This document provides information about the Pharmaceutical Analysis course BP102T. It includes the teaching and evaluation scheme, course objectives and outcomes, syllabus overview divided into 5 units, and a sample of previous question papers. The course involves 3 hours of theory, 4 hours of practical and 1 hour of tutorial per week. It is evaluated based on an internal assessment of 25% and external end semester exam of 75% for theory, and internal of 15% and external of 35% for practical. The course aims to explain various analytical techniques like volumetric, electrochemical and gravimetric analysis methods to estimate compounds in pharmacopeia. It covers topics like acid-base titrations, precipitation titrations, redox titr
This power point presentation can be useful to student to know content of syllabus of Subject Pharmaceutical analysis-I included in B-pharmacy I- semester.
Development and Validation of the HPLC Method for the Analysis of Ametridio...iosrphr_editor
The IOSR Journal of Pharmacy (IOSRPHR) is an open access online & offline peer reviewed international journal, which publishes innovative research papers, reviews, mini-reviews, short communications and notes dealing with Pharmaceutical Sciences( Pharmaceutical Technology, Pharmaceutics, Biopharmaceutics, Pharmacokinetics, Pharmaceutical/Medicinal Chemistry, Computational Chemistry and Molecular Drug Design, Pharmacognosy & Phytochemistry, Pharmacology, Pharmaceutical Analysis, Pharmacy Practice, Clinical and Hospital Pharmacy, Cell Biology, Genomics and Proteomics, Pharmacogenomics, Bioinformatics and Biotechnology of Pharmaceutical Interest........more details on Aim & Scope).
Pharmaceutical analysis Definition and scope Different techniques of analysis Methods of expressing concentration Primary and secondary standards. Preparation and standardization of various molar and normal solutions Oxalic acid, sodium hydroxide, hydrochloric acid, sodium thiosulphate, sulphuric acid, potassium permanganate and ceric ammonium sulphate Errors :Sources of errors, types of errors, methods of minimizing errors, accuracy, precision and significant figures
INTRODUCTION TO PHARMACEUTICAL CHEMISTRY AND LIMIT TESTSUJATA WANKHEDE
INTRODUCTION TO PHARMACEUTICAL CHEMISTRY, INTRODUCTION TO LIMIT TESTS, LIMIT TEST OF IRON, CHLORIDE, SULPHATE, ARSENIC AND THERE DIAGRAMS WITHTHE PRINCIPAL AND PROCEDURE OF ALL THE LIMIT TEST WITH THEIR RESULTS
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This will be used as part of your Personal Professional Portfolio once graded.
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Prepare a presentation or a paper using research, basic comparative analysis, data organization and application of economic information. You will make an informed assessment of an economic climate outside of the United States to accomplish an entertainment industry objective.
This power point presentation can be useful to student to know content of syllabus of Subject Pharmaceutical analysis-I included in B-pharmacy I- semester.
Development and Validation of the HPLC Method for the Analysis of Ametridio...iosrphr_editor
The IOSR Journal of Pharmacy (IOSRPHR) is an open access online & offline peer reviewed international journal, which publishes innovative research papers, reviews, mini-reviews, short communications and notes dealing with Pharmaceutical Sciences( Pharmaceutical Technology, Pharmaceutics, Biopharmaceutics, Pharmacokinetics, Pharmaceutical/Medicinal Chemistry, Computational Chemistry and Molecular Drug Design, Pharmacognosy & Phytochemistry, Pharmacology, Pharmaceutical Analysis, Pharmacy Practice, Clinical and Hospital Pharmacy, Cell Biology, Genomics and Proteomics, Pharmacogenomics, Bioinformatics and Biotechnology of Pharmaceutical Interest........more details on Aim & Scope).
Pharmaceutical analysis Definition and scope Different techniques of analysis Methods of expressing concentration Primary and secondary standards. Preparation and standardization of various molar and normal solutions Oxalic acid, sodium hydroxide, hydrochloric acid, sodium thiosulphate, sulphuric acid, potassium permanganate and ceric ammonium sulphate Errors :Sources of errors, types of errors, methods of minimizing errors, accuracy, precision and significant figures
INTRODUCTION TO PHARMACEUTICAL CHEMISTRY AND LIMIT TESTSUJATA WANKHEDE
INTRODUCTION TO PHARMACEUTICAL CHEMISTRY, INTRODUCTION TO LIMIT TESTS, LIMIT TEST OF IRON, CHLORIDE, SULPHATE, ARSENIC AND THERE DIAGRAMS WITHTHE PRINCIPAL AND PROCEDURE OF ALL THE LIMIT TEST WITH THEIR RESULTS
Macroeconomics- Movie Location
This will be used as part of your Personal Professional Portfolio once graded.
Objective:
Prepare a presentation or a paper using research, basic comparative analysis, data organization and application of economic information. You will make an informed assessment of an economic climate outside of the United States to accomplish an entertainment industry objective.
