U2' renewal, SEL certification ( China Special Equipment License ) Nano disperser awarded in "NANO KOREA 2013 AWARD", 'GOOD DESIGN", "IT INNOVATION" iF DESIGN AWARD in Germany ( Nano Disperser) Developed products Pilot scale of supercritical water system (LG chem) Industrial scale of supercritical extraction system (JNBC) Waterjet Nano disperser for high capacity High shear mixer 3 roll mill / Paste mixer 2011 2012 2013 2014 2010~2014 SUFLUX means our brand for components produced by ourselves for high pressure and temperature control. It is a compound word of super and flux. SUFLUX stands for "high value and continuous effort to make it changed", thus providing high quality and reliable performance. Our continuous effort to make innovative products is included in SUFLUX. Overview - ‘ILSHIN AUTOCLAVE's brand
  • 4. ASME S STAMP ASME U STAMP ASME U2 STAMP SEL Agitator Seal type (O-ring/gasket) Port(Inlet/Outlet) Thermocouple Pressure Vessel Liner FEATURE CERTIFICATION 18 HIGH PRESSURE REACTOR04 It has diverse applications which are hydrothermal and decomposition, sublimation, extraction in laboratory by high pressure and temperature with various optional device. 1 2 3 Bench top type Multi-purpose system Hydrothermal synthesis Reaction system for polymerization (Customized) Reaction system for hydride (Customize) Reaction system with catalyst (Customized) t ith t l t Temperature(℃ ) Pressure(㎏/㎠) Volume(ℓ) Pressure vessel based on ASME Various size and pressure & temperature Various optional device for easy maintenance - Agitator, upload / lift system, etc..
  • 5. Guide of option PTFE or Stainless steel Liner Belt driven or Motor driven (direct with magnetic coupling) Adjustable speed 0~1700 rpm Touch screen for control/monitor Heat insulated jacket on cover Up&down of body by air cylinder Front&rear of body by air cylinder Front&rear of body by air cylinder Analog pressure gauge Digital pressure transmitter 05 HIGH PRESSURE REACTOR Reactor for Self-propagation (Customized) Reactor with rotation (Customized) Reaction system for thermal decomposiotion (Customized) Reaction system for blasting (Customized) Reaction system with ultra high temperature & pressure (Customized) Reaction system with continuous operation (Customized) Stirrer parts Cover & Body
  • 6. It has application for lamination and to remove voids both layers in industries of touch panel and LCD, PDP, semi conductor. Effect of removing voids by pressure and temperature Effect of hardness by temperature Effect of adhesive strength by pressure Solderball Top and Bottom Die Die Attach Film/Paste Air Bubbles (기포) Dieelectric Before After Before After Before After Mold Cap FR-5 Substrate Silicon ICEpoxy Undrfill Air Bubbles Solder Ball (63Sn/37Pb) Bubble Pressure curing oven06 Completed lamination and removed voids TPVB or EVA film Glass 1 2 3 Clutch Door Chamber Touch Screen Pressure gauge (Seal / Inlet / Chamber) Three color light Glass (GA) Touch panel screen, Film (FA) ass GA) panel screen, m (FA) Semiconductor of package process (HA)
