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International Journal of Scientific Research and Engineering Development-– Volume 2 Issue 5, Sep – Oct 2019
Available at www.ijsred.com
ISSN : 2581-7175 ©IJSRED: All Rights are Reserved Page 853
Testing of Coconut Shell Reinforced Brake PADS
P.Pathmanaban1*
, A. Musharath Aalam, 1
A.selvaganesh2
, S.Sr,iamrish3
1*
Assistant professor, Department of Automobile Engineering, Velammal Engineering College, Chennai-66
123
UG Students, Department of Automobile Engineering, Velammal Engineering College, Chennai-66
Abstract:
Asbestos had been used by manufacturers to produce brake pads, but it turned out to be harmful and toxic in
nature. So the manufacturers had decided not to manufacture brake pads using Asbestos. It can cause health issues like
asbestosis, mesothelioma and lung cancers too. Thus the brake pads can be manufactured using some natural fibres like
coconut shell as reinforcement material, along with Graphite which can act as better friction material, Alumina as
abrasive material, and, Epoxy resin as a binder. This will make brake pads function well with high friction co-efficient
and less wear rate and by using natural waste material as reinforced material, it is good for the environment too. It has its
advantages as it makes less noise than metallic brake pads, thus reducing noise pollution. About the tests conducted,
various samples were collected by varying the compositions and were tested at various speeds. The wear rate was
calculated and, the co-efficient of friction was also investigated. Sample four has given the better result than others. It is
observed that, the naturally produced brake pads can be a considerable alternate for Asbestos.
Keywords: Coconut Shell powder, Wear rate, brake pads, Epoxy Resin, compression strength.
I.INTRODUCTION
Composite materials are getting trending nowadays for
manufacturing of several materials based upon
automobile and aerospace components. Study of
Tribology and R&D will be concentrating on the
continual growth of natural fibres ( i.e. palm kernel,
coconut shells etc..).coconut shells are more relatively
similar to wood as it consists of cellulose, lignin,
pentosans and Ash. domination of bio and agro-based
products will contribute the engineering materials in
coming times. The main aspect for the usage of natural
fibre instead of artificial components is lightweight and
good in matrix adhesion of fibres for eco-friendly
condition and environmental regulation industries
triggered towards natural fibre materials.in current
situation, 33billion coconut is harvested throughout the
world in that only 1/6 of coconut are used for their
fibres[1,2]. for safety purpose and resist of motion at a
high or moderate speed of the vehicle or to control any
prime movers, the braking system plays a major role in
this scenario with help brake pads[3]. Brake pad
consists of brake lining when it subjected braking effect
it causes high friction and high heat liberation by a
material which simultaneously increases the wear rate.
Brake pads were made out categorized material like
organic, metallic, semi-metallic. moreover, modern
brake pad consists of asbestos ceramic, graphite. These
material are used due to high resistant wear and reduce
heat liberation but the major drawback is asbestos
causes a series effect on human health like
mesothelioma and asbestos-related lung cancer
[4].advantage in natural fibre polymer such as leading
high strength, it can be recycled easily and also a
RESEARCH ARTICLE OPEN ACCESS
International Journal of Scientific Research and Engineering Development-– Volume 2 Issue 5, Sep – Oct 2019
Available at www.ijsred.com
ISSN : 2581-7175 ©IJSRED: All Rights are Reserved Page 854
renewable source. Natural fibre enhances the reduction
in weight of material than other metallic materials and
it will be low in economical wise; in an environmental
point of view, natural fibre is more eco-friendly than
others[5]. 30% of coconut shell and epoxy or resin
polymer matrix tends to form a filled composite of
natural fibre. The simultaneously enhance tensile
strength and young modulus of material [6].
Concentration on the effect of reduction in wear rate
will spontaneously reduce the harmful effect of
environment tragedies. More than 50 components are
reinforced in their desired category to the material
highly efficient brake pad. Multiple components in
brake pads are categorized mainly as fibres, Fillers,
blinders, frictional reduction agent. However
mechanical properties will be influence Brake pads
using fibres. Moreover, production cost and
machinability of brake pads are improved using filler
material. For better optimise performance filler
contributes its roll in brake pads [7]. Wear rate and
friction properties of brake pad will further growth by
addition of blinders[8].in this research, aims to use of
waste agro material as utilization of brake pads
material, through investigation of this research, strength
and friction rate on brake pads are highly efficient when
subjected to commercial use of this reinforced
composite materials.
II. MATERIALS AND METHODS
A. Materials
Material of reinforcement used here is Coconut shell,
obtained from a coconut trader in Chennai from a local
industry, whereas, the graphite powder, which is going
to act as a friction modifier, is extracted from 1.5 V dry
cell batteries and Alumina, which is suited to act as an
abrasive material is purchased from a local chemical
store in Chennai. And also, Epoxy resin which serves as
binder is obtained from a chemical store in Chennai
was used jointly with a hardener to give desired
property.
