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IJESM Volume 2, Issue 1 ISSN: 2320-0294
_________________________________________________________
A Quarterly Double-Blind Peer Reviewed Refereed Open Access International e-Journal - Included in the International Serial Directories
Indexed & Listed at: Ulrich's Periodicals Directory ©, U.S.A., Open J-Gage, India as well as in Cabell’s Directories of Publishing Opportunities, U.S.A.
International Journal of Engineering, Science and Mathematics
http://www.ijmra.us
214
March
2013
Determination of flux consumption when reuse of
slag as flux in submerged arc welding when welding
parameters selected by Response Surface
Methodology techniques
KrishanKant*
Mohit Bector*
Amandeep Vohra**
Vikas Yadav***
__________________________________________________________
Abstract
The Objectives of this research is to study the effect of mixture of reused and new flux on
chemical composition in weld metal of Submerged Arc Welding process (SAW). Slag generated
during submerged arc welding has been recycled by mixing varying percentages of crushed slag
with fresh flux to use in subsequent runs. Slag generated during submerged arc welding is normally
thrown away as a waste. This poses the problem of storage, disposal, and environmental pollution
and needs landfill space apart from exhaust of non-renewable resources. Reusing of slag will not
only solve these problems but also be economical. In the present work an attempt has been made to
use the submerged arc welding slag as flux in the same submerged arc welding process. Fused slag
was crusher to the desired particle size as that of the original flux. The process is characterized by
the use of granular flux blanket that covers the molten weld pool during operation. Protection
through atmospheric contamination of the weld bead and slower cooling rate, achieved by this
arrangement can enhance mechanical properties of the weldment. Selection of process parameters
has great influence on the quality of a welded connection. Welding input parameters play a very
significant role in determining the quality of a weld joint. Slag formed during the welding process
* Faculty of Mechanical Engineering, Galaxy Global Group of Institutions, Dinarpur, Ambala,
India.
** Faculty of Mathematics, Galaxy Global Group of Institutions, Dinarpur, Ambala, India.
*** Faculty of Mechanical Engineering, Ram Devi Jindal Group of Institutions, Lalru , India.
IJESM Volume 2, Issue 1 ISSN: 2320-0294
_________________________________________________________
A Quarterly Double-Blind Peer Reviewed Refereed Open Access International e-Journal - Included in the International Serial Directories
Indexed & Listed at: Ulrich's Periodicals Directory ©, U.S.A., Open J-Gage, India as well as in Cabell’s Directories of Publishing Opportunities, U.S.A.
International Journal of Engineering, Science and Mathematics
http://www.ijmra.us
215
March
2013
that is subsequently crushed for use as a welding flux is defined as crushed slag.In Our Research
work we used 40 % slag in Virgin Flux and find out the consumption when changing the values of
welding parameters accordingly Experiment run order.
Keyword : Submerged arc Welding , Reused Flux , R.S.M Technique ,Design Expert Software.
1. Introduction
The traditional welding flux is costly and the flux used in Submerged Arc Welding (SAW)
generates wastages known as Slag. It is generally thrown away as a waste after use. This poses the
problem of storage, disposal, and environmental pollution and needs landfill space apart from
exhaust of non-renewable resources. If by recycling the used flux can be reused in product yielding
same quality parameter as the new flux, then the cost of the input will go down significantly.
However, this requires extensive trial and error experimentation because it is often difficult to
know how the slag ingredients interact after recycling to determine the operational characteristics
of the recycled flux and the final performance of the welded structure. Keeping this in mind an
experiment has been conducted in a manufacturing unit with small investment. As far as possible
weld qualification tests were performed using recycled flux to get it to be qualified in a National
Accreditation Board of Laboratories in the final products made from recycled slag. Submerged arc
welding is a versatile welding process in which coalescence is produced by heating the metal with
an arc maintained between a bare metal electrode and the workpiece. The arc is shielded by a
blanket of granular fusible material known as flux placed over the welding area. Filler metal is
obtained from the electrode and sometimes a supplementary welding rod or metallic addition. Flux
contributes a major part towards welding cost in submerged arc welding. The Flux is converted into
slag during welding which is treated as waste and discarded.
IJESM Volume 2, Issue 1 ISSN: 2320-0294
_________________________________________________________
A Quarterly Double-Blind Peer Reviewed Refereed Open Access International e-Journal - Included in the International Serial Directories
Indexed & Listed at: Ulrich's Periodicals Directory ©, U.S.A., Open J-Gage, India as well as in Cabell’s Directories of Publishing Opportunities, U.S.A.
International Journal of Engineering, Science and Mathematics
http://www.ijmra.us
216
March
2013
SAW fluxes are granular, fusible mineral compounds of various proportions and quantities,
manufactured by several different methods. In addition, some fluxes may contain intimately mixed
metallic ingredients to deoxidize the weld pool. Any flux is likely to produce weld metal of
somewhat different composition from that of the electrode used with it due to chemical reactions in
the arc and sometimes to the presence of metallic ingredients in the flux. A change in arc voltage
during welding will change the quantity of flux interacting with a given quantity of electrode and
may, therefore, change the composition of the weld metal. Reuse of slag can not only minimize the
above problems, but can also save non-renewable mineral resources. The slag is normally reused
after its processing & recycling so as to reclaim its original characteristics. However this requires a
considerable amount of effort and money to be spent on it. However if this slag is reused as flux
again only after crushing it to the normal particle size of the original slag without any new
additions/processing, the cost of reuse of this slag will be quite low. However the quality of
weld/clad metal obtained using this reused slag needs to be analyzed before recommending its
reuse. The preset study aims at exploring the possibility of reused of the crushed slag as flux &
effects of use this flux on the chemical composition and weld bead characteristics of the
welds/clads obtained using this flux. Ingredients for use in welding fluxes are very carefully chosen
to provide specific benefits to the submerged arc welding process, including cleansing the weld
metal, providing appropriate weld metal composition (carbon, manganese, silicon, oxygen,
nitrogen, etc.), protecting the weld puddle from atmospheric contamination, stabilizing the arc,
allowing for ease of slag removal from the weld metal, and providing the appropriate slag viscosity
and freezing range for intended applications. When virgin flux is melted by a welding arc, it does
not fully reach an equilibrium state. Although the specific elements contained in the slag may be
similar, the chemical form of these elements in the generated slag will be significantly different
from that of the virgin flux. Blending crushed slag with virgin flux is a common practice by flux
processors. Crushed slag is approximately 20% more dense than the virgin flux it was generated
IJESM Volume 2, Issue 1 ISSN: 2320-0294
_________________________________________________________
A Quarterly Double-Blind Peer Reviewed Refereed Open Access International e-Journal - Included in the International Serial Directories
Indexed & Listed at: Ulrich's Periodicals Directory ©, U.S.A., Open J-Gage, India as well as in Cabell’s Directories of Publishing Opportunities, U.S.A.
