FULL HD PLASTIC ™ REPORT
ΔL Δa Δ
Rate replication from the mold surface (%)
Rev.: A
GLOSS RESULTS (ISO 2813 Standard)
T=90°C - Conventional - WITHOUT 40,3 94,9T=140°C - Roctool - WITH
TRADE NAME
0,53
17/01/2018 TRIAL # HDP-17-022 MOLD HD PLAQUE
MATERIAL
FAMILY PC GF50
FORM
FOR-TEC-111
Page 1 of 3
QUALITY SURFACE CHARACTERIZATION REPORT
LNP™ THERMOCOMP™ COMPOUND GRADE D551
DATE
DELTACOLOR SCALE
L* ( Lightness)
MEASUREMENTS
PROCESS TECHNOLOGY
0,03
T=140°C - Roctool - WITH
SUPPLIER SABIC
0,57
ΔE
COLOR
DIFFERENCE
LAB - COLOR DEPHT RESULTS (DIN 5033 Standard)
0,2
T=90°C - Conventional - WITHOUT
26,83 -0,21 -0,87
27,36
a*
-0,18
b*
-0,67
Note: L* = 0 yields black and L* = 100 indicates diffuse white. a*: negative values indicate green while positive values indicate red. b*: negative values indicate blue and positive values
indicate yellow. ΔE> , usual olor tolera e.
Roughness profile - Conventional VS Roctool Technology
T=140°C - Roctool - WITHT=90°C - Conventional - WITHOUT
PICTURES OF INJECTED SAMPLES
3D TEXTURATION RESULTS
T=90°C - Conventional - WITHOUT T=140°C - Roctool - WITH
Conventional (µm3
) Roctool technology (µm3
) Improvement (%)Roughness parameters
14802 20307
59% 81%
37%
Volume cavity (µm3
)
Note: In conventional molding, the measurements of the VDI roughness are not mentionned as the presence of glass fibers on the surface disturb the measurement impacting the Ra
value.
VDI 18 (Ra=±0.80 µm) VDI 22 (Ra=±1.26 µm) VDI 27 (Ra=±2.20 µm)
Roctool technology 140°C
0,75
0,89
1,11 1,73
0,96 1,45
1,03 1,56
2,27 Ra (µm)
EDM Ra (µm)
LASER Ra (µm)
CHEMICAL
COMMENTS
Rz (µm) 6,4 0,72 -89%
Roughness parameters
Quality surface characterization:
1) Visible improvements using Roctool technology are observed: weld line and sink marks are removed. Glass fibers and defects are removed
from the surface.
2) Significant improvement on the gloss value up to 135%. However, we measured an impact of the mold temperature on the color perception
and Roctool technology allows a darker color with a perfect surface finish compared to conventional process.
3) The different textured areas hightlight the positive impact on the replication using Roctool technology.
Also, the different roughnesses are well felt when touched. The roughness measurement carried out using optical rugosimeter confirms the
above with repliction rate of up to 81% : an improvement of 37% with Roctool compared to conventional technology (CIM).
Also, the Rz value has been carried out and shows the positive impact of Roctool with an important reduction of the roughness on high gloss
surface due to the elimination of glass fibers at the surface.
Rev.: A
Page 2 of 3
QUALITY SURFACE CHARACTERIZATION REPORT
FORM
FOR-TEC-111
Conventional (90°C) Roctool technology (140°C) Improvement (%)
TEXTURE RESULTS - Rz (Mean roughness depth)
T=90°C - Conventional - WITHOUT T=140°C - Roctool - WITH
TEXTURE RESULTS - Ra (Amplitude roughness parameter)
MEASUREMENT AREAS
1) The high gloss area framed in blue is the measurement area for the
gloss, color and specific roughness Rz* .
2) The red rectangle define the nano-replication area.
3) The green box correspond to the multi-textured (VDI) area were the
roughness is measured.
