SlideShare a Scribd company logo
1 of 11
Download to read offline
IOSR Journal of Mechanical and Civil Engineering (IOSR-JMCE)
e-ISSN: 2278-1684,p-ISSN: 2320-334X, Volume 13, Issue 1 Ver. I (Jan. - Feb. 2016), PP 68-78
www.iosrjournals.org
DOI: 10.9790/1684-13116878 www.iosrjournals.org 68 | Page
Sliding Wear Characteristics of Bone Powder Filled Hybrid Fiber
Reinforced Epoxy Composites
Sudeep Deshpande1
, T. Rangaswamy2
1
Department of Mechanical Engineering, SKSVMACET, Laxmeshwar - 582116, Karnataka, India
2
Department of Mechanical Engineering, G.E.C, Hassan, Karnataka, India
Abstract: The aim of the research article is to study the dry sliding wear behaviour of epoxy with different
wt.% of bone powder filled E-glass/jute fiber reinforced composites. Taguchi’s orthogonal array (L27) was used
to investigate the influence of tribological parameters. The results indicated that when the filler content was
increased up to 10 wt.% the specific wear rate was decreased but coefficient of friction increases. Form 10 wt.%
to 15 wt.% of filler content specific wear rate was increased but coefficient of friction decreases. After the
thorough analysis of control factors, optimal factor setting has been suggested for specific wear rate and
coefficient of friction. Furthermore, the worn surfaces of the samples were analyzed by scanning electron
microscopy (SEM) to study the wear mechanisms and to correlate them with the wear test results.
Keywords: hybrid composites, wear test, Taguchi’s analysis, scanning electron microscopy.
I. Introduction
Natural fibers are a renewable resource and have several advantages associated with them, such as,
they impart the composite high specific stiffness and strength, a desirable fiber aspect ratio, biodegradability,
they are readily available from natural sources and more importantly they have a low cost per unit volume basis
[1]. These natural fibers can be used in the manufacture of fiber based polymer composites because they posses
attractive physical and mechanical properties. Polymer composites have a special property of self lubrication
and this made the composites suitable in tribological applications such as cams, seals, brakes, bearings etc. F.
Asuke et al., [2] have studied the effect of applied load on the wear behavior of polymer matrix composites
produced by using carbonized bone particles (CBp) as reinforcement. The result shows that the wear rate
increased with increases in applied load and decreased with increasing in carbonized bone particles. B. Suresha
et al., [3] have done experiment on dry sliding wear and two-body abrasive wear behaviour of graphite filled
carbon fabric reinforced epoxy composites. The results show that for increased load and sliding velocity, higher
wear loss was recorded and wear is reduced to a greater extent by addition of the graphite filler in carbon-epoxy
composite which was dominated by microplowing/microcutting mechanisms instead of microcracking. B. N.
Ramesh and B. Suresha [4] have studied the abrasive wear behavior of carbon fabric reinforced epoxy
composites filled with functional fillers like alumina (Al2O3) and molybdenum disulphide (MoS2) separately in
different proportions. The experiments were planned according to Taguchi L18 orthogonal array. The result
showed that the grit size, type of filler and filler loading were the most significant factors in controlling the
specific wear rate of the C-E composite. S. Basavarajappa et al., [5] have experimentally investigated glass–
epoxy composite with influence of graphite filler under varying applied load, sliding distance and sliding
velocity by using a pin-on-disc apparatus. For increased applied load situation for pure glass–epoxy composite
higher weight loss was recorded. As the percentage of graphite increases lower weight loss was observed in the
glass–epoxy composite. Rashmi et al., [6] studied the dry sliding wear behaviour of epoxy with different wt.%
of organo-modified montmorillonite (OMMT) filled nanocomposites and concluded that sliding distance was
the most significant factor affecting wear rate of epoxy nanocomposites. Experimental results showed that the
inclusion of 5 wt.% OMMT nanofiller increased the wear resistance of the epoxy nanocomposite. A. Rout and
A. Satapathy [7] have done experiment on rice husk filled epoxy composites. Taguchi orthogonal array design
and artificial neural network analysis was also carried out. The result showed that sliding velocity was the most
infusing factor followed by filler content and normal load. They have concluded that rice husk filled composites
improves the wear resistance. T. B. Yallew et al., [8] have fabricated woven jute fiber reinforced PP composites.
The tribological behavior was analyzed by a computerized pin-on-disc wear testing machine at an dry operating
condition with different working parameters of sliding speed (1–3 m/s), applied load (10–30 N) and sliding
distance (1000–3000 m). The incorporation of woven jute fiber as reinforcement into PP matrix shows more
than 65% reduction in specific wear rate and 45% reduction in the coefficient of friction. N. Mohan et al., [9]
have fabricated with and without Tantalum Niobium Carbide (Ta/NbC) filled glass epoxy composites. These
composites wear tested for dry sliding wear behavior at elevated temperatures. The result showed that as the
temperature increases specific wear loss increases. Ta/NbC filled glass epoxy composites exhibited lower wear
rate and higher coefficient of friction as compared with pure composite and worn surface was analyzed by
Sliding Wear Characteristics Of Bone Powder Filled Hybrid Fiber Reinforced Epoxy Composites
DOI: 10.9790/1684-13116878 www.iosrjournals.org 69 | Page
scanning electron microscopy. F. Asuke et al., [10] have been studied the effects of uncarbonized (fresh) and
carbonized bone particles on the microstructure and mechanical properties of polypropylene composites. The
results showed that the addition of carbonized bone particles reinforcement composite has superior mechanical
properties than uncarbonized bone particles composite. They have concluded that for optimum service condition
and to have better mechanical properties bone particle addition should not exceed 15 wt.%. In view of the
above, an attempt was made to study the effect of bone powder as a filler material in E-glass/jute fiber
reinforced epoxy composites. The wear characteristics of these hybrid composites were investigated.
II. Experimental Details
2.1. Materials
In this work, 7-mil E-glass fiber as a reinforcement material was used which was supplied by Suntech
Fibers Private Ltd. Woven jute fiber as a reinforcement material was used which was supplied by Jute Cottage,
Bangalore. Unsaturated polyester epoxy L-12 (3202) manufactured by Atul LTD, Gujarat, India and supplied by
Yuge marketing, Bangalore was used as matrix material and K-6 hardener was added to epoxy while fabricating
the composite materials. Goat bones were washed and cleaned. Thin top surface layer of the bone was removed
by using grinding machine and powder was prepared. An approximate density value of bone powder was 1.95
g/cc.
2.2. Fabrication of Composites
The hybrid fiber reinforced epoxy composites were prepared by keeping constant 50 wt.% of epoxy
and 50 wt.% of fiber (40 wt.% of E-glass fiber and 10 wt.% of jute fiber) as shown in “Table 1”. The composites
filled with varying concentrations (0 wt.%, 10 wt.% and 15 wt.%) of bone powder were fabricated by using
hand layup technique. Jute plies were placed in between E-glass plies and also E-glass plies were placed at
extreme ends of the composites. The epoxy, hardener and fillers were mixed thoroughly in a basin and the
mixture was subsequently stirred constantly. The woven E-glass and woven jute fiber was positioned manually.
Mixture so made was brushed uniformly over the E-glass and jute plies. Entrapped air was removed manually
with squeezes or rollers to complete the composite structure. The composites were put under load for about 24
hours for proper curing at room temperature.
Table 1: Fabricated composites with constant 40 wt. % of E-glass fiber and 10 wt. % of jute fiber
Hybrid composites
Epoxy
(wt.%)
Filler material
(wt.%)
GJE 50 0%
GJEB1 40 10%
GJEB2 35 15%
2.3. Specimen Preparation
The fabricated hybrid composites were taken out from the mould and then specimens of suitable
dimensions were prepared from the composites for wear tests according to ASTM G99 standards. The
composites were cut by using Zigzag board cutter machine. Three identical test specimens were prepared for
each test.
2.4. Test of Density
The theoretical density (ρt) of hybrid composite material in terms of weight fractions of different
constituents can be obtained from the following “equation 1” [15].
𝜌𝑡 =
1
𝑊 𝑔
𝜌 𝑔
+
𝑊 𝑗
𝜌 𝑗
+
𝑊 𝑚
𝜌 𝑚
+
𝑊 𝑓
𝜌 𝑓
(1)
where, W and ρ represent the weight fraction and density respectively. The suffixes g, j, m and f stands
for the E- glass fiber, jute fiber, matrix (epoxy) and filler respectively.
The actual density (ρe) of the composite can be determined experimentally by simple water immersion
technique. The volume fraction of voids (Vv) in the composites was calculated using the following “equation 2”
[15].
𝑉𝑣 =
𝜌 𝑡−𝜌 𝑒
𝜌 𝑡
(2)
Sliding Wear Characteristics Of Bone Powder Filled Hybrid Fiber Reinforced Epoxy Composites
DOI: 10.9790/1684-13116878 www.iosrjournals.org 70 | Page
2.5. Dry Sliding Wear Test Apparatus
DUCOM pin on disc test apparatus was used to investigate the dry sliding wear characteristics of
hybrid composite specimens as per ASTM G99 standards. The disc made of hardened EN-31 hardened ground
steel to 62 HRC, surface roughness 1.6 μm Ra, 120 mm track diameter and 8 mm thick. Specimen with size of
10 mm x 10 mm x 30 mm was subjected vertically to the counter face where the contact area was constant.
Wear test was carried out for the constant sliding distance of 2000 m, sliding velocities of 1.4 m/sec, 2 m/sec
and 2.6 m/sec against normal loads of 20 N, 40 N, and 60 N and wear rate data reported was the average of two
runs. Care was to see that the specimen was continuously cleaned with woolen cloth to avoid the entrapment of
wear debris and to achieve uniform experimental procedure. After each test the disc was cleaned using acetone
solution. The initial weight before run and final weight after run was measured using a precision electronic
balance with an accuracy of ± 0.01 mg.
The specific wear rate (mm3
/Nm) was then expressed on „volume loss basis as shown below “equation
3” [4].
𝐾𝑠 =
∆𝑚
𝜌𝑡𝑣𝐹
(3)
where, Ks = Specific wear rate (mm3
/Nm), ∆m = Mass loss (gms), 𝜌 = Density of specimen (g/cc), t =
Test duration (sec), v = sliding velocity (m/s), F = Applied load (N).
2.6. Taguchi Experimental Design
Taguchi technique was used for analyzing the influence of control factors on performance output. The
most important stage in the design of experiment lies in the selection of the control factors. In the present work,
the impact of three parameters such as sliding velocity, normal load and filler content were studied using L27
(313
) Taguchi orthogonal design. The experimental results were transformed into a signal-to-noise (S/N) ratio.
The S/N ratio for minimum wear rate coming under “smaller is better” characteristic, and it was calculated as
logarithmic transformation of the loss function as shown below “equation 4” [8].
𝑆
𝑁
= −10 𝑙𝑜𝑔
1
𝑛
𝑦1
2
+ 𝑦2
2
+ ⋯ 𝑦𝑛
2
(4)
where „n‟ indicates the repeated number of trial conditions, y1, y2….yn indicates the response of the dry
sliding wear characteristics respectively. For „„Lower is better” (LB) characteristic of the above S/N ratio
transformation, it was suitable for minimizations of coefficient of friction and specific wear rate. The standard
linear graph was used to assign the factors and interactions to various columns of the orthogonal array.
The plan of the experiments: The experiments were conducted as per the standard orthogonal array L27
(313
). The selection of the orthogonal array was based on the condition that the degree of freedom for the
orthogonal array should be greater than or equal to sum of those wear parameters.
In the present investigation L27 Taguchi orthogonal array was chosen, this has 27 rows and 13 columns.
The wear parameters chosen were (1) sliding velocity (2) normal load and (3) filler content and their levels
indicated in “Table 2”. The experiments consisted of 27 tests (each row in the L27 orthogonal array) and were
assigned with parameters. The first column in table was assigned to sliding velocity (S), second column was
assigned to normal load (L), fifth column was assigned to filler content (FC) and remaining columns were
assigned to their interactions. The dry sliding wear tests results were subjected to the analysis of variance.
Table 2: Levels of variables used in the experiments
Control factor
Symbols
Level
I II III Units
Sliding velocity A 1.4 2 2.6 m/s
Normal load B 20 40 60 N
Filler content C 0 10 15 %
III. Results and Discussion
3.1. Density
In the present research work, the theoretical and experimental densities of hybrid composites along
with the corresponding volume fraction of voids are presented in “Table 3”. It was found that the composite
density values calculated theoretically from weight fractions were not equal to the experimentally measured
values. It was evident that the density values for hybrid composites increase with the addition of filler content. It
was further observed that with the incorporation of fillers, the void fractions in these composites also increase.
Similar observation has been reported earlier for hybrid composites filled with different filler content.
Sliding Wear Characteristics Of Bone Powder Filled Hybrid Fiber Reinforced Epoxy Composites
DOI: 10.9790/1684-13116878 www.iosrjournals.org 71 | Page
Table 3: Theoretical and experimental densities of hybrid composites
Hybrid composites
Theoretical density
in gm/cc
Experimental density
in gm/cc
Volume fraction of voids
in
%
GJE 1.6183 1.5621 3.47
GJEB1 1.6919 1.6255 3.92
GJEB2 1.7312 1.6120 6.88
3.2. Wear Properties
The experimental data for specific wear rate and coefficient of friction of bone powder filled hybrid
composites reported in the “Table 4”. The overall mean for the S/N ratio of the specific wear rate and the
coefficient of friction are found to be 91.995 db and 7.105 db respectively.
Table 4: Experimental design using L27 array for bone powder filled hybrid composites
S. No Sliding
Velocity (S)
in m/s
Normal
Load
(L) in
N
Filler
content (FC)
in %
Specific Wear
Rate (W) in
mm3
/Nm
S/N Ratio
(db)
Coefficient of
Friction (μ)
S/N Ratio
(db)
1 1.4 20 GJE 8.01E-05 81.93 0.396 8.046
2 1.4 20 GJEB1 1.58E-05 96.05 0.593 4.539
3 1.4 20 GJEB2 1.58E-05 96.02 0.195 14.199
4 1.4 40 GJE 7.20E-05 82.85 0.427 7.391
5 1.4 40 GJEB1 7.88E-06 102.07 0.528 5.547
6 1.4 40 GJEB2 5.53E-05 85.14 0.37 8.636
7 1.4 60 GJE 4.27E-05 87.39 0.48 6.375
8 1.4 60 GJEB1 1.58E-05 96.05 0.636 3.931
9 1.4 60 GJEB2 2.11E-05 93.52 0.414 7.660
10 2 20 GJE 7.99E-05 81.95 0.369 8.659
11 2 20 GJEB1 1.57E-05 96.07 0.612 4.265
12 2 20 GJEB2 6.31E-05 84.00 0.507 5.900
13 2 40 GJE 3.99E-05 87.97 0.452 6.897
14 2 40 GJEB1 1.57E-05 96.07 0.675 3.414
15 2 40 GJEB2 1.58E-05 96.04 0.398 8.002
16 2 60 GJE 3.73E-05 88.57 0.293 10.663
17 2 60 GJEB1 1.05E-05 99.60 0.467 6.614
18 2 60 GJEB2 1.58E-05 96.04 0.352 9.069
19 2.6 20 GJE 6.41E-05 83.86 0.366 8.730
20 2.6 20 GJEB1 4.73E-05 86.50 0.689 3.236
21 2.6 20 GJEB2 3.17E-05 89.99 0.37 8.636
22 2.6 40 GJE 4.81E-05 86.36 0.437 7.190
23 2.6 40 GJEB1 7.89E-06 102.06 0.617 4.194
24 2.6 40 GJEB2 7.91E-06 102.03 0.339 9.396
25 2.6 60 GJE 2.67E-05 91.46 0.479 6.393
26 2.6 60 GJEB1 3.68E-05 88.68 0.637 3.917
27 2.6 60 GJEB2 5.28E-06 105.55 0.304 10.343
Table 5: Response table for specific wear rate of bone powder filled hybrid composites
Level A B C
1 91.23 88.49 85.82
2 91.81 93.4 95.91
3 92.95 94.1 94.26
Delta 1.72 5.61 10.09
Rank 3 2 1
Sliding Wear Characteristics Of Bone Powder Filled Hybrid Fiber Reinforced Epoxy Composites
DOI: 10.9790/1684-13116878 www.iosrjournals.org 72 | Page
2.62.01.4
95.0
92.5
90.0
87.5
85.0
604020
GJEB2GJEB1GJE
95.0
92.5
90.0
87.5
85.0
Sliding Velocity (S) in m/s
MeanofSNratios
Load
Filler content (FC) in %
