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Baking Stability of Pie Crust Using Natural Humectants
Olivia Coroneos, Elizabeth Fitterer, Noelle Bartness, Sayali Bhadke, and *Dr. Eun Joo Lee
Department of Food and Nutrition, University of Wisconsin-Stout, Menomonie, WI 54751.
Introduction
 Humectants are common food additives used to bind the
water molecule in a system for maintaining the product
moist and texture, reducing water activity and microbial
activity, and enhancing baking stability.
 Sorbitol, glycerol and propylene glycol have been used as a
food humectants.
 However, due to the consumer demand for natural
ingredients and label friendly trend, bakery industry has
been seeking natural humectants, which have similar value
of water activity depressant (WAD) with sugars (8-10 range).
Objective
 The objective of this study was to determine the baking
stability of pie crust with different types and concentrations
of natural humectants included honey, molasses, and maple
syrup.
Methods and Materials
 Control dough sample was prepared with mixing flour
(49.5%), unsalted butter (35.0%), ice water (13.9%), salt
(0.8%), and sugar (0.8%).
 For natural humectant treatments, 0.5, 1.0, and 1.5% natural
humectants were added instead of the same amount of ice
water (Table 1).
 0.5% glycerol, the most common humectant in food
industry, was used as a control treatment.
 After storage of doughs covered by the plastic wrap for
overnight in the refrigerator, dough was rolled to a thickness
of 6.35 mm, cut into 2 square inch pieces, placed on a full
sheet tray lined with parchment paper, and baked for 15
minutes at 350 °F (Figure 1).
 Water activity (aw), moisture contents, and pH were
determined for baking stability and the surface texture of pie
crust was measured by scanning electron microscope (SEM).
Tube # % Humectant Ice Water (g) Humectant
1 0.0 22.5 (none)
2 0.5 21.7 0.82 g glycerol
3 0.5 21.7 0.82 g honey
4 1.0 20.9 1.06 g honey
5 1.5 20.1 1.42 g honey
6 0.5 21.7 0.82 g molasses
7 1.0 20.9 1.06 g molasses
8 1.5 20.1 1.42 g molasses
9 0.5 21.7 0.82 g maple syrup
10 1.0 20.9 1.06 g maple syrup
11 1.5 20.1 1.42 g maple syrup
Sample % Moisture pH Aw
Water 49.75 6.33 0.77
0.5% Glycerol 58.89 5.83 0.70
0.5% Honey 54.36 5.51 0.57
1.0% Honey 54.45 5.23 0.43
1.5% Honey 53.25 5.42 0.56
0.5% Molasses 55.43 5.37 0.79
1.0% Molasses 47.51 5.46 0.70
1.5% Molasses 47.71 5.49 0.76
0.5% Maple Syrup 54.93 5.39 0.76
1.0% Maple Syrup 62.32 5.43 0.61
1.5% Maple Syrup 53.24 5.46 0.42
P Value 0.866 0.00015 0.298
Discussion
 1.0% maple syrup treatment showed highest moisture
content (62.3%) while 1.0 and 1.5% molasses treatments
were lowest moisture content (47.5%) (Table 2).
 All natural humectant treatments had lower pH values
(5.23-5.51) than glycerol (5.83) and control (6.33) sample.
 All molasses treatment samples had high values of water
activity (0.70-0.79) similar with water (0.77) and glycerol
(0.70) sample.
 0.5, 1.0, and 1.5% Honey treatments showed the lowest
water activity (0.57, 0.43, and 0.56).
 Compared to 0.5% glycerol treatment, 1.5 % maple syrup
and all honey treatments were similar moisture contents
with low water activity values,
 It indicated that those treatments were similar water
holding capacity (humectant effect) and higher
antimicrobial effect than 0.5% glycerol.
 SEM photos showed the surface texture of the pie crusts,
but there are no differences between treatments (Figure
2-5).
Conclusion
 All honey samples and 1.5% maple syrup sample showed
similar moisture content with 0.5% glycerol.
 All honey samples and 1.5% maple syrup sample have
lower water activity.