*Rz: Maximal amplitude roughness mesured for filled materials
ROUGHNESS MEASUREMENT PRINCIPLE
Optical rugosimeter is a measuring instrument used to measure a
surface's profile, in order to quantify its roughness.
In the context of HD Plastics™, two information are carried out using
Alicona equipment according to the standard ISO 4287:
- Replication rate : volume of the specific texture defined versus the one
textured on the mold surface quavity
- The surface roughness parameters : Arithmetical mean deviation (Ra)
which evaluate the roughness amplitude on a profile and Mean roughness
depth (Rz) which measure the maximal amplitude roughness average of
the profile.
GLOSS PRINCIPLE
FORM
FOR-TEC-111 Rev.: A
Page 3 of 3
QUALITY SURFACE CHARACTERIZATION REPORT
ANNEXES
LAB COLOR PRINCIPLE
The Lab color space describes all perceivable colors in the three
di e sio s L for light ess a d a a d for the olor oppo e ts gree –red
a d lue– ello .
In the context of HD Plastics™, a spectrophotometer is used to carried
out the LAB alue : spe tro-guide / gloss BYK . HD Plasti s™ is
following the DIN 5033 Standard.
The graph shows the LAB color scale. The lightness, L*, represents the
darkest black at L* = 0, and the brightest white at L* = 100. The a* and b*
value represent the color channels. a*: negative values indicate green
while positive values indicate red. b*: negative values indicate blue and
positive values indicate yellow
Gloss is an optical property which indicates how well a surface reflects
light in a specular direction. It is one of important parameters that are
used to describe the visual appearance of an object. The factors that affect
gloss are the refractive index of the material, the angle of incident light
and the surface topography.
I the o te t of HD Plasti s™, a glossmeter is used to carried out the
gloss value with a incident angle of 60° : spectro-guide 45/0 gloss (BYK).
HD Plasti s™ is follo i g the ISO 8 Sta dard.
The graph shows the gloss scale using glossmeter following 60° angle in
the gloss unit. Low Gloss corresponds to a textured surface, Semi Gloss
and High Gloss to high polished surface.
White
L* = 100
Black
L* = 0
Sensor 1 Sensor 2 Sensor 1 Sensor 2 Sensor 1 Sensor 2 Sensor 1 Sensor 2 Sensor 1 Sensor 2 Sensor 1 Sensor 2
243,5 0 754,33 266,67 1169,7 592,33 456 322,5 914,33 654,5 1336 967,7
Sensors
Mold Pressure Avg
Pressure Drop (%)
PRESSURE DROP BETWEEN THE TWO PRESSURE SENSORS
CONVENTIONAL TECHNOLOGY (100°C) ROCTOOL TECHNOLOGY (180°C)
Pressure (Bar) 500 1000 1500 500 1000 1500
-62,8%
- 78,5%
FLOW LENGTH MEASUREMENT AT DIFFERENT IMM PRESSURE IMM PRESSURE DROP AT ISO FLOW LENGTH
Sabic
32,8% 140°C
500 1000 1500 Flow Length (cm) 5 10
Flow length improvement IMM Pressure improvement
T=100°C - Conventional - WITHOUT (1000 Bar)
PC GF FR
MELT TEMPERATURE (°C) DRYING TEMPERATURE (°C)305
Pressure (Bar)
180°C 328,3% 172,4% 123,0% 180°C - 82,8% - 79,5%
T=180°C - RocTool - WITH (1000 Bar)
160°C
140°C 98,4% 39,9% -56,9% -29,3% -23,3%
205,3% 105,2% 76,1% 160°C -69,0% -66,5%
15
FORM
FOR-TEC-101 Rev.: B
Page 1 of 3