Main Effects Plot for SN ratios
Data Means
Signal-to-noise: Smaller is better
Table 6: ANOVA table for specific wear rate of bone powder filled hybrid composites
Source DF Seq SS Adj SS Adj MS Test F P (%)
A 2 1.50 1.498 0.75 0.38 1.05
B 2 23.89 23.89 11.95 6.13 16.67
C 2 63.41 63.41 31.71 16.26 44.25
A*B 4 13.02 13.02 3.26 1.67 9.09
A*C 4 15.06 15.06 3.77 1.93 10.51
B*C 4 10.84 10.84 2.71 1.39 7.57
Residual Error 8 15.57 15.57 1.95 10.87
Total 26 143.29 100.00
DF - degree of freedom, Seq SS - sequential sum of squares, Adj. SS - extra sum of squares, Seq MS -
sequential mean squares, F - F-test and P - percent contribution
Figure 1: Effect of control factors on specific wear rate of hybrid composites
Figure 2: Interaction graph between sliding velocity and filler content for specific wear rate
2.62.01.4
100.0
97.5
95.0
92.5
90.0
87.5
85.0
Sliding Velocity (S) in m/s
SNratios
GJE
GJEB1
GJEB2
(FC) in %
Filler content
Interaction Plot for SN ratios
Data Means
Signal-to-noise: Smaller is better
Sliding Wear Characteristics Of Bone Powder Filled Hybrid Fiber Reinforced Epoxy Composites
DOI: 10.9790/1684-13116878 www.iosrjournals.org 73 | Page
Figure 3: Interaction graph between sliding velocity and normal load for specific wear rate
Figure 4: Interaction graph between normal load and filler content for specific wear rate
3.2.1 ANOVA and Effects of Factors on Specific Wear Rate
From the ANOVA “Table 6” it was observed that the filler content (C) factor (P = 44.25%), normal
load (B) factor (P = 16.67%) and interaction (AxC) between sliding velocity x filler content (P = 10.51%) have
great influence on the specific wear rate and hence theses are physically and statistically highly significant.
However interaction (AxB) between sliding velocity x normal load (P = 9.09%), (BxC) interaction between
normal load x filler content (P = 7.57%) and sliding velocity (A) factor (P = 1.10%) have lesser effect on
specific wear rate as error value (P = 10.87) was higher side hence less significant. From the analysis of
ANOVA and response “Table 5” of the S/N ratio for specific wear rate, it was observed that the filler content
has major impact on specific wear rate followed by normal load and sliding velocity.
The influence of each control factor (sliding velocity, normal load and filler content) on the specific
wear rate was analysed with a main effects plot as shown in “Fig. 1” and an interaction plot as shown in “Figs. 2
to 4”. From the analysis of ANOVA and response “Table 5” of the S/N ratio for specific wear rate, it was
observed that the filler content (C) has major impact on the specific wear rate followed by the normal load (B)
and sliding velocity (A). It means that for bone powder filled hybrid composites with the increases of the filler
604020
100
95
90
85
80
Load
SNratios
GJE
GJEB1
GJEB2
(FC) in %
Filler content
Interaction Plot for SN ratios
Data Means
Signal-to-noise: Smaller is better
2.62.01.4
98
96
94
92
90
88
86
Sliding Velocity (S) in m/s
SNratios
20
40
60
Load
Interaction Plot for SN ratios
Data Means
Signal-to-noise: Smaller is better
Sliding Wear Characteristics Of Bone Powder Filled Hybrid Fiber Reinforced Epoxy Composites
DOI: 10.9790/1684-13116878 www.iosrjournals.org 74 | Page
2.62.01.4
9
8
7
6
5
604020
GJEB2GJEB1GJE
9
8
7
6
5
Sliding Velocity (S) in m/s
MeanofSNratios
Load
Filler content (FC) in %
Main Effects Plot for SN ratios
Data Means
Signal-to-noise: Smaller is better
content, sliding velocity and normal load the specific wear rate decreases i.e., good wear resistance. It was also
observed that the filler content plays adverse effect, when the filler content was increased from 0 wt.% to 10
wt.% the specific wear rate was decreased and for 10 wt.% to 15 wt.% it further increases. Analysis of these
results leads to the conclusion that optimal values of the parameters for minimizing the wear rate when the
sliding velocity and normal load were at level 3 and the filler content was at level 2.
Table 7: Response table for COF of bone powder filled hybrid composites
Level A B C
1 7.369 7.357 7.816
2 7.054 6.741 4.406
3 6.893 7.218 9.093
Delta 0.477 0.616 4.687
Rank 3 2 1
Table 8: ANOVA table for COF of bone powder filled hybrid composites
Source DF Seq SS Adj SS Adj MS Test F P (%)
A 2 0.00900 0.00900 0.00450 1.52718 2.07
B 2 0.00022 0.00022 0.00011 0.03733 0.05
C 2 0.30110 0.30110 0.15055 51.09278 69.33
A*B 4 0.05480 0.05480 0.01370 4.64943 12.62
A*C 4 0.02850 0.02850 0.00713 2.41804 6.56
B*C 4 0.01711 0.01711 0.00428 1.45167 3.94
Residual Error 8 0.02357 0.02357 0.00295 5.43
Total 26 0.43430 100.00
DF - degree of freedom, Seq SS - sequential sum of squares, Adj. SS - extra sum of squares, Seq MS -
sequential mean squares, F - F-test and P - percent contribution
Figure 5: Effect of control factors on COF hybrid composites
3.2.2 ANOVA and Effects of Factors on Coefficient Of Friction
ANOVA “Table 8” for the coefficient of friction that the filler content (C) factor (P = 69.33%),
interaction between sliding velocity x normal load (AxB) and the interactions between sliding velocity x filler
content (AxC) have significant influence on the coefficient of friction. However interaction of normal load x
filler content (P = 3.94%), sliding velocity (P = 2.07%) and normal load (B) factor (P = 0.05%) do not have a
significant effect (both physically and statistical) on coefficient of friction as their values are quite smaller than
error (P = 5.43%) so they are neglected. From the analysis of ANOVA and response “Table 7” of the S/N ratio
Sliding Wear Characteristics Of Bone Powder Filled Hybrid Fiber Reinforced Epoxy Composites
DOI: 10.9790/1684-13116878 www.iosrjournals.org 75 | Page
of coefficient of friction, it was observed that the control parameter filler content (C) has major impact on
coefficient of friction followed by normal load and sliding velocity.
The influence of each control factor on the coefficient of friction was analyzed with a main effects plot
as shown in “Fig. 5” and an interaction plot as shown in “Figs. 6 to 8”. From the analysis of ANOVA and
response “Table 7” of the S/N ratio for coefficient of friction, it was observed that the control factor filler
content (C) has major impact on the coefficient of friction. It means that for bone powder filled hybrid
composites, with the increases of the filler content from 0 wt.% to 10 wt.% coefficient of friction increases and
from 10 wt.% to 15 wt.% coefficient of friction decreases. The same trend was observed for normal load. With
the increase of sliding velocity coefficient of friction decreases. Analysis of these results leads to the conclusion
that optimal values of the parameters for minimizing the wear rate when the sliding velocity and normal load
were at level 1 and the filler content was at level 3.
Figure 6: Interaction graph between sliding velocity and normal load for coefficient of friction
Figure 7: Interaction graph between sliding velocity and filler content for coefficient of friction
2.62.01.4
9.0
8.5
8.0
7.5
7.0
6.5
6.0
Sliding Velocity (S) in m/s
SNratios
20
40
60
Load
Interaction Plot for SN ratios
Data Means
Signal-to-noise: Smaller is better
2.62.01.4
11
10
9
8
7
6
5
4
3
Sliding Velocity (S) in m/s
SNratios
GJE
GJEB1
GJEB2
(FC) in %
Filler content
Interaction Plot for SN ratios
Data Means
Signal-to-noise: Smaller is better
Sliding Wear Characteristics Of Bone Powder Filled Hybrid Fiber Reinforced Epoxy Composites
DOI: 10.9790/1684-13116878 www.iosrjournals.org 76 | Page
Figure 8: Interaction graph between normal load and filler content for coefficient of friction
3.2.3 Surface Morphology of Bone Powder Filled Hybrid Composites
(a)
(b)
(c)
(d)
604020
10
9
8
7
6
5
4
Load
SNratios
GJE
GJEB1
GJEB2
(FC) in %
Filler content
Interaction Plot for SN ratios
Data Means
Signal-to-noise: Smaller is better
Sliding Wear Characteristics Of Bone Powder Filled Hybrid Fiber Reinforced Epoxy Composites
DOI: 10.9790/1684-13116878 www.iosrjournals.org 77 | Page
(e) (f)
Figure 9: SEM pictures of composites for bone powder filled hybrid composites
When compared with sliding velocity and normal load the effect of filler content on specific wear rate
was more as seen from main effect plot as shown in “Fig. 1”. For analysis different filler content hybrid
composite samples with all samples tested for 20N normal load were selected. “Figs. 9(a) to 9(c)” shows the
SEM pictures of composites for different filler content (0, 10 and 15 wt.%) of bone powder filled hybrid
composites. The micrograph in “Fig. 9(a)” shows the wedge formation, fiber exposure and plastic deformation
of matrix which results maximum wear. The SEM picture as shown in “Fig. 9(b)” illustrates only a few fibers
exposure when compared with “Fig. 9(a)” and less deformation of the matrix which indicates less wear. “Fig.
9(c)” shows more plastic deformation of the matrix which slightly increases the wear rate when compared with
“Fig. 9(b)”.
Similarly, coefficient of friction was affected by filler content as seen from main effect plot (“Fig. 5”),
So SEM images were selected for different filler content of hybrid composites. “Figs. 9(d) to 9(e)” shows the
SEM pictures for different filler content (0 wt.%, 10 wt.% and 15 wt.%) of bone powder filled hybrid
composites. The worn surface of the “Figs. 9(d) and 9(f)” shows the wear track, minor crack and only few fibers
exposed from the matrix which has less coefficient of friction. The SEM picture for “Fig. 9(e)” sample shows
the wear track on the surface, breakage of fibers and more number of fibers exposed which increased the
coefficient of friction due to the rubbing action of the fibers with the disc surface.
IV. Conclusions
The experimental investigation on dry sliding wear behaviour of bone powder filled epoxy composites
leads to the following conclusions:
 Successful fabrication of bone powder filled E-glass/jute fiber reinforced epoxy composite has been done
by the hand lay-up technique.
 Dry sliding wear response of these hybrid composites under different loads, filler content and sliding
velocities can be successfully analyzed using Taguchi‟s experimental design method. Taguchi‟s method
provides a simple, systematic and efficient methodology for the optimization of the control factors. While
filler content emerges as the most significant factor affecting wear rate of bone power filled epoxy hybrid
composites, other factors like load and sliding velocity have less influence on specific wear rate.
 The SEM micrographs of the specimen revels wear track, exposure of fibers due to wear of the matrix,
debris formation, fiber breakage, plastic deformation of matrix and fiber matrix debonding.
References
[1] T. Sen, H. N. Jagannatha Reddy, ”Efficacy of bio derived jute FRP composite based technique for shear strength retrofitting of
reinforced concrete beams and its comparative analysis with carbon and glass FRP shear retrofitting schemes”, Sustainable Cities
and Society, Vol. 13, 2014, pp 105-124
[2] F. Asuke, M. Abdulwahab, V.S. Aigbodion, O. S. I. Fayomi and O. Aponbiede, “Effect of load on the wear behavior of
polypropylene/carbonized bone ash particulate composite”, Egyptian Journal of Basic and Applied Sciences, Vol. 1, 2014, pp 67-70
[3] B. Suresha, Siddaramaiah, Kishore, S. Seetharamu and P. S. Kumaran, “Investigations on the influence of graphite filler on dry
sliding wear and abrasive wear behaviour of carbon fabric reinforced epoxy composites”, Wear Vol. 267, 2009, pp 1405-1414
[4] B. N. Ramesh and B. Suresha, “Optimization of tribological parameters in abrasive wear mode of carbon-epoxy hybrid
composites”, Materials and Design, Vol. 59, 2014, pp 38-49
[5] S. Basavarajappa, S. Ellangovan and K. V. Arun, “Studies on dry sliding wear behaviour of graphite filled glass–epoxy
composites”, Materials and Design, Vol. 30, 2009, pp 2670-2675
Sliding Wear Characteristics Of Bone Powder Filled Hybrid Fiber Reinforced Epoxy Composites
DOI: 10.9790/1684-13116878 www.iosrjournals.org 78 | Page
[6] Rashmi, N. M. Renukappa, B. Suresha, R. M. Devarajaiah and K. N. Shivakumar, “Dry sliding wear behaviour of organo-modified
montmorillonite filled epoxy nanocomposites using Taguchi‟s techniques”, Materials and Design, Vol. 32, 2011, pp 4528-4536
[7] A. Rout and A. Satapathy, “Analysis of dry sliding wear behavior of rice husk filled epoxy composites using design of experiment
and ANN”, Proc Engineering, Vol. 38, 2012, pp 1218-1232
[8] T. B. Yallew, Pradeep Kumar and I. Singh, “Sliding wear properties of jute fabric reinforced polypropylene composites”, Proc
Engineering, Vol. 97, 2014, pp 402-411
[9] N. Mohan, C. R. Mahesha, Shivarudraiah, N. R. Mathivanan and B. shivamurthy, “Dry sliding wear behavior of Ta/Nbc filled-
epoxy composites at elevated temperatures”, Proc Engineering, Vol. 64, 2013, pp 1166-1172
[10] F. Asuke, V. S. Aigbodion, M. Abdulwahab, O. S. I. Fayomi, A. P. I. Popoola, C.I. Nwoyi and B. Garba, “Effects of bone particle
on the properties and microstructure of polypropylene/bone ash particulate composites”, Results in Physics,Vol. 2, 2012, pp 135-
141.
[11] H. Abdellaoui, H. Bensalah, J. Echaabi, R. Bouhfid and A. Qaiss, “Fabrication, characterization and modelling of laminated
composites based on woven jute fibres reinforced epoxy resin”, Materials and Design, Vol. 68, 2015, pp 104-133
[12] Md. R. Rahman, Md. M. Huque, Md. N. Islam and M. Hasan, “Improvement of physico-mechanical properties of jute fiber
reinforced polypropylene composites by post-treatment”, Composites: Part A, Vol. 39, 2008, pp 1739-1747
[13] M. Jawaid, H. P. S. Abdul Khalil, A. Abu Bakar and P. N. Khanam, “Chemical resistance, void content and tensile properties of oil
palm/jute fibre reinforced polymer hybrid composites”, Materials and Design, Vol. 32, 2011, pp 1014-1019
[14] V. Mishra and S. Biswas, “Physical and mechanical properties of bi-directional jute fiber epoxy composites”, Proc Engineering,
Vol. 51, 2013, pp 561-566
[15] A. Gopinatha, M. Senthil Kumar and A. Elayaperumal, “Experimental investigations on mechanical properties of jute fiber
reinforced composites with polyester and epoxy resin matrices”, Proc Engineering, Vol. 97, 2014, pp 2052-2063
[16] C. Fukuda, K. Goto, M. Imamura, M. Neo and T. Nakamura, “Bone bonding ability and handling properties of a titania–
polymethylmethacrylate(PMMA) composite bioactive bone cement modified with a unique PMMA powder”, Acta Biomaterialia,
Vol. 7, 2011, pp 3595-3600
[17] J. Sudeepan, K. Kumar, T. K. Barman and P. Sahoo, “Study of friction and wear of ABS/Zno polymer composite using Taguchi
technique”, Proc Materials Science, Vol. 6, 2014, pp 391-400
[18] N. Dayma, B. K. Satapathy and A. Patnaik, “Structural correlations to sliding wear performance of PA-6/PP-g-MA/nanoclay ternary
nanocomposites”, Wear, Vol. 271, 2011, pp 827-836
[19] B. Suresha, R. M. Devarajaiah, T. Pasang and C. Ranganathaiah, “Investigation of organo-modified montmorillonite loading effect
on the abrasion resistance of hybrid composites”, Materials and Design, Vol. 47, 2013, pp 750-758
[20] U. Nirmal, J. Hashim and M. M. H. Megat Ahmad, “A review on tribological performance of natural fibre polymeric composites”,
Tribology International, Vol. 83, 2015, pp 77-104
[21] H. Md. Akil, C. Santulli, F. Sarasini, J. Tirillo and T. Valente, “Environmental effects on the mechanical behaviour of pultruded
jute/glass fibre-reinforced polyester hybrid composites”, Composites Science and Technology, Vol. 94, 2014, pp 62-70
[22] Y. Arao, T. Fujiura, S. Itani and T. Tanaka, “Strength improvement in injection-molded jute-fiber-reinforced polylactide green-
composites”, Composites: Part B, Vol. 68, 2015, pp 200-206
[23] R. Codispoti, D. V. Oliveira , R. S. Olivito , P. B. Lourenco and R. Fangueiro, “Mechanical performance of natural fiber-reinforced
composites for the strengthening of masonry”, Composites: Part B, Vol. 77, 2015, pp 74-83
[24] Pantamanatsopa, W. Ariyawiriyanan, T. Meekeaw, R. Suthamyong, K. Arrub and H. Hamada, “Effect of modified jute fiber on
mechanical properties of green rubber composite”, Energy Proc, Vol. 56, 2014, pp 641-647
[25] M. Ramesh, K. Palanikumar and K. H. Reddy, “Comparative evaluation on properties of hybrid glass fiber- sisal/jute reinforced
epoxy composites”, Proc Engineering, Vol. 51, 2013, pp 745-750