  • 7. Parts of system FEATURE CONSIDERATION TO ORDER Main O-ring To seal cover Heating & Cooling Internal air circulation To pressurize the vessel Pressure curing oven 07 M/D Air circulation Cooling system Heater Main O-ring Heater and cooling coil Fan and motor Booster Compacted size Reasonable price Durability BoosterAward for safety Internal air flow Before sealed cover After sealed cover Uniformity : +/-3deg C Size (A, B)1 1 2 3 Pressure2 Temperature3 Cooling4 Booster or compressed air5 Gas media (Air or gas )6 A B B
  • 8. ISOSTATIC PRESS The mold by isodirectional force Lamination The sterilization by high pressure It has the technology of isodirectional force with solvent liquid inside pressure vessel by high pressure. There are applications of lamination in electronic industry and sterilization in food industry, etc.. 08 11 2 1 2 1 2 Customized system (Size, operating process) Design according to ASME, CSEL Wire Wounding Reasonable price Rapid response Easy operation Easy maintenance CIP (Cold Isostatic Press) Laboratory Laboratory Production Production Laboratory Production WIP (Warm Isostatic Press) Engineering FIP (Food Isostatic Press) Technology Competitiveness Convenience FEATURE
  • 9. 1 2 3 4 5 6 1 2 3 4 5 6 Pin Closing Type It has many different high pressure depending on application of metal forming process, electrical parts, food. CIP series WIP series FIP series Custom Custom Custom OIL / WATER OIL / WATER OIL / WATER 0 ~ 6000 bar 0 ~ 6000 bar 0 ~ 6000 bar RT 50 - 120 ℃ RT - 80 ℃ COLD ISOSTATIC PRESS Macromolecule, Ceramic, Metal, Carbon, etc. MLCC, LTCC, multi other chips Fruit juice, Sea food, etc. CIP series WARM ISOSTATIC PRESSWIP series FOOD ISOSTATIC PRESSFIP series ISOSTATIC PRESS 09 Pressure : ~1000 bar Temperature : RT ~80 ℃ Volume : ~ Custom Air Driven Liquid Pump / Hydraulic Pump O-ring /U-packing / Energizer seal CIP /WIP Pressure : ~4000 bar & Custom Temperature: RT ~120 ℃ Volume : ~ 100L & Custom Air Driven Liquid Pump / Hydraulic Pump O-ring / U-packing CIP / WIP / Laboratory FIP Pressure : ~6000 bar Temperature : ~RT Volume : ~ 200L & Custom Hydraulic Pump O-ring Seal /U-packing / Energizer seal CIP / FIP (Wire wounding) Model PRESSURE INTERNAL DIAMETER WORKING MEDIA TEMPERATURE Pin Clos C-clamp Type Press frame closing type 1 2 3 4 5 6 ng type
  • 10. Pressure Vessel Industrial scale & Customized pressure vessel Reactor for reaction or special purpose Wide rage of material and optional close method for the use of environment in industries of chemical and pharmaceuticals, others. 350 ℃ 250 ℃ 350 ℃ 250 ℃ 300 bar 50 bar 700 bar 200 bar BV series CV series PV series VCV series Bolt Closure type Cap Closure type Plug & Cap Closure type View Cell O-ring/Teflon/Metal O-ring O-ring/Teflon Urethane/O-ring/Teflon O / X X O / X O / X Steam generator Reactor for external pressure test Reactor for micro-organisms Heater exchanger MODEL METHOD OF CONTRACT TEMPERATURE PRESSURE SEAL TYPE AGITATION FEATURE Pressure vessel based on ASME Optional gas line depending on required gas. Customized service ASME S STAMP ASME U STAMP ASME U2 STAMP SEL CERTIFICATION 10 1 2 3 ILSHIIN AUTOCALVE is providing many different size of pressure vessel. Depending on application and customer's requirement, it's available many different size with high pressure and temperature, optional diveces.
