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1
Ozonation
Bottled Package Drinking
Water
- Index
2
1. Objective
2. Ozone Associate Equipments
3. Air Preparation & Purification
4. Oxygen Concentrator
5. IV Generation Ozonator
6. Associate Equipments
7. Selection / Sizing Formulas
8. Testing | Monitoring | Log | Maintenance
9. References
- Objective Of Ozonation
3
• For Raw Water Treatment • Final Product Water Additive
Removes Pesticides & Insecticides
Oxidizes All Organic Impurities
Oxidizes Inorganics to Precipitate
Micro Flocculent
Strong Disinfectant
Improves Taste & Oxidizes Colour
Eliminates Any Present Odor
Increased Shelf Life
Keeps Lines & Equipments Disinfected
Provides Overall Bacterio-static Condition
Disinfects New Molded Bottles & Caps
Disinfects Free air in Bottles
Improves Taste
Refill Jar Disinfection & Rinsing
- Ozonation – Associated Equipments
4
• Ozone Generator
• Oxygen Concentrator
• Air Compressor
• Air Dryer
• Back-Flow Preventer
• Ventury Injection
• Static Mixture
- Ozonation – Associated Equipments
5
• Quality Of Ozone Depends Upon
»Quality & Technology of Ozone Generator
»Quality Of Feed Gas - Oxygen
• Quality Of Oxygen Depends Upon
»Quality & Technology of Oxygen Concentrator
»Quality Of Feed Gas – Air
• Quality Of Air Depends Upon
»Quality & Technology of Air Compressor
»Quality Of Air Purification [Pre-treatment]
Ozone Generator
Air Purification &
Oxygen Separation
Air Preparation &
Air Purification
Flow Diagram – Ozone Associate Equipments
6
A i r P r e p a r a t i o n & P u r i f i c a t i o n
Air
Compress
or
Moisture
Separatio
n
Pre
Filter
Oil
Filter
Air
Dryer
Air
Cooler
Air
Dryer
Pressure
Swing
Adsorption
Pre
Filter
Oil Removal
Filter
Fine
Filter
O x y g e n
C o n c e n t r a t o r
O Z O N E G E N E R AT O R
- Air & Oxygen Line - Factory Layout
7
- Air Preparation & Purification
8
1. Oil Free Screw Compressor
2. After Cooler / Heat Exchanger
3. Moisture Separator
4. Wet Air Receiver
5. Pre Filter & Oil Removal Filter
6. Refrigerant Air Dryer / Heatless Air Dryer
7. Dry Air Receiver
- Flow Diagram - Air Preparation & Purification
9
- Air Quality Specification - Requirements
10
• Dust [Solids] - < 5.0 Micron
• Oil - < 0.1 ppm
• Temperature - < 40°C
• Moisture - < 200 ppm
• Due Point - < - 15 ° C
• Pressure - 7.0 bar (min.)
- Oxygen Concentrator
11
• Pre Filter + Oil Filter + Air Dryer – With Auto Drain
• Pressure Swing Adsorption [PSA] Oxygen Concentrator
• High Pressure Zeolite Molecular Sieves [ZMS] - - - 6 – 8 bar
• High Strength, Friction & Abrasive Resistant ZMS
• Longer Operation Life - - - - - - - - - 4 – 6 years
• Serge Tank for Stabilization & Purity
• PLC Bases Operation - Precise Timing Control
• Pneumatically Operating High Speed Solenoid
12
- Flow Diagram – Oxygen Concentrator
- Oxygen Specification
13
• Concentration - 93 % ± 3 %
• Solids - < 0.02 Micron
• Moisture - < 80 ppm [0.1 ml / m³ of Oxygen]
• Oil Content - < 0.1 ppm
• Due Point - Standard – 40 °C ; - 60 °C [If Required]
• Oil Content - < 0.1 ppm
• Out Put Pressure - 40 psi (min.)