More Related Content

What's hot

Physical and mechanical properties of concrete incorporating industrial and a...
Physical and mechanical properties of concrete incorporating industrial and a...Physical and mechanical properties of concrete incorporating industrial and a...
Physical and mechanical properties of concrete incorporating industrial and a...eSAT Journals
 
6.a review on wear behaviour of clutch plate made of peek composite material
6.a review on wear behaviour of clutch plate made of  peek composite material6.a review on wear behaviour of clutch plate made of  peek composite material
6.a review on wear behaviour of clutch plate made of peek composite materialEditorJST
 
ppt gursharan singh m.tech civil engineering
ppt gursharan singh m.tech civil engineering ppt gursharan singh m.tech civil engineering
ppt gursharan singh m.tech civil engineering GURSHARANSINGH119
 
A Study on Effect of Carbon and Ash Fillers on Flexural Properties in GFRP Co...
A Study on Effect of Carbon and Ash Fillers on Flexural Properties in GFRP Co...A Study on Effect of Carbon and Ash Fillers on Flexural Properties in GFRP Co...
A Study on Effect of Carbon and Ash Fillers on Flexural Properties in GFRP Co...IRJET Journal
 
EXPERIMENTAL STUDY ON WEAR BEHAVIOUR OF SIC FILLED HYBRID COMPOSITES USING TA...
EXPERIMENTAL STUDY ON WEAR BEHAVIOUR OF SIC FILLED HYBRID COMPOSITES USING TA...EXPERIMENTAL STUDY ON WEAR BEHAVIOUR OF SIC FILLED HYBRID COMPOSITES USING TA...
EXPERIMENTAL STUDY ON WEAR BEHAVIOUR OF SIC FILLED HYBRID COMPOSITES USING TA...IAEME Publication
 
Fiberglass strength tests (2)
Fiberglass strength tests (2)Fiberglass strength tests (2)
Fiberglass strength tests (2)Jhonny Ccanchi
 
Experimental Study on the Mechanical Properties of Concrete Incorporating PET...
Experimental Study on the Mechanical Properties of Concrete Incorporating PET...Experimental Study on the Mechanical Properties of Concrete Incorporating PET...
Experimental Study on the Mechanical Properties of Concrete Incorporating PET...ijsrd.com
 
Resilient Characteristics of Stone Matrix Asphalt Mixes
Resilient Characteristics of Stone Matrix Asphalt MixesResilient Characteristics of Stone Matrix Asphalt Mixes
Resilient Characteristics of Stone Matrix Asphalt MixesIDES Editor
 
STRENGTH CHARACTERIZATION OF GLASSCARON HYBRID REINFORCEMENTS - AN EXPERIMENT...
STRENGTH CHARACTERIZATION OF GLASSCARON HYBRID REINFORCEMENTS - AN EXPERIMENT...STRENGTH CHARACTERIZATION OF GLASSCARON HYBRID REINFORCEMENTS - AN EXPERIMENT...
STRENGTH CHARACTERIZATION OF GLASSCARON HYBRID REINFORCEMENTS - AN EXPERIMENT...IAEME Publication
 
Taguchi Analysis of Erosion Wear Maize Husk Based Polymer Composite
Taguchi Analysis of Erosion Wear Maize Husk Based Polymer CompositeTaguchi Analysis of Erosion Wear Maize Husk Based Polymer Composite
Taguchi Analysis of Erosion Wear Maize Husk Based Polymer CompositeIJMER
 
Development of Graphite Particles filled Epoxy Resin Composite Material and i...
Development of Graphite Particles filled Epoxy Resin Composite Material and i...Development of Graphite Particles filled Epoxy Resin Composite Material and i...
Development of Graphite Particles filled Epoxy Resin Composite Material and i...IDES Editor
 
A0412401011
A0412401011A0412401011
A0412401011IOSR-JEN
 

What's hot (19)

Physical and mechanical properties of concrete incorporating industrial and a...
Physical and mechanical properties of concrete incorporating industrial and a...Physical and mechanical properties of concrete incorporating industrial and a...
Physical and mechanical properties of concrete incorporating industrial and a...
 
