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KAMDHENU UNIVERSITY
College of Dairy Science
Amreli
Topic :- Drying Technology
kishor jadav
Drying means……
 Drying is commonly the last stage in a manufacture process.
 Drying is the final removal of water from material.
 Drying: the removal of all or most of the liquid by supplying latent heat
to cause thermal vaporization.
 Most pharmaceutical materials are not completely free from moisture
but contain some residual water, which may vary with the temperature
and humidity
Why we use drying???
 Drying makes materials more convenient in
 Packaging,
 Transporting,
 Preserving,
 Improves quality of products.
Drying curve
DIFFERENT TYPES OF DRYING
Spray Drying
• Pasteurized milk is first concentrated in
an evaporator to approximately 50% milk
solids. The resulting concentrated milk is
then sprayed into a heated chamber
the water almost instantly evaporates,
leaving fine particles of powdered milk
solids.
Drum Drying
• Milk is applied as a thin film to the
surface of a heated drum, and the dried
milk solids are then scraped off.
powdered milk made this way tends to
have a cooked flavor, due
to caramelization caused by greater heat
exposure.
Freeze Drying
• Same as drum drying
but involves freezing
which retains more
amount of nutrition.
Spray drying
Spray drying involves atomising the milk
concentrate from the evaporator into fine droplets.
Done inside a large drying chamber in a flow of hot
air (up to 200˚C) using either a spinning disk
atomiser or a series of high pressure nozzles.
The milk droplets are cooled by evaporation and
they never reach the temperature of the air.
Contd….
The concentrate may be heated prior to atomisation to
reduce its viscosity and to increase the energy available
for drying.
The remaining water is evaporated in the drying
chamber, leaving a fine powder of around 6% moisture
content with a mean particle size typically of < 0.1 mm
diameter.
Secondary drying takes place in a fluid bed, or in a
series of such beds, in which hot air is blown through a
layer of fluidised powder removing water to give
product with a moisture content of 2-4%.
SPRAY DRYER
The spray dryer provides a large surface area for heat
and mass transfer by atomizing the liquid to small
droplets.
These are sprayed into a stream of hot air, so that each
droplet dries to a solid particle.
The drying chamber resembles the cyclone ensuring
good circulation of air, to facilitate heat and mass transfer,
and that dried particles are separated by the centrifugal
action.
Spray dryer can be operated efficiently at various feed
rates.
Essential Processes
Heating of the air
Atomizing the concentrate in the air
Mixing hot air and atomized liquid
Separating powder and consumed drying air
Aggregation of powder particles
SPRAY DRYER
SPRAY DRIER NOZZLE ROTARY SPTAY NOZZLE
COMPACT SPRAY DRYER
 F:STUDYDairy TechnologyCondesing and DryingCompact-Dryer-GEA-
Niro.exe
Advantages of the spray drying process
 The droplets are small, giving a large surface area for heat transfer, so that
evaporation is very rapid.
 The actual drying time of a droplet is only a fraction of a second, and the
overall time in the dryer is only a few seconds.
 Because evaporation is very rapid, the droplets do not attain a high
temperature, most of the heat being used as latent heat of vaporization.
 The characteristic particle form gives the product a high bulk density and, in
turn, ready solubility.
 The powder will have a uniform and controllable particle size.
Contd….
 The product is free-flowing, with almost spherical particles, and is
especially convenient for tablet manufacture.
 Labour costs are low, the process yielding a dry, free-flowing powder from
a dilute solution, in a single operation with no handling.
 It is possible to operate spray driers aseptically using heated filtered air
to dry products such as serum hydrolysate.
Disadvantages
The equipment is very bulky, connected to
accessories, fans, heaters.
 That is make it expensive.
Drum Dryer (Film Drying)
 Milk or milk products can be dried in a thin film (~ 0.1 mm)
on an internally steam heated rotating drum.
 Often, two drums are set up side by side at a very small
distance apart.
 The water evaporates within a few seconds, which is possible
due to the high drying temperature (>100°C).
 On a drum drier, the product enters as a liquid and leaves as
a solid.
 The product is removed from the exterior of the drum by a
"doctor" blade. The dried film is scraped off from the drum
by means of a steel knife, collected, and ground.
 The major disadvantage of drum drying is that the dry
product may have a scorched flavor and solubility is much
lower because of protein denaturation.
 Considerable product damage due to heating occurs, mainly
because scraping off is always imperfect and, accordingly, a
part of the milk is repeatedly wetted and dried.
 Now a days the roller drying process is little used.
Contd….
IN A DRUM DRYER……
 Vacuum: For vacuum drum drying, the vacuum between the drum and
the housing surrounding the drum is maintained at 68.5 to 73.6 cm Hg
vacuum.
 Size & Speed: The drums used for a drier are 61 to 122 cm in diameter,
and up to 3.6 m in length.
 The speed of the drums is adjustable usually being from 6 to 24 rpm;
however, the range of speed may be from 1 to 36 rpm.
 Product Contact: The product is removed after 3/4th to 7/8th of a
revolution of the drum has taken place. The product is in contact with the
drum for about 3 s or less.