B. Method
The initial process flow involves preparation of coconut
shell and graphite powder by carrying out processes
like removing of shell fibres from coconut and washing
the obtained shell with soap and detergent, followed by
cleaning using a clean dry cloth and drying it in the
oven at 150 0
C for nearly 3 hours. After that, crushing
the dried coconut shell using mortar and pestle is done
and fine grain size of 100 micrometres is obtained. The
sieve size of 100 micrometres of Coconut shell was
added in varying percentages to Aluminum oxide,
Graphite and epoxy resin based on 176 g weight of
commercial brake pad. To achieve homogenous steady-
state condition for the moulding process, each sample
combination is separately dry-mixed using a blender.
Fig . 1 Compression moulding machine
International Journal of Scientific Research and Engineering Development-– Volume 2 Issue 5, Sep – Oct 2019
Available at www.ijsred.com
ISSN : 2581-7175 ©IJSRED: All Rights are Reserved Page 855
Table 1: composition variation for different samples
C. Preparation:
Compression moulding machine is used in the
production of brake pad samples and a standard method
specified [11] is followed. During the process, the
sample composition is varied and the process factors
like Molding pressure (MP), Molding temperature
(MT), Curing time (CT), Heat treatment time (HTT) is
kept constant for all samples. Fig 1 shows the moulding
machine and Table 2 shows the detailed specification of
the machine.
Molding pressure (MP) = 14(MPa)
Capacity = 750 k N
Molding temperature (MT) = 140(0
C)
Curing time (CT) = 8(min)
Heat treatment time (HTT) = 1(hr)
The samples, which are in various proportions are
manually stirred in the definite composition as referred
in Table 1 and are stirred thoroughly and were
transferred into the mould for compression moulding.
Furthermore, the moulded samples are heated at 150 0
C
for particular heat treatment time as shown above.
D. Wear rate:
Wear rate of samples pin on the Disc Wear Testing
Machine per the ASTM G-99 standard [9]]. The sample
is of cylindrical in shape of size 8mm in diameter and
30mm length
were prepared for all compositions of the fibres which
is as shown in Fig.2. These tests were carried out at a
load of 20N at different speeds. The accompanying
condition is utilized to calculate the wear rate [10]. The
sliding distance (D) and wear rate (Wr) were calculated
using the following Equations.
.
Sliding distance (D) = 2Nπdt
Wr =
	 	 	( )	
	 	( )								
Where d is the disk diameter
t is the time of exposure of the specimen to
abrasion and
N is the radial speed, respectively.
Table 2: Hotpress specifications
E. Observations
Fig.2. Wear rate comparison of samples
WEARRATE(MG/METRE)
SPEED(RPM)
GRAPH
sample 1
sample 2
sample 3
sample 4
COMPOSITION (%)
Samp
le no.
Coconut
shell
Aluminiu
m oxide
Graphite
Epoxy
resin
S1 10 20 35 35
S2 20 15 30 35
S3 30 10 25 35
S4 40 5 20 35
Particulars Specifications
Max. Day Light 150 mm
No. Of Day Light 2
Platen size 350mm X 350mm
Ram Diameter 200 mm
Heating Capacity 400ºC
Max Pressure 210 bars
International Journal of Scientific Research and Engineering Development
ISSN : 2581-7175
Fig. 3 sample compositions
Table 3. Wear rate at different speeds of samples
It was observed that as speed increases the wear rate
also increases for any sample irrespective of the
composition.The reason is the increase in contact
pressure between the rotor and brake pads, and this is
confirmed [12]. But the wear rate data obtain
different for all formulations, due to different additives
and their weight percentages used in their compositions.
The following conclusions can be made from the above
experimental values. The wear rate was higher in
sample 1 and sample 4 since the reinforcement material
is low in sample 1 and the amount of abrasive material
is less in sample 4. Sample 3 is concluded to be the
better composition at high speeds and sample 2 is found
to be the better composite to be used at low speeds.
F. Compressive Hardness:
The compressive hardness of the material is the ability
to resist against plastic deformation such as scratches,
Speed
(rpm)
SAMPLE WEAR RATE (mg.m
Sample 1 Sample2 Sample 3
150 0.9 0.6 0.7
250 1.4 1 1.3
300 2.1 1.6 1.8
450 3.7 2.2 2.1
International Journal of Scientific Research and Engineering Development-– Volume 2 Issue 5, Sep
Available at www.ijsred.com
7175 ©IJSRED: All Rights are Reserved
Fig. 3 sample compositions
Table 3. Wear rate at different speeds of samples
It was observed that as speed increases the wear rate
also increases for any sample irrespective of the
composition.The reason is the increase in contact
pressure between the rotor and brake pads, and this is
. But the wear rate data obtained were
different for all formulations, due to different additives
and their weight percentages used in their compositions.