  • 11. Pressure vessel 11 BV TYPE (BOLT CLOSURE PRESSURE VESSEL) Basic type Sealed by bolts(Screws) Easy to make tubing and ports. 1 2 3 CV TYPE (CAP CLOSURE PRESSURE VESSEL) Easy to open and close cover PTFE liner PV TYPE (PLUG TYPE PRESSURE VESSEL) 1 2 Easy to open and close cover Sealed for high pressure and temperature 1 2 VCV TYPE (VIEW CELL PRESSURE VESSEL) Quick to open and close1 QCQ TYPE (QUICK CLAMP CLOSURE PRESSURE VESSEL) Quick to open and close For high pressure maximum 6000bar 1 2 QCP TYPE (PIN CLOSURE PRESSURE VESSEL) Quick to open and close For high pressure maximum 6000bar 1 2 QCY TYPE (YOKE FLAME CLOSURE PRESSURE VESSEL) Easy to open and close For high pressure maximum 6000bar 1 2
  • 12. SUPERCRITICAL CARBON DIOXIDE FLUID SYSTEM12 It has application of extraction and drying system by technology of supercritical point with carbon dioxide. Supercritical making nano-particle system Supercritical degreasing system Supercritical extraction system Supercritical expansion system Supercritical drying system Critical Point Pressure Temperature Supercritical Fluid Solid Phase Liquid Phase Gaseous Phase Liquid and gas Increasing Supercrtical condition Density of gas & liquid Supercritical CO2 + Oil Liquid CO2 Gas CO2 Gas CO2 Supercritical CO2 Extractor Chiller CO2 Reservoir PumpHeater Control valve Control Valve Seperator Extract yield Pressure vessel based on ASME Eco-friendly For high quality production Supercritical Fluid GAS LIQID High diffusion coefficient Low viscosity Low surface tension High density High solubility FEATURE
  • 13. [C-Clamp type] [Yoke frame type] BPR (Back Pressure Regulator) Extractor Extractor Reservoir Reservoir Heater Separator Separator Pump for co-solvent Touch Screen CO2 Pump CO2 Pump Chiller Hydraulic unity Extractor : Yoke frame / C-clamp type Reservoir Condenser High pressure pump Pre heater SUPERCRITICAL CARBON DIOXIDE FLUID SYSTEM SUPERCRITICAL CARBON DIOXIDE FLUID SYSTEM 13 Pressure Gauge Separator [Cover type] [Open type] Main pressure vessel for extraction with supercritical condition Yoke, clamp close/open type Operated by hydraulic unit Process to break supercritical condition. To get extract yield For storage/recycle of CO2 in liquid Cooling device to make CO2 to liquid High pressure pump system of intensifier type by hydraulic unit Heating device to make temperature for supercritical condition
  • 14. Lab. Scale Pilot Scale Product Scale 30 - 80 ℃ 30 - 80 ℃ 30 - 80 ℃ Custom Custom Custom 0.3 ~ 2 ℓ 5 ~ 50 ℓ Custom Solid & liquid Solid & liquid Solid & liquid 14 SUPERCRITICAL CARBON DIOXIDE FLUID SYSTEM SUPERCRITICAL EXTRACTION SERIES VOLUME MAX. PRESSURE MAX.TEMPERATURE RAW MATERIAL PHASE Debinding system Debinding system EXTRACTOR : 100 ℓ X 2 uints WORKING PRESSURE : 250 bar EXTRACTOR : 100 ℓ X 2 uints WORKING PRESSURE : 700bar To extract the sesame oil To de-grease the pernicious ingredients EXTRACTOR : 2300 ℓ X 3 uints WORKING PRESSURE : 450 bar EXTRACTOR : 600 ℓ X 2 uints WORKING PRESSURE : 460bar Available custom size and specification