 Spacing: The spacing between drums of a double cylinder drier is about
0.05 to 0.1 cm when the drums are cold.
DRUM DRIER
Advantages of the drum dryer
 The method gives rapid drying, the thin film spread over a large area
resulting in rapid heat and mass transfer.
 The equipment is compact, occupying much less space than other
dryers.
 Heating time is short, being only a few seconds.
 The drum can be enclosed in a vacuum jacket, enabling the
temperature of drying to be reduced.
 The product is obtained in flake form, which is convenient for many
purposes.
Freeze Drying
 Freeze drying is a process used to dry extremely heat – sensitive
materials. It allows the drying , without excessive damage, of proteins,
blood products and even microorganisms, which retain a small but
significant viability.
 In this process the initial liquid solution or suspension is frozen, the
pressure above the frozen state is reduced and the water removed by
sublimation.
 Thus a liquid –to-vapour transition takes place, but here three states of
matter involved: liquid to solid, then solid to vapour.
Condt….
 Technically known as lyophilisation.
 The food material is placed in a vacuum chamber and frozen
until the water crystallizes. The air pressure is lowered,
creating a partial vacuum, forcing air out of the chamber; next
heat is applied, sublimating the ice; finally a freezing coil traps
the vaporized water.
 Freeze drying, which preserves many nutrients in milk,
compared to drum drying.
Advantages
Damage due to heating does not occur but that is
also true of spray drying if skillfully performed.
Suitable for processing in small quantities and is
applied to lactic starters, etc.
Disadvantages
The method is expensive.
The fat globules are subject to partial
coalescence; this causes freeze-dried whole
milk powder to show segregation after its
reconstitution. Freeze drying costs about 5 to
10 times the conventional drying for foods.
Freeze dryer production type
Loading a freeze dryer
Foam mat drying
 Foam-mat drying is one of the simple methods of drying in
which a liquid food concentrate along with a suitable
foaming agent is whipped to form a stable foam and is
subjected to dehydration in the form of a mat of foam at
relatively low temperature .
 Rate of drying in this process is comparatively very high
because of an enormous increase in the liquid-gas interface,
in spite of the fact that the heat transfer is impeded by a
large volume of gas present in the foamed mass.
Foam Spray Drying
 Foam spray drying, is new and has caused interest in new
products. Common dairy products, skim milk, whole milk,
buttermilk, sweet and sour cream (up to 3:1 fat to SNF)
 whey and emulsified cheese slurry can be foam spray dried.
 Air is commonly used as the added gas for making foam
spray nonfat dry milk.
 Nitrogen is commonly used for making foam spray dried
whole milk.
Thank you…

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Drying

  • 1. KAMDHENU UNIVERSITY College of Dairy Science Amreli Topic :- Drying Technology kishor jadav
  • 2. Drying means……  Drying is commonly the last stage in a manufacture process.  Drying is the final removal of water from material.  Drying: the removal of all or most of the liquid by supplying latent heat to cause thermal vaporization.  Most pharmaceutical materials are not completely free from moisture but contain some residual water, which may vary with the temperature and humidity
  • 3. Why we use drying???  Drying makes materials more convenient in  Packaging,  Transporting,  Preserving,  Improves quality of products.
  • 5. DIFFERENT TYPES OF DRYING Spray Drying • Pasteurized milk is first concentrated in an evaporator to approximately 50% milk solids. The resulting concentrated milk is then sprayed into a heated chamber the water almost instantly evaporates, leaving fine particles of powdered milk solids. Drum Drying • Milk is applied as a thin film to the surface of a heated drum, and the dried milk solids are then scraped off. powdered milk made this way tends to have a cooked flavor, due to caramelization caused by greater heat exposure. Freeze Drying • Same as drum drying but involves freezing which retains more amount of nutrition.
  • 6. Spray drying Spray drying involves atomising the milk concentrate from the evaporator into fine droplets. Done inside a large drying chamber in a flow of hot air (up to 200˚C) using either a spinning disk atomiser or a series of high pressure nozzles. The milk droplets are cooled by evaporation and they never reach the temperature of the air.
  • 7. Contd…. The concentrate may be heated prior to atomisation to reduce its viscosity and to increase the energy available for drying. The remaining water is evaporated in the drying chamber, leaving a fine powder of around 6% moisture content with a mean particle size typically of < 0.1 mm diameter. Secondary drying takes place in a fluid bed, or in a series of such beds, in which hot air is blown through a layer of fluidised powder removing water to give product with a moisture content of 2-4%.
  • 8. SPRAY DRYER The spray dryer provides a large surface area for heat and mass transfer by atomizing the liquid to small droplets. These are sprayed into a stream of hot air, so that each droplet dries to a solid particle. The drying chamber resembles the cyclone ensuring good circulation of air, to facilitate heat and mass transfer, and that dried particles are separated by the centrifugal action. Spray dryer can be operated efficiently at various feed rates.