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3. Teaching & Evaluation Scheme
Course
Code
Course Name Lectures Assigned
Theory Practical Tutorial Total
BP102T Pharmacy 03 Hrs. per
week
04 Hrs. per
week
01 Hrs. per
week
04 Hrs. per
week
Course
Code
Course
Name
Evaluation Scheme
BP102T Pharmacy Theory Practical Total
Credit
4
Internal
25
External
75
Total
100
Internal
15
External
35
Total
50
4. Evaluation Guidelines
End Semester Examination [ 75 Marks]:
Paper pattern and marks distribution for End Semester Exam: As per
university guideline.
Internal Examination [ 25 Marks]:
Sessional exam shall be conducted for 30 marks for theory and shall be
computed for 15 marks. Similarly Sessional exam for practical shall
be conducted for 40 marks and shall be computed for 10 marks.
Sr. no Question type Marks
1 Objective Types Questions (Answer 5 out of 7) 5x3=15
2 Long Answers (Answer 2 out of 4) 2x10=20
3 Short Answers (Answer 8 out of 10) 8x5=40
Total = 75M
5.
6. Course Outcomes (COs):
After successful completion of course student will able to
CO1
After successful completion of course student will able to Explain volumetric
analysis method for estimation of selected compound officially
pharmacopeia.
CO2
After successful completion of course student will able to Explain
electrochemical analysis method for estimation of selected compound
officially pharmacopeia.
CO3
After successful completion of course student will able to Explain
gravimetric analysis method for estimation of selected compound officially
pharmacopeia.
CO4
After successful completion of course student will able to Explain various
method of expressing conc. & uses of primary and secondary std. for
chemical analysis.
CO5
After successful completion of course student will able to Explain error in
measurement.
7. UNIT-I
Pharmaceutical analysis-
Definition and scope
Different techniques of analysis
Methods of expressing concentration
Primary and secondary standards.
Preparation and standardization of various molar and normal
solutionsOxalic acid, sodium hydroxide, hydrochloric acid, sodium
thiosulphate, sulphuric acid, potassium permanganate and ceric
ammonium sulphate
Errors :Sources of errors, types of errors, methods of minimizing errors,
accuracy, precision and significant figures
8. UNIT-II
Acid base titration:
Theories of acid base indicators, classification of acid base titrations
and theory involved in titrations of strong, weak, and very weak
acids and bases, neutralization curves.
Non aqueous titration:
Solvents, acidimetry and alkalimetry titration and estimation of
Sodium benzoate and Ephedrine HCl
9. UNIT-III
Precipitation titrations:
Mohr’s method, Volhard’s, Modified Volhard’s, Fajans method,
estimation of sodium chloride.
Complexometric titration:
Classification, metal ion indicators, maskingand demasking reagents,
estimation of Magnesium sulphate, and calcium gluconate.
Gravimetry:
Principle and steps involved in gravimetric analysis. Purity of the
precipitate: co-precipitation and post precipitation, Estimation of barium
sulphate.
10. UNIT-IV
Redox titrations
(a) Concepts of oxidation and reduction
(b) Types of redox titrations (Principles and applications)
Cerimetry, Iodimetry, Iodometry, Bromatometry, Dichrometry,Titration
with potassium iodate
11. UNIT-V
Electrochemical methods of analysis
Conductometry-
Introduction, Conductivity cell, Conductometric titrations, applications.
Potentiometry –
Electrochemical cell, construction and working of reference (Standard
hydrogen, silver chloride electrode and calomel electrode) and indicator
electrodes (metal electrodes and glass electrode), methods to determine end
pointt of potentiometric titration and applications.
Polarography –
Principle, Ilkovic equation, construction and working of dropping mercury
electrode and rotating platinum electrode, applications
Refractometry –
Introduction, refractive index, specific and molar refraction, measurement
of RI, Abbe’s refractometer and applications
12. Previous Question Paper
Q1) Answer the following [10 × 2 = 20]
a) How will you calculate equivalent weight of acid and base? Explain
with example.
b) Starch indicator give blue color with iodine, justify it.
c) Define the term normality and molality
d) Explain accuracy and precision.
e) Give the preparation of 0. 1N potassium permanganate with reaction.
f) Give applications of polarography.
g) Define oxidation and reduction with examples.
h) How will you standardize 0.05 M disodium EDTA solution?
i) What is half wave potential? j) How will you prepare and standardize
0.1 N Silver nitrate solution?
13. Previous Question Paper
Q2) Answer of the following (any two) [2 × 10 = 20]
a) What is volumetric analysis. Classify them with example. Write
principle, reaction of assay for Boric acid and Aspirin.
b) Explain methods to determine end point of potentiometric titrations
and its application.
c) What is complex metric titration? Classify them with example. Write
detailed about types of complexometric titrations.
14. Previous Question Paper
Q3) Answer the following (any seven) : [7 × 5 = 35]
a) Explain assay sodium benzoate by non aqueous titration.
b) Write a note on accuracy and precision.
c) Give an account on solvents used in non aqueous titration.
d) Write about limit test of lead.
e) Write principle and application of Diazotization titrations.
f) Explain construction and working of dropping mercury electrode.
g) Write a note on K Fajan’s method?
h) Explain principle, reaction of calcium gluconate injection.
i) Explain mechanism of co precipitatio