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Company ConfidentialCompany Confidential
World Precision Instruments, LLC (WPI)
LWCC
Liquid Waveguide Capillary Cells
Company Confidential
Liquid Waveguide Capillary Cell
The LWCC System(Longpass Flow Cells) measure liquids
• In a continuous flow, or
• Using discrete samples
The Longpass Flow Cells connects directly to a pump, a chromatography column,
A WPI Sample Injector Kit or the LWCC Injection System.
Company ConfidentialCompany Confidential
LWCC Overview
• Optical sample flow cells that combine an increased optical pathlength (50-500 cm)
with small sample volumes (125-1250 µL).
• Connects with 600um core optical fibers to fiber optic spectrometers and light
sources via SMA terminations
• Efficient measurement of low-volume or low-concentration (ppb-ppt) aqueous
samples.
• Functions with most liquids(with the exception of perfluorinated solvents) having a
refractive index ≥ 1.30.
• Absorbance measurements can be performed in the UV, VIS, and NIR ranges to
detect low sample concentrations in a lab or process environment.
Company ConfidentialCompany Confidential
Longpass Flow Cell Properties
• Similar to optical fibers, light is confined with the (liquid) core of an LWCC by
total internal reflection at the core/wall interface.
• Made from fused silica tubing with an outer coating of a low refractive index
polymer.
Company ConfidentialCompany Confidential
Pressure and Flow Rate
• Flow is proportional to pressure and to the fourth power of the diameter of
the fluid capillary, as well as reciprocal to the length of the capillary and
fluid viscosity.
• 1 m of 55um ID waveguide requires ~1.5 PSI for water flow of 1 mL/min
• LWCC has been operated at 100 to 200PSI without observed malfunction
• Maximum hydrostatic pressure the Longpass Flow Cell can withstand has
not been established
Company Confidential
Efficiency Curves for LWCC
Company Confidential
Light Throughput of Fiber Optic Cables
Company Confidential
Microliter Sample Volumes – exceptional sensitivity
Company ConfidentialCompany Confidential
Nutrient Analysis:
• Applications in both Oceanology and Limnology
o Ammonia Bromate
o Chromate Chromium (IV)
o Iron (II) Magnesium
o Nitrate Nitrite
o Phosphate Silicate
• Waste Water Analysis
• Drinking Water Analysis
• Colored Dissolved Organic Matter (CDOM)
• Atmospheric Aerosols
• Semiconductor Industry
o Heavy Metal Content in Doping Tanks
• Pollution / Environmental Contaminants
o Heavy Metal Contamination
o Phenol Detection
Selected Applications
Company ConfidentialCompany Confidential
LWCC Longpass Flow Cell Accessories
• Mini Peristaltic Pump Part No. MINISTAR
• Sample Injector Assembly Part No. 58006
• Spare set of external syring adapters Part No. 58450
• LWCC Injection System (optional) Part No. 89372
• Waveguide Cleaning Kit Part No. 501609
Company ConfidentialCompany Confidential
MicroLWCC, LWCC-M Series
Low volume flow cell for FIA, HPLC and Process Analysis
Also connects directly to a pump, a chromatography column, A WPI Sample Injector Kit or the
LWCC Injection System.
Company ConfidentialCompany Confidential
Measure Low volume samples with UV/VIS absorbance spectroscopy
Company ConfidentialCompany Confidential
ISO9001 Certified
Quality Processes WPI has instituted:
• Implemented and documented Quality Management System
• Management process in place for the review of quality performance that identifies areas of
improvement
• Formal procedure that identifies corrective and preventative actions (CAPA)
• On-going employee training on quality assurance
• Quality manual with documented procedures for ISO9001:2008.
• Documented complaint handling procedure
Company Confidential
Questions?
Tiana L. Ruchti
OEM Sales Manger
tianar@wpiinc.com
941.320.1972