FLOW AND PRESSURE STUDY REPORT- SPIRAL MOLD
ROCTOOL TECHNOLOGY IMPROVEMENT VERSUS CONVENTIONAL TECHNOLOGY
TRADE NAME GRADE D551
PICTURES OF INJECTED SAMPLES
TRIAL # HDP-17-022 MOLD Spiral 1 mm
MATERIAL
FAMILY
110
12/10/2017DATE
SUPPLIER
100,00% 64,65% 49,36% 29,28% 28,42% 27,57%
Sensor 1
Sensor 2
Sensor 1
Sensor 2
Sensor 1 Sensor 2 Sensor 1 Sensor 2 Sensor 1 Sensor 2 Sensor 1 Sensor 2 Sensor 1 Sensor 2 Sensor 1 Sensor 2
444,33 233,83 924,83 620,67 1350 967 470,83 421,83 956 840,17 1398,7 1202
-49,0% -44,9%
- 69,1%180°C 139,0% 100,5% 88,9% 180°C
47,6%
1500
ROCTOOL TECHNOLOGY (180°C)CONVENTIONAL TECHNOLOGY (100°C)
IMM PRESSURE DROP AT ISO FLOW LENGTH
160°C
Mold Pressure Avg
12,12%
_
PRESSURE DROP BETWEEN THE TWO PRESSURE SENSORS
-58,3%
20
ROCTOOL TECHNOLOGY IMPROVEMENT VERSUS CONVENTIONAL TECHNOLOGY
15Pressure (Bar)
FLOW LENGTH MEASUREMENT AT DIFFERENT IMM PRESSURE
47,37% 32,89% 28,37% 10,41%
HDP-17-022 MOLD Spiral 1.5 mm
SUPPLIER
Flow length improvement IMM Pressure improvement
25
-15,4%
500 1000
TRIAL #
Flow Length (cm)1500
FORM
T=180°C - RocTool - WITH (1000 Bar)
MATERIAL
FAMILY PC GF FR Sabic
TRADE NAME GRADE D551
FOR-TEC-101 Rev.: B
Page 2 of 3
FLOW AND PRESSURE STUDY REPORT- SPIRAL MOLD
DATE 12/10/2017
MELT TEMPERATURE (°C) 305 DRYING TEMPERATURE (°C) 110
PICTURES OF INJECTED SAMPLES
T=100°C - Conventional - WITHOUT (1000 Bar)
14,06%Pressure Drop (%)
Sensors
Pressure (Bar) 500 1000 1500 500 1000
13,3% 140°C -23,3% -16,3%
43,5% 160°C
140°C 29,9% 14,2%
65,8%
- 69,4%
Sensor 1
Sensor 2
Sensor 1
Sensor 2
Flow Length improvement vs Injection Pressure in function of Mold Temperature/Mold Thickness
Results Evaluations
The graph above shows a flow length for the two thicknesses
at two temperature (100°C and 180°C). By comparing these
curves, a significant reduction in thickness can be observed.
With Roctool technology, we are able to achieve an superior
flow length at 1 mm compare to 1.5 mm in conventional
technology.
Also, the following diagram shows the pressure drop
measured between the two sensors for the two thicknesses at
1000 bars of injection pressure. The reduction of pressure
drop in the cavity is important up to 175%.
GLOBAL COMMENTS & RECOMMENDATIONS
temperature is 180°C regarding to the trials performed with this material. We obtain the longest flow with an important
reduction of the pressure drop compared to the conventional mold temperature.
Also, we demonstrated that we could reduce the thickness of injected part from 1.5 mm to 1 mm.
Note : All the injection trials and the pressure measurements were carried out according to the protocol defined by RocTool (injection process, 2 heating sides,
cold sprue, mold design).
All pressure data are measured using eDart system (RJG).
HDP-17-022 MOLD Spiral
FORM
FOR-TEC-101
MATERIAL
FAMILY PC GF FR SUPPLIER Sabic
TRADE NAME GRADE D551
Rev.: B
Page 3 of 3
Pressure Drop between the 2 Sensors vs Mold Thickness at Injection
Pressure = 1000 Bars
FLOW AND PRESSURE STUDY REPORT- SPIRAL MOLD
DATE 12/10/2017 TRIAL #
MELT TEMPERATURE (°C) 305 DRYING TEMPERATURE (°C) 110

thermocomp D551

  • 1.