International Journal of Engineering, Science and Mathematics
http://www.ijmra.us
217
March
2013
from. This will promote segregation of any blends of crushed slag with virgin flux. It can also
significantly increase the consumption of welding flux and increase the slag to metal ratio.
2. Experimental Procedure :
For carrying out this study, experimental procedure consisting of the following steps was
followed:-
1. Collection of slag and Crushing and sieving of Slag :
Slag was generated during the SAW welding process & it was collected free of cost.
The slag was crushed using a crusher to convert it into reusable granular flux. Crushed
mass was then sieved so that the grains of the reusable flux(slag) should confirm to the
particle size of the original flux (10 mesh sieves).
2. Mixing slag with Pure Flux :The crashed & sieved slag mix with pure flux with the ratio
of 40 % slag & 60 % Pure flux for the welding on plates.
3. The Preparation of High Strength Low Alloy Steel Plates 250 x 150 x 10 mm .
4. The Preparation of welding electrode for Submerged arc welding , EH 14 (AWS grade
EH-14) of diameter 3.2 mm.
5. The Experiment Designed based on BOX-BEHNKEN DESIGN (BBD) using state ease
6.0 Version of design of experiment.
6. The Experiment was conducted as per the design matrix using TORNANDO SAW M-
800 equipment at Mullana University Mullana.
7. Reuse slag as Flux consumption measured each 29 experiment run according to design
matrix reading.
3. Welding Parameters & Chemical Composition :-
(A) Welding Current :-
In SAW ,Current plays a major role where it controls the melting rate of the electrode and
thereby the weld deposition rate. It also controls the depth of penetration and thereby the
IJESM Volume 2, Issue 1 ISSN: 2320-0294
_________________________________________________________
A Quarterly Double-Blind Peer Reviewed Refereed Open Access International e-Journal - Included in the International Serial Directories
Indexed & Listed at: Ulrich's Periodicals Directory ©, U.S.A., Open J-Gage, India as well as in Cabell’s Directories of Publishing Opportunities, U.S.A.
International Journal of Engineering, Science and Mathematics
http://www.ijmra.us
218
March
2013
extent of dilution of the weld metal by the base metal. The current density controls the
depth of penetration - the higher the current density the greater the penetration For a given
flux, arc stability will be lost below a minimum threshold current density so that if the
current for a given electrode diameter is too low arc stability is lost and a rugged, irregular
bead is obtained. Too high a current density also leads to instability because the electrode
overheats and undercutting may also occur weld reinforcement which is wasteful, and burn-
through in the case of thinner plates or in badly fitted joints, which are not provided with
proper backing [4]. Excessive current also produces a high narrow bead and undercut.
Excessively low current gives an unstable arc, inadequate penetration and overlapping.
SAW equipment is usually provided with an ammeter to monitor and control the welding
current .
(B) Voltage Arc
Voltage affects dilution rather than penetration. Bead on plate welds and square edged
closed butt welds have increased width and dilution as the arc voltage increases, but
depth of penetration remains the same. If the joint preparation is open, for example in a
butt joint with a small angled 'V' preparation, increasing the arc voltage can decrease the
penetration. Arc voltage, also called welding voltage, means the electrical potential
difference between the electrode wire tip and the surface of the molten weld puddle.
(C) Weld Speed
Welding speed or travel speed controls depth of penetration. Bead size is inversely
proportional to travel speed. Faster speeds reduce penetration and bead width, increase
the
likelihood of porosity and, if taken to the extreme, produce undercutting and irregular
beads. At high welding speeds the arc voltage should be kept fairly low otherwise arc
blow is likely too occur [4]. If the welding speed is too slow burn through can occur. A
combination of high arc voltage and slow welding speed can produce a mushroom
shaped weld bead with solidification cracks at the bead sides.
(D) Nozzle to Plate Distance
SAW filler material usually is a standard wire as well as other special forms. This wire
normally has a thickness of 1/16 in. to 1/4 in. (1.6 mm to 6 mm). In certain circumstances,
twisted wire can be used to give the arc an oscillating movement. In SAW welding nozzle
IJESM Volume 2, Issue 1 ISSN: 2320-0294
_________________________________________________________
A Quarterly Double-Blind Peer Reviewed Refereed Open Access International e-Journal - Included in the International Serial Directories
Indexed & Listed at: Ulrich's Periodicals Directory ©, U.S.A., Open J-Gage, India as well as in Cabell’s Directories of Publishing Opportunities, U.S.A.
International Journal of Engineering, Science and Mathematics
http://www.ijmra.us
219
March
2013
to plate distance plays a major role. To operate welding smoothly ,generally in saw
welding distance between nozzle to tip and work piece is 15 mm to 30 mm.