15. IJSER -2013
15. IJSER -201315. IJSER -2013
15. IJSER -2013
 
Ijtra130513
Ijtra130513Ijtra130513
Ijtra130513
 
K012538188
K012538188K012538188
K012538188
 
6.a review on wear behaviour of clutch plate made of peek composite material
6.a review on wear behaviour of clutch plate made of  peek composite material6.a review on wear behaviour of clutch plate made of  peek composite material
6.a review on wear behaviour of clutch plate made of peek composite material
 
Igc 2013 paper
Igc 2013 paperIgc 2013 paper
Igc 2013 paper
 
ppt gursharan singh m.tech civil engineering
ppt gursharan singh m.tech civil engineering ppt gursharan singh m.tech civil engineering
ppt gursharan singh m.tech civil engineering
 
IEEE my paper
IEEE my paperIEEE my paper
IEEE my paper
 
A Study on Effect of Carbon and Ash Fillers on Flexural Properties in GFRP Co...
A Study on Effect of Carbon and Ash Fillers on Flexural Properties in GFRP Co...A Study on Effect of Carbon and Ash Fillers on Flexural Properties in GFRP Co...
A Study on Effect of Carbon and Ash Fillers on Flexural Properties in GFRP Co...
 
EXPERIMENTAL STUDY ON WEAR BEHAVIOUR OF SIC FILLED HYBRID COMPOSITES USING TA...
EXPERIMENTAL STUDY ON WEAR BEHAVIOUR OF SIC FILLED HYBRID COMPOSITES USING TA...EXPERIMENTAL STUDY ON WEAR BEHAVIOUR OF SIC FILLED HYBRID COMPOSITES USING TA...
EXPERIMENTAL STUDY ON WEAR BEHAVIOUR OF SIC FILLED HYBRID COMPOSITES USING TA...
 
Fiberglass strength tests (2)
Fiberglass strength tests (2)Fiberglass strength tests (2)
Fiberglass strength tests (2)
 
Experimental Study on the Mechanical Properties of Concrete Incorporating PET...
Experimental Study on the Mechanical Properties of Concrete Incorporating PET...Experimental Study on the Mechanical Properties of Concrete Incorporating PET...
Experimental Study on the Mechanical Properties of Concrete Incorporating PET...
 
Resilient Characteristics of Stone Matrix Asphalt Mixes
Resilient Characteristics of Stone Matrix Asphalt MixesResilient Characteristics of Stone Matrix Asphalt Mixes
Resilient Characteristics of Stone Matrix Asphalt Mixes
 
STRENGTH CHARACTERIZATION OF GLASSCARON HYBRID REINFORCEMENTS - AN EXPERIMENT...
STRENGTH CHARACTERIZATION OF GLASSCARON HYBRID REINFORCEMENTS - AN EXPERIMENT...STRENGTH CHARACTERIZATION OF GLASSCARON HYBRID REINFORCEMENTS - AN EXPERIMENT...
STRENGTH CHARACTERIZATION OF GLASSCARON HYBRID REINFORCEMENTS - AN EXPERIMENT...
 
A04650110
A04650110A04650110
A04650110
 
Taguchi Analysis of Erosion Wear Maize Husk Based Polymer Composite
Taguchi Analysis of Erosion Wear Maize Husk Based Polymer CompositeTaguchi Analysis of Erosion Wear Maize Husk Based Polymer Composite
Taguchi Analysis of Erosion Wear Maize Husk Based Polymer Composite
 
Development of Graphite Particles filled Epoxy Resin Composite Material and i...
Development of Graphite Particles filled Epoxy Resin Composite Material and i...Development of Graphite Particles filled Epoxy Resin Composite Material and i...
Development of Graphite Particles filled Epoxy Resin Composite Material and i...
 
A0412401011
A0412401011A0412401011
A0412401011
 
El33827831
El33827831El33827831
El33827831
 

Viewers also liked

Viewers also liked (20)

A010230105
A010230105A010230105
A010230105
 
Novel Battery Charging Control System for Batteries Using On/Off and Pwm Cont...
Novel Battery Charging Control System for Batteries Using On/Off and Pwm Cont...Novel Battery Charging Control System for Batteries Using On/Off and Pwm Cont...
Novel Battery Charging Control System for Batteries Using On/Off and Pwm Cont...
 
N1303047887
N1303047887N1303047887
N1303047887
 
H010344552
H010344552H010344552
H010344552
 
F012515059
F012515059F012515059
F012515059
 
E010132529
E010132529E010132529
E010132529
 
A010520107
A010520107A010520107
A010520107
 
Heuristic Searching: A* Search
Heuristic Searching: A* SearchHeuristic Searching: A* Search
Heuristic Searching: A* Search
 
H1304025762
H1304025762H1304025762
H1304025762
 
L012438186
L012438186L012438186
L012438186
 
C017521927
C017521927C017521927
C017521927
 
H010335459
H010335459H010335459
H010335459
 
C017221821
C017221821C017221821
C017221821
 
E017163033
E017163033E017163033
E017163033
 
J012256367
J012256367J012256367
J012256367
 
I017235662
I017235662I017235662
I017235662
 
Analysis of Interfacial Microsstructure of Post Weld Heat Treated Dissimilar ...
Analysis of Interfacial Microsstructure of Post Weld Heat Treated Dissimilar ...Analysis of Interfacial Microsstructure of Post Weld Heat Treated Dissimilar ...
Analysis of Interfacial Microsstructure of Post Weld Heat Treated Dissimilar ...
 
B017150823
B017150823B017150823
B017150823
 
C012231827
C012231827C012231827
C012231827
 
P01725105109
P01725105109P01725105109
P01725105109
 

Similar to H013116878

Shellfish shell as a Bio-filler: Preparation, characterization and its effec...
	Shellfish shell as a Bio-filler: Preparation, characterization and its effec...	Shellfish shell as a Bio-filler: Preparation, characterization and its effec...
Shellfish shell as a Bio-filler: Preparation, characterization and its effec...theijes
 
Fabrication, experimental investigation of jute fiber reinforced epoxy compos...
Fabrication, experimental investigation of jute fiber reinforced epoxy compos...Fabrication, experimental investigation of jute fiber reinforced epoxy compos...
Fabrication, experimental investigation of jute fiber reinforced epoxy compos...Adib Bin Rashid
 
EVALUATION OFTENSILE PROPERTIESOF EPOXY RESIN BASED COMPOSITES REINFORCED WIT...
EVALUATION OFTENSILE PROPERTIESOF EPOXY RESIN BASED COMPOSITES REINFORCED WIT...EVALUATION OFTENSILE PROPERTIESOF EPOXY RESIN BASED COMPOSITES REINFORCED WIT...
EVALUATION OFTENSILE PROPERTIESOF EPOXY RESIN BASED COMPOSITES REINFORCED WIT...IAEME Publication
 
Role of Natural and Synthetic Fillers on Erosive Wear Behavior of Basalt -Epo...
Role of Natural and Synthetic Fillers on Erosive Wear Behavior of Basalt -Epo...Role of Natural and Synthetic Fillers on Erosive Wear Behavior of Basalt -Epo...
Role of Natural and Synthetic Fillers on Erosive Wear Behavior of Basalt -Epo...IJRES Journal
 
Fabrication and Characterization of Kevlar/Jute Reinforced Epoxy
Fabrication and Characterization of Kevlar/Jute Reinforced EpoxyFabrication and Characterization of Kevlar/Jute Reinforced Epoxy
Fabrication and Characterization of Kevlar/Jute Reinforced EpoxyIRJET Journal
 
IRJET - A Review on Multi-Layered Armour using Sugarcane Bagasse Waste
IRJET -  	  A Review on Multi-Layered Armour using Sugarcane Bagasse WasteIRJET -  	  A Review on Multi-Layered Armour using Sugarcane Bagasse Waste
IRJET - A Review on Multi-Layered Armour using Sugarcane Bagasse WasteIRJET Journal
 
Enhancing Mechanical Properties of Jute Fibre/Glass Fiber and Epoxy Combined ...
Enhancing Mechanical Properties of Jute Fibre/Glass Fiber and Epoxy Combined ...Enhancing Mechanical Properties of Jute Fibre/Glass Fiber and Epoxy Combined ...
Enhancing Mechanical Properties of Jute Fibre/Glass Fiber and Epoxy Combined ...IRJET Journal
 
Investigations of Mechanical Characteristics of Chicken Feather-Teak wood Dus...
Investigations of Mechanical Characteristics of Chicken Feather-Teak wood Dus...Investigations of Mechanical Characteristics of Chicken Feather-Teak wood Dus...
Investigations of Mechanical Characteristics of Chicken Feather-Teak wood Dus...IJERDJOURNAL
 
CHARACTERIZATION OF TENSILE PROPERTIES OF TREATED BAMBOO NATURAL FIBRE POLYME...
CHARACTERIZATION OF TENSILE PROPERTIES OF TREATED BAMBOO NATURAL FIBRE POLYME...CHARACTERIZATION OF TENSILE PROPERTIES OF TREATED BAMBOO NATURAL FIBRE POLYME...
CHARACTERIZATION OF TENSILE PROPERTIES OF TREATED BAMBOO NATURAL FIBRE POLYME...IAEME Publication
 
s12008-023-012hhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhh15-w.pdf
s12008-023-012hhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhh15-w.pdfs12008-023-012hhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhh15-w.pdf
s12008-023-012hhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhh15-w.pdf32216116
 
Preparation and mechanical characterization of epoxy based composite develope...
Preparation and mechanical characterization of epoxy based composite develope...Preparation and mechanical characterization of epoxy based composite develope...
Preparation and mechanical characterization of epoxy based composite develope...eSAT Journals
 
Effect of Temperature on Wear Rate of Si-Epoxy- Eglass Polymer composite Mate...
Effect of Temperature on Wear Rate of Si-Epoxy- Eglass Polymer composite Mate...Effect of Temperature on Wear Rate of Si-Epoxy- Eglass Polymer composite Mate...
Effect of Temperature on Wear Rate of Si-Epoxy- Eglass Polymer composite Mate...IDES Editor
 
chemistry final year
chemistry final yearchemistry final year
chemistry final yearmalani pankaj
 
Fabrication & Characterization of Bio Composite Materials Based On Sunnhemp F...
Fabrication & Characterization of Bio Composite Materials Based On Sunnhemp F...Fabrication & Characterization of Bio Composite Materials Based On Sunnhemp F...
Fabrication & Characterization of Bio Composite Materials Based On Sunnhemp F...IJMER
 
Effect of Nanoparticles on E-Glass Fiber Epoxy Resin Composites
Effect of Nanoparticles on E-Glass Fiber Epoxy Resin CompositesEffect of Nanoparticles on E-Glass Fiber Epoxy Resin Composites
Effect of Nanoparticles on E-Glass Fiber Epoxy Resin CompositesIJMER
 
Analysis of the Flexure Behavior and Compressive Strength of Fly Ash Core San...
Analysis of the Flexure Behavior and Compressive Strength of Fly Ash Core San...Analysis of the Flexure Behavior and Compressive Strength of Fly Ash Core San...
Analysis of the Flexure Behavior and Compressive Strength of Fly Ash Core San...IJERA Editor
 
Study of the effects of carbon and glass fibre reinforcement and other filler...
Study of the effects of carbon and glass fibre reinforcement and other filler...Study of the effects of carbon and glass fibre reinforcement and other filler...
Study of the effects of carbon and glass fibre reinforcement and other filler...eSAT Journals
 
Study of the effects of carbon and glass fibre reinforcement and other filler...
Study of the effects of carbon and glass fibre reinforcement and other filler...Study of the effects of carbon and glass fibre reinforcement and other filler...
Study of the effects of carbon and glass fibre reinforcement and other filler...eSAT Publishing House
 

Similar to H013116878 (20)

Shellfish shell as a Bio-filler: Preparation, characterization and its effec...
	Shellfish shell as a Bio-filler: Preparation, characterization and its effec...	Shellfish shell as a Bio-filler: Preparation, characterization and its effec...
Shellfish shell as a Bio-filler: Preparation, characterization and its effec...
 