    FULL HD PLASTIC™ REPORT
  • 2.
    ΔL Δa Δ Ratereplication from the mold surface (%) Rev.: A GLOSS RESULTS (ISO 2813 Standard) T=90°C - Conventional - WITHOUT 40,3 94,9T=140°C - Roctool - WITH TRADE NAME 0,53 17/01/2018 TRIAL # HDP-17-022 MOLD HD PLAQUE MATERIAL FAMILY PC GF50 FORM FOR-TEC-111 Page 1 of 3 QUALITY SURFACE CHARACTERIZATION REPORT LNP™ THERMOCOMP™ COMPOUND GRADE D551 DATE DELTACOLOR SCALE L* ( Lightness) MEASUREMENTS PROCESS TECHNOLOGY 0,03 T=140°C - Roctool - WITH SUPPLIER SABIC 0,57 ΔE COLOR DIFFERENCE LAB - COLOR DEPHT RESULTS (DIN 5033 Standard) 0,2 T=90°C - Conventional - WITHOUT 26,83 -0,21 -0,87 27,36 a* -0,18 b* -0,67 Note: L* = 0 yields black and L* = 100 indicates diffuse white. a*: negative values indicate green while positive values indicate red. b*: negative values indicate blue and positive values indicate yellow. ΔE> , usual olor tolera e. Roughness profile - Conventional VS Roctool Technology T=140°C - Roctool - WITHT=90°C - Conventional - WITHOUT PICTURES OF INJECTED SAMPLES 3D TEXTURATION RESULTS T=90°C - Conventional - WITHOUT T=140°C - Roctool - WITH Conventional (µm3 ) Roctool technology (µm3 ) Improvement (%)Roughness parameters 14802 20307 59% 81% 37% Volume cavity (µm3 )
  • 3.
    Note: In conventionalmolding, the measurements of the VDI roughness are not mentionned as the presence of glass fibers on the surface disturb the measurement impacting the Ra value. VDI 18 (Ra=±0.80 µm) VDI 22 (Ra=±1.26 µm) VDI 27 (Ra=±2.20 µm) Roctool technology 140°C 0,75 0,89 1,11 1,73 0,96 1,45 1,03 1,56 2,27 Ra (µm) EDM Ra (µm) LASER Ra (µm) CHEMICAL COMMENTS Rz (µm) 6,4 0,72 -89% Roughness parameters Quality surface characterization: 1) Visible improvements using Roctool technology are observed: weld line and sink marks are removed. Glass fibers and defects are removed from the surface. 2) Significant improvement on the gloss value up to 135%. However, we measured an impact of the mold temperature on the color perception and Roctool technology allows a darker color with a perfect surface finish compared to conventional process. 3) The different textured areas hightlight the positive impact on the replication using Roctool technology. Also, the different roughnesses are well felt when touched. The roughness measurement carried out using optical rugosimeter confirms the above with repliction rate of up to 81% : an improvement of 37% with Roctool compared to conventional technology (CIM). Also, the Rz value has been carried out and shows the positive impact of Roctool with an important reduction of the roughness on high gloss surface due to the elimination of glass fibers at the surface. Rev.: A Page 2 of 3 QUALITY SURFACE CHARACTERIZATION REPORT FORM FOR-TEC-111 Conventional (90°C) Roctool technology (140°C) Improvement (%) TEXTURE RESULTS - Rz (Mean roughness depth) T=90°C - Conventional - WITHOUT T=140°C - Roctool - WITH TEXTURE RESULTS - Ra (Amplitude roughness parameter)
  • 4.