- Ozone Generator - IV Generation
14
• Ozone Cell Cooling - Internally & Externally Water Cooled [Both Electrodes]
• Insulated Gate Bipolar Transistor [IGBT]
• Isolated Enclosures – Electronics : IP 54 ; Ozone Cell : IP 65
• Enclosure CE Marked & UL Certified
• Switch Mode Power Supply [SMPS]
• Soft Start & Soft Shut Off
• Ozone Cell Life – 20,000 Working Hours
- Ozone Generator - IV Generation
15
2.0 G/hr to 250 G/hr
- Ozone Generator – Driver Circuit Protections
16
• Power Line – Surge & Spike Protection
• Over Voltage - Supply
• Under Voltage - Supply
• Over Heat [Temperature]
• Over Current – High Voltage
• Open Circuit – High Voltage
• Short Circuit – High Voltage
- Ozone Generator – Specification
17
• Ozone Concentration - 80 – 130 G/m³ - 100 G/m³ (min.) w/v
• Ozone Gas Pressure - 1.0 – 1.5 bar – 1.2 bar (Max.)
- Ozonation – Associated Equipments
18
• Back Flow Protection | Water Trap
• Moulded Ventury Injector
• Static Mixer
• Oxygen Monitor
• ORP Monitor
• Dissolved Ozone Monitor
• Ozone Percentage Indicator *
* Under Testing – Will be available from Jan 2016
- Ozonation – Associated Equipments – Static Mixer
19
Cube : 1.0 mm³
Bubble Dia : 1.0 mm
No. Of Bubble : 01 no.
Surface Area : 3.14 mm²
Total S. Area : 3.14 mm²
Cube : 1.0 mm³
Bubble Dia : 0.5 mm
No. Of Bubble : 08 nos.
Surface Area : 0.786 mm²
Total S. Area : 6.29 mm²
Cube : 1.0 mm³
Bubble Dia : 0.1 mm
No. Of Bubble : 1,000 nos.
Surface Area : 0.0314 mm²
Total S. Area : 31.43 mm²
1.0 mm
1.0 mm
1.0 mm
As the Bubble Size Decreases, Total Surface Area Increases
- Process Flow Diagram – Raw Water Ozonation
20
- Process Flow Diagram – Processed Water
Ozonation
21
- Equipment Selection & Sizing Calculation
22
Design Calculation for Ozonator
Ozone Dose – Raw Water Treatment : 3.0 – 5.0 ppm
Ozone Dose – Processed Water Additive : 1.5 – 2.5 ppm
Ozone Generator Capacity = Water Flow Rate (m3/hr) X Ozone Dose (gm/m3)
For Example = 25 (m3/hr) X 2.0 – 2.5 (gm/m3) = 50 - 63 gm/hr
= 25 – 32 gm/hr X 3 nos. (2 W + 1S)
= 95 gm/hr (Total installed Capacity)
Recommended Ozonator Model: OG/HC –50 x 3 nos. (2 W + 1 S)
- Equipment Selection & Sizing Calculation
23
Design Calculation for Oxygen Concentrator
•Feed Gas : Pure Oxygen Gas with following specification
•Purity : ≥ 92 %
•Oxygen Pressure : 1.0 – 1.4 bar
Required Oxygen
Quantity Ozone Concentration (gm/m3)
0.15 = 1.1 Nm3/hr i.e. 18 LPM
Total Ozone Capacity (gm/hr)
95 (gm/hr)
100 (gm/m3)
=
O2 Drying %
[16.0 %]+
+
=
- Equipment Selection & Sizing Calculation
24
Design Calculation for Air Compressor
Quality of feed gas as per following specification:
Dryness : < - 40 o C (Dew Point)
Solids / Dust : < 5.0 micron
Oil : < 0.1 ppm
Feed Air for Oxygen = Capacity of Oxygen (Nm3/hr) x 16 (Multiplying Factor)
= 1.1 (Nm3/hr ) X 16
= 17.6 Nm3/hr i.e. 10.4 CFM
- Testing | Monitoring | Logs | Routine Maintenance
25
Equipment Maintenance Log Sheet
Month- Ozonation System for Package Drinking Water
Frequency Daily Monthly
Sr.
No.
Date
Oxygen
Flow
(LPM)
Ozonator
Current
(Amp)
Hour
Meter
Reading
(Hrs)
ORP
Meter
Reading
(mV)
Temp.