Fabrication, experimental investigation of jute fiber reinforced epoxy compos...
Fabrication, experimental investigation of jute fiber reinforced epoxy compos...Fabrication, experimental investigation of jute fiber reinforced epoxy compos...
Fabrication, experimental investigation of jute fiber reinforced epoxy compos...
 
EVALUATION OFTENSILE PROPERTIESOF EPOXY RESIN BASED COMPOSITES REINFORCED WIT...
EVALUATION OFTENSILE PROPERTIESOF EPOXY RESIN BASED COMPOSITES REINFORCED WIT...EVALUATION OFTENSILE PROPERTIESOF EPOXY RESIN BASED COMPOSITES REINFORCED WIT...
EVALUATION OFTENSILE PROPERTIESOF EPOXY RESIN BASED COMPOSITES REINFORCED WIT...
 
Ijciet 08 02_037
Ijciet 08 02_037Ijciet 08 02_037
Ijciet 08 02_037
 
Role of Natural and Synthetic Fillers on Erosive Wear Behavior of Basalt -Epo...
Role of Natural and Synthetic Fillers on Erosive Wear Behavior of Basalt -Epo...Role of Natural and Synthetic Fillers on Erosive Wear Behavior of Basalt -Epo...
Role of Natural and Synthetic Fillers on Erosive Wear Behavior of Basalt -Epo...
 
Fabrication and Characterization of Kevlar/Jute Reinforced Epoxy
Fabrication and Characterization of Kevlar/Jute Reinforced EpoxyFabrication and Characterization of Kevlar/Jute Reinforced Epoxy
Fabrication and Characterization of Kevlar/Jute Reinforced Epoxy
 
IRJET - A Review on Multi-Layered Armour using Sugarcane Bagasse Waste
IRJET -  	  A Review on Multi-Layered Armour using Sugarcane Bagasse WasteIRJET -  	  A Review on Multi-Layered Armour using Sugarcane Bagasse Waste
IRJET - A Review on Multi-Layered Armour using Sugarcane Bagasse Waste
 
U130403146155
U130403146155U130403146155
U130403146155
 
Enhancing Mechanical Properties of Jute Fibre/Glass Fiber and Epoxy Combined ...
Enhancing Mechanical Properties of Jute Fibre/Glass Fiber and Epoxy Combined ...Enhancing Mechanical Properties of Jute Fibre/Glass Fiber and Epoxy Combined ...
Enhancing Mechanical Properties of Jute Fibre/Glass Fiber and Epoxy Combined ...
 
Investigations of Mechanical Characteristics of Chicken Feather-Teak wood Dus...
Investigations of Mechanical Characteristics of Chicken Feather-Teak wood Dus...Investigations of Mechanical Characteristics of Chicken Feather-Teak wood Dus...
Investigations of Mechanical Characteristics of Chicken Feather-Teak wood Dus...
 
CHARACTERIZATION OF TENSILE PROPERTIES OF TREATED BAMBOO NATURAL FIBRE POLYME...
CHARACTERIZATION OF TENSILE PROPERTIES OF TREATED BAMBOO NATURAL FIBRE POLYME...CHARACTERIZATION OF TENSILE PROPERTIES OF TREATED BAMBOO NATURAL FIBRE POLYME...
CHARACTERIZATION OF TENSILE PROPERTIES OF TREATED BAMBOO NATURAL FIBRE POLYME...
 
s12008-023-012hhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhh15-w.pdf
s12008-023-012hhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhh15-w.pdfs12008-023-012hhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhh15-w.pdf
s12008-023-012hhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhhh15-w.pdf
 
Preparation and mechanical characterization of epoxy based composite develope...
Preparation and mechanical characterization of epoxy based composite develope...Preparation and mechanical characterization of epoxy based composite develope...
Preparation and mechanical characterization of epoxy based composite develope...
 
Effect of Temperature on Wear Rate of Si-Epoxy- Eglass Polymer composite Mate...
Effect of Temperature on Wear Rate of Si-Epoxy- Eglass Polymer composite Mate...Effect of Temperature on Wear Rate of Si-Epoxy- Eglass Polymer composite Mate...
Effect of Temperature on Wear Rate of Si-Epoxy- Eglass Polymer composite Mate...
 
chemistry final year
chemistry final yearchemistry final year
chemistry final year
 
Fabrication & Characterization of Bio Composite Materials Based On Sunnhemp F...
Fabrication & Characterization of Bio Composite Materials Based On Sunnhemp F...Fabrication & Characterization of Bio Composite Materials Based On Sunnhemp F...
Fabrication & Characterization of Bio Composite Materials Based On Sunnhemp F...
 
Effect of Nanoparticles on E-Glass Fiber Epoxy Resin Composites
Effect of Nanoparticles on E-Glass Fiber Epoxy Resin CompositesEffect of Nanoparticles on E-Glass Fiber Epoxy Resin Composites
Effect of Nanoparticles on E-Glass Fiber Epoxy Resin Composites
 
Analysis of the Flexure Behavior and Compressive Strength of Fly Ash Core San...
Analysis of the Flexure Behavior and Compressive Strength of Fly Ash Core San...Analysis of the Flexure Behavior and Compressive Strength of Fly Ash Core San...
Analysis of the Flexure Behavior and Compressive Strength of Fly Ash Core San...
 
Study of the effects of carbon and glass fibre reinforcement and other filler...
Study of the effects of carbon and glass fibre reinforcement and other filler...Study of the effects of carbon and glass fibre reinforcement and other filler...
Study of the effects of carbon and glass fibre reinforcement and other filler...
 
Study of the effects of carbon and glass fibre reinforcement and other filler...
Study of the effects of carbon and glass fibre reinforcement and other filler...Study of the effects of carbon and glass fibre reinforcement and other filler...
Study of the effects of carbon and glass fibre reinforcement and other filler...
 

More from IOSR Journals (20)

A011140104
A011140104A011140104
A011140104
 
M0111397100
M0111397100M0111397100
M0111397100
 
L011138596
L011138596L011138596
L011138596
 
K011138084
K011138084K011138084
K011138084
 
J011137479
J011137479J011137479
J011137479
 
I011136673
I011136673I011136673
I011136673
 
G011134454
G011134454G011134454
G011134454
 
H011135565
H011135565H011135565
H011135565
 
F011134043
F011134043F011134043
F011134043
 
E011133639
E011133639E011133639
E011133639
 
D011132635
D011132635D011132635
D011132635
 
C011131925
C011131925C011131925
C011131925
 
B011130918
B011130918B011130918
B011130918
 
A011130108
A011130108A011130108
A011130108
 
I011125160
I011125160I011125160
I011125160
 
H011124050
H011124050H011124050
H011124050
 
G011123539
G011123539G011123539
G011123539
 
F011123134
F011123134F011123134
F011123134
 
E011122530
E011122530E011122530
E011122530
 
D011121524
D011121524D011121524
D011121524
 

Recently uploaded

CloudStudio User manual (basic edition):
CloudStudio User manual (basic edition):CloudStudio User manual (basic edition):
CloudStudio User manual (basic edition):comworks
 
Transcript: #StandardsGoals for 2024: What’s new for BISAC - Tech Forum 2024
Transcript: #StandardsGoals for 2024: What’s new for BISAC - Tech Forum 2024Transcript: #StandardsGoals for 2024: What’s new for BISAC - Tech Forum 2024
Transcript: #StandardsGoals for 2024: What’s new for BISAC - Tech Forum 2024BookNet Canada
 
Automating Business Process via MuleSoft Composer | Bangalore MuleSoft Meetup...
Automating Business Process via MuleSoft Composer | Bangalore MuleSoft Meetup...Automating Business Process via MuleSoft Composer | Bangalore MuleSoft Meetup...
Automating Business Process via MuleSoft Composer | Bangalore MuleSoft Meetup...shyamraj55
 
Beyond Boundaries: Leveraging No-Code Solutions for Industry Innovation
Beyond Boundaries: Leveraging No-Code Solutions for Industry InnovationBeyond Boundaries: Leveraging No-Code Solutions for Industry Innovation
Beyond Boundaries: Leveraging No-Code Solutions for Industry InnovationSafe Software
 
"Federated learning: out of reach no matter how close",Oleksandr Lapshyn
"Federated learning: out of reach no matter how close",Oleksandr Lapshyn"Federated learning: out of reach no matter how close",Oleksandr Lapshyn
"Federated learning: out of reach no matter how close",Oleksandr LapshynFwdays
 
Integration and Automation in Practice: CI/CD in Mule Integration and Automat...
Integration and Automation in Practice: CI/CD in Mule Integration and Automat...Integration and Automation in Practice: CI/CD in Mule Integration and Automat...
Integration and Automation in Practice: CI/CD in Mule Integration and Automat...Patryk Bandurski
 
AI as an Interface for Commercial Buildings
AI as an Interface for Commercial BuildingsAI as an Interface for Commercial Buildings
AI as an Interface for Commercial BuildingsMemoori
 
Artificial intelligence in the post-deep learning era
Artificial intelligence in the post-deep learning eraArtificial intelligence in the post-deep learning era
Artificial intelligence in the post-deep learning eraDeakin University
 
Understanding the Laravel MVC Architecture
Understanding the Laravel MVC ArchitectureUnderstanding the Laravel MVC Architecture
Understanding the Laravel MVC ArchitecturePixlogix Infotech
 
Key Features Of Token Development (1).pptx
Key  Features Of Token  Development (1).pptxKey  Features Of Token  Development (1).pptx
Key Features Of Token Development (1).pptxLBM Solutions
 
#StandardsGoals for 2024: What’s new for BISAC - Tech Forum 2024
#StandardsGoals for 2024: What’s new for BISAC - Tech Forum 2024#StandardsGoals for 2024: What’s new for BISAC - Tech Forum 2024
#StandardsGoals for 2024: What’s new for BISAC - Tech Forum 2024BookNet Canada
 
costume and set research powerpoint presentation
costume and set research powerpoint presentationcostume and set research powerpoint presentation
costume and set research powerpoint presentationphoebematthew05
 
Pigging Solutions in Pet Food Manufacturing
Pigging Solutions in Pet Food ManufacturingPigging Solutions in Pet Food Manufacturing
Pigging Solutions in Pet Food ManufacturingPigging Solutions
 
Unleash Your Potential - Namagunga Girls Coding Club
Unleash Your Potential - Namagunga Girls Coding ClubUnleash Your Potential - Namagunga Girls Coding Club
Unleash Your Potential - Namagunga Girls Coding ClubKalema Edgar
 
Pigging Solutions Piggable Sweeping Elbows
Pigging Solutions Piggable Sweeping ElbowsPigging Solutions Piggable Sweeping Elbows
Pigging Solutions Piggable Sweeping ElbowsPigging Solutions
 
Benefits Of Flutter Compared To Other Frameworks
Benefits Of Flutter Compared To Other FrameworksBenefits Of Flutter Compared To Other Frameworks
Benefits Of Flutter Compared To Other FrameworksSoftradix Technologies
 
Connect Wave/ connectwave Pitch Deck Presentation
Connect Wave/ connectwave Pitch Deck PresentationConnect Wave/ connectwave Pitch Deck Presentation
Connect Wave/ connectwave Pitch Deck PresentationSlibray Presentation
 
Advanced Test Driven-Development @ php[tek] 2024
Advanced Test Driven-Development @ php[tek] 2024Advanced Test Driven-Development @ php[tek] 2024
Advanced Test Driven-Development @ php[tek] 2024Scott Keck-Warren
 
Install Stable Diffusion in windows machine
Install Stable Diffusion in windows machineInstall Stable Diffusion in windows machine
Install Stable Diffusion in windows machinePadma Pradeep
 
My Hashitalk Indonesia April 2024 Presentation
My Hashitalk Indonesia April 2024 PresentationMy Hashitalk Indonesia April 2024 Presentation
My Hashitalk Indonesia April 2024 PresentationRidwan Fadjar
 

Recently uploaded (20)

CloudStudio User manual (basic edition):
CloudStudio User manual (basic edition):CloudStudio User manual (basic edition):
CloudStudio User manual (basic edition):
 
Transcript: #StandardsGoals for 2024: What’s new for BISAC - Tech Forum 2024
Transcript: #StandardsGoals for 2024: What’s new for BISAC - Tech Forum 2024Transcript: #StandardsGoals for 2024: What’s new for BISAC - Tech Forum 2024
Transcript: #StandardsGoals for 2024: What’s new for BISAC - Tech Forum 2024
 
Automating Business Process via MuleSoft Composer | Bangalore MuleSoft Meetup...
Automating Business Process via MuleSoft Composer | Bangalore MuleSoft Meetup...Automating Business Process via MuleSoft Composer | Bangalore MuleSoft Meetup...
Automating Business Process via MuleSoft Composer | Bangalore MuleSoft Meetup...
 