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Small Volume -Long pathlength Flow Cells for FIA, HPLC and more

  • 1. Company ConfidentialCompany Confidential World Precision Instruments, LLC (WPI) LWCC Liquid Waveguide Capillary Cells
  • 2. Company Confidential Liquid Waveguide Capillary Cell The LWCC System(Longpass Flow Cells) measure liquids • In a continuous flow, or • Using discrete samples The Longpass Flow Cells connects directly to a pump, a chromatography column, A WPI Sample Injector Kit or the LWCC Injection System.
  • 3. Company ConfidentialCompany Confidential LWCC Overview • Optical sample flow cells that combine an increased optical pathlength (50-500 cm) with small sample volumes (125-1250 µL). • Connects with 600um core optical fibers to fiber optic spectrometers and light sources via SMA terminations • Efficient measurement of low-volume or low-concentration (ppb-ppt) aqueous samples. • Functions with most liquids(with the exception of perfluorinated solvents) having a refractive index ≥ 1.30. • Absorbance measurements can be performed in the UV, VIS, and NIR ranges to detect low sample concentrations in a lab or process environment.
  • 4. Company ConfidentialCompany Confidential Longpass Flow Cell Properties • Similar to optical fibers, light is confined with the (liquid) core of an LWCC by total internal reflection at the core/wall interface. • Made from fused silica tubing with an outer coating of a low refractive index polymer.
  • 5. Company ConfidentialCompany Confidential Pressure and Flow Rate • Flow is proportional to pressure and to the fourth power of the diameter of the fluid capillary, as well as reciprocal to the length of the capillary and fluid viscosity. • 1 m of 55um ID waveguide requires ~1.5 PSI for water flow of 1 mL/min • LWCC has been operated at 100 to 200PSI without observed malfunction • Maximum hydrostatic pressure the Longpass Flow Cell can withstand has not been established
  • 8. Company Confidential Microliter Sample Volumes – exceptional sensitivity
  • 9. Company ConfidentialCompany Confidential Nutrient Analysis: • Applications in both Oceanology and Limnology o Ammonia Bromate o Chromate Chromium (IV) o Iron (II) Magnesium o Nitrate Nitrite o Phosphate Silicate • Waste Water Analysis • Drinking Water Analysis • Colored Dissolved Organic Matter (CDOM) • Atmospheric Aerosols • Semiconductor Industry o Heavy Metal Content in Doping Tanks • Pollution / Environmental Contaminants o Heavy Metal Contamination o Phenol Detection Selected Applications
  • 10. Company ConfidentialCompany Confidential LWCC Longpass Flow Cell Accessories • Mini Peristaltic Pump Part No. MINISTAR • Sample Injector Assembly Part No. 58006 • Spare set of external syring adapters Part No. 58450 • LWCC Injection System (optional) Part No. 89372 • Waveguide Cleaning Kit Part No. 501609
  • 11. Company ConfidentialCompany Confidential MicroLWCC, LWCC-M Series Low volume flow cell for FIA, HPLC and Process Analysis Also connects directly to a pump, a chromatography column, A WPI Sample Injector Kit or the LWCC Injection System.
  • 12. Company ConfidentialCompany Confidential Measure Low volume samples with UV/VIS absorbance spectroscopy
  • 13. Company ConfidentialCompany Confidential ISO9001 Certified Quality Processes WPI has instituted: • Implemented and documented Quality Management System • Management process in place for the review of quality performance that identifies areas of improvement • Formal procedure that identifies corrective and preventative actions (CAPA) • On-going employee training on quality assurance • Quality manual with documented procedures for ISO9001:2008. • Documented complaint handling procedure
  • 14. Company Confidential Questions? Tiana L. Ruchti OEM Sales Manger tianar@wpiinc.com 941.320.1972

Editor's Notes

  1. Showing best light transmission band, as path gets longer it cuts out light. The decrease is the result of the absorbance by water in the sample