 Therefore, honey and 1.5% maple syrup can be the most
comparable natural sugar humectant to glycerol.
References
 Farris, S., Piergiovanni, L., & Limbo, S. (2008). Effect of bamboo fibre and glucose
syrup as new ingredients in the manufacture of amaretti cookies. Italian Journal of
Food Science, 20(1), 75-90.
 (2009). Instron 3340 series single column table frames. Illinois Tool Works, Inc.
 Karimi, M., Sahraiyan, B., Naghipour, F., Sheikholeslami, Z., & Davoodi, M.G. (2013).
Functional effect of different humectants on dough rheology and flat bread
(Barbari) quality. International Journal of Agriculture and Crop Sciences. 5(11),
1209-1213.
 Robbins, R. (2015). Scanning electron microscope operation. University of Texas at
Dallas
 Severini, C., Corbo, M.R., Derossi A., Bevilacqua, A., & Giuliani, R. (2008). Use of
humectants for the stabilization of pesto sauce. International Journal of Food
Science and Technology, 43, 1041- 1046. doi: 10.1111/j.1365-2621.2007.01560.x
 Thomas, R., Anjaneyulu, A.S.R., Mendiratta, S.K., & Kondaiah, N. (2008). Effect of
humectants on the quality of pork sausage. American Journal of Food Technology,
3(2), 56-67.
Acknowledgements
Erik Williams; Research Scientist (Cereals); Kerry and Vamshi Krishna Chintha; Teaching
Assistant; Food and Nutrition Department; University of Wisconsin – Stout.
Figure 2. SEM photos of control
(Left: Water; Right 0.5% Glycerol)
Figure 3. SEM photos of honey samples
(Left: 0.5%; Middle: 1.0%; Right: 1.5%)
Figure 4. SEM photo of molasses samples
(Left: 0.5%; Middle: 1.0%; Right: 1.5%)
Figure 5. SEM photo of Maple Syrup samples
(Left: 0.5%; Middle: 1.0%; Right: 1.5%)
Figure 1. Baked Pie Crust Samples
Table 1. Humectants and water additions for dough variations
Table 2. Baking stability of pie dough with various natural
humectants

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Baking Stability of Pie Crust Using Natural Humectants

  • 1. Results Baking Stability of Pie Crust Using Natural Humectants Olivia Coroneos, Elizabeth Fitterer, Noelle Bartness, Sayali Bhadke, and *Dr. Eun Joo Lee Department of Food and Nutrition, University of Wisconsin-Stout, Menomonie, WI 54751. Introduction  Humectants are common food additives used to bind the water molecule in a system for maintaining the product moist and texture, reducing water activity and microbial activity, and enhancing baking stability.  Sorbitol, glycerol and propylene glycol have been used as a food humectants.  However, due to the consumer demand for natural ingredients and label friendly trend, bakery industry has been seeking natural humectants, which have similar value of water activity depressant (WAD) with sugars (8-10 range). Objective  The objective of this study was to determine the baking stability of pie crust with different types and concentrations of natural humectants included honey, molasses, and maple syrup. Methods and Materials  Control dough sample was prepared with mixing flour (49.5%), unsalted butter (35.0%), ice water (13.9%), salt (0.8%), and sugar (0.8%).  For natural humectant treatments, 0.5, 1.0, and 1.5% natural humectants were added instead of the same amount of ice water (Table 1).  0.5% glycerol, the most common humectant in food industry, was used as a control treatment.  After storage of doughs covered by the plastic wrap for overnight in the refrigerator, dough was rolled to a thickness of 6.35 mm, cut into 2 square inch pieces, placed on a full sheet tray lined with parchment paper, and baked for 15 minutes at 350 °F (Figure 1).  