The following conclusions can be made from the above
experimental values. The wear rate was higher in
e reinforcement material
is low in sample 1 and the amount of abrasive material
is less in sample 4. Sample 3 is concluded to be the
better composition at high speeds and sample 2 is found
to be the better composite to be used at low speeds.
The compressive hardness of the material is the ability
to resist against plastic deformation such as scratches,
indentation and abrasion. The
with speed is determined by using an inertia
dynamometer. The hardness determin
experimentation is the time taken by the brake pad to
return to its normal state from maximum stress.
Fig. 4.Hardness vs Speed
Table 4. Compressive Strength of samples
From the observation, it is clear that the time taken to
return to the original state for the brake pad is constant
and does not change with speed. Although they vary
based on the composition of the brake pads
SAMPLE WEAR RATE (mg.m-1
)
Sample 3 Sample 4
1.1
1.7
2.4
3.6
Compressive strength(hours)
Speed
(rpm)
Sample1 Sample2
150 3.1 3.5
250 3.11 3.52
350 3.1 3.5
450 3.12 3.51
Volume 2 Issue 5, Sep – Oct 2019
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©IJSRED: All Rights are Reserved Page 856
indentation and abrasion. The variation of hardness
with speed is determined by using an inertia
dynamometer. The hardness determined from the
experimentation is the time taken by the brake pad to
return to its normal state from maximum stress.
Fig. 4.Hardness vs Speed
Table 4. Compressive Strength of samples
From the observation, it is clear that the time taken to
return to the original state for the brake pad is constant
hange with speed. Although they vary
based on the composition of the brake pads
Compressive strength(hours)
Sample3 Sample4
3.9 4.485
3.9 4.484
3.91 4.485
3.92 4.485
International Journal of Scientific Research and Engineering Development
ISSN : 2581-7175
G. Coefficient of friction:
The coefficient of friction is the relation between the
normal force acting on the object and the frictional
force. The coefficient of friction is gi
formula. The coefficient of friction is an important
parameter in braking as it varies with speed
sometimes this parameter is neglected when
considering the performance of brake pads at various
speed.
Fig.5. Speed Vs Coefficient of friction
From the graph, it is observed that the coefficient of
friction remained constant for various range of
speed(RPM).The constant value observed may be due
to absence of steel fibres as stated and
coefficient of friction will increase if steel fibres are
used due adhesion of steel particles or maybe the
absence of trapped asperities[14]. In the sliding surfa
the composition of the same changes their coefficient of
friction also changes due to various properties of the
Coefficient of friction
Rpm Sample 1 Sample2
150 0.24 0.29
250 0.24 0.29
350 0. 42 0.29
450 0.24 0.29
International Journal of Scientific Research and Engineering Development-– Volume 2 Issue 5, Sep
Available at www.ijsred.com
7175 ©IJSRED: All Rights are Reserved
The coefficient of friction is the relation between the
normal force acting on the object and the frictional
force. The coefficient of friction is given by the
coefficient of friction is an important
parameter in braking as it varies with speed [13]. but
sometimes this parameter is neglected when
considering the performance of brake pads at various
of friction
From the graph, it is observed that the coefficient of
friction remained constant for various range of
he constant value observed may be due
and reported that
coefficient of friction will increase if steel fibres are
used due adhesion of steel particles or maybe the
In the sliding surface,
the composition of the same changes their coefficient of
friction also changes due to various properties of the
elements and their varying compositions
highest coefficient of friction was found to be in
sample4 and the lowest was observed for
sample 2 and 3 had a coefficient of friction between o.3
to 0.35
From the existing literature, it is found that coconut
fibres are abundant in nature. The
in coconut fibres are as follows;
Compound
Lignin
Pentosans
Cellulose
Moisture
Solvent extracts
Uronic hydrides
Ash
III. Results and discussions:
H. Tribological properties:
The wear rate for sample 1, sample 2,
sample 3, sample 4 composites at different
fractions of coconut shells at different speed limits
are presented in the Table in the observations
mentioned above. The wear rate table shows
as speed increases, the wear rate
irrespective of the composition for any samples.
The wear results of such composites show that the
Coefficient of friction
Sample3 Sample4
0.36 0.42
0.36 0.42
0.36 0.42
0.36 0.42
Volume 2 Issue 5, Sep – Oct 2019
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©IJSRED: All Rights are Reserved Page 857
elements and their varying compositions [15]. The
highest coefficient of friction was found to be in
sample4 and the lowest was observed for sample 1, The
sample 2 and 3 had a coefficient of friction between o.3
From the existing literature, it is found that coconut
nature. The element composition
in coconut fibres are as follows;
percentage
Lignin 29.4%
27.7%
26%
8%
4.2
3.5%
0.6%
Tribological properties:
rate for sample 1, sample 2,
sample 3, sample 4 composites at different
fractions of coconut shells at different speed limits
are presented in the Table in the observations
mentioned above. The wear rate table shows that,
wear rate also increases
irrespective of the composition for any samples.