    MEASUREMENT AREAS 1) Thehigh gloss area framed in blue is the measurement area for the gloss, color and specific roughness Rz* . 2) The red rectangle define the nano-replication area. 3) The green box correspond to the multi-textured (VDI) area were the roughness is measured. *Rz: Maximal amplitude roughness mesured for filled materials ROUGHNESS MEASUREMENT PRINCIPLE Optical rugosimeter is a measuring instrument used to measure a surface's profile, in order to quantify its roughness. In the context of HD Plastics™, two information are carried out using Alicona equipment according to the standard ISO 4287: - Replication rate : volume of the specific texture defined versus the one textured on the mold surface quavity - The surface roughness parameters : Arithmetical mean deviation (Ra) which evaluate the roughness amplitude on a profile and Mean roughness depth (Rz) which measure the maximal amplitude roughness average of the profile. GLOSS PRINCIPLE FORM FOR-TEC-111 Rev.: A Page 3 of 3 QUALITY SURFACE CHARACTERIZATION REPORT ANNEXES LAB COLOR PRINCIPLE The Lab color space describes all perceivable colors in the three di e sio s L for light ess a d a a d for the olor oppo e ts gree –red a d lue– ello . In the context of HD Plastics™, a spectrophotometer is used to carried out the LAB alue : spe tro-guide / gloss BYK . HD Plasti s™ is following the DIN 5033 Standard. The graph shows the LAB color scale. The lightness, L*, represents the darkest black at L* = 0, and the brightest white at L* = 100. The a* and b* value represent the color channels. a*: negative values indicate green while positive values indicate red. b*: negative values indicate blue and positive values indicate yellow Gloss is an optical property which indicates how well a surface reflects light in a specular direction. It is one of important parameters that are used to describe the visual appearance of an object. The factors that affect gloss are the refractive index of the material, the angle of incident light and the surface topography. I the o te t of HD Plasti s™, a glossmeter is used to carried out the gloss value with a incident angle of 60° : spectro-guide 45/0 gloss (BYK). HD Plasti s™ is follo i g the ISO 8 Sta dard. The graph shows the gloss scale using glossmeter following 60° angle in the gloss unit. Low Gloss corresponds to a textured surface, Semi Gloss and High Gloss to high polished surface. White L* = 100 Black L* = 0
  • 5.
    Sensor 1 Sensor2 Sensor 1 Sensor 2 Sensor 1 Sensor 2 Sensor 1 Sensor 2 Sensor 1 Sensor 2 Sensor 1 Sensor 2 243,5 0 754,33 266,67 1169,7 592,33 456 322,5 914,33 654,5 1336 967,7 Sensors Mold Pressure Avg Pressure Drop (%) PRESSURE DROP BETWEEN THE TWO PRESSURE SENSORS CONVENTIONAL TECHNOLOGY (100°C) ROCTOOL TECHNOLOGY (180°C) Pressure (Bar) 500 1000 1500 500 1000 1500 -62,8% - 78,5% FLOW LENGTH MEASUREMENT AT DIFFERENT IMM PRESSURE IMM PRESSURE DROP AT ISO FLOW LENGTH Sabic 32,8% 140°C 500 1000 1500 Flow Length (cm) 5 10 Flow length improvement IMM Pressure improvement T=100°C - Conventional - WITHOUT (1000 Bar) PC GF FR MELT TEMPERATURE (°C) DRYING TEMPERATURE (°C)305 Pressure (Bar) 180°C 328,3% 172,4% 123,0% 180°C - 82,8% - 79,5% T=180°C - RocTool - WITH (1000 Bar) 160°C 140°C 98,4% 39,9% -56,9% -29,3% -23,3% 205,3% 105,2% 76,1% 160°C -69,0% -66,5% 15 FORM FOR-TEC-101 Rev.: B Page 1 of 3 FLOW AND PRESSURE STUDY REPORT- SPIRAL MOLD ROCTOOL TECHNOLOGY IMPROVEMENT VERSUS CONVENTIONAL TECHNOLOGY TRADE NAME GRADE D551 PICTURES OF INJECTED SAMPLES TRIAL # HDP-17-022 MOLD Spiral 1 mm MATERIAL FAMILY 110 12/10/2017DATE SUPPLIER 100,00% 64,65% 49,36% 29,28% 28,42% 27,57% Sensor 1 Sensor 2 Sensor 1 Sensor 2
  • 6.