  • 15. The graph of density depending on pressure and temperature The graph of extract time depending on pressure. X100 TO EXTRACT OIL TO EXTRACT OIL SUPERCRITICAL CARBON DIOXIDE FLUID SYSTEM 15 TEST SERVICE Product Extract yield Condition Pressure (㎏/㎠) Temperature (℃) 300~500 bar 300~500 bar 300~450 bar 300~450 bar 300~450 bar 200~400 bar 400~500 bar 300~500 bar 400~500 bar 200~350 bar 200~350 bar 100~300 bar 200~350 bar 400~500 bar 300~400 bar 350~400 bar 200~350 bar 300~400 bar 150~200 bar 200~300 bar 300~500 bar sesame corn germ seed soybean rape blossoms seeds sunflower seeds paprika castor grape seeds red pepper seed coffee green tea iris medicinal herbs rice bran raspberry turmeric citron yolk fish oil camellia oil Bija 40~60 ℃ 40~60 ℃ 40~60 ℃ 40~60 ℃ 40~60 ℃ 40~50 ℃ 40~60 ℃ 40~60 ℃ 50~60 ℃ 40~60 ℃ 40~60 ℃ 40~50 ℃ 40~60 ℃ 55~60 ℃ 50~60 ℃ 55~60 ℃ 45~50 ℃ 40~60 ℃ 40~60 ℃ 40~60 ℃ 50~60 ℃ 40 % 35 % 15 % 25 % 34 % 6 % 25 % 8 % 20 % 7 % Cosolvents 6 % Cosolvents 10 % 15 % 10 % Incense component 30 % Deodorization Deodorization 20 %
  • 16. AGITATOR16 The graph of extract time depending on pressure. MDB - Thread Type MDD - Thread Type MDD - Flange Type MDB - Flange Type MDB series MDD series 1000~8000 psi 1000~8000 psi Thread/ Flange Type Thread/ Flange Type Φ 5~50 Φ 5~50 MDB series MDD series SERIES SHAFT DIAPRESSURE TYPE
  • 17. HIGH SHEAR MIXER 17 We're providing a solution for dispersion and mixing by using high shear system which are Homo mixer, Inline mixer, Ultra high shear nozzle High pressure homogenizer (NLM100, NH series) less than 10,000 cp High shear mixer ( homo mixer, inline mixer ) less than 70,000 cp 3RollMill, Paste mixer less than 200,000 cp To save time and To reduce cost 원료 The existing process Heating & Mixing Pre Mixing In-line Mixing Packing PackingCooling & Mixing High shear mixer process Difference 9 hours 6hr 6hr 12hr 1hr 2hr 3hr Water 1 cp 15,000 cp 30,000 cp 45,000 cp 200,000 cp70,000 cp Milk Kerosene Honey Glue Mayo Ink/Paint Mustard Paste RANGE OF VISCOSITY (EXAMPLE) Pre mixer (Agitator) less than 100,000 cp
  • 18. 18 FLOW DIRECTION FLOW DIRECTION HIGH SHEAR MIXER High shear homo-mixer is driven by high speed motor (max. 8,000rpm) and it's a specially designed nozzle and this precision machined nozzle offers great versatility by allowing any machine to perform a wide range of mixing operation. HIGH SHEAR HOMO-MIXER Depending on customer's application, it's providing diverse system. HIGH SHEAR INLINE MIXER Blade shaft Stator guide Stator Rotor Stator Rotor OUTLET INLET PORT MOTOR ROTATOR SHAFT ROTOR BLADE HOUSING
  • 19. 19 Ultra high shear nozzle makes highest shear force and highest cavitation by consisting multi-stage nozzle. Precise stator as fineness holes Suitable for emulsion application TYPE SYSTEM TYPE Combination type HIGH SHEAR MIXER SUPER HIGH SHEAR INLINE MIXER Chamber type Nozzle type Cone type Arched rotator and stator Suitable for emulsion/homogenization/dispersion Precise stator as fineness holes Suitable for emulsion application Cylindrical shape of rotator Suitable for emulsion/homogenization/dispersion Liquid + Additive Next Process Next Process Liquid + AdditiveAdded hopper Next Process Liquid + Additive Basic Optional agitator Optional added hopper