The wear results of such composites show that the
International Journal of Scientific Research and Engineering Development-– Volume 2 Issue 5, Sep – Oct 2019
Available at www.ijsred.com
ISSN : 2581-7175 ©IJSRED: All Rights are Reserved Page 858
trend of graph increases but it decreases for sample
2. It depends on the adhesion properties of
graphite, epoxy resin and Aluminum oxide.
I. Mechanical properties:
The compressive Hardness values for all
sample composites at different volume fractions is
shown in the graph drawn between compressive
hardness (Mpa) and speed (RPM) in the
observation section.It is observed that the
compressive hardness shows a linear deflection
with the increase in speed respective for the
samples. From the graph, it is concluded that
sample 4 is having more hardness value compared
to all other samples used.
J. Physical properties:
The values of coefficient of friction for all
sample composites at different volume fractions
are shown in the graph drawn between the
coefficient of friction and speed (RPM). It is
observed that sample 4 develops a high coefficient
of friction whereas sample 1 shows the very
minimal coefficient of friction according to the
graph shown in the observation section.
IV.CONCLUSIONS:
The wear rate was higher in sample 1 and sample 4
since the reinforcement material is low in sample 1
and the amount of abrasive material is less in
sample 4. Sample 3 is concluded to be the better
composition at high speeds and sample 2 is found
to be the better composite to be used at low speeds.
The coefficient of friction is observed to be very
high in sample 4 and to be very low in sample 1.
The compressive hardness values are high in
sample 4 and are very low in sample 1. It is
concluded that sample 4 shows better hardness than
all other samples
REFERENCE
[1] Monteiro, S. N., Terrones, L. A. H., & D’Almeida, J. R. M.
(2008). Mechanical performance of coir fibre/polyester composites.
Polymer Testing, 27(5), 591–595.
DOI:10.1016/j.polymertesting.2008.03.00
[2]W Wary and G Haung, "characterization and utilization of Natural
coconut fibres composite” materials &design Volume 30,no.7,2009
,pp:2714-2744. (doi:10.1016/j.matdes.2008.11.002.)
[3]Ruzadi,C.M kamarddin,H.shamsul,J.B & Abdullah MMA
(2012).”Mechanical properties wear behaviour of brake Pads
produced from palm kerenel”,pp:341-342,26.30
[4]Blau P.J(2001) compostion,function amd testing of friction brake
materials and their additives.
[5]EL-shehekil YA, salit MS, Abdank and zainudin ES.
Devolpement of a new kneaf blast fibre reinforced thermoplastic
polyurethane composite /bio resource, 2011 ;6: pp:4662-4672.
[6]Sapuan, M. & Harimi,M. (2003) Mechanical properties of
epoxy/coconut shell filler
particle composites. The Arabian Journal for Science and
Engineering, 28,(2B), 171-181.
[7]Kumar M. and Bijwe, J. Role of Different Metallic Fillers in Non-
Asbestos Organic (NAO) Friction Composites for Controlling
Sensitivity of coefficient of Friction to Load and Speed.Tribology
International, 43, 2010, pp. 965-974.
[8]. Rohatgi, P. K., Menezes, P. L. and Lovell, M. R. Tribological
Properties of Fly Ash-Based
Green Friction Products. In: Nosonovsky M., Bhushan B. (eds) Green
Tribology. Green
Energy and Technology. Berin: Springer, 2012, pp. 429-443.
International Journal of Scientific Research and Engineering Development-– Volume 2 Issue 5, Sep – Oct 2019
Available at www.ijsred.com
ISSN : 2581-7175 ©IJSRED: All Rights are Reserved Page 859
[9] Hemanth Kumar TR, Swamy RP, Chandrashekar TK. An
experimental investigation on wear test parameters of metal matrix
composites using taguchi technique. Indian J Eng Mater Sci
2013;20:329e33.
[10] Yallew TB, Kumar P, Singh I. Sliding wear properties of jute
fabric reinforced polypropylene composites. Procedia Engineering
2014;97:402e11.
[11]Abutu, J., Lawal, S. A., Ndaliman, M. B., Lafia-Araga, R. A.,
Adedipe, O., & Choudhury, I. A. (2018). Production and
characterization of brake pad developed from coconut shell
reinforcement material using central composite design. SN Applied
Sciences, 1(1). doi:10.1007/s42452-018-0084-x
[12]Ibhadode, A. O. A., & Dagwa, I. M. (2008). Development of
asbestos-free friction lining material from palm kernel shell. Journal
of the Brazilian Society of Mechanical Sciences and Engineering,
30(2). doi:10.1590/s1678-58782008000200010 .
[13]Xiao, X., Yin, Y., Bao, J., Lu, L., & Feng, X. (2016). Review on
the friction and wear of brake materials. Advances in Mechanical
Engineering, 8(5), 168781401664730.
