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Bright Science Bright Tomorrow
Water & Enzyme Assisted Degumming
For Rice Bran Oil
By
Mr. Javed Husain
MUEZ HEST INDIA PVT.LTD
"69th Annual Convention &
International Conference on Sustainable
Technologies and Futuristic
Trends: Oilseeds - Oils Processing Surfactants & Expo 2014"
November 14 -16 2014
Hotel Radisson Blue, Agra, India
Industry & Technology in Progress
Non Edible Rice Bran Oil for soap industry
First Commercial Trial of Enzymatically Degummed & Physically Refined Rice Bran oil successfully
carried out in joint venture with :
• IICT, Hyderabad
• M/s.Ramcharan Industries, Hyderabad
• M/s.Muez-Hest Mumbai.
1986
1992
1995
1996
2003
2008
2014
2Bright Science Bright Tomorrowmuezhest.com
Physical Refining of Rice Bran Oil (FFA ≤ 40 % ) progressed. But ‘P’ content was critical issue. Mr.Javed
Husain played key role in Physical Refining of RBO at M/s.Darshan Oils Ltd.,Aligarh.
First Physically Refined, marketable Rice Bran oil Produced at M/s.Sudha Agro & Chemicals Industries Ltd.
at samalkot, A.P. ;plant supplied by Muez-Hest, Mumbai.
CSIR-IICT-RRLT, Ministry of agriculture TMOP & M Grant Aid to encourage industries to use enzymatic
process.
Health Ministry ammended Food Standards of Refined Rice Bran Oil: Unsap Matter 3%-4.5 % to maintain
oryzanol.
Emergence of new value added process: combination of Water Degumming & Dry Enzymatic
Degumming followed by Bleaching : IICT, Hyderabad & Muez-Hest, Mumbai.
3Bright Science Bright Tomorrowmuezhest.com
To Control HIS in Rice Lecithin for
Better Quality Oil and Byproduct
Harvest Rice Mill Transport
Meal
Oil
Filtration
Filtered Oil
Animal Feed
Try to Control what’s Happening in your Plant
Extraction
4Bright Science Bright Tomorrowmuezhest.com
Crude Oil Filtration
5Bright Science Bright Tomorrowmuezhest.com
Principles of Water (pH 6) Assisted Degumming
Phospholipids (HP + NHP)
Water
‘P’ Content
610 ppm
Oil
SeparatorCentrifugal
Fatty acid
Fatty acid
Glycerol
P
Oil Phase
Water Phase
‘P’ Content
148 ppmHIS > 55
Oil
Phospholipids (HP + NHP)
Fatty acid
Fatty acid
Glycerol
P
6Bright Science Bright Tomorrowmuezhest.com
Water Degumming
7Bright Science Bright Tomorrowmuezhest.com
Principles of Enzyme Assisted Gum Conditioning
‘P‘ content - 148 ppm
(Non hydratables)
Water Oil
Enzyme
Lecitase Ultra
Fatty acid
Glycerol
P
Enzyme
Lecitase Ultra
Hydratable
Oil
Free Fatty
Acids
HYDROXYL
Fatty acid
Glycerol
P
8Bright Science Bright Tomorrowmuezhest.com
Enzymatic Conditioning
9Bright Science Bright Tomorrowmuezhest.com
Benefits
• More Fatty acid released
from phospholipid molecule
due to enzyme attack
• More Oil Released
• New protocol simpler than
existing Enzymatic process
• Easily adoptable in existing
Industry
• Continuous process
• Better Quality of Gums
(HIS>55)
• Improved quality of oil at
lower cost
• Low Energy
• Low Enzyme Consumption
• Low Water
• Low cost of Lecithin Plant
• One separator
• No Washing
YIELD QUALITY PROCESS ECONOMICS
10Bright Science Bright Tomorrowmuezhest.com
Data Generated at Pilot Scale
Processing Step Color Acid Number Phosphorous
(ppm)
Oryzanol
wt %
Crude Oil 44* 31 621 1.6
Water
Degumming
44* 31 148 1.6
Enzymatic
Conditioning
51* 31.6 148 -
Bleaching 32** 31.6 9 1.6
Dewaxing 27** 31.2 4.8 -
¼” cell
** 1” cell
11Bright Science Bright Tomorrowmuezhest.com
Industry - Process Game Changer
• Attentive Critical Design
Details due to Validation
• Best Equipment Design
• Key personnel;
Training at Muez Hest
and in Plant
• In field support by
Enzyme Supplier
• At Muez Hest R&D
centre
• IPR in Process
• EASY Measurement
and Control
• SAFE from process
DisturbanceKey Success
Operation
Technology
Process
Development
12Bright Science Bright Tomorrowmuezhest.com
Industry Experience
• Pilot Trial Done
• IICT-Muez-Hest : highly Encouraged with process result
• First Industrial Plant Being Set up at M/s. HCS Foods Ltd., Punjab
• Joint Tri-Party agreement among:
I. M/s. HCS Foods Ltd. Punjab
II. IICT, Hyderabad
III. Muez-Hest, Mumbai
13Bright Science Bright Tomorrowmuezhest.com
Contact Details
Address: 230/231, Blue Rose, W.E. Highway, Borivali (E), Mumbai - 400066, INDIA
Tel/Fax: +91 22 2854 1758 / 2870 1752
E-Mail: info@muezhest.com
Visit Us: www.muezhest.com
14Bright Science Bright Tomorrowmuezhest.com
Acknowledgement
IICT, Hyderabad
SEA of India, Mumbai
MuezHest R&D Team, Mumbai
Novozymes, Brenntag
Water & Enzyme Assisted Degumming for Rice Bran Oil

