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Fractional Distillation
1.
2. Fractional distillation is one of the widely used
distillation technique used in R & D sector because
of its efficiency and accuracy.
It is more efficient in separating ideal solutions
into their pure components than the traitional
method of distillation
3. Heat Source for e.g a hot plate with a bath
A distillation flask (preferably a round-bottom flask)
A collecting flask ( conical shaped or round-bottom flask)
Fractionating column ( elongated glass ware for solvent
cooling)
Distillation head
Thermometer (to measure the temperature of the solvent
placed)
Condenser
Vaccumed Adapter (to carry out distillations under reduced
pressure)
Boiling chips or Anti-bumping granules
Rubber bungs, unless laboratory glassware with ground
4. Purification of water and ethanol mixture is
usually carried in the research labs
The separation of ethanol and water is based upon
the different boiling point of the two solvent.
Ethanol require boiling point of 78.5 ° water boils
at a temperature of 100 degree Celsius
Boiling the mixture in fractional distillation
column separates the liquid into its respective
components
Usaully 96% of pure ethanol is extracted by
fractional distillation technique
5. Similarly various other Azeotropic mixture can be
extracted using fractional distillation technique
such as a mixture of cyclohexane and toluene, etc.
Fractional Distillation has gained a wider
application in scientific research laboratories and
in industrial application to extract the pure form of
solvent from its solvent mixture