[14]EL-Tayeb, N. S. M., & Liew, K. W. (2009). On the dry and wet
sliding performance of potentially new frictional brake pad materials
for automotive industry. Wear, 266(1-2), 275–
287. doi:10.1016/j.wear.2008.07.003
[15]Liew, K. W., & Nirmal, U. (2013). Frictional performance
evaluation of newly designed brake pad materials. Materials &
Design, 48, 25–33. doi:10.1016/j.matdes.2012.07.055

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Testing of Coconut Shell Reinforced Brake PADS

  • 1. International Journal of Scientific Research and Engineering Development-– Volume 2 Issue 5, Sep – Oct 2019 Available at www.ijsred.com ISSN : 2581-7175 ©IJSRED: All Rights are Reserved Page 853 Testing of Coconut Shell Reinforced Brake PADS P.Pathmanaban1* , A. Musharath Aalam, 1 A.selvaganesh2 , S.Sr,iamrish3 1* Assistant professor, Department of Automobile Engineering, Velammal Engineering College, Chennai-66 123 UG Students, Department of Automobile Engineering, Velammal Engineering College, Chennai-66 Abstract: Asbestos had been used by manufacturers to produce brake pads, but it turned out to be harmful and toxic in nature. So the manufacturers had decided not to manufacture brake pads using Asbestos. It can cause health issues like asbestosis, mesothelioma and lung cancers too. Thus the brake pads can be manufactured using some natural fibres like coconut shell as reinforcement material, along with Graphite which can act as better friction material, Alumina as abrasive material, and, Epoxy resin as a binder. This will make brake pads function well with high friction co-efficient and less wear rate and by using natural waste material as reinforced material, it is good for the environment too. It has its advantages as it makes less noise than metallic brake pads, thus reducing noise pollution. About the tests conducted, various samples were collected by varying the compositions and were tested at various speeds. The wear rate was calculated and, the co-efficient of friction was also investigated. Sample four has given the better result than others. It is observed that, the naturally produced brake pads can be a considerable alternate for Asbestos. Keywords: Coconut Shell powder, Wear rate, brake pads, Epoxy Resin, compression strength. I.INTRODUCTION Composite materials are getting trending nowadays for manufacturing of several materials based upon automobile and aerospace components. Study of Tribology and R&D will be concentrating on the continual growth of natural fibres ( i.e. palm kernel, coconut shells etc..).coconut shells are more relatively similar to wood as it consists of cellulose, lignin, pentosans and Ash. domination of bio and agro-based products will contribute the engineering materials in coming times. The main aspect for the usage of natural fibre instead of artificial components is lightweight and good in matrix adhesion of fibres for eco-friendly condition and environmental regulation industries triggered towards natural fibre materials.in current situation, 33billion coconut is harvested throughout the world in that only 1/6 of coconut are used for their fibres[1,2]. for safety purpose and resist of motion at a high or moderate speed of the vehicle or to control any prime movers, the braking system plays a major role in this scenario with help brake pads[3]. Brake pad consists of brake lining when it subjected braking effect it causes high friction and high heat liberation by a material which simultaneously increases the wear rate. Brake pads were made out categorized material like organic, metallic, semi-metallic. moreover, modern brake pad consists of asbestos ceramic, graphite. These material are used due to high resistant wear and reduce heat liberation but the major drawback is asbestos causes a series effect on human health like mesothelioma and asbestos-related lung cancer [4].advantage in natural fibre polymer such as leading high strength, it can be recycled easily and also a RESEARCH ARTICLE OPEN ACCESS
  • 2. International Journal of Scientific Research and Engineering Development-– Volume 2 Issue 5, Sep – Oct 2019 Available at www.ijsred.com ISSN : 2581-7175 ©IJSRED: All Rights are Reserved Page 854 renewable source. Natural fibre enhances the reduction in weight of material than other metallic materials and it will be low in economical wise; in an environmental point of view, natural fibre is more eco-friendly than others[5]. 30% of coconut shell and epoxy or resin polymer matrix tends to form a filled composite of natural fibre. The simultaneously enhance tensile strength and young modulus of material [6]. Concentration on the effect of reduction in wear rate will spontaneously reduce the harmful effect of environment tragedies. More than 50 components are reinforced in their desired category to the material highly efficient brake pad. Multiple components in brake pads are categorized mainly as fibres, Fillers, blinders, frictional reduction agent. However mechanical properties will be influence Brake pads using fibres. Moreover, production cost and machinability of brake pads are improved using filler material. For better optimise performance filler contributes its roll in brake pads [7]. Wear rate and friction properties of brake pad will further growth by addition of blinders[8].in this research, aims to use of waste