Parameters Units Limits
-2 -1 0 1 2
Current (C) amp 300 350 400 450 500
Voltage (V) volts 26 28 30 32 34
Welding Speed
(S)
m/hr 21 24 27 30 33
N.P. Distance (D) mm 16 18 20 22 24
Type Grade Chemical Composition(%)
C Mn P S Si Cr Mo Ni Fe
W.Piece Hsla
945X
0.22 1.35 0.04 0.05 0.90 0.04 0.05 0.87 Bal
Electrode
Wire
EH14 0.15 1.9 - 0.05 - - - 0.4 Bal
% age C Mn Si S P
With fresh
Flux 0.357 0.325 0.188 0.04867 0.4876
With 40 %
reused Slag 0.1812 0.4312 0.1071 0.0264 0.0289
IJESM Volume 2, Issue 1 ISSN: 2320-0294
_________________________________________________________
A Quarterly Double-Blind Peer Reviewed Refereed Open Access International e-Journal - Included in the International Serial Directories
Indexed & Listed at: Ulrich's Periodicals Directory ©, U.S.A., Open J-Gage, India as well as in Cabell’s Directories of Publishing Opportunities, U.S.A.
International Journal of Engineering, Science and Mathematics
http://www.ijmra.us
220
March
2013
4. Methodology
Identification of the process parameters :- The following independently controllable process
parameters were identified to carry out the experiments: open-circuit voltage (V); wire feed rate
(F); welding speed (S); and nozzle-to-plate distance (N) .
Finding the limits of the process variables:- Trial runs were carried out by varying one of the
process parameters whilst keeping the rest of them at constant values [6]. The working range was
decided upon by inspecting the bead for smooth appearance and the absence of any visible defects.
The upper limit of a factor was coded as +2 and the lower limit as -2, the coded values being
calculated from the following relationship:
Xi = 2[2X-(Xmax-Xmin)]
(Xmax-Xmin)
where Xi is the required coded value of a variable X; and X is any value of the variable from Xmin
to Xmax. The selected process parameters with their limits, units and notations .
IJESM Volume 2, Issue 1 ISSN: 2320-0294
_________________________________________________________
A Quarterly Double-Blind Peer Reviewed Refereed Open Access International e-Journal - Included in the International Serial Directories
Indexed & Listed at: Ulrich's Periodicals Directory ©, U.S.A., Open J-Gage, India as well as in Cabell’s Directories of Publishing Opportunities, U.S.A.
International Journal of Engineering, Science and Mathematics
http://www.ijmra.us
221
March
2013
Developing the design matrix :- The selected design matrix, is a central composite rotatable
factorial design consisting of 31 sets of coded conditions. It comprises a full replication of 24 (=16)
factorial design plus seven center points and eight star points. All welding variables at the
intermediate level (0) constitute the center points and the combinations of each of the welding
variables at either its lowest (-2) level or highest (+2) level with the other three variables at the
intermediate levels constitute the star points.[8] Thus the 29 experimental runs allowed the
estimation of the linear, quadratic and two-way interactive effects of the process parameters on the
bead geometry
Conducting the experiment as per the design matrix :- The experiments were conducted as per
the design matrix at random, to avoid the possibility of systematic errors infiltrating the system.
Recording of the responses :- During the experiments flux consumption was measured after each
run. Measured quantity of flux was put into the flux hopper before taking the bead and again
measured after taking the bead. Difference of the two quantities was taken as the flux consumption.
Development of mathematical models :-
The response function representing any of the weld bead dimensions can be expressed as : Y= f (
V, F, S, N). The relationship selected being a second degree response surface expressed as follows:
Y=b0+b1V+b2F+b3S+b4N+b11V2+b22F2+b33S2+b44N2+b12VF+b13VS+b14VN+b23FS
+b24FN+b34SN
Checking the adequacy of the models developed :-
The adequacy of the models was tested using the analysis of variance technique (ANOVA). The
calculated value of the F-ratio of the model developed should be greater than the standard tabulated
value of F-ratio for a desired level of confidence (say 95%) for the model to be significant.
IJESM Volume 2, Issue 1 ISSN: 2320-0294
_________________________________________________________
A Quarterly Double-Blind Peer Reviewed Refereed Open Access International e-Journal - Included in the International Serial Directories
Indexed & Listed at: Ulrich's Periodicals Directory ©, U.S.A., Open J-Gage, India as well as in Cabell’s Directories of Publishing Opportunities, U.S.A.
International Journal of Engineering, Science and Mathematics
http://www.ijmra.us
222
March
2013
Experiment Process Parameters Responses Factors
Standard Run Current Voltage Welding Speed
Nozzle to Plate
Distance
Reuse Slag as
Flux Consumption
Limits Numbers (Amperes) (Volts) (M/hr) (M.M)
(Gms)
1
11 300 26 27 20 43.0
2
26 500 26 27 20 89.0
3
17 300 34 27 20 55.0
4
19 500 34 27 20 65.0
5
9 400 30 21 16 38.0
6
23 400 30 33 16 45.0
7
6 400 30 21 24 48.0
8
7 400 30 33 24 52.0
9
28 300 30 27 16 37.0
10
3 500 30 27 16 82.0
11
25 300 30 27 24 52.0
12
20 500 30 27 24 67.0
13
27 400 26 21 20 44.0
14
12 400 34 21 20 41.0
15
8 400 26 33 20 47.0
16
2 400 34 33 20 48.0
17
15 300 30 21 20 42.0
18
4 500 30 21 20 56.0
19
18 300 30 33 20 27.0
20
14 500 30 33 20 84.0
21
5 400 26 27 16 52.0
22
24 400 34 27 16 47.0
23
1 400 26 27 24 54.0
IJESM Volume 2, Issue 1 ISSN: 2320-0294
_________________________________________________________
A Quarterly Double-Blind Peer Reviewed Refereed Open Access International e-Journal - Included in the International Serial Directories
Indexed & Listed at: Ulrich's Periodicals Directory ©, U.S.A., Open J-Gage, India as well as in Cabell’s Directories of Publishing Opportunities, U.S.A.
