This document summarizes an experiment to optimize biodiesel production from palm oil through a transesterification reaction. The experiment tested varying amounts of palm oil, methanol, and potassium hydroxide catalyst. The highest biodiesel yield of 55.4 ml was obtained with 60 ml palm oil, 12 ml methanol, and 2 grams of KOH catalyst. Regression analysis was performed on the results to obtain an equation correlating biodiesel production to catalyst amount. Upcoming work will vary temperature and stirrer speed to further optimize the process.