agro material as utilization of brake pads material, through investigation of this research, strength and friction rate on brake pads are highly efficient when subjected to commercial use of this reinforced composite materials. II. MATERIALS AND METHODS A. Materials Material of reinforcement used here is Coconut shell, obtained from a coconut trader in Chennai from a local industry, whereas, the graphite powder, which is going to act as a friction modifier, is extracted from 1.5 V dry cell batteries and Alumina, which is suited to act as an abrasive material is purchased from a local chemical store in Chennai. And also, Epoxy resin which serves as binder is obtained from a chemical store in Chennai was used jointly with a hardener to give desired property. B. Method The initial process flow involves preparation of coconut shell and graphite powder by carrying out processes like removing of shell fibres from coconut and washing the obtained shell with soap and detergent, followed by cleaning using a clean dry cloth and drying it in the oven at 150 0 C for nearly 3 hours. After that, crushing the dried coconut shell using mortar and pestle is done and fine grain size of 100 micrometres is obtained. The sieve size of 100 micrometres of Coconut shell was added in varying percentages to Aluminum oxide, Graphite and epoxy resin based on 176 g weight of commercial brake pad. To achieve homogenous steady- state condition for the moulding process, each sample combination is separately dry-mixed using a blender. Fig . 1 Compression moulding machine
  • 3. International Journal of Scientific Research and Engineering Development-– Volume 2 Issue 5, Sep – Oct 2019 Available at www.ijsred.com ISSN : 2581-7175 ©IJSRED: All Rights are Reserved Page 855 Table 1: composition variation for different samples C. Preparation: Compression moulding machine is used in the production of brake pad samples and a standard method specified [11] is followed. During the process, the sample composition is varied and the process factors like Molding pressure (MP), Molding temperature (MT), Curing time (CT), Heat treatment time (HTT) is kept constant for all samples. Fig 1 shows the moulding machine and Table 2 shows the detailed specification of the machine. Molding pressure (MP) = 14(MPa) Capacity = 750 k N Molding temperature (MT) = 140(0 C) Curing time (CT) = 8(min) Heat treatment time (HTT) = 1(hr) The samples, which are in various proportions are manually stirred in the definite composition as referred in Table 1 and are stirred thoroughly and were transferred into the mould for compression moulding. Furthermore, the moulded samples are heated at 150 0 C for particular heat treatment time as shown above. D. Wear rate: Wear rate of samples pin on the Disc Wear Testing Machine per the ASTM G-99 standard [9]]. The sample is of cylindrical in shape of size 8mm in diameter and 30mm length were prepared for all compositions of the fibres which is as shown in Fig.2. These tests were carried out at a load of 20N at different speeds. The accompanying condition is utilized to calculate the wear rate [10]. The sliding distance (D) and wear rate (Wr) were calculated using the following Equations. . Sliding distance (D) = 2Nπdt Wr = ( ) ( ) Where d is the disk diameter t is the time of exposure of the specimen to abrasion and N is the radial speed, respectively. Table 2: Hotpress specifications E. Observations Fig.2. Wear rate comparison of samples WEARRATE(MG/METRE) SPEED(RPM) GRAPH sample 1 sample 2 sample 3 sample 4 COMPOSITION (%) Samp le no. Coconut shell Aluminiu m oxide Graphite Epoxy resin S1 10 20 35 35 S2 20 15 30 35 S3 30 10 25 35 S4 40 5 20 35 Particulars Specifications Max. Day Light 150 mm No. Of Day Light 2 Platen size 350mm X 350mm Ram Diameter 200 mm Heating Capacity 400ºC Max Pressure 210 bars
  • 4. International Journal of Scientific Research and Engineering Development ISSN : 2581-7175 Fig. 3 sample compositions Table 3. Wear rate at different speeds of samples It was observed that as speed increases the wear rate also increases for any sample irrespective of the composition.The reason is the increase in contact pressure between the rotor and brake pads, and this is confirmed [12]. But the wear rate data obtain different for all formulations, due to different additives and their weight percentages used in their compositions. The following conclusions can be made from the above experimental values. The wear rate was higher in sample 1 and sample 4 since the reinforcement material is low in sample 1 and the amount of abrasive material is less in sample 4. Sample 3 is concluded to be the better composition at high speeds and sample 2 is found to be the better composite to be used at low speeds. F. Compressive Hardness: The compressive hardness of the material is the ability to resist against plastic deformation such as scratches, Speed (rpm) SAMPLE WEAR RATE (mg.m Sample 1 Sample2 Sample 3 150 0.9 0.6 0.7 250 1.4 1 1.3 300 2.1 1.6 1.8 450 3.7 2.2 2.1 International Journal of Scientific Research and Engineering Development-– Volume 2 Issue 5, Sep Available at www.ijsred.com 7175 ©IJSRED: All Rights are Reserved Fig. 3 sample compositions Table 3. Wear rate at different speeds of samples It was observed that as speed increases the wear rate also increases for any sample irrespective