Meter
Reading
(oC)
Oxygen
Purity
(%)
Dissolved
Ozone at
Venture
End
(PPM)
Dissolved
Ozone at
Filling End
(PPM)
Ozone
Out Put
(gm/hr)
Operator
Signature
Remark
1
2
3
Thank You
26
Solution Engineer : Mr. Sunil Shah
Contact : +91-93212 34527
Mail ID : sunilshah@chemtronicsindia.com
URL : www.chemtronicsindia.com
www.ozonegeneratorindia.com
www.m.chemtronicsindia.com

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Ozone in package bottled drinking water

  • 2. - Index 2 1. Objective 2. Ozone Associate Equipments 3. Air Preparation & Purification 4. Oxygen Concentrator 5. IV Generation Ozonator 6. Associate Equipments 7. Selection / Sizing Formulas 8. Testing | Monitoring | Log | Maintenance 9. References
  • 3. - Objective Of Ozonation 3 • For Raw Water Treatment • Final Product Water Additive Removes Pesticides & Insecticides Oxidizes All Organic Impurities Oxidizes Inorganics to Precipitate Micro Flocculent Strong Disinfectant Improves Taste & Oxidizes Colour Eliminates Any Present Odor Increased Shelf Life Keeps Lines & Equipments Disinfected Provides Overall Bacterio-static Condition Disinfects New Molded Bottles & Caps Disinfects Free air in Bottles Improves Taste Refill Jar Disinfection & Rinsing
  • 4. - Ozonation – Associated Equipments 4 • Ozone Generator • Oxygen Concentrator • Air Compressor • Air Dryer • Back-Flow Preventer • Ventury Injection • Static Mixture
  • 5. - Ozonation – Associated Equipments 5 • Quality Of Ozone Depends Upon »Quality & Technology of Ozone Generator »Quality Of Feed Gas - Oxygen • Quality Of Oxygen Depends Upon »Quality & Technology of Oxygen Concentrator »Quality Of Feed Gas – Air • Quality Of Air Depends Upon »Quality & Technology of Air Compressor »Quality Of Air Purification [Pre-treatment] Ozone Generator Air Purification & Oxygen Separation Air Preparation & Air Purification
  • 6. Flow Diagram – Ozone Associate Equipments 6 A i r P r e p a r a t i o n & P u r i f i c a t i o n Air Compress or Moisture Separatio n Pre Filter Oil Filter Air Dryer Air Cooler Air Dryer Pressure Swing Adsorption Pre Filter Oil Removal Filter Fine Filter O x y g e n C o n c e n t r a t o r O Z O N E G E N E R AT O R
  • 7. - Air & Oxygen Line - Factory Layout 7
  • 8. - Air Preparation & Purification 8 1. Oil Free Screw Compressor 2. After Cooler / Heat Exchanger 3. Moisture Separator 4. Wet Air Receiver 5. Pre Filter & Oil Removal Filter 6. Refrigerant Air Dryer / Heatless Air Dryer 7. Dry Air Receiver
  • 9. - Flow Diagram - Air Preparation & Purification 9
  • 10. - Air Quality Specification - Requirements 10 • Dust [Solids] - < 5.0 Micron • Oil - < 0.1 ppm • Temperature - < 40°C • Moisture - < 200 ppm • Due Point - < - 15 ° C • Pressure - 7.0 bar (min.)
  • 11. - Oxygen Concentrator 11 • Pre Filter + Oil Filter + Air Dryer – With Auto Drain • Pressure Swing Adsorption [PSA] Oxygen Concentrator • High Pressure Zeolite Molecular Sieves [ZMS] - - - 6 – 8 bar • High Strength, Friction & Abrasive Resistant ZMS • Longer Operation Life - - - - - - - - - 4 – 6 years • Serge Tank for Stabilization & Purity • PLC Bases Operation - Precise Timing Control • Pneumatically Operating High Speed Solenoid
  • 12. 12 - Flow Diagram – Oxygen Concentrator
  • 13. - Oxygen Specification 13 • Concentration - 93 % ± 3 % • Solids - < 0.02 Micron • Moisture - < 80 ppm [0.1 ml / m³ of Oxygen] • Oil Content - < 0.1 ppm • Due Point - Standard – 40 °C ; - 60 °C [If Required] • Oil Content - < 0.1 ppm • Out Put Pressure - 40 psi (min.)