Beyond Boundaries: Leveraging No-Code Solutions for Industry Innovation
Beyond Boundaries: Leveraging No-Code Solutions for Industry InnovationBeyond Boundaries: Leveraging No-Code Solutions for Industry Innovation
Beyond Boundaries: Leveraging No-Code Solutions for Industry Innovation
 
"Federated learning: out of reach no matter how close",Oleksandr Lapshyn
"Federated learning: out of reach no matter how close",Oleksandr Lapshyn"Federated learning: out of reach no matter how close",Oleksandr Lapshyn
"Federated learning: out of reach no matter how close",Oleksandr Lapshyn
 
Integration and Automation in Practice: CI/CD in Mule Integration and Automat...
Integration and Automation in Practice: CI/CD in Mule Integration and Automat...Integration and Automation in Practice: CI/CD in Mule Integration and Automat...
Integration and Automation in Practice: CI/CD in Mule Integration and Automat...
 
AI as an Interface for Commercial Buildings
AI as an Interface for Commercial BuildingsAI as an Interface for Commercial Buildings
AI as an Interface for Commercial Buildings
 
Artificial intelligence in the post-deep learning era
Artificial intelligence in the post-deep learning eraArtificial intelligence in the post-deep learning era
Artificial intelligence in the post-deep learning era
 
Understanding the Laravel MVC Architecture
Understanding the Laravel MVC ArchitectureUnderstanding the Laravel MVC Architecture
Understanding the Laravel MVC Architecture
 
Key Features Of Token Development (1).pptx
Key  Features Of Token  Development (1).pptxKey  Features Of Token  Development (1).pptx
Key Features Of Token Development (1).pptx
 
#StandardsGoals for 2024: What’s new for BISAC - Tech Forum 2024
#StandardsGoals for 2024: What’s new for BISAC - Tech Forum 2024#StandardsGoals for 2024: What’s new for BISAC - Tech Forum 2024
#StandardsGoals for 2024: What’s new for BISAC - Tech Forum 2024
 
costume and set research powerpoint presentation
costume and set research powerpoint presentationcostume and set research powerpoint presentation
costume and set research powerpoint presentation
 
Pigging Solutions in Pet Food Manufacturing
Pigging Solutions in Pet Food ManufacturingPigging Solutions in Pet Food Manufacturing
Pigging Solutions in Pet Food Manufacturing
 
Unleash Your Potential - Namagunga Girls Coding Club
Unleash Your Potential - Namagunga Girls Coding ClubUnleash Your Potential - Namagunga Girls Coding Club
Unleash Your Potential - Namagunga Girls Coding Club
 
Pigging Solutions Piggable Sweeping Elbows
Pigging Solutions Piggable Sweeping ElbowsPigging Solutions Piggable Sweeping Elbows
Pigging Solutions Piggable Sweeping Elbows
 
Benefits Of Flutter Compared To Other Frameworks
Benefits Of Flutter Compared To Other FrameworksBenefits Of Flutter Compared To Other Frameworks
Benefits Of Flutter Compared To Other Frameworks
 
Connect Wave/ connectwave Pitch Deck Presentation
Connect Wave/ connectwave Pitch Deck PresentationConnect Wave/ connectwave Pitch Deck Presentation
Connect Wave/ connectwave Pitch Deck Presentation
 
Advanced Test Driven-Development @ php[tek] 2024
Advanced Test Driven-Development @ php[tek] 2024Advanced Test Driven-Development @ php[tek] 2024
Advanced Test Driven-Development @ php[tek] 2024
 
Install Stable Diffusion in windows machine
Install Stable Diffusion in windows machineInstall Stable Diffusion in windows machine
Install Stable Diffusion in windows machine
 
My Hashitalk Indonesia April 2024 Presentation
My Hashitalk Indonesia April 2024 PresentationMy Hashitalk Indonesia April 2024 Presentation
My Hashitalk Indonesia April 2024 Presentation
 