    Sensor 1 Sensor2 Sensor 1 Sensor 2 Sensor 1 Sensor 2 Sensor 1 Sensor 2 Sensor 1 Sensor 2 Sensor 1 Sensor 2 444,33 233,83 924,83 620,67 1350 967 470,83 421,83 956 840,17 1398,7 1202 -49,0% -44,9% - 69,1%180°C 139,0% 100,5% 88,9% 180°C 47,6% 1500 ROCTOOL TECHNOLOGY (180°C)CONVENTIONAL TECHNOLOGY (100°C) IMM PRESSURE DROP AT ISO FLOW LENGTH 160°C Mold Pressure Avg 12,12% _ PRESSURE DROP BETWEEN THE TWO PRESSURE SENSORS -58,3% 20 ROCTOOL TECHNOLOGY IMPROVEMENT VERSUS CONVENTIONAL TECHNOLOGY 15Pressure (Bar) FLOW LENGTH MEASUREMENT AT DIFFERENT IMM PRESSURE 47,37% 32,89% 28,37% 10,41% HDP-17-022 MOLD Spiral 1.5 mm SUPPLIER Flow length improvement IMM Pressure improvement 25 -15,4% 500 1000 TRIAL # Flow Length (cm)1500 FORM T=180°C - RocTool - WITH (1000 Bar) MATERIAL FAMILY PC GF FR Sabic TRADE NAME GRADE D551 FOR-TEC-101 Rev.: B Page 2 of 3 FLOW AND PRESSURE STUDY REPORT- SPIRAL MOLD DATE 12/10/2017 MELT TEMPERATURE (°C) 305 DRYING TEMPERATURE (°C) 110 PICTURES OF INJECTED SAMPLES T=100°C - Conventional - WITHOUT (1000 Bar) 14,06%Pressure Drop (%) Sensors Pressure (Bar) 500 1000 1500 500 1000 13,3% 140°C -23,3% -16,3% 43,5% 160°C 140°C 29,9% 14,2% 65,8% - 69,4% Sensor 1 Sensor 2 Sensor 1 Sensor 2
  • 7.
    Flow Length improvementvs Injection Pressure in function of Mold Temperature/Mold Thickness Results Evaluations The graph above shows a flow length for the two thicknesses at two temperature (100°C and 180°C). By comparing these curves, a significant reduction in thickness can be observed. With Roctool technology, we are able to achieve an superior flow length at 1 mm compare to 1.5 mm in conventional technology. Also, the following diagram shows the pressure drop measured between the two sensors for the two thicknesses at 1000 bars of injection pressure. The reduction of pressure drop in the cavity is important up to 175%. GLOBAL COMMENTS & RECOMMENDATIONS temperature is 180°C regarding to the trials performed with this material. We obtain the longest flow with an important reduction of the pressure drop compared to the conventional mold temperature. Also, we demonstrated that we could reduce the thickness of injected part from 1.5 mm to 1 mm. Note : All the injection trials and the pressure measurements were carried out according to the protocol defined by RocTool (injection process, 2 heating sides, cold sprue, mold design). All pressure data are measured using eDart system (RJG). HDP-17-022 MOLD Spiral FORM FOR-TEC-101 MATERIAL FAMILY PC GF FR SUPPLIER Sabic TRADE NAME GRADE D551 Rev.: B Page 3 of 3 Pressure Drop between the 2 Sensors vs Mold Thickness at Injection Pressure = 1000 Bars FLOW AND PRESSURE STUDY REPORT- SPIRAL MOLD DATE 12/10/2017 TRIAL # MELT TEMPERATURE (°C) 305 DRYING TEMPERATURE (°C) 110