  • 9. Essential Processes Heating of the air Atomizing the concentrate in the air Mixing hot air and atomized liquid Separating powder and consumed drying air Aggregation of powder particles
  • 11. SPRAY DRIER NOZZLE ROTARY SPTAY NOZZLE
  • 12. COMPACT SPRAY DRYER  F:STUDYDairy TechnologyCondesing and DryingCompact-Dryer-GEA- Niro.exe
  • 13. Advantages of the spray drying process  The droplets are small, giving a large surface area for heat transfer, so that evaporation is very rapid.  The actual drying time of a droplet is only a fraction of a second, and the overall time in the dryer is only a few seconds.  Because evaporation is very rapid, the droplets do not attain a high temperature, most of the heat being used as latent heat of vaporization.  The characteristic particle form gives the product a high bulk density and, in turn, ready solubility.  The powder will have a uniform and controllable particle size.
  • 14. Contd….  The product is free-flowing, with almost spherical particles, and is especially convenient for tablet manufacture.  Labour costs are low, the process yielding a dry, free-flowing powder from a dilute solution, in a single operation with no handling.  It is possible to operate spray driers aseptically using heated filtered air to dry products such as serum hydrolysate.
  • 15. Disadvantages The equipment is very bulky, connected to accessories, fans, heaters.  That is make it expensive.
  • 16. Drum Dryer (Film Drying)  Milk or milk products can be dried in a thin film (~ 0.1 mm) on an internally steam heated rotating drum.  Often, two drums are set up side by side at a very small distance apart.  The water evaporates within a few seconds, which is possible due to the high drying temperature (>100°C).  On a drum drier, the product enters as a liquid and leaves as a solid.  The product is removed from the exterior of the drum by a "doctor" blade. The dried film is scraped off from the drum by means of a steel knife, collected, and ground.
  • 17.  The major disadvantage of drum drying is that the dry product may have a scorched flavor and solubility is much lower because of protein denaturation.  Considerable product damage due to heating occurs, mainly because scraping off is always imperfect and, accordingly, a part of the milk is repeatedly wetted and dried.  Now a days the roller drying process is little used. Contd….
  • 18. IN A DRUM DRYER……  Vacuum: For vacuum drum drying, the vacuum between the drum and the housing surrounding the drum is maintained at 68.5 to 73.6 cm Hg vacuum.  Size & Speed: The drums used for a drier are 61 to 122 cm in diameter, and up to 3.6 m in length.  The speed of the drums is adjustable usually being from 6 to 24 rpm; however, the range of speed may be from 1 to 36 rpm.  Product Contact: The product is removed after 3/4th to 7/8th of a revolution of the drum has taken place. The product is in contact with the drum for about 3 s or less.  Spacing: The spacing between drums of a double cylinder drier is about 0.05 to 0.1 cm when the drums are cold.
  • 20. Advantages of the drum dryer  The method gives rapid drying, the thin film spread over a large area resulting in rapid heat and mass transfer.  The equipment is compact, occupying much less space than other dryers.  Heating time is short, being only a few seconds.  The drum can be enclosed in a vacuum jacket, enabling the temperature of drying to be reduced.  The product is obtained in flake form, which is convenient for many purposes.
  • 21. Freeze Drying  Freeze drying is a process used to dry extremely heat – sensitive materials. It allows the drying , without excessive damage, of proteins, blood products and even microorganisms, which retain a small but significant viability.  In this process the initial liquid solution or suspension is frozen, the pressure above the frozen state is reduced and the water removed by sublimation.  Thus a liquid –to-vapour transition takes place, but here three states of matter involved: liquid to solid, then solid to vapour.
  • 22. Condt….  Technically known as lyophilisation.  The food material is placed in a vacuum chamber and frozen until the water crystallizes. The air pressure is lowered, creating a partial vacuum, forcing air out of the chamber; next heat is applied, sublimating the ice; finally a freezing coil traps the vaporized water.  Freeze drying, which preserves many nutrients in milk, compared to drum drying.
  • 23. Advantages Damage due to heating does not occur but that is also true of spray drying if skillfully performed. Suitable for processing in small quantities and is applied to lactic starters, etc.
  • 24. Disadvantages The method is expensive. The fat globules are subject to partial coalescence; this causes freeze-dried whole milk powder to show segregation after its reconstitution. Freeze drying costs about 5 to 10 times the conventional drying for foods.
  • 25. Freeze dryer production type Loading a freeze dryer
  • 26. Foam mat drying  Foam-mat drying is one of the simple methods of drying in which a liquid food concentrate along with a suitable foaming agent is whipped to form a stable foam and is subjected to dehydration in the form of a mat of foam at relatively low temperature .  Rate of drying in this process is comparatively very high because of an enormous increase in the liquid-gas interface, in spite of the fact that the heat transfer is impeded by a large volume of gas present in the foamed mass.
  • 27. Foam Spray Drying  Foam spray drying, is new and has caused interest in new products. Common dairy products, skim milk, whole milk, buttermilk, sweet and sour cream (up to 3:1 fat to SNF)  whey and emulsified cheese slurry can be foam spray dried.  Air is commonly used as the added gas for making foam spray nonfat dry milk.  Nitrogen is commonly used for making foam spray dried whole milk.