  • 20. Pressure GaugeHigh Pressure Pump Inlet Before After Outlet Heat Exchanger SHEAR FORCECAVITATION IMPACT Particle Size Reduction Emulsions Suspensions Liposomes Cell Disruption E-coil Yeast Nano-Encapsulation Polymers Liposomes Emulsions Nano Disperser make dispersion of particle passing through the nozzle chamber with ultra high pressure and there are force of impact, cavitation and share stress in the nozzle chamber. It used in applications of chemical, food, cosmetics, petroleum and paints. HIGH PRESSURE HOMOGENIZER20 NANO DISPERSER VS MICRO DISPERSER NANO DISPERSER Dia chamber Adjustable valve Dispersion Emulsion Chemical, Electronic parts Food, Cosmetic Ultra high pressure High pressure Nozzle Chamber MICRO DISPERSER NOZZLE MAIN APPLICATION MAIN INDUSTRY PRESSURE
  • 21. Motor driven and single piston Air vent valve One Stage Valve Two Stage Valve Adjustable pressure b y motor speed Motor driven and single piston Adjustable pressure by motor speed Cooling tank after process HIGH PRESSURE HOMOGENIZER 21 MICRO DISPERSER(MLM100) NANO DISPERSER (NLM100) Operating Pressure Flow rate Pump system Inlet reservoir Dimension Weight Max. 1,500bar Max. 100ml/min Motor driven type [ 220VAC, 1PH, 60Hz, 1HP ] 300ml 490(D) x 580(W) x 445(H)mm Approx. 40kg NLM100-Z75 NLM100-Y75 100 ml / min 100 ml / min 1500 bar 1500 bar 75 um 75 um Z type Y type Max Pressure Size Interaction Chamber Type Flow RateFlow Rate Operating Pressure Flow rate Pump system Inlet reservoir Dimension Weight Max. 2,000bar Max. 100ml/min Motor driven type [ 220VAC, 1PH, 60Hz, 1HP ] 300ml 490(D) x 450(W) x 300(H)mm Approx. 35kg 100 ml / min 1500 bar Variation 2 Stage vlave Max Pressure Size Interaction Chamber Type Flow Rate
  • 22. Back flushing system Cooling tank after process Protective case Adjustable pressure by hydraulic unit HIGH PRESSURE HOMOGENIZER 22 NANO DISPERSER (NH 500) NANO DISPERSER (NH 4000) Operating Pressure Flow rate Pump system Inlet reservoir Dimension Weight Max. 2,000bar Max. 500ml/min Hydraulic unit system 2000ml 800(D) x 850(W) x 1500(H)mm Approx. 300kg 500ml/min 2000 bar 100um Z type / Y type Max Pressure Size Interaction Chamber Type Flow Rate Operating Pressure Flow rate Pump system Inlet reservoir Dimension Weight Max. 2,000bar Max. 100ml/min Motor driven type [ 220VAC, 1PH, 60Hz, 1HP ] 300ml 490(D) x 580(W) x 445(H)mm Approx. 40kg Solution tank to prevent the solidification Monitor and Alarm system Cooling line on high pressure part Back flushing system NH8000 NH2000 NH2000 NH4000 NH8000 2l / min 4l / min 8l / min 2000 bar 2000 bar 2000 bar 200, 400um 200, 400um 200, 400um Z / Y type Z / Y type Z / Y type Max Pressure Size Interaction Chamber Type Flow RateSeries
  • 23. HIGH PRESSURE HOMOGENIZER 23 Emulsion Rupture Dispersion AFTERBEFORE Product Number of pass Effect Milk Soybean milk, CNT Water + Oil CERAMIC(Si) TiO3 Graphite(Carbon) CeO2 raw materials for cosmetics Pigment a high molecular substance Al2O3 Dispersion Homogenization Dispersion Suavity Dispersion Crushed Crushed Dispersion Suavity Dispersion Crushed Dispersion 1800 bar [1 pass] 2000 bar [5 pass] 2000 bar [3 pass] 2500 bar [5 pass] 2000 bar [5 pass] 2500 bar [3 pass] 2000 bar [3 pass] 2500 bar [3 pass] 1000 bar [3 pass] 2500 bar [3 pass] 2500 bar [3 pass] 2000 bar [3 pass]