Water activity (aw), moisture contents, and pH were determined for baking stability and the surface texture of pie crust was measured by scanning electron microscope (SEM). Tube # % Humectant Ice Water (g) Humectant 1 0.0 22.5 (none) 2 0.5 21.7 0.82 g glycerol 3 0.5 21.7 0.82 g honey 4 1.0 20.9 1.06 g honey 5 1.5 20.1 1.42 g honey 6 0.5 21.7 0.82 g molasses 7 1.0 20.9 1.06 g molasses 8 1.5 20.1 1.42 g molasses 9 0.5 21.7 0.82 g maple syrup 10 1.0 20.9 1.06 g maple syrup 11 1.5 20.1 1.42 g maple syrup Sample % Moisture pH Aw Water 49.75 6.33 0.77 0.5% Glycerol 58.89 5.83 0.70 0.5% Honey 54.36 5.51 0.57 1.0% Honey 54.45 5.23 0.43 1.5% Honey 53.25 5.42 0.56 0.5% Molasses 55.43 5.37 0.79 1.0% Molasses 47.51 5.46 0.70 1.5% Molasses 47.71 5.49 0.76 0.5% Maple Syrup 54.93 5.39 0.76 1.0% Maple Syrup 62.32 5.43 0.61 1.5% Maple Syrup 53.24 5.46 0.42 P Value 0.866 0.00015 0.298 Discussion  1.0% maple syrup treatment showed highest moisture content (62.3%) while 1.0 and 1.5% molasses treatments were lowest moisture content (47.5%) (Table 2).  All natural humectant treatments had lower pH values (5.23-5.51) than glycerol (5.83) and control (6.33) sample.  All molasses treatment samples had high values of water activity (0.70-0.79) similar with water (0.77) and glycerol (0.70) sample.  0.5, 1.0, and 1.5% Honey treatments showed the lowest water activity (0.57, 0.43, and 0.56).  Compared to 0.5% glycerol treatment, 1.5 % maple syrup and all honey treatments were similar moisture contents with low water activity values,  It indicated that those treatments were similar water holding capacity (humectant effect) and higher antimicrobial effect than 0.5% glycerol.  SEM photos showed the surface texture of the pie crusts, but there are no differences between treatments (Figure 2-5). Conclusion  All honey samples and 1.5% maple syrup sample showed similar moisture content with 0.5% glycerol.  All honey samples and 1.5% maple syrup sample have lower water activity.  Therefore, honey and 1.5% maple syrup can be the most comparable natural sugar humectant to glycerol. References  Farris, S., Piergiovanni, L., & Limbo, S. (2008). Effect of bamboo fibre and glucose syrup as new ingredients in the manufacture of amaretti cookies. Italian Journal of Food Science, 20(1), 75-90.  (2009). Instron 3340 series single column table frames. Illinois Tool Works, Inc.  Karimi, M., Sahraiyan, B., Naghipour, F., Sheikholeslami, Z., & Davoodi, M.G. (2013). Functional effect of different humectants on dough rheology and flat bread (Barbari) quality. International Journal of Agriculture and Crop Sciences. 5(11), 1209-1213.  Robbins, R. (2015). Scanning electron microscope operation. University of Texas at Dallas  Severini, C., Corbo, M.R., Derossi A., Bevilacqua, A., & Giuliani, R. (2008). Use of humectants for the stabilization of pesto sauce. International Journal of Food Science and Technology, 43, 1041- 1046. doi: 10.1111/j.1365-2621.2007.01560.x  Thomas, R., Anjaneyulu, A.S.R., Mendiratta, S.K., & Kondaiah, N. (2008). Effect of humectants on the quality of pork sausage. American Journal of Food Technology, 3(2), 56-67. Acknowledgements Erik Williams; Research Scientist (Cereals); Kerry and Vamshi Krishna Chintha; Teaching Assistant; Food and Nutrition Department; University of Wisconsin – Stout. Figure 2. SEM photos of control (Left: Water; Right 0.5% Glycerol) Figure 3. SEM photos of honey samples (Left: 0.5%; Middle: 1.0%; Right: 1.5%) Figure 4. SEM photo of molasses samples (Left: 0.5%; Middle: 1.0%; Right: 1.5%) Figure 5. SEM photo of Maple Syrup samples (Left: 0.5%; Middle: 1.0%; Right: 1.5%) Figure 1. Baked Pie Crust Samples Table 1. Humectants and water additions for dough variations Table 2. Baking stability of pie dough with various natural humectants