International Journal of Engineering, Science and Mathematics
http://www.ijmra.us
223
March
2013
5. Results
Interaction effects :-The difference in effect of one variable when a second variable is
changed from one level to another is known as interaction effect and study of interaction effects
of process variables on bead dimensions is interesting and very useful for understanding the
process behavior. In this study, the effect of welding current, arc voltage, welding speed and
distance between tip of nozzle & work piece on the reused slag as flux consumption. These
figures shows results of the slag as flux consumption according to the welding parameters.
Fig 5.1 Fig 5.2
Figure 5.1 shows Slag as flux consumption Decreases when increases the Voltage , while
Figure 5.2 shows Slag as flux consumption Increases when welding current increases .
24
16 400 34 27 24 51.0
25
21 400 30 27 20 51.0
26
29 400 30 27 20 52.0
27
10 400 30 27 20 48.0
28
13 400 30 27 20 52.0
29
22 400 30 27 20 44.0
IJESM Volume 2, Issue 1 ISSN: 2320-0294
_________________________________________________________
A Quarterly Double-Blind Peer Reviewed Refereed Open Access International e-Journal - Included in the International Serial Directories
Indexed & Listed at: Ulrich's Periodicals Directory ©, U.S.A., Open J-Gage, India as well as in Cabell’s Directories of Publishing Opportunities, U.S.A.
International Journal of Engineering, Science and Mathematics
http://www.ijmra.us
224
March
2013
Fig 5.3 Fig 5.4
Figure 5.3 shows Slag as flux consumption Increases when increases the welding speed ,
while Figure 5.4 shows Slag as flux consumption Increases when Nozzle to plate distance
increases .
Interaction effect
The difference in effect of one variable when a second variable is changed from one level to
another is known as interaction effect and study of interaction effects of process variables
on bead dimensions is interesting and very useful for understanding the process behavior. In
this study, to avoid complexity two way interactive effects of the variables are selected.
Fig 5.5 Fig 5.6
IJESM Volume 2, Issue 1 ISSN: 2320-0294
_________________________________________________________
A Quarterly Double-Blind Peer Reviewed Refereed Open Access International e-Journal - Included in the International Serial Directories
Indexed & Listed at: Ulrich's Periodicals Directory ©, U.S.A., Open J-Gage, India as well as in Cabell’s Directories of Publishing Opportunities, U.S.A.
International Journal of Engineering, Science and Mathematics
http://www.ijmra.us
225
March
2013
Fig 5.7 Fig 5.8
CONCLUSIONS :-
On the basis of present study the following conclusions can
be drawn:
1. RSM can be used effectively in analyzing the cause and the effect of process parameters on
response. The RSM is also used to draw contour graphs for various responses to show the
interaction effects of different process parameters.
2. Arc Stability & slag detachability were acceptable and SAW slag can be reused as welding
flux after crushing & sieving and mixing with pure flux .
3. Flux consumption increased with the increase in open circuit voltage and very small
increases with increases in current , Welding speed has negative effect on flux
consumption.
4. Flux consumption also small decreases with the increase in nozzle to plate distance.
IJESM Volume 2, Issue 1 ISSN: 2320-0294
_________________________________________________________
A Quarterly Double-Blind Peer Reviewed Refereed Open Access International e-Journal - Included in the International Serial Directories
Indexed & Listed at: Ulrich's Periodicals Directory ©, U.S.A., Open J-Gage, India as well as in Cabell’s Directories of Publishing Opportunities, U.S.A.
International Journal of Engineering, Science and Mathematics
http://www.ijmra.us
226
March
2013
REFERENCES
 V.Gunaraja,N.Murugan,”Application of Response surface methodology for predicting weld
bead quality in submerged are welding of pipes”,Journal of material processing technology
“,88(1999)266-275 Received at 26 November 1997.
 R.S.Chandel,”The Effects of process variables on the flux consumption in Submerged arc
welding”,Materials and Manufacturing Process,Vol 13,No-2,181-188,1998.
 Jasvinder Singh , Kulwant & Jastinder Garg ;” Reuse of slag as flux in saw & its effect on
chemical composition , bead geometry & microstructure of the weld metal,Vol.1 No.1 July-
Dec 2011
 C.S Chai and T.W. Eagar., Slag-Metal Reaction during Welding, Metall. Trans. B, Vol.12,
1991.p 65-100.
 U. MITRA and T.W. EGAR. Slag Metal Reaction during Welding: Part 1. Evaluation and
Research of Exiting Theories., 1991
 Mitra U. and Eagar T.W., “Slag Metal Reaction during Welding; part I. Evaluation and
Reassessment of Existing Theories”, Metallurgical Transactions, American Society for
Metals, Vol.22B, 1991,65-79.
 Singh K, Pandey S, Arul Mani R (2006) “Recycling of Submerged Arc Welding Slag”,
Australasian Welding Journal, Vol 51(2), pp 34-38.
 Datta S, Bandyopadhyay A, Pal PK (2008) “Slag Recycling in Submerged Arc Welding and
its influence on Weld Quality leading to Parametric Optimization”, International Journal of
Advanced Manufacturing Technology, Vol. 39(10), pp 229-238.