  • 14. - Ozone Generator - IV Generation 14 • Ozone Cell Cooling - Internally & Externally Water Cooled [Both Electrodes] • Insulated Gate Bipolar Transistor [IGBT] • Isolated Enclosures – Electronics : IP 54 ; Ozone Cell : IP 65 • Enclosure CE Marked & UL Certified • Switch Mode Power Supply [SMPS] • Soft Start & Soft Shut Off • Ozone Cell Life – 20,000 Working Hours
  • 15. - Ozone Generator - IV Generation 15 2.0 G/hr to 250 G/hr
  • 16. - Ozone Generator – Driver Circuit Protections 16 • Power Line – Surge & Spike Protection • Over Voltage - Supply • Under Voltage - Supply • Over Heat [Temperature] • Over Current – High Voltage • Open Circuit – High Voltage • Short Circuit – High Voltage
  • 17. - Ozone Generator – Specification 17 • Ozone Concentration - 80 – 130 G/m³ - 100 G/m³ (min.) w/v • Ozone Gas Pressure - 1.0 – 1.5 bar – 1.2 bar (Max.)
  • 18. - Ozonation – Associated Equipments 18 • Back Flow Protection | Water Trap • Moulded Ventury Injector • Static Mixer • Oxygen Monitor • ORP Monitor • Dissolved Ozone Monitor • Ozone Percentage Indicator * * Under Testing – Will be available from Jan 2016
  • 19. - Ozonation – Associated Equipments – Static Mixer 19 Cube : 1.0 mm³ Bubble Dia : 1.0 mm No. Of Bubble : 01 no. Surface Area : 3.14 mm² Total S. Area : 3.14 mm² Cube : 1.0 mm³ Bubble Dia : 0.5 mm No. Of Bubble : 08 nos. Surface Area : 0.786 mm² Total S. Area : 6.29 mm² Cube : 1.0 mm³ Bubble Dia : 0.1 mm No. Of Bubble : 1,000 nos. Surface Area : 0.0314 mm² Total S. Area : 31.43 mm² 1.0 mm 1.0 mm 1.0 mm As the Bubble Size Decreases, Total Surface Area Increases
  • 20. - Process Flow Diagram – Raw Water Ozonation 20
  • 21. - Process Flow Diagram – Processed Water Ozonation 21
  • 22. - Equipment Selection & Sizing Calculation 22 Design Calculation for Ozonator Ozone Dose – Raw Water Treatment : 3.0 – 5.0 ppm Ozone Dose – Processed Water Additive : 1.5 – 2.5 ppm Ozone Generator Capacity = Water Flow Rate (m3/hr) X Ozone Dose (gm/m3) For Example = 25 (m3/hr) X 2.0 – 2.5 (gm/m3) = 50 - 63 gm/hr = 25 – 32 gm/hr X 3 nos. (2 W + 1S) = 95 gm/hr (Total installed Capacity) Recommended Ozonator Model: OG/HC –50 x 3 nos. (2 W + 1 S)
  • 23. - Equipment Selection & Sizing Calculation 23 Design Calculation for Oxygen Concentrator •Feed Gas : Pure Oxygen Gas with following specification •Purity : ≥ 92 % •Oxygen Pressure : 1.0 – 1.4 bar Required Oxygen Quantity Ozone Concentration (gm/m3) 0.15 = 1.1 Nm3/hr i.e. 18 LPM Total Ozone Capacity (gm/hr) 95 (gm/hr) 100 (gm/m3) = O2 Drying % [16.0 %]+ + =
  • 24. - Equipment Selection & Sizing Calculation 24 Design Calculation for Air Compressor Quality of feed gas as per following specification: Dryness : < - 40 o C (Dew Point) Solids / Dust : < 5.0 micron Oil : < 0.1 ppm Feed Air for Oxygen = Capacity of Oxygen (Nm3/hr) x 16 (Multiplying Factor) = 1.1 (Nm3/hr ) X 16 = 17.6 Nm3/hr i.e. 10.4 CFM
  • 25. - Testing | Monitoring | Logs | Routine Maintenance 25 Equipment Maintenance Log Sheet Month- Ozonation System for Package Drinking Water Frequency Daily Monthly Sr. No. Date Oxygen Flow (LPM) Ozonator Current (Amp) Hour Meter Reading (Hrs) ORP Meter Reading (mV) Temp. Meter Reading (oC) Oxygen Purity (%) Dissolved Ozone at Venture End (PPM) Dissolved Ozone at Filling End (PPM) Ozone Out Put (gm/hr) Operator Signature Remark 1 2 3
  • 26. Thank You 26 Solution Engineer : Mr. Sunil Shah Contact : +91-93212 34527 Mail ID : sunilshah@chemtronicsindia.com URL : www.chemtronicsindia.com www.ozonegeneratorindia.com www.m.chemtronicsindia.com