  • 24. Three roll mill is a machine that uses shear force created by three horizontally positioned rolls rotating in opposite directions and different speeds relative to each other, in order to mix, refine, disperse, or homogenize viscous materials fed into it. FEATURE Precise roll Materials of roll Heating/Cooling system Adjustable micro gap Adjustable speed Minimized noise and vibration Stainless steel / Ceramic / Alloy steel THREE ROLL MILL24 1 2 3 4 5 MICRO GAP SHEAR FORCE & PRESSURE Transmission ration After Scraper Before Shear gap 1 V 1 << V2 << V3 Shear gap 2 Specimen Draw-in roll Middle roll Scrapper roll Draw in roll Middle roll Scraper roll 1 : 3 1 : 3 1 : 9 1 : 3 : 9 Shear Gap(Elinination size) V1 V1 < V2 V2 V1 V2 1 1 3 3 2 2
  • 25. THREE ROLL MILL 25 Alarm Gap control knob End plate Draw-in roll Middle roll Scraper roll Control part Roll size (mm) Roll speed (RPM) Roll ratio Throughput (LPH) Gap (micron) Size (W x D x H) Weight (Kg) Electrical power TRM 50 Model Lab scale Product scale TRM 80 TRM 145 TRM 230 φ 50 * 150 533 : 213 : 85 1 : 2.5 : 6.25 0.2 ~ 6 2 ~ 50 340 x 290 x 300 20 220V, 200W φ 80 * 250 600 : 200 : 67 1 : 3 : 9 0.5 ~ 12 2 ~ 20 550 x 450 x 600 65 220V, 750W φ 145 * 360 350 : 210 : 105 1 : 1.6 : 2.5 5.1 ~ 20 5 ~ 20 810 x 690 x 900 650 220/380V, 3φ, 3.7KW φ 230 * 600 350 : 210 : 105 1 : 1.6 : 2.5 13.6 ~ 54.6 5 ~ 20 1100 x 1200 x 1300 1200 220/380V, 3φ, 7.5KW Lab scale Product scale
  • 26. PASTE MIXER26 FEATURE Wide range of viscosity No agitator Compacted size Easy control system and operation Mounted electronic scale(optional) 1 2 3 4 5 Paste mixer is used for mixing wide range of viscosity without agitator and it has high speed of rotation and orbital as same time which it make good a result of homogenization and mixing. High speed of rotation and orbital makes high acceleration of gravity and it make good result of mixing in a short time.
  • 27. PASTE MIXER 27 COMPARING WITH AGITATOR AND PASTE MIXER SAMPLE TEST Mixing Volume Acceleration of gravity (G) Orbital speed (rpm) Rotation speed(rpm) Time setting Weight(kg) Demension (W x D x H) Operating conditions Power supply Safety interlocks Vauum PM-150D PM-150DV PM-370D PM-370V PM-500D 150 ml x 2 bottles 420 ~1000 200~2000 24 351 x 412 x 432 28 421 x 471 x 487 65 - 70 - 35 - 150 ml x 2 bottles 420 ~1000 200~2000 500 ml x 2 bottles 300 ~ 400 200~1000 370 ml x 2 bottles 400 ~1000 200~2000 370 ml x 2 bottles 420 ~1000 200~2000 5 ~ 35℃, 35 ~ 85% RH (without condensationals) 220V AC, 1-Phase, 50/60Hz Door / Vibration / Rotation sensor, Emergency stop switch EPOXY RESIN + CaCO3 particle AGITATOR PASTE MIXER AGITATOR PASTE MIXER 1000rpm 30sec 1000rpm 60sec AGITATOR PASTE MIXER 1000rpm 30sec GREASE 49G : PAINT 1G AGITATOR PASTE MIXER 1000rpm 30sec EPOXY RESIN + CALCIUM CARBONATE 0 sec ~ 99 min V -- V -
