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Designation: C 1012 – 034
GROUP MEMBERS; 
SAFIULLAH(13ce07) 
NASIR ALI(13ce32) 
SECTION; A 
SUBMITTED TO; ENGG SOHAIL SALEH 
DEPARTMENT; CIVIL
Sequence of Presentation 
 Scope 
 Significance and Use 
 Apparatus 
 Reagents and Materials 
 Procedure 
 Calculation 
 Report 
 Keywords
Scope 
 This test method covers the determination of length 
change of mortar bars immersed in a sulfate 
solution. 
 The values stated in SI units are to be regarded as 
the standard. 
 This standard does not purport to address all of the 
safety concerns, if any, associated with its use.
Significance and Use 
 This test method provides a means of assessing the 
sulfate resistance of mortars and blended hydraulic 
cements. 
 The standard exposure solution used in this test 
method, may be used to simulate the environmental 
exposure of interest.
Apparatus 
(a) 
(b) 
(c) 
(d) 
(f ) 
 Mixer. (a) 
 Cube Molds, (b) 
 Bar Molds. (c) 
 Comparator, (d) 
 Containers, (e) 
 Curing Tank, (f )
4. Reagents and Materials 
 USP or technical grade chemicals may be used. 
 Sodium Sulfate (Na2SO 4) 
 Sulfate Solution 
 Graded Standard Sand. 
 Stainless Steel Gage Studs .
Procedure 
 Molding and Initial Curing of Specimens—Mold the 
test bars and the cubes in accordance with Test. A set of 
specimens to test one cement consists of 6 bars and up 
to 21 cubes .after molding, cover the molds, and place 
the mold in the curing tank in water at 35 6 3°C for 23 h 
30 min. Place the sealed molds in the curing tank. 
remove molds from tank and demold the specimens.
Subsequent Curing and Preparation for Test; 
 store all bars in a curing tank of saturated limewater. 
Break two cubes if the mean strength is 2850 psi or 
more place all the bars in the sulfate solution. 
If it is less than 2850 psi store all the demold cubes and 
bars in the curing tank and test additional cubes 
When reach to 2850 psi record comparator readings and 
place all the bars in the sulfate solution
Measurements of Length Change: 
 At 1, 2, 3, 4, 8, 13, and 15 weeks after the bars are placed in the 
sulfate solution, test them for length change. Review the data at 15 
weeks. If uniform length change is taking place, make the next 
subsequent measurements at a minimum of 4, 6, 9, and 12 
months. When the expansion is changing rapidlybmeasure the 
bars at 4, 6, 9, 12, 15, and 18 months
Calculation 
 10.1 Calculate the length change at any age as follows: 
DL=[(Lx – Li)/Lg] 100 
 where: 
DL = change in length at x age, %, 
L x = comparator reading of specimen at x age 
L i = initial comparator reading of specimen-reference bar 
comparator reading, at the same time 
Lg = nominal gage length, or 250 mm (10 in.) as applicable. 
 Calculate length change values for each bar to the nearest 0.001 
% and report averages to the nearest 0.01 %.
Report 
 Report type of cement, and, if blending material is used, 
its identification and amount and whether cement and 
blending material, if used, meet the applicable 
specifications. Report the initial comparator reading of 
each bar at the time of immersion in sulfate solution; 
this is the base value for calculation of length changes. 
Report the subsequent length changes in percent of base 
value to the nearest 0.001 % for individual bars and the 
nearest 0.01 % for averages.
Keywords 
 acceptability; expansion; fly ash; mortars; pozzolans; 
precision; search report; slag; sulfate attack; sulfate-resisting 
cements; tests
Standard test method for length change of hydraulic cement mortars exposed to a sulfate solution

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Standard test method for length change of hydraulic cement mortars exposed to a sulfate solution

  • 1.
  • 3. GROUP MEMBERS; SAFIULLAH(13ce07) NASIR ALI(13ce32) SECTION; A SUBMITTED TO; ENGG SOHAIL SALEH DEPARTMENT; CIVIL
  • 4. Sequence of Presentation  Scope  Significance and Use  Apparatus  Reagents and Materials  Procedure  Calculation  Report  Keywords
  • 5. Scope  This test method covers the determination of length change of mortar bars immersed in a sulfate solution.  The values stated in SI units are to be regarded as the standard.  This standard does not purport to address all of the safety concerns, if any, associated with its use.
  • 6. Significance and Use  This test method provides a means of assessing the sulfate resistance of mortars and blended hydraulic cements.  The standard exposure solution used in this test method, may be used to simulate the environmental exposure of interest.
  • 7. Apparatus (a) (b) (c) (d) (f )  Mixer. (a)  Cube Molds, (b)  Bar Molds. (c)  Comparator, (d)  Containers, (e)  Curing Tank, (f )
  • 8. 4. Reagents and Materials  USP or technical grade chemicals may be used.  Sodium Sulfate (Na2SO 4)  Sulfate Solution  Graded Standard Sand.  Stainless Steel Gage Studs .
  • 9. Procedure  Molding and Initial Curing of Specimens—Mold the test bars and the cubes in accordance with Test. A set of specimens to test one cement consists of 6 bars and up to 21 cubes .after molding, cover the molds, and place the mold in the curing tank in water at 35 6 3°C for 23 h 30 min. Place the sealed molds in the curing tank. remove molds from tank and demold the specimens.
  • 10. Subsequent Curing and Preparation for Test;  store all bars in a curing tank of saturated limewater. Break two cubes if the mean strength is 2850 psi or more place all the bars in the sulfate solution. If it is less than 2850 psi store all the demold cubes and bars in the curing tank and test additional cubes When reach to 2850 psi record comparator readings and place all the bars in the sulfate solution
  • 11. Measurements of Length Change:  At 1, 2, 3, 4, 8, 13, and 15 weeks after the bars are placed in the sulfate solution, test them for length change. Review the data at 15 weeks. If uniform length change is taking place, make the next subsequent measurements at a minimum of 4, 6, 9, and 12 months. When the expansion is changing rapidlybmeasure the bars at 4, 6, 9, 12, 15, and 18 months
  • 12.
  • 13. Calculation  10.1 Calculate the length change at any age as follows: DL=[(Lx – Li)/Lg] 100  where: DL = change in length at x age, %, L x = comparator reading of specimen at x age L i = initial comparator reading of specimen-reference bar comparator reading, at the same time Lg = nominal gage length, or 250 mm (10 in.) as applicable.  Calculate length change values for each bar to the nearest 0.001 % and report averages to the nearest 0.01 %.
  • 14. Report  Report type of cement, and, if blending material is used, its identification and amount and whether cement and blending material, if used, meet the applicable specifications. Report the initial comparator reading of each bar at the time of immersion in sulfate solution; this is the base value for calculation of length changes. Report the subsequent length changes in percent of base value to the nearest 0.001 % for individual bars and the nearest 0.01 % for averages.
  • 15. Keywords  acceptability; expansion; fly ash; mortars; pozzolans; precision; search report; slag; sulfate attack; sulfate-resisting cements; tests