 Krishankant, Sandeep jindal, Shashi kant shekhar ,” Determination of Flux Consumption
in Submerged arc welding by the effect of welding Parameters by using R.S.M Techniques
,GJRE Volume 12 Issue 2.ISSN 0975-5861
 Sermsuk Buochareon , Bovornchok Pupat ,” Effect of reused flux and new welding flux
blend or saw due to chemical composition of hard facing weld bead formation.IE
Conference 24-25 Oct 2007

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Determination of flux consumption when reuse of slag as flux in submerged arc welding when welding parameters selected by Response Surface Methodology techniques

  • 1. IJESM Volume 2, Issue 1 ISSN: 2320-0294 _________________________________________________________ A Quarterly Double-Blind Peer Reviewed Refereed Open Access International e-Journal - Included in the International Serial Directories Indexed & Listed at: Ulrich's Periodicals Directory ©, U.S.A., Open J-Gage, India as well as in Cabell’s Directories of Publishing Opportunities, U.S.A. International Journal of Engineering, Science and Mathematics http://www.ijmra.us 214 March 2013 Determination of flux consumption when reuse of slag as flux in submerged arc welding when welding parameters selected by Response Surface Methodology techniques KrishanKant* Mohit Bector* Amandeep Vohra** Vikas Yadav*** __________________________________________________________ Abstract The Objectives of this research is to study the effect of mixture of reused and new flux on chemical composition in weld metal of Submerged Arc Welding process (SAW). Slag generated during submerged arc welding has been recycled by mixing varying percentages of crushed slag with fresh flux to use in subsequent runs. Slag generated during submerged arc welding is normally thrown away as a waste. This poses the problem of storage, disposal, and environmental pollution and needs landfill space apart from exhaust of non-renewable resources. Reusing of slag will not only solve these problems but also be economical. In the present work an attempt has been made to use the submerged arc welding slag as flux in the same submerged arc welding process. Fused slag was crusher to the desired particle size as that of the original flux. The process is characterized by the use of granular flux blanket that covers the molten weld pool during operation. Protection through atmospheric contamination of the weld bead and slower cooling rate, achieved by this arrangement can enhance mechanical properties of the weldment. Selection of process parameters has great influence on the quality of a welded connection. Welding input parameters play a very significant role in determining the quality of a weld joint. Slag formed during the welding process * Faculty of Mechanical Engineering, Galaxy Global Group of Institutions, Dinarpur, Ambala, India. ** Faculty of Mathematics, Galaxy Global Group of Institutions, Dinarpur, Ambala, India. *** Faculty of Mechanical Engineering, Ram Devi Jindal Group of Institutions, Lalru , India.
  • 2. IJESM Volume 2, Issue 1 ISSN: 2320-0294 _________________________________________________________ A Quarterly Double-Blind Peer Reviewed Refereed Open Access International e-Journal - Included in the International Serial Directories Indexed & Listed at: Ulrich's Periodicals Directory ©, U.S.A., Open J-Gage, India as well as in Cabell’s Directories of Publishing Opportunities, U.S.A. International Journal of Engineering, Science and Mathematics http://www.ijmra.us 215 March 2013 that is subsequently crushed for use as a welding flux is defined as crushed slag.In Our Research work we used 40 % slag in Virgin Flux and find out the consumption when changing the values of welding parameters accordingly Experiment run order. Keyword : Submerged arc Welding , Reused Flux , R.S.M Technique ,Design Expert Software. 1. Introduction The traditional welding flux is costly and the flux used in Submerged Arc Welding (SAW) generates wastages known as Slag. It is generally thrown away as a waste after use. This poses the problem of storage, disposal, and environmental pollution and needs landfill space apart from exhaust of non-renewable resources. If by recycling the used flux can be reused in product yielding same quality parameter as the new flux, then the cost of the input will go down significantly. However, this requires extensive trial and error experimentation because it is often difficult to know how the slag ingredients interact after recycling to determine the operational characteristics of the recycled flux and the final performance of the welded structure. Keeping this in mind an experiment has been conducted in a manufacturing unit with small investment. As far as possible weld qualification tests were performed using recycled flux to get it to be qualified in a National Accreditation Board of Laboratories in the final products made from recycled slag. Submerged arc welding is a versatile welding process in which coalescence is produced by heating the metal with an arc maintained between a bare metal electrode and the workpiece. The arc is shielded by a blanket of granular fusible material known as flux placed over the welding area. Filler metal is obtained from the electrode and sometimes a supplementary welding rod or metallic addition. Flux contributes a major part towards welding cost in submerged arc welding. The Flux is converted into slag during welding which is treated as waste and discarded.