H013116878

  • 1. IOSR Journal of Mechanical and Civil Engineering (IOSR-JMCE) e-ISSN: 2278-1684,p-ISSN: 2320-334X, Volume 13, Issue 1 Ver. I (Jan. - Feb. 2016), PP 68-78 www.iosrjournals.org DOI: 10.9790/1684-13116878 www.iosrjournals.org 68 | Page Sliding Wear Characteristics of Bone Powder Filled Hybrid Fiber Reinforced Epoxy Composites Sudeep Deshpande1 , T. Rangaswamy2 1 Department of Mechanical Engineering, SKSVMACET, Laxmeshwar - 582116, Karnataka, India 2 Department of Mechanical Engineering, G.E.C, Hassan, Karnataka, India Abstract: The aim of the research article is to study the dry sliding wear behaviour of epoxy with different wt.% of bone powder filled E-glass/jute fiber reinforced composites. Taguchi’s orthogonal array (L27) was used to investigate the influence of tribological parameters. The results indicated that when the filler content was increased up to 10 wt.% the specific wear rate was decreased but coefficient of friction increases. Form 10 wt.% to 15 wt.% of filler content specific wear rate was increased but coefficient of friction decreases. After the thorough analysis of control factors, optimal factor setting has been suggested for specific wear rate and coefficient of friction. Furthermore, the worn surfaces of the samples were analyzed by scanning electron microscopy (SEM) to study the wear mechanisms and to correlate them with the wear test results. Keywords: hybrid composites, wear test, Taguchi’s analysis, scanning electron microscopy. I. Introduction Natural fibers are a renewable resource and have several advantages associated with them, such as, they impart the composite high specific stiffness and strength, a desirable fiber aspect ratio, biodegradability, they are readily available from natural sources and more importantly they have a low cost per unit volume basis [1]. These natural fibers can be used in the manufacture of fiber based polymer composites because they posses attractive physical and mechanical properties. Polymer composites have a special property of self lubrication and this made the composites suitable in tribological applications such as cams, seals, brakes, bearings etc. F. Asuke et al., [2] have studied the effect of applied load on the wear behavior of polymer matrix composites produced by using carbonized bone particles (CBp) as reinforcement. The result shows that the wear rate increased with increases in applied load and decreased with increasing in carbonized bone particles. B. Suresha et al., [3] have done experiment on dry sliding wear and two-body abrasive wear behaviour of graphite filled carbon fabric reinforced epoxy composites. The results show that for increased load and sliding velocity, higher wear loss was recorded and wear is reduced to a greater extent by addition of the graphite filler in carbon-epoxy composite which was dominated by microplowing/microcutting mechanisms instead of microcracking. B. N. Ramesh and B. Suresha [4] have studied the abrasive wear behavior of carbon fabric reinforced epoxy composites filled with functional fillers like alumina (Al2O3) and molybdenum disulphide (MoS2) separately in different proportions. The experiments were planned according to Taguchi L18 orthogonal array. The result showed that the grit size, type of filler and filler loading were the most significant factors in controlling the specific wear rate of the C-E composite. S. Basavarajappa et al., [5] have experimentally investigated glass– epoxy composite with influence of graphite filler under varying applied load, sliding distance and sliding velocity by using a pin-on-disc apparatus. For increased applied load situation for pure glass–epoxy composite higher weight loss was recorded. As the percentage of graphite increases lower weight loss was observed in the glass–epoxy composite. Rashmi et al., [6] studied the dry sliding wear behaviour of epoxy with different wt.% of organo-modified montmorillonite (OMMT) filled nanocomposites and concluded that sliding distance was the most significant factor affecting wear rate of epoxy nanocomposites. Experimental results showed that the inclusion of 5 wt.% OMMT nanofiller increased the wear resistance of the epoxy nanocomposite. A. Rout and A. Satapathy [7] have done experiment on rice husk filled epoxy composites. Taguchi orthogonal array design and artificial neural network analysis was also carried out. The result showed that sliding velocity was the most infusing factor followed by filler content and normal load. They have concluded that rice husk filled composites improves the wear resistance. T. B. Yallew et al., [8] have fabricated woven jute fiber reinforced PP composites. The tribological behavior was analyzed by a computerized pin-on-disc wear testing machine at an dry operating condition with different working parameters of sliding speed (1–3 m/s), applied load (10–30 N) and sliding distance (1000–3000 m). The incorporation of woven jute fiber as reinforcement into PP matrix shows more than 65% reduction in specific wear rate and 45% reduction in the coefficient of friction. N. Mohan et al., [9] have fabricated with and without Tantalum Niobium Carbide (Ta/NbC) filled glass epoxy composites. These composites wear tested for dry sliding wear behavior at elevated temperatures. The result showed that as the temperature increases specific wear loss increases. Ta/NbC filled glass epoxy composites exhibited lower wear rate and higher coefficient of friction as compared with pure composite and worn surface was analyzed by
  • 2. Sliding Wear Characteristics Of Bone Powder Filled Hybrid Fiber Reinforced Epoxy Composites DOI: 10.9790/1684-13116878 www.iosrjournals.org 69 | Page scanning electron microscopy. F. Asuke et al., [10] have been studied the effects of uncarbonized (fresh) and carbonized bone particles on the microstructure and mechanical properties of polypropylene composites. The results showed that the addition of carbonized bone particles reinforcement composite has superior mechanical properties than uncarbonized bone particles composite. They have concluded that for optimum service condition and to have better mechanical properties bone particle addition should not exceed 15 wt.%. In view of the above, an attempt was made to study the effect of bone powder as a filler material in E-glass/jute fiber reinforced epoxy composites. The wear characteristics of these hybrid composites were investigated. II. Experimental Details 2.1. Materials In this work, 7-mil E-glass fiber as a reinforcement material was used which was supplied by Suntech Fibers Private Ltd. Woven jute fiber as a reinforcement material was used which was supplied by Jute Cottage, Bangalore. Unsaturated polyester epoxy L-12 (3202) manufactured by Atul LTD, Gujarat, India and supplied by Yuge marketing, Bangalore was used as matrix material and K-6 hardener was added to epoxy while fabricating the composite materials. Goat bones were washed and cleaned. Thin top surface layer of the bone was removed by using grinding machine and powder was prepared. An approximate density value of bone powder was 1.95 g/cc. 2.2. Fabrication of Composites The hybrid fiber reinforced epoxy composites were prepared by keeping constant 50 wt.% of epoxy and 50 wt.% of fiber (40 wt.% of E-glass fiber and 10 wt.% of jute fiber) as shown in “Table 1”. The composites filled with varying concentrations (0 wt.%, 10 wt.% and 15 wt.%) of bone powder were fabricated by using hand layup technique. Jute plies were placed in between E-glass plies and also E-glass plies were placed at extreme ends of the composites. The epoxy, hardener and fillers were mixed thoroughly in a basin and the mixture was subsequently stirred constantly. The woven E-glass and woven jute fiber was positioned manually. Mixture so made was brushed uniformly over the E-glass and jute plies. Entrapped air was removed manually with squeezes or rollers to complete the composite structure. The composites were put under load for about 24 hours for proper curing at room temperature. Table 1: Fabricated composites with constant 40 wt. % of E-glass fiber and 10 wt. % of jute fiber Hybrid composites Epoxy (wt.%) Filler material (wt.%) GJE 50 0% GJEB1 40 10% GJEB2 35 15% 2.3. Specimen Preparation The fabricated hybrid composites were taken out from the mould and then specimens of suitable dimensions were prepared from the composites for wear tests according to ASTM G99 standards. The composites were cut by using Zigzag board cutter machine. Three identical test specimens were prepared for each test. 2.4. Test of Density The theoretical density (ρt) of hybrid composite material in terms of weight fractions of different constituents can be obtained from the following “equation 1” [15]. 𝜌𝑡 = 1 𝑊 𝑔 𝜌 𝑔 + 𝑊 𝑗 𝜌 𝑗 + 𝑊 𝑚 𝜌 𝑚 + 𝑊 𝑓 𝜌 𝑓 (1) where, W and ρ represent the weight fraction and density respectively. The suffixes g, j, m and f stands for the E- glass fiber, jute fiber, matrix (epoxy) and filler respectively. The actual density (ρe) of the composite can be determined experimentally by simple water immersion technique. The volume fraction of voids (Vv) in the composites was calculated using the following “equation 2” [15]. 𝑉𝑣 = 𝜌 𝑡−𝜌 𝑒 𝜌 𝑡 (2)
  • 3. Sliding Wear Characteristics Of Bone Powder Filled Hybrid Fiber Reinforced Epoxy Composites DOI: 10.9790/1684-13116878 www.iosrjournals.org 70 | Page 2.5. Dry Sliding Wear Test Apparatus DUCOM pin on disc test apparatus was used to investigate the dry sliding wear characteristics of hybrid composite specimens as per ASTM G99 standards. The disc made of hardened EN-31 hardened ground steel to 62 HRC, surface roughness 1.6 μm Ra, 120 mm track diameter and 8 mm thick. Specimen with size of 10 mm x 10 mm x 30 mm was subjected vertically to the counter face where the contact area was constant. Wear test was carried out for the constant sliding distance of 2000 m, sliding velocities of 1.4 m/sec, 2 m/sec and 2.6 m/sec against normal loads of 20 N, 40 N, and 60 N and wear rate data reported was the average of two runs. Care was to see that the specimen was continuously cleaned with woolen cloth to avoid the entrapment of wear debris and to achieve uniform experimental procedure. After each test the disc was cleaned using acetone solution. The initial weight before run and final weight after run was measured using a precision electronic balance with an accuracy of ± 0.01 mg. The specific wear rate (mm3 /Nm) was then expressed on „volume loss basis as shown below “equation 3” [4]. 𝐾𝑠 = ∆𝑚 𝜌𝑡𝑣𝐹 (3) where, Ks = Specific wear rate (mm3 /Nm), ∆m = Mass loss (gms), 𝜌 = Density of specimen (g/cc), t = Test duration (sec), v = sliding velocity (m/s), F = Applied load (N). 2.6. Taguchi Experimental Design Taguchi technique was used for analyzing the influence of control factors on performance output. The most important stage in the design of experiment lies in the selection of the control factors. In the present work, the impact of three parameters such as sliding velocity, normal load and filler content were studied using L27 (313 ) Taguchi orthogonal design. The experimental results were transformed into a signal-to-noise (S/N) ratio. The S/N ratio for minimum wear rate coming under “smaller is better” characteristic, and it was calculated as logarithmic transformation of the loss function as shown below “equation 4” [8]. 𝑆 𝑁 = −10 𝑙𝑜𝑔 1 𝑛 𝑦1 2 + 𝑦2 2 + ⋯ 𝑦𝑛 2 (4) where „n‟ indicates the repeated number of trial conditions, y1, y2….yn indicates the response of the dry sliding wear characteristics respectively. For „„Lower is better” (LB) characteristic of the above S/N ratio transformation, it was suitable for minimizations of coefficient of friction and specific wear rate. The standard linear graph was used to assign the factors and interactions to various columns of the orthogonal array. The plan of the experiments: The experiments were conducted as per the standard orthogonal array L27 (313 ). The selection of the orthogonal array was based on the condition that the degree of freedom for the orthogonal array should be greater than or equal to sum of those wear parameters. In the present investigation L27 Taguchi orthogonal array was chosen, this has 27 rows and 13 columns. The wear parameters chosen were (1) sliding velocity (2) normal load and (3) filler content and their levels indicated in “Table 2”. The experiments consisted of 27 tests (each row in the L27 orthogonal array) and were assigned with parameters. The first column in table was assigned to sliding velocity (S), second column was assigned to normal load (L), fifth column was assigned to filler content (FC) and remaining columns were assigned to their interactions. The dry sliding wear tests results were subjected to the analysis of variance. Table 2: Levels of variables used in the experiments Control factor Symbols Level I II III Units Sliding velocity A 1.4 2 2.6 m/s Normal load B 20 40 60 N Filler content C 0 10 15 % III. Results and Discussion 3.1. Density In the present research work, the theoretical and experimental densities of hybrid composites along with the corresponding volume fraction of voids are presented in “Table 3”. It was found that the composite density values calculated theoretically from weight fractions were not equal to the experimentally measured values. It was evident that the density values for hybrid composites increase with the addition of filler content. It was further observed that with the incorporation of fillers, the void fractions in these composites also increase. Similar observation has been reported earlier for hybrid composites filled with different filler content.
  • 4. Sliding Wear Characteristics Of Bone Powder Filled Hybrid Fiber Reinforced Epoxy Composites DOI: 10.9790/1684-13116878 www.iosrjournals.org 71 | Page Table 3: Theoretical and experimental densities of hybrid composites Hybrid composites Theoretical density in gm/cc Experimental density in gm/cc Volume fraction of voids in % GJE 1.6183 1.5621 3.47 GJEB1 1.6919 1.6255 3.92 GJEB2 1.7312 1.6120 6.88 3.2. Wear Properties The experimental data for specific wear rate and coefficient of friction of bone powder filled hybrid composites reported in the “Table 4”. The overall mean for the S/N ratio of the specific wear rate and the coefficient of friction are found to be 91.995 db and 7.105 db respectively. Table 4: Experimental design using L27 array for bone powder filled hybrid composites S. No Sliding Velocity (S) in m/s Normal Load (L) in N Filler content (FC) in % Specific Wear Rate (W) in mm3 /Nm S/N Ratio (db) Coefficient of Friction (μ) S/N Ratio (db) 1 1.4 20 GJE 8.01E-05 81.93 0.396 8.046 2 1.4 20 GJEB1 1.58E-05 96.05 0.593 4.539 3 1.4 20 GJEB2 1.58E-05 96.02 0.195 14.199 4 1.4 40 GJE 7.20E-05 82.85 0.427 7.391 5 1.4 40 GJEB1 7.88E-06 102.07 0.528 5.547 6 1.4 40 GJEB2 5.53E-05 85.14 0.37 8.636 7 1.4 60 GJE 4.27E-05 87.39 0.48 6.375 8 1.4 60 GJEB1 1.58E-05 96.05 0.636 3.931 9 1.4 60 GJEB2 2.11E-05 93.52 0.414 7.660 10 2 20 GJE 7.99E-05 81.95 0.369 8.659 11 2 20 GJEB1 1.57E-05 96.07 0.612 4.265 12 2 20 GJEB2 6.31E-05 84.00 0.507 5.900 13 2 40 GJE 3.99E-05 87.97 0.452 6.897 14 2 40 GJEB1 1.57E-05 96.07 0.675 3.414 15 2 40 GJEB2 1.58E-05 96.04 0.398 8.002 16 2 60 GJE 3.73E-05 88.57 0.293 10.663 17 2 60 GJEB1 1.05E-05 99.60 0.467 6.614 18 2 60 GJEB2 1.58E-05 96.04 0.352 9.069 19 2.6 20 GJE 6.41E-05 83.86 0.366 8.730 20 2.6 20 GJEB1 4.73E-05 86.50 0.689 3.236 21 2.6 20 GJEB2 3.17E-05 89.99 0.37 8.636 22 2.6 40 GJE 4.81E-05 86.36 0.437 7.190 23 2.6 40 GJEB1 7.89E-06 102.06 0.617 4.194 24 2.6 40 GJEB2 7.91E-06 102.03 0.339 9.396 25 2.6 60 GJE 2.67E-05 91.46 0.479 6.393 26 2.6 60 GJEB1 3.68E-05 88.68 0.637 3.917 27 2.6 60 GJEB2 5.28E-06 105.55 0.304 10.343 Table 5: Response table for specific wear rate of bone powder filled hybrid composites Level A B C 1 91.23 88.49 85.82 2 91.81 93.4 95.91 3 92.95 94.1 94.26 Delta 1.72 5.61 10.09 Rank 3 2 1
