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RESEARCH POSTER PRESENTATION DESIGN © 2012
www.PosterPresentations.com
 Nickel-base superalloys are widely used in
aerospace applications.
 They possess excellent mechanical properties
and corrosion resistance in high temperature
gaseous environment.
BACKGROUND
OBJECTIVES
RESULTS & DISCUSSIONS
CONCLUSIONS
 Chromium is essential in the filler alloy for
TLP bonding of Nickel-base aerospace
superalloy IN738 to aid corrosion resistance.
 TLP bonding produces deleterious centerline
eutectic which reduces the corrosion
resistance of the joint .
 A new method of powder mixture filler
produces eutectic-free joint at shorter time
with nearly uniform chromium distribution
which translates to better corrosion
resistance in TLP bonded joints.
 Nickel-base superalloys are highly
susceptibility to cracking during
conventional welding processes.
 Transient Liquid Phase bonding (TLPB) has
evolved as a viable joining process for this
difficult to weld alloys.
 Limited information on the corrosion
performance when joined by TLPB process.
Department of Mechanical and Manufacturing Engineering University of Manitoba, Winnipeg, MB R3T 5V6
O. Adebajo and O.A. Ojo
Effect of Transient Liquid Phase Bonding on the Corrosion Performance of Nickel-base
Aerospace Superalloy
The objective of the current work is to evaluate
the effect of TLP bonding on corrosion
performance of nickel-base aerospace
superalloy.
Microstructure of Brazed Joint with Eutectic
 Eutectic width increases as gap width increases.
Effect of Brazing Parameters on Eutectic width
0
200
400
600
800
1000
1200
200 400 600 800 1000 1200 1400 1600
Gapwidth(µm)
Eutectic width (µm)
Fig. 3: Effect of Gap width in size of Eutectic
50
100
150
200
250
300
350
400
450
50 100 150 200 250 300 350 400
EutecticWidth(µm)
Square Root of Time (Sec 1/2)
Fig. 4: Variation of Eutectic Width with Root of Holding Time
RESULTS & DISCUSSIONS
 Centreline eutectic consists of Nickel and
Chromium rich borides.
 Corrosion resistance increases as eutectic
width decreases.
Microstructure of Joint with No Eutectic
RESULTS & DISCUSSIONS
 Eutectic width decreases as hold time increases.
Brazed NE
BM
Brazed WE
HNO3
80oC
Financial support from NSERC is gratefully
acknowledged
ACKNOWLEDGEMENT
Fig. 1: Jet turbine engine [1] M. France, FRANCE-METALLURGIE, 2015 (2015)
MATERIALS AND METHODS
 Nickel-base single crystal superalloy IN738
was used as the base material.
 Ni-base Chromium bearing and Chromium
free inter-fillers were used.
 Bonding was done in a vacuum furnace for
different gaps sizes, bonding temperatures
and holding time.
 Test coupons were mounted on bakelite and
surface prepared according to ASTM G5 for
electrochemical polarization.
Substrate Substrate
Fig. 2: Joint microstructure with Chromium distribution across joint
Uneven Cr peaks
Joint
Electrochemical Polarization
Fig. 5: Effect of Chromium in the filler
Chromium Free Filler
Chromium Bearing Filler
HNO3
Fig. 6: Variation of Eutectic Width with Corrosion Resistance
400µm<EW<1000µm
EW<50µm
200EW>400µm
50µm>EW<200µm
EW
CR
HNO3
25oC
It is possible to produce eutectic free joint by
a new method using powder mixture as filler
Substrate SubstrateJoint
Cr Distribution NE
Fairly uniform Cr peaks
Fig. 7: Joint microstructure with Chromium distribution across joint
Brazed NE
BM
BrazedWE
HNO3
25oC
Brazed NE
BM
Brazed WE
H2SO4
25oC
Fig. 8: Brazed with eutectic and with no eutectic in HNO3 and H2SO4
 No eutectic joint shows comparable
corrosion resistance with the base material
in both HNO3 and H2SO4.
Electrochemical Polarization
Brazed Joint with Eutectic vs without Eutectic
 As temperature increases from 25-80oC,the
corrosion resistance generally reduces but
that of the joint with no eutectic remains
comparable to that of the base material.
Fig. 6: Effect of Temperature on Corrosion Resistance of Brazed joints
Cr 20 wt %
Cr 16 wt %
 Chromium bearing filler shows better
corrosion resistance than Chromium free
filler
Electrochemical Polarization Electrochemical Polarization

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MMC 2015 Poster presentation Olaniyi

  • 1. RESEARCH POSTER PRESENTATION DESIGN © 2012 www.PosterPresentations.com  Nickel-base superalloys are widely used in aerospace applications.  They possess excellent mechanical properties and corrosion resistance in high temperature gaseous environment. BACKGROUND OBJECTIVES RESULTS & DISCUSSIONS CONCLUSIONS  Chromium is essential in the filler alloy for TLP bonding of Nickel-base aerospace superalloy IN738 to aid corrosion resistance.  TLP bonding produces deleterious centerline eutectic which reduces the corrosion resistance of the joint .  A new method of powder mixture filler produces eutectic-free joint at shorter time with nearly uniform chromium distribution which translates to better corrosion resistance in TLP bonded joints.  Nickel-base superalloys are highly susceptibility to cracking during conventional welding processes.  Transient Liquid Phase bonding (TLPB) has evolved as a viable joining process for this difficult to weld alloys.  Limited information on the corrosion performance when joined by TLPB process. Department of Mechanical and Manufacturing Engineering University of Manitoba, Winnipeg, MB R3T 5V6 O. Adebajo and O.A. Ojo Effect of Transient Liquid Phase Bonding on the Corrosion Performance of Nickel-base Aerospace Superalloy The objective of the current work is to evaluate the effect of TLP bonding on corrosion performance of nickel-base aerospace superalloy. Microstructure of Brazed Joint with Eutectic  Eutectic width increases as gap width increases. Effect of Brazing Parameters on Eutectic width 0 200 400 600 800 1000 1200 200 400 600 800 1000 1200 1400 1600 Gapwidth(µm) Eutectic width (µm) Fig. 3: Effect of Gap width in size of Eutectic 50 100 150 200 250 300 350 400 450 50 100 150 200 250 300 350 400 EutecticWidth(µm) Square Root of Time (Sec 1/2) Fig. 4: Variation of Eutectic Width with Root of Holding Time RESULTS & DISCUSSIONS  Centreline eutectic consists of