  • 3. IJESM Volume 2, Issue 1 ISSN: 2320-0294 _________________________________________________________ A Quarterly Double-Blind Peer Reviewed Refereed Open Access International e-Journal - Included in the International Serial Directories Indexed & Listed at: Ulrich's Periodicals Directory ©, U.S.A., Open J-Gage, India as well as in Cabell’s Directories of Publishing Opportunities, U.S.A. International Journal of Engineering, Science and Mathematics http://www.ijmra.us 216 March 2013 SAW fluxes are granular, fusible mineral compounds of various proportions and quantities, manufactured by several different methods. In addition, some fluxes may contain intimately mixed metallic ingredients to deoxidize the weld pool. Any flux is likely to produce weld metal of somewhat different composition from that of the electrode used with it due to chemical reactions in the arc and sometimes to the presence of metallic ingredients in the flux. A change in arc voltage during welding will change the quantity of flux interacting with a given quantity of electrode and may, therefore, change the composition of the weld metal. Reuse of slag can not only minimize the above problems, but can also save non-renewable mineral resources. The slag is normally reused after its processing & recycling so as to reclaim its original characteristics. However this requires a considerable amount of effort and money to be spent on it. However if this slag is reused as flux again only after crushing it to the normal particle size of the original slag without any new additions/processing, the cost of reuse of this slag will be quite low. However the quality of weld/clad metal obtained using this reused slag needs to be analyzed before recommending its reuse. The preset study aims at exploring the possibility of reused of the crushed slag as flux & effects of use this flux on the chemical composition and weld bead characteristics of the welds/clads obtained using this flux. Ingredients for use in welding fluxes are very carefully chosen to provide specific benefits to the submerged arc welding process, including cleansing the weld metal, providing appropriate weld metal composition (carbon, manganese, silicon, oxygen, nitrogen, etc.), protecting the weld puddle from atmospheric contamination, stabilizing the arc, allowing for ease of slag removal from the weld metal, and providing the appropriate slag viscosity and freezing range for intended applications. When virgin flux is melted by a welding arc, it does not fully reach an equilibrium state. Although the specific elements contained in the slag may be similar, the chemical form of these elements in the generated slag will be significantly different from that of the virgin flux. Blending crushed slag with virgin flux is a common practice by flux processors. Crushed slag is approximately 20% more dense than the virgin flux it was generated
  • 4. IJESM Volume 2, Issue 1 ISSN: 2320-0294 _________________________________________________________ A Quarterly Double-Blind Peer Reviewed Refereed Open Access International e-Journal - Included in the International Serial Directories Indexed & Listed at: Ulrich's Periodicals Directory ©, U.S.A., Open J-Gage, India as well as in Cabell’s Directories of Publishing Opportunities, U.S.A. International Journal of Engineering, Science and Mathematics http://www.ijmra.us 217 March 2013 from. This will promote segregation of any blends of crushed slag with virgin flux. It can also significantly increase the consumption of welding flux and increase the slag to metal ratio. 2. Experimental Procedure : For carrying out this study, experimental procedure consisting of the following steps was followed:- 1. Collection of slag and Crushing and sieving of Slag : Slag was generated during the SAW welding process & it was collected free of cost. The slag was crushed using a crusher to convert it into reusable granular flux. Crushed mass was then sieved so that the grains of the reusable flux(slag) should confirm to the particle size of the original flux (10 mesh sieves). 2. Mixing slag with Pure Flux :The crashed & sieved slag mix with pure flux with the ratio of 40 % slag & 60 % Pure flux for the welding on plates. 3. The Preparation of High Strength Low Alloy Steel Plates 250 x 150 x 10 mm . 4. The Preparation of welding electrode for Submerged arc welding , EH 14 (AWS grade EH-14) of diameter 3.2 mm. 5. The Experiment Designed based on BOX-BEHNKEN DESIGN (BBD) using state ease 6.0 Version of design of experiment. 6. The Experiment was conducted as per the design matrix using TORNANDO SAW M- 800 equipment at Mullana University Mullana. 7. Reuse slag as Flux consumption measured each 29 experiment run according to design matrix reading. 3. Welding Parameters & Chemical Composition :- (A) Welding Current :- In SAW ,Current plays a major role where it controls the melting rate of the electrode and thereby the weld deposition rate. It also controls the depth of penetration and thereby the
  • 5. IJESM Volume 2, Issue 1 ISSN: 2320-0294 _________________________________________________________ A Quarterly Double-Blind Peer Reviewed Refereed Open Access International e-Journal - Included in the International Serial Directories Indexed & Listed at: Ulrich's Periodicals Directory ©, U.S.A., Open J-Gage, India as well as in Cabell’s Directories of Publishing Opportunities, U.S.A. International Journal of Engineering, Science and Mathematics http://www.ijmra.us 218 March 2013 extent of dilution of the weld metal by the base metal. The current density controls the depth of penetration - the higher the current density the greater the penetration For a given flux, arc stability will be lost below a minimum threshold current density so that if the current for a given electrode diameter is too low arc stability is lost and a rugged, irregular bead is obtained. Too high a current density also leads to instability because the electrode overheats and undercutting may also occur weld reinforcement which is wasteful, and burn- through in the case of thinner plates or in badly fitted joints, which are not provided with proper backing [4]. Excessive current also produces a high narrow bead and undercut. Excessively low current gives an unstable arc, inadequate penetration and overlapping. SAW equipment is usually provided with an ammeter to monitor and control the welding current . (B) Voltage Arc Voltage affects dilution rather than penetration. Bead on plate welds and square edged closed butt welds have increased width and dilution as the arc voltage increases, but depth of penetration remains the