  • 5. Sliding Wear Characteristics Of Bone Powder Filled Hybrid Fiber Reinforced Epoxy Composites DOI: 10.9790/1684-13116878 www.iosrjournals.org 72 | Page 2.62.01.4 95.0 92.5 90.0 87.5 85.0 604020 GJEB2GJEB1GJE 95.0 92.5 90.0 87.5 85.0 Sliding Velocity (S) in m/s MeanofSNratios Load Filler content (FC) in % Main Effects Plot for SN ratios Data Means Signal-to-noise: Smaller is better Table 6: ANOVA table for specific wear rate of bone powder filled hybrid composites Source DF Seq SS Adj SS Adj MS Test F P (%) A 2 1.50 1.498 0.75 0.38 1.05 B 2 23.89 23.89 11.95 6.13 16.67 C 2 63.41 63.41 31.71 16.26 44.25 A*B 4 13.02 13.02 3.26 1.67 9.09 A*C 4 15.06 15.06 3.77 1.93 10.51 B*C 4 10.84 10.84 2.71 1.39 7.57 Residual Error 8 15.57 15.57 1.95 10.87 Total 26 143.29 100.00 DF - degree of freedom, Seq SS - sequential sum of squares, Adj. SS - extra sum of squares, Seq MS - sequential mean squares, F - F-test and P - percent contribution Figure 1: Effect of control factors on specific wear rate of hybrid composites Figure 2: Interaction graph between sliding velocity and filler content for specific wear rate 2.62.01.4 100.0 97.5 95.0 92.5 90.0 87.5 85.0 Sliding Velocity (S) in m/s SNratios GJE GJEB1 GJEB2 (FC) in % Filler content Interaction Plot for SN ratios Data Means Signal-to-noise: Smaller is better
  • 6. Sliding Wear Characteristics Of Bone Powder Filled Hybrid Fiber Reinforced Epoxy Composites DOI: 10.9790/1684-13116878 www.iosrjournals.org 73 | Page Figure 3: Interaction graph between sliding velocity and normal load for specific wear rate Figure 4: Interaction graph between normal load and filler content for specific wear rate 3.2.1 ANOVA and Effects of Factors on Specific Wear Rate From the ANOVA “Table 6” it was observed that the filler content (C) factor (P = 44.25%), normal load (B) factor (P = 16.67%) and interaction (AxC) between sliding velocity x filler content (P = 10.51%) have great influence on the specific wear rate and hence theses are physically and statistically highly significant. However interaction (AxB) between sliding velocity x normal load (P = 9.09%), (BxC) interaction between normal load x filler content (P = 7.57%) and sliding velocity (A) factor (P = 1.10%) have lesser effect on specific wear rate as error value (P = 10.87) was higher side hence less significant. From the analysis of ANOVA and response “Table 5” of the S/N ratio for specific wear rate, it was observed that the filler content has major impact on specific wear rate followed by normal load and sliding velocity. The influence of each control factor (sliding velocity, normal load and filler content) on the specific wear rate was analysed with a main effects plot as shown in “Fig. 1” and an interaction plot as shown in “Figs. 2 to 4”. From the analysis of ANOVA and response “Table 5” of the S/N ratio for specific wear rate, it was observed that the filler content (C) has major impact on the specific wear rate followed by the normal load (B) and sliding velocity (A). It means that for bone powder filled hybrid composites with the increases of the filler 604020 100 95 90 85 80 Load SNratios GJE GJEB1 GJEB2 (FC) in % Filler content Interaction Plot for SN ratios Data Means Signal-to-noise: Smaller is better 2.62.01.4 98 96 94 92 90 88 86 Sliding Velocity (S) in m/s SNratios 20 40 60 Load Interaction Plot for SN ratios Data Means Signal-to-noise: Smaller is better
  • 7. Sliding Wear Characteristics Of Bone Powder Filled Hybrid Fiber Reinforced Epoxy Composites DOI: 10.9790/1684-13116878 www.iosrjournals.org 74 | Page 2.62.01.4 9 8 7 6 5 604020 GJEB2GJEB1GJE 9 8 7 6 5 Sliding Velocity (S) in m/s MeanofSNratios Load Filler content (FC) in % Main Effects Plot for SN ratios Data Means Signal-to-noise: Smaller is better content, sliding velocity and normal load the specific wear rate decreases i.e., good wear resistance. It was also observed that the filler content plays adverse effect, when the filler content was increased from 0 wt.% to 10 wt.% the specific wear rate was decreased and for 10 wt.% to 15 wt.% it further increases. Analysis of these results leads to the conclusion that optimal values of the parameters for minimizing the wear rate when the sliding velocity and normal load were at level 3 and the filler content was at level 2. Table 7: Response table for COF of bone powder filled hybrid composites Level A B C 1 7.369 7.357 7.816 2 7.054 6.741 4.406 3 6.893 7.218 9.093 Delta 0.477 0.616 4.687 Rank 3 2 1 Table 8: ANOVA table for COF of bone powder filled hybrid composites Source DF Seq SS Adj SS Adj MS Test F P (%) A 2 0.00900 0.00900 0.00450 1.52718 2.07 B 2 0.00022 0.00022 0.00011 0.03733 0.05 C 2 0.30110 0.30110 0.15055 51.09278 69.33 A*B 4 0.05480 0.05480 0.01370 4.64943 12.62 A*C 4 0.02850 0.02850 0.00713 2.41804 6.56 B*C 4 0.01711 0.01711 0.00428 1.45167 3.94 Residual Error 8 0.02357 0.02357 0.00295 5.43 Total 26 0.43430 100.00 DF - degree of freedom, Seq SS - sequential sum of squares, Adj. SS - extra sum of squares, Seq MS - sequential mean squares, F - F-test and P - percent contribution Figure 5: Effect of control factors on COF hybrid composites 3.2.2 ANOVA and Effects of Factors on Coefficient Of Friction ANOVA “Table 8” for the coefficient of friction that the filler content (C) factor (P = 69.33%), interaction between sliding velocity x normal load (AxB) and the interactions between sliding velocity x filler content (AxC) have significant influence on the coefficient of friction. However interaction of normal load x filler content (P = 3.94%), sliding velocity (P = 2.07%) and normal load (B) factor (P = 0.05%) do not have a significant effect (both physically and statistical) on coefficient of friction as their values are quite smaller than error (P = 5.43%) so they are neglected. From the analysis of ANOVA and response “Table 7” of the S/N ratio
  • 8. Sliding Wear Characteristics Of Bone Powder Filled Hybrid Fiber Reinforced Epoxy Composites DOI: 10.9790/1684-13116878 www.iosrjournals.org 75 | Page of coefficient of friction, it was observed that the control parameter filler content (C) has major impact on coefficient of friction followed by normal load and sliding velocity. The influence of each control factor on the coefficient of friction was analyzed with a main effects plot as shown in “Fig. 5” and an interaction plot as shown in “Figs. 6 to 8”. From the analysis of ANOVA and response “Table 7” of the S/N ratio for coefficient of friction, it was observed that the control factor filler content (C) has major impact on the coefficient of friction. It means that for bone powder filled hybrid composites, with the increases of the filler content from 0 wt.% to 10 wt.% coefficient of friction increases and from 10 wt.% to 15 wt.% coefficient of friction decreases. The same trend was observed for normal load. With the increase of sliding velocity coefficient of friction decreases. Analysis of these results leads to the conclusion that optimal values of the parameters for minimizing the wear rate when the sliding velocity and normal load were at level 1 and the filler content was at level 3. Figure 6: Interaction graph between sliding velocity and normal load for coefficient of friction Figure 7: Interaction graph between sliding velocity and filler content for coefficient of friction 2.62.01.4 9.0 8.5 8.0 7.5 7.0 6.5 6.0 Sliding Velocity (S) in m/s SNratios 20 40 60 Load Interaction Plot for SN ratios Data Means Signal-to-noise: Smaller is better 2.62.01.4 11 10 9 8 7 6 5 4 3 Sliding Velocity (S) in m/s SNratios GJE GJEB1 GJEB2 (FC) in % Filler content Interaction Plot for SN ratios Data Means Signal-to-noise: Smaller is better
  • 9. Sliding Wear Characteristics Of Bone Powder Filled Hybrid Fiber Reinforced Epoxy Composites DOI: 10.9790/1684-13116878 www.iosrjournals.org 76 | Page Figure 8: Interaction graph between normal load and filler content for coefficient of friction 3.2.3 Surface Morphology of Bone Powder Filled Hybrid Composites (a) (b) (c) (d) 604020 10 9 8 7 6 5 4 Load SNratios GJE GJEB1 GJEB2 (FC) in % Filler content Interaction Plot for SN ratios Data Means Signal-to-noise: Smaller is better
  • 10. Sliding Wear Characteristics Of Bone Powder Filled Hybrid Fiber Reinforced Epoxy Composites DOI: 10.9790/1684-13116878 www.iosrjournals.org 77 | Page (e) (f) Figure 9: SEM pictures of composites for bone powder filled hybrid composites When compared with sliding velocity and normal load the effect of filler content on specific wear rate was more as seen from main effect plot as shown in “Fig. 1”. For analysis different filler content hybrid composite samples with all samples tested for 20N normal load were selected. “Figs. 9(a) to 9(c)” shows the SEM pictures of composites for different filler content (0, 10 and 15 wt.%) of bone powder filled hybrid composites. The micrograph in “Fig. 9(a)” shows the wedge formation, fiber exposure and plastic deformation of matrix which results maximum wear. The SEM picture as shown in “Fig. 9(b)” illustrates only a few fibers exposure when compared with “Fig. 9(a)” and less deformation of the matrix which indicates less wear. “Fig. 9(c)” shows more plastic deformation of the matrix which slightly increases the wear rate when compared with “Fig. 9(b)”. Similarly, coefficient of friction was affected by filler content as seen from main effect plot (“Fig. 5”), So SEM images were selected for different filler content of hybrid composites. “Figs. 9(d) to 9(e)” shows the SEM pictures for different filler content (0 wt.%, 10 wt.% and 15 wt.%) of bone powder filled hybrid composites. The worn surface of the “Figs. 9(d) and 9(f)” shows the wear track, minor crack and only few fibers exposed from the matrix which has less coefficient of friction. The SEM picture for “Fig. 9(e)” sample shows the wear track on the surface, breakage of fibers and more number of fibers exposed which increased the coefficient of friction due to the rubbing action of the fibers with the disc surface. IV. Conclusions The experimental investigation on dry sliding wear behaviour of bone powder filled epoxy composites leads to the following conclusions:  Successful fabrication of bone powder filled E-glass/jute fiber reinforced epoxy composite has been done by the hand lay-up technique.  Dry sliding wear response of these hybrid composites under different loads, filler content and sliding velocities can be successfully analyzed using Taguchi‟s experimental design method. Taguchi‟s method provides a simple, systematic and efficient methodology for the optimization of the control factors. While filler content emerges as the most significant factor affecting wear rate of bone power filled epoxy hybrid composites, other factors like load and sliding velocity have less influence on specific wear rate.  The SEM micrographs of the specimen revels wear track, exposure of fibers due to wear of the matrix, debris formation, fiber breakage, plastic deformation of matrix and fiber matrix debonding. References [1] T. Sen, H. N. Jagannatha Reddy, ”Efficacy of bio derived jute FRP composite based technique for shear strength retrofitting of reinforced concrete beams and its comparative analysis with carbon and glass FRP shear retrofitting schemes”, Sustainable Cities and Society, Vol. 13, 2014, pp 105-124 [2] F. Asuke, M. Abdulwahab, V.S. Aigbodion, O. S. I. Fayomi and O. Aponbiede, “Effect of load on the wear behavior of polypropylene/carbonized bone ash particulate composite”, Egyptian Journal of Basic and Applied Sciences, Vol. 1, 2014, pp 67-70 [3] B. Suresha, Siddaramaiah, Kishore, S. Seetharamu and P. S. Kumaran, “Investigations on the influence of graphite filler on dry sliding wear and abrasive wear behaviour of carbon fabric reinforced epoxy composites”, Wear Vol. 267, 2009, pp 1405-1414 [4] B. N. Ramesh and B. Suresha, “Optimization of tribological parameters in abrasive wear mode of carbon-epoxy hybrid composites”, Materials and Design, Vol. 59, 2014, pp 38-49 [5] S. Basavarajappa, S. Ellangovan and K. V. Arun, “Studies on dry sliding wear behaviour of graphite filled glass–epoxy composites”, Materials and Design, Vol. 30, 2009, pp 2670-2675
  • 11. Sliding Wear Characteristics Of Bone Powder Filled Hybrid Fiber Reinforced Epoxy Composites DOI: 10.9790/1684-13116878 www.iosrjournals.org 78 | Page [6] Rashmi, N. M. Renukappa, B. Suresha, R. M. Devarajaiah and K. N. Shivakumar, “Dry sliding wear behaviour of organo-modified montmorillonite filled epoxy nanocomposites using Taguchi‟s techniques”, Materials and Design, Vol. 32, 2011, pp 4528-4536 [7] A. Rout and A. Satapathy, “Analysis of dry sliding wear behavior of rice husk filled epoxy composites using design of experiment and ANN”, Proc Engineering, Vol. 38, 2012, pp 1218-1232 [8] T. B. Yallew, Pradeep Kumar and I. Singh, “Sliding wear properties of jute fabric reinforced polypropylene composites”, Proc Engineering, Vol. 97, 2014, pp 402-411 [9] N. Mohan, C. R. Mahesha, Shivarudraiah, N. R. Mathivanan and B. shivamurthy, “Dry sliding wear behavior of Ta/Nbc filled- epoxy composites at elevated temperatures”, Proc Engineering, Vol. 64, 2013, pp 1166-1172 [10] F. Asuke, V. S. Aigbodion, M. Abdulwahab, O. S. I. Fayomi, A. P. I. Popoola, C.I. Nwoyi and B. Garba, “Effects of bone particle on the properties and microstructure of polypropylene/bone ash particulate composites”, Results in Physics,Vol. 2, 2012, pp 135- 141. [11] H. Abdellaoui, H. Bensalah, J. Echaabi, R. Bouhfid and A. Qaiss, “Fabrication, characterization and modelling of laminated composites based on woven jute fibres reinforced epoxy resin”, Materials and Design, Vol. 68, 2015, pp 104-133 [12] Md. R. Rahman, Md. M. Huque, Md. N. Islam and M. Hasan, “Improvement of physico-mechanical properties of jute fiber reinforced polypropylene composites by post-treatment”, Composites: Part A, Vol. 39, 2008, pp 1739-1747 [13] M. Jawaid, H. P. S. Abdul Khalil, A. Abu Bakar and P. N. Khanam, “Chemical resistance, void content and tensile properties of oil palm/jute fibre reinforced polymer hybrid composites”, Materials and Design, Vol. 32, 2011, pp 1014-1019 [14] V. Mishra and S. Biswas, “Physical and mechanical properties of bi-directional jute fiber epoxy composites”, Proc Engineering, Vol. 51, 2013, pp 561-566 [15] A. Gopinatha, M. Senthil Kumar and A. Elayaperumal, “Experimental investigations on mechanical properties of jute fiber reinforced composites with polyester and epoxy resin matrices”, Proc Engineering, Vol. 97, 2014, pp 2052-2063 [16] C. Fukuda, K. Goto, M. Imamura, M. Neo and T. Nakamura, “Bone bonding ability and handling properties of a titania– polymethylmethacrylate(PMMA) composite bioactive bone cement modified with a unique PMMA powder”, Acta Biomaterialia, Vol. 7, 2011, pp 3595-3600 [17] J. Sudeepan, K. Kumar, T. K. Barman and P. Sahoo, “Study of friction and wear of ABS/Zno polymer composite using Taguchi technique”, Proc Materials Science, Vol. 6, 2014, pp 391-400 [18] N. Dayma, B. K. Satapathy and A. Patnaik, “Structural correlations to sliding wear performance of PA-6/PP-g-MA/nanoclay ternary nanocomposites”, Wear, Vol. 271, 2011, pp 827-836 [19] B. Suresha, R. M. Devarajaiah, T. Pasang and C. Ranganathaiah, “Investigation of organo-modified montmorillonite loading effect on the abrasion resistance of hybrid composites”, Materials and Design, Vol. 47, 2013, pp 750-758 [20] U. Nirmal, J. Hashim and M. M. H. Megat Ahmad, “A review on tribological performance of natural fibre polymeric composites”, Tribology International, Vol. 83, 2015, pp 77-104 [21] H. Md. Akil, C. Santulli, F. Sarasini, J. Tirillo and T. Valente, “Environmental effects on the mechanical behaviour of pultruded jute/glass fibre-reinforced polyester hybrid composites”, Composites Science and Technology, Vol. 94, 2014, pp 62-70 [22] Y. Arao, T. Fujiura, S. Itani and T. Tanaka, “Strength improvement in injection-molded jute-fiber-reinforced polylactide green- composites”, Composites: Part B, Vol. 68, 2015, pp 200-206 [23] R. Codispoti, D. V. Oliveira , R. S. Olivito , P. B. Lourenco and R. Fangueiro, “Mechanical performance of natural fiber-reinforced composites for the strengthening of masonry”, Composites: Part B, Vol. 77, 2015, pp 74-83 [24] Pantamanatsopa, W. Ariyawiriyanan, T. Meekeaw, R. Suthamyong, K. Arrub and H. Hamada, “Effect of modified jute fiber on mechanical properties of green rubber composite”, Energy Proc, Vol. 56, 2014, pp 641-647 [25] M. Ramesh, K. Palanikumar and K. H. Reddy, “Comparative evaluation on properties of hybrid glass fiber- sisal/jute reinforced epoxy composites”, Proc Engineering, Vol. 51, 2013, pp 745-750