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Water & Enzyme Assisted Degumming for Rice Bran Oil

  • 1. Bright Science Bright Tomorrow Water & Enzyme Assisted Degumming For Rice Bran Oil By Mr. Javed Husain MUEZ HEST INDIA PVT.LTD "69th Annual Convention & International Conference on Sustainable Technologies and Futuristic Trends: Oilseeds - Oils Processing Surfactants & Expo 2014" November 14 -16 2014 Hotel Radisson Blue, Agra, India
  • 2. Industry & Technology in Progress Non Edible Rice Bran Oil for soap industry First Commercial Trial of Enzymatically Degummed & Physically Refined Rice Bran oil successfully carried out in joint venture with : • IICT, Hyderabad • M/s.Ramcharan Industries, Hyderabad • M/s.Muez-Hest Mumbai. 1986 1992 1995 1996 2003 2008 2014 2Bright Science Bright Tomorrowmuezhest.com Physical Refining of Rice Bran Oil (FFA ≤ 40 % ) progressed. But ‘P’ content was critical issue. Mr.Javed Husain played key role in Physical Refining of RBO at M/s.Darshan Oils Ltd.,Aligarh. First Physically Refined, marketable Rice Bran oil Produced at M/s.Sudha Agro & Chemicals Industries Ltd. at samalkot, A.P. ;plant supplied by Muez-Hest, Mumbai. CSIR-IICT-RRLT, Ministry of agriculture TMOP & M Grant Aid to encourage industries to use enzymatic process. Health Ministry ammended Food Standards of Refined Rice Bran Oil: Unsap Matter 3%-4.5 % to maintain oryzanol. Emergence of new value added process: combination of Water Degumming & Dry Enzymatic Degumming followed by Bleaching : IICT, Hyderabad & Muez-Hest, Mumbai.
  • 3. 3Bright Science Bright Tomorrowmuezhest.com To Control HIS in Rice Lecithin for Better Quality Oil and Byproduct Harvest Rice Mill Transport Meal Oil Filtration Filtered Oil Animal Feed Try to Control what’s Happening in your Plant Extraction
  • 4. 4Bright Science Bright Tomorrowmuezhest.com Crude Oil Filtration
  • 5. 5Bright Science Bright Tomorrowmuezhest.com Principles of Water (pH 6) Assisted Degumming Phospholipids (HP + NHP) Water ‘P’ Content 610 ppm Oil SeparatorCentrifugal Fatty acid Fatty acid Glycerol P Oil Phase Water Phase ‘P’ Content 148 ppmHIS > 55 Oil Phospholipids (HP + NHP) Fatty acid Fatty acid Glycerol P
  • 6. 6Bright Science Bright Tomorrowmuezhest.com Water Degumming
  • 7. 7Bright Science Bright Tomorrowmuezhest.com Principles of Enzyme Assisted Gum Conditioning ‘P‘ content - 148 ppm (Non hydratables) Water Oil Enzyme Lecitase Ultra Fatty acid Glycerol P Enzyme Lecitase Ultra Hydratable Oil Free Fatty Acids HYDROXYL Fatty acid Glycerol P
  • 8. 8Bright Science Bright Tomorrowmuezhest.com Enzymatic Conditioning
  • 9. 9Bright Science Bright Tomorrowmuezhest.com Benefits • More Fatty acid released from phospholipid molecule due to enzyme attack • More Oil Released • New protocol simpler than existing Enzymatic process • Easily adoptable in existing Industry • Continuous process • Better Quality of Gums (HIS>55) • Improved quality of oil at lower cost • Low Energy • Low Enzyme Consumption • Low Water • Low cost of Lecithin Plant • One separator • No Washing YIELD QUALITY PROCESS ECONOMICS
  • 10. 10Bright Science Bright Tomorrowmuezhest.com Data Generated at Pilot Scale Processing Step Color Acid Number Phosphorous (ppm) Oryzanol wt % Crude Oil 44* 31 621 1.6 Water Degumming 44* 31 148 1.6 Enzymatic Conditioning 51* 31.6 148 - Bleaching 32** 31.6 9 1.6 Dewaxing 27** 31.2 4.8 - ¼” cell ** 1” cell
  • 11. 11Bright Science Bright Tomorrowmuezhest.com Industry - Process Game Changer • Attentive Critical Design Details due to Validation • Best Equipment Design • Key personnel; Training at Muez Hest and in Plant • In field support by Enzyme Supplier • At Muez Hest R&D centre • IPR in Process • EASY Measurement and Control • SAFE from process DisturbanceKey Success Operation Technology Process Development
  • 12. 12Bright Science Bright Tomorrowmuezhest.com Industry Experience • Pilot Trial Done • IICT-Muez-Hest : highly Encouraged with process result • First Industrial Plant Being Set up at M/s. HCS Foods Ltd., Punjab • Joint Tri-Party agreement among: I. M/s. HCS Foods Ltd. Punjab II. IICT, Hyderabad III. Muez-Hest, Mumbai
  • 13. 13Bright Science Bright Tomorrowmuezhest.com Contact Details Address: 230/231, Blue Rose, W.E. Highway, Borivali (E), Mumbai - 400066, INDIA Tel/Fax: +91 22 2854 1758 / 2870 1752 E-Mail: info@muezhest.com Visit Us: www.muezhest.com
  • 14. 14Bright Science Bright Tomorrowmuezhest.com Acknowledgement IICT, Hyderabad SEA of India, Mumbai MuezHest R&D Team, Mumbai Novozymes, Brenntag