same. If the joint preparation is open, for example in a butt joint with a small angled 'V' preparation, increasing the arc voltage can decrease the penetration. Arc voltage, also called welding voltage, means the electrical potential difference between the electrode wire tip and the surface of the molten weld puddle. (C) Weld Speed Welding speed or travel speed controls depth of penetration. Bead size is inversely proportional to travel speed. Faster speeds reduce penetration and bead width, increase the likelihood of porosity and, if taken to the extreme, produce undercutting and irregular beads. At high welding speeds the arc voltage should be kept fairly low otherwise arc blow is likely too occur [4]. If the welding speed is too slow burn through can occur. A combination of high arc voltage and slow welding speed can produce a mushroom shaped weld bead with solidification cracks at the bead sides. (D) Nozzle to Plate Distance SAW filler material usually is a standard wire as well as other special forms. This wire normally has a thickness of 1/16 in. to 1/4 in. (1.6 mm to 6 mm). In certain circumstances, twisted wire can be used to give the arc an oscillating movement. In SAW welding nozzle
  • 6. IJESM Volume 2, Issue 1 ISSN: 2320-0294 _________________________________________________________ A Quarterly Double-Blind Peer Reviewed Refereed Open Access International e-Journal - Included in the International Serial Directories Indexed & Listed at: Ulrich's Periodicals Directory ©, U.S.A., Open J-Gage, India as well as in Cabell’s Directories of Publishing Opportunities, U.S.A. International Journal of Engineering, Science and Mathematics http://www.ijmra.us 219 March 2013 to plate distance plays a major role. To operate welding smoothly ,generally in saw welding distance between nozzle to tip and work piece is 15 mm to 30 mm. Parameters Units Limits -2 -1 0 1 2 Current (C) amp 300 350 400 450 500 Voltage (V) volts 26 28 30 32 34 Welding Speed (S) m/hr 21 24 27 30 33 N.P. Distance (D) mm 16 18 20 22 24 Type Grade Chemical Composition(%) C Mn P S Si Cr Mo Ni Fe W.Piece Hsla 945X 0.22 1.35 0.04 0.05 0.90 0.04 0.05 0.87 Bal Electrode Wire EH14 0.15 1.9 - 0.05 - - - 0.4 Bal % age C Mn Si S P With fresh Flux 0.357 0.325 0.188 0.04867 0.4876 With 40 % reused Slag 0.1812 0.4312 0.1071 0.0264 0.0289
  • 7. IJESM Volume 2, Issue 1 ISSN: 2320-0294 _________________________________________________________ A Quarterly Double-Blind Peer Reviewed Refereed Open Access International e-Journal - Included in the International Serial Directories Indexed & Listed at: Ulrich's Periodicals Directory ©, U.S.A., Open J-Gage, India as well as in Cabell’s Directories of Publishing Opportunities, U.S.A. International Journal of Engineering, Science and Mathematics http://www.ijmra.us 220 March 2013 4. Methodology Identification of the process parameters :- The following independently controllable process parameters were identified to carry out the experiments: open-circuit voltage (V); wire feed rate (F); welding speed (S); and nozzle-to-plate distance (N) . Finding the limits of the process variables:- Trial runs were carried out by varying one of the process parameters whilst keeping the rest of them at constant values [6]. The working range was decided upon by inspecting the bead for smooth appearance and the absence of any visible defects. The upper limit of a factor was coded as +2 and the lower limit as -2, the coded values being calculated from the following relationship: Xi = 2[2X-(Xmax-Xmin)] (Xmax-Xmin) where Xi is the required coded value of a variable X; and X is any value of the variable from Xmin to Xmax. The selected process parameters with their limits, units and notations .
  • 8. IJESM Volume 2, Issue 1 ISSN: 2320-0294 _________________________________________________________ A Quarterly Double-Blind Peer Reviewed Refereed Open Access International e-Journal - Included in the International Serial Directories Indexed & Listed at: Ulrich's Periodicals Directory ©, U.S.A., Open J-Gage, India as well as in Cabell’s Directories of Publishing Opportunities, U.S.A. International Journal of Engineering, Science and Mathematics http://www.ijmra.us 221 March 2013 Developing the design matrix :- The selected design matrix, is a central composite rotatable factorial design consisting of 31 sets of coded conditions. It comprises a full replication of 24 (=16) factorial design plus seven center points and eight star points. All welding variables at the intermediate level (0) constitute the center points and the combinations of each of the welding variables at either its lowest (-2) level or highest (+2) level with the other three variables at the intermediate levels constitute the star points.[8] Thus the 29 experimental runs allowed the estimation of the linear, quadratic and two-way interactive effects of the process parameters on the bead geometry Conducting the experiment as per the design matrix :- The experiments were conducted as per the design matrix at random, to avoid the possibility of systematic errors infiltrating the system. Recording of the responses :- During the experiments flux consumption was measured after each run. Measured quantity of flux was put into the flux hopper before taking the bead and again measured after taking the bead. Difference of the two quantities was taken as the flux consumption. Development of mathematical models :- The response function representing any of the weld bead dimensions can be expressed as : Y= f ( V, F, S, N). The relationship selected being a second degree response surface expressed as follows: Y=b0+b1V+b2F+b3S+b4N+b11V2+b22F2+b33S2+b44N2+b12VF+b13VS+b14VN+b23FS +b24FN+b34SN Checking the adequacy of the models developed :- The adequacy of the models was tested using the analysis of variance technique (ANOVA). The calculated value of the F-ratio of the model developed should be greater than the standard tabulated value of F-ratio for a desired level of confidence (say 95%) for the model to be significant.