of the composition.The reason is the increase in contact pressure between the rotor and brake pads, and this is . But the wear rate data obtained were different for all formulations, due to different additives and their weight percentages used in their compositions. The following conclusions can be made from the above experimental values. The wear rate was higher in e reinforcement material is low in sample 1 and the amount of abrasive material is less in sample 4. Sample 3 is concluded to be the better composition at high speeds and sample 2 is found to be the better composite to be used at low speeds. The compressive hardness of the material is the ability to resist against plastic deformation such as scratches, indentation and abrasion. The with speed is determined by using an inertia dynamometer. The hardness determin experimentation is the time taken by the brake pad to return to its normal state from maximum stress. Fig. 4.Hardness vs Speed Table 4. Compressive Strength of samples From the observation, it is clear that the time taken to return to the original state for the brake pad is constant and does not change with speed. Although they vary based on the composition of the brake pads SAMPLE WEAR RATE (mg.m-1 ) Sample 3 Sample 4 1.1 1.7 2.4 3.6 Compressive strength(hours) Speed (rpm) Sample1 Sample2 150 3.1 3.5 250 3.11 3.52 350 3.1 3.5 450 3.12 3.51 Volume 2 Issue 5, Sep – Oct 2019 www.ijsred.com ©IJSRED: All Rights are Reserved Page 856 indentation and abrasion. The variation of hardness with speed is determined by using an inertia dynamometer. The hardness determined from the experimentation is the time taken by the brake pad to return to its normal state from maximum stress. Fig. 4.Hardness vs Speed Table 4. Compressive Strength of samples From the observation, it is clear that the time taken to return to the original state for the brake pad is constant hange with speed. Although they vary based on the composition of the brake pads Compressive strength(hours) Sample3 Sample4 3.9 4.485 3.9 4.484 3.91 4.485 3.92 4.485
  • 5. International Journal of Scientific Research and Engineering Development ISSN : 2581-7175 G. Coefficient of friction: The coefficient of friction is the relation between the normal force acting on the object and the frictional force. The coefficient of friction is gi formula. The coefficient of friction is an important parameter in braking as it varies with speed sometimes this parameter is neglected when considering the performance of brake pads at various speed. Fig.5. Speed Vs Coefficient of friction From the graph, it is observed that the coefficient of friction remained constant for various range of speed(RPM).The constant value observed may be due to absence of steel fibres as stated and coefficient of friction will increase if steel fibres are used due adhesion of steel particles or maybe the absence of trapped asperities[14]. In the sliding surfa the composition of the same changes their coefficient of friction also changes due to various properties of the Coefficient of friction Rpm Sample 1 Sample2 150 0.24 0.29 250 0.24 0.29 350 0. 42 0.29 450 0.24 0.29 International Journal of Scientific Research and Engineering Development-– Volume 2 Issue 5, Sep Available at www.ijsred.com 7175 ©IJSRED: All Rights are Reserved The coefficient of friction is the relation between the normal force acting on the object and the frictional force. The coefficient of friction is given by the coefficient of friction is an important parameter in braking as it varies with speed [13]. but sometimes this parameter is neglected when considering the performance of brake pads at various of friction From the graph, it is observed that the coefficient of friction remained constant for various range of he constant value observed may be due and reported that coefficient of friction will increase if steel fibres are used due adhesion of steel particles or maybe the In the sliding surface, the composition of the same changes their coefficient of friction also changes due to various properties of the elements and their varying compositions highest coefficient of friction was found to be in sample4 and the lowest was observed for sample 2 and 3 had a coefficient of friction between o.3 to 0.35 From the existing literature, it is found that coconut fibres are abundant in nature. The in coconut fibres are as follows; Compound Lignin Pentosans Cellulose Moisture Solvent extracts Uronic hydrides Ash III. Results and discussions: H. Tribological properties: The wear rate for sample 1, sample 2, sample 3, sample 4 composites at different fractions of coconut shells at different speed limits are presented in the Table in the observations mentioned above. The wear rate table shows as speed increases, the wear rate irrespective of the composition for any samples. The wear results of such composites show that the Coefficient of friction Sample3 Sample4 0.36 0.42 0.36 0.42 0.36 0.42 0.36 0.42 Volume 2 Issue 5, Sep – Oct 2019 www.ijsred.com ©IJSRED: All Rights are Reserved Page 857 elements and their varying compositions [15]. The highest coefficient of friction was found to be in sample4 and the lowest was observed for sample 1, The sample 2 and 3 had a coefficient of friction between o.3 From the existing literature, it is found that coconut nature. The element composition in coconut fibres are as follows; percentage Lignin 29.4% 27.7% 26% 8% 4.2 3.5% 0.6% Tribological properties: rate for sample 1, sample 2, sample 3, sample 4 composites at different fractions of coconut shells at different speed limits are presented in the Table in the observations mentioned above. The wear rate table shows that, wear rate also increases irrespective of the composition for any samples. The wear results of such composites show that the