  • 28. FlimGlass Acrylic Recycle system: filtering used abrasive substance and fill into the pressure vessel. High pressure pump: To generate high pressure to make abrasive and water into jet stream. 3axis stage system: To cut products into required form. Abrasive Suspension Water-jet28 Cutting Zig High Pressure Pump Abrasive Recycle Cutting Stage Impact Nozzle Material Abrasive Water Hoper Unit High pressure valve High pressure pump PumpPump Filtering Unit Nozzle High pressure valve Pressure Vessel Catch Tank Drain SAMPLE TEST PRINCIPLE SD CARDSD CARD PCB GLASS, ACRYLIC Router Waterjet
  • 29. Year/Month : 2006/06 Client : OTTUGI Purpose : sesame oil extraction Spec : 400bar, 80℃ Supercritical CO2 extraction system Year/Month : 2009/10 Client : LG CHEMICAL Purpose : Nano powder production Spec : 400bar, 450 ℃ Supercritical Hydrothermal Synthesis system Pressure Vessel Year/Month : 2012/10 Client : KIMM Purpose : Steam Generator & Stroage Spec : 200bar, 365 ℃ Control Element Drive Mechanism (CEDM) Year/Month : 2008/10 Client : DOOSAN Purpose : Performance test loop system Spec : 160bar, 345 ℃ Hydrogenation Catalyst Process System Year/Month : 2013/01 Client : NEUROPID Purpose : High added-value powder production Spec : 200bar, 80 ℃ Hydrothermal Carbonization Process System Year/Month : 2014/5 Client : S 화학회사 Purpose : High Temperature Cabonization Spec : 100bar at 260°C Hydrothermal Synthesis synthetic resins System Year/Month : 2015/1 Client : SOGANG UNIVERSITY Purpose : Synthesis Synthetic resin Spec : 100bar at 260°C PLANT 29
  • 30. Extraction Drying Others Forming Lamination Sterilization for food Hydrothermal synthesis Reaction SUPERCRITICAL CARBON DIOXIDE EXTRACTION SYSTEM Extractor Seperator 1,2 CO2 Flow rate Co-Solvent flow rate 500bar / 80℃ (300ml) 100bar / 80℃ 70ml/min Max. 24ml/min ISOSTATIC PRESS Max. Operating Pressure Temperature Max. Flow rate Volume 6000bar RT ~ 80℃ I,D 50mm X I.L 200mm 300ml HIGH PRESSURE REACTOR Max. Operating Pressure Temperature Size(Volume) Type 200bar 230℃ I.D 60mm X I.L 170mm Stirred type In order to make requirement and satisfaction to customers, engineers in R&D team are providing the test service always. TEST SERVICE30 1 2 3 1 2 3 1 2 Inquiry Schedule Test Report with data
  • 31. TEST SERVICE 31 Dispersion Emulsion Disruption HIGH PRESSURE HOMOGENIZER Max. Operating Pressure Max. Flow rate Pump system 1500bar 100ml/min Motor driven type 1 2 3 Dispersion Emulsion Rupture HIGH PRESSURE HOMOGENIZER Max. Operating Pressure Max. Flow rate Pump system 1500bar 100ml/min Motor driven type 1 2 3 Disruption Dispersion and mixing THREE ROLL MILL Dimension Roller Power Roller materials Ratio 310(W) X 450(D) X 300(H) Φ50 * 150l 220VAC Alumina, Stainless steel 3.6:1.8:1 1 2 Dimension Capacity Rotation Cup volume Power 330(W) X 410(D) X 430(H) 700g * 2cup Rotation 2,000rpm / Revolution 1000rpm 500ml 220VAC, 300W Disruption Dispersion and mixing Homogenization PASTE MIXER 1 2 3 Dimension Hopper capacity Flow rate Motor 1400(W) X 650(D) X 1000(H) 40 L 4,000L/hr (@3500rpm) 5HP (Max. 3500rpm) Disruption Dispersion and mixing Homogenization INLINE MIXER 1 2 3
  • 32. 1503-Total Cat.- EN -Ver.3-01 We make your idea possible ILSHIN AUTOCLAVE CO.,LTD 255,Techno 2-ro,Yuseong-gu, Daejeon, Korea (Daedeok techno valley) Tel: +82-42-931-6100 Fax: +82-42-935-6103 Homepage: www.suflux.com E-mail: webmaster@suflux.com