  • 9. IJESM Volume 2, Issue 1 ISSN: 2320-0294 _________________________________________________________ A Quarterly Double-Blind Peer Reviewed Refereed Open Access International e-Journal - Included in the International Serial Directories Indexed & Listed at: Ulrich's Periodicals Directory ©, U.S.A., Open J-Gage, India as well as in Cabell’s Directories of Publishing Opportunities, U.S.A. International Journal of Engineering, Science and Mathematics http://www.ijmra.us 222 March 2013 Experiment Process Parameters Responses Factors Standard Run Current Voltage Welding Speed Nozzle to Plate Distance Reuse Slag as Flux Consumption Limits Numbers (Amperes) (Volts) (M/hr) (M.M) (Gms) 1 11 300 26 27 20 43.0 2 26 500 26 27 20 89.0 3 17 300 34 27 20 55.0 4 19 500 34 27 20 65.0 5 9 400 30 21 16 38.0 6 23 400 30 33 16 45.0 7 6 400 30 21 24 48.0 8 7 400 30 33 24 52.0 9 28 300 30 27 16 37.0 10 3 500 30 27 16 82.0 11 25 300 30 27 24 52.0 12 20 500 30 27 24 67.0 13 27 400 26 21 20 44.0 14 12 400 34 21 20 41.0 15 8 400 26 33 20 47.0 16 2 400 34 33 20 48.0 17 15 300 30 21 20 42.0 18 4 500 30 21 20 56.0 19 18 300 30 33 20 27.0 20 14 500 30 33 20 84.0 21 5 400 26 27 16 52.0 22 24 400 34 27 16 47.0 23 1 400 26 27 24 54.0
  • 10. IJESM Volume 2, Issue 1 ISSN: 2320-0294 _________________________________________________________ A Quarterly Double-Blind Peer Reviewed Refereed Open Access International e-Journal - Included in the International Serial Directories Indexed & Listed at: Ulrich's Periodicals Directory ©, U.S.A., Open J-Gage, India as well as in Cabell’s Directories of Publishing Opportunities, U.S.A. International Journal of Engineering, Science and Mathematics http://www.ijmra.us 223 March 2013 5. Results Interaction effects :-The difference in effect of one variable when a second variable is changed from one level to another is known as interaction effect and study of interaction effects of process variables on bead dimensions is interesting and very useful for understanding the process behavior. In this study, the effect of welding current, arc voltage, welding speed and distance between tip of nozzle & work piece on the reused slag as flux consumption. These figures shows results of the slag as flux consumption according to the welding parameters. Fig 5.1 Fig 5.2 Figure 5.1 shows Slag as flux consumption Decreases when increases the Voltage , while Figure 5.2 shows Slag as flux consumption Increases when welding current increases . 24 16 400 34 27 24 51.0 25 21 400 30 27 20 51.0 26 29 400 30 27 20 52.0 27 10 400 30 27 20 48.0 28 13 400 30 27 20 52.0 29 22 400 30 27 20 44.0
  • 11. IJESM Volume 2, Issue 1 ISSN: 2320-0294 _________________________________________________________ A Quarterly Double-Blind Peer Reviewed Refereed Open Access International e-Journal - Included in the International Serial Directories Indexed & Listed at: Ulrich's Periodicals Directory ©, U.S.A., Open J-Gage, India as well as in Cabell’s Directories of Publishing Opportunities, U.S.A. International Journal of Engineering, Science and Mathematics http://www.ijmra.us 224 March 2013 Fig 5.3 Fig 5.4 Figure 5.3 shows Slag as flux consumption Increases when increases the welding speed , while Figure 5.4 shows Slag as flux consumption Increases when Nozzle to plate distance increases . Interaction effect The difference in effect of one variable when a second variable is changed from one level to another is known as interaction effect and study of interaction effects of process variables on bead dimensions is interesting and very useful for understanding the process behavior. In this study, to avoid complexity two way interactive effects of the variables are selected. Fig 5.5 Fig 5.6
  • 12. IJESM Volume 2, Issue 1 ISSN: 2320-0294 _________________________________________________________ A Quarterly Double-Blind Peer Reviewed Refereed Open Access International e-Journal - Included in the International Serial Directories Indexed & Listed at: Ulrich's Periodicals Directory ©, U.S.A., Open J-Gage, India as well as in Cabell’s Directories of Publishing Opportunities, U.S.A. International Journal of Engineering, Science and Mathematics http://www.ijmra.us 225 March 2013 Fig 5.7 Fig 5.8 CONCLUSIONS :- On the basis of present study the following conclusions can be drawn: 1. RSM can be used effectively in analyzing the cause and the effect of process parameters on response. The RSM is also used to draw contour graphs for various responses to show the interaction effects of different process parameters. 2. Arc Stability & slag detachability were acceptable and SAW slag can be reused as welding flux after crushing & sieving and mixing with pure flux . 3. Flux consumption increased with the increase in open circuit voltage and very small increases with increases in current , Welding speed has negative effect on flux consumption. 4. Flux consumption also small decreases with the increase in nozzle to plate distance.
  • 13. IJESM Volume 2, Issue 1 ISSN: 2320-0294 _________________________________________________________ A Quarterly Double-Blind Peer Reviewed Refereed Open Access International e-Journal - Included in the International Serial Directories Indexed & Listed at: Ulrich's Periodicals Directory ©, U.S.A., Open J-Gage, India as well as in Cabell’s Directories of Publishing Opportunities, U.S.A. International Journal of Engineering, Science and Mathematics http://www.ijmra.us 226 March 2013 REFERENCES  V.Gunaraja,N.Murugan,”Application of Response surface methodology for predicting weld bead quality in submerged are welding of pipes”,Journal of material processing technology “,88(1999)266-275 Received at 26 November 1997.  R.S.Chandel,”The Effects of process variables on the flux consumption in Submerged arc welding”,Materials and Manufacturing Process,Vol 13,No-2,181-188,1998.  Jasvinder Singh , Kulwant & Jastinder Garg ;” Reuse of slag as flux in saw & its effect on chemical composition , bead geometry & microstructure of the weld metal,Vol.1 No.1 July- Dec 2011  C.S Chai and T.W. Eagar., Slag-Metal Reaction during Welding, Metall. Trans. B, Vol.12, 1991.p 65-100.  U. MITRA and T.W. EGAR. Slag Metal Reaction during Welding: Part 1. Evaluation and Research of Exiting Theories., 1991  Mitra U. and Eagar T.W., “Slag Metal Reaction during Welding; part I. Evaluation and Reassessment of Existing Theories”, Metallurgical Transactions, American Society for Metals, Vol.22B, 1991,65-79.  Singh K, Pandey S, Arul Mani R (2006) “Recycling of Submerged Arc Welding Slag”, Australasian Welding Journal, Vol 51(2), pp 34-38.  Datta S, Bandyopadhyay A, Pal PK (2008) “Slag Recycling in Submerged Arc Welding and its influence on Weld Quality leading to Parametric Optimization”, International Journal of Advanced Manufacturing Technology, Vol. 39(10), pp 229-238.  Krishankant, Sandeep jindal, Shashi kant shekhar ,” Determination of Flux Consumption in Submerged arc welding by the effect of welding Parameters by using R.S.M Techniques ,GJRE Volume 12 Issue 2.ISSN 0975-5861  Sermsuk Buochareon , Bovornchok Pupat ,” Effect of reused flux and new welding flux blend or saw due to chemical composition of hard facing weld bead formation.IE Conference 24-25 Oct 2007