  • 6. International Journal of Scientific Research and Engineering Development-– Volume 2 Issue 5, Sep – Oct 2019 Available at www.ijsred.com ISSN : 2581-7175 ©IJSRED: All Rights are Reserved Page 858 trend of graph increases but it decreases for sample 2. It depends on the adhesion properties of graphite, epoxy resin and Aluminum oxide. I. Mechanical properties: The compressive Hardness values for all sample composites at different volume fractions is shown in the graph drawn between compressive hardness (Mpa) and speed (RPM) in the observation section.It is observed that the compressive hardness shows a linear deflection with the increase in speed respective for the samples. From the graph, it is concluded that sample 4 is having more hardness value compared to all other samples used. J. Physical properties: The values of coefficient of friction for all sample composites at different volume fractions are shown in the graph drawn between the coefficient of friction and speed (RPM). It is observed that sample 4 develops a high coefficient of friction whereas sample 1 shows the very minimal coefficient of friction according to the graph shown in the observation section. IV.CONCLUSIONS: The wear rate was higher in sample 1 and sample 4 since the reinforcement material is low in sample 1 and the amount of abrasive material is less in sample 4. Sample 3 is concluded to be the better composition at high speeds and sample 2 is found to be the better composite to be used at low speeds. The coefficient of friction is observed to be very high in sample 4 and to be very low in sample 1. The compressive hardness values are high in sample 4 and are very low in sample 1. It is concluded that sample 4 shows better hardness than all other samples REFERENCE [1] Monteiro, S. N., Terrones, L. A. H., & D’Almeida, J. R. M. (2008). Mechanical performance of coir fibre/polyester composites. Polymer Testing, 27(5), 591–595. DOI:10.1016/j.polymertesting.2008.03.00 [2]W Wary and G Haung, "characterization and utilization of Natural coconut fibres composite” materials &design Volume 30,no.7,2009 ,pp:2714-2744. (doi:10.1016/j.matdes.2008.11.002.) [3]Ruzadi,C.M kamarddin,H.shamsul,J.B & Abdullah MMA (2012).”Mechanical properties wear behaviour of brake Pads produced from palm kerenel”,pp:341-342,26.30 [4]Blau P.J(2001) compostion,function amd testing of friction brake materials and their additives. [5]EL-shehekil YA, salit MS, Abdank and zainudin ES. Devolpement of a new kneaf blast fibre reinforced thermoplastic polyurethane composite /bio resource, 2011 ;6: pp:4662-4672. [6]Sapuan, M. & Harimi,M. (2003) Mechanical properties of epoxy/coconut shell filler particle composites. The Arabian Journal for Science and Engineering, 28,(2B), 171-181. [7]Kumar M. and Bijwe, J. Role of Different Metallic Fillers in Non- Asbestos Organic (NAO) Friction Composites for Controlling Sensitivity of coefficient of Friction to Load and Speed.Tribology International, 43, 2010, pp. 965-974. [8]. Rohatgi, P. K., Menezes, P. L. and Lovell, M. R. Tribological Properties of Fly Ash-Based Green Friction Products. In: Nosonovsky M., Bhushan B. (eds) Green Tribology. Green Energy and Technology. Berin: Springer, 2012, pp. 429-443.
  • 7. International Journal of Scientific Research and Engineering Development-– Volume 2 Issue 5, Sep – Oct 2019 Available at www.ijsred.com ISSN : 2581-7175 ©IJSRED: All Rights are Reserved Page 859 [9] Hemanth Kumar TR, Swamy RP, Chandrashekar TK. An experimental investigation on wear test parameters of metal matrix composites using taguchi technique. Indian J Eng Mater Sci 2013;20:329e33. [10] Yallew TB, Kumar P, Singh I. Sliding wear properties of jute fabric reinforced polypropylene composites. Procedia Engineering 2014;97:402e11. [11]Abutu, J., Lawal, S. A., Ndaliman, M. B., Lafia-Araga, R. A., Adedipe, O., & Choudhury, I. A. (2018). Production and characterization of brake pad developed from coconut shell reinforcement material using central composite design. SN Applied Sciences, 1(1). doi:10.1007/s42452-018-0084-x [12]Ibhadode, A. O. A., & Dagwa, I. M. (2008). Development of asbestos-free friction lining material from palm kernel shell. Journal of the Brazilian Society of Mechanical Sciences and Engineering, 30(2). doi:10.1590/s1678-58782008000200010 . [13]Xiao, X., Yin, Y., Bao, J., Lu, L., & Feng, X. (2016). Review on the friction and wear of brake materials. Advances in Mechanical Engineering, 8(5), 168781401664730. [14]EL-Tayeb, N. S. M., & Liew, K. W. (2009). On the dry and wet sliding performance of potentially new frictional brake pad materials for automotive industry. Wear, 266(1-2), 275– 287. doi:10.1016/j.wear.2008.07.003 [15]Liew, K. W., & Nirmal, U. (2013). Frictional performance evaluation of newly designed brake pad materials. Materials & Design, 48, 25–33. doi:10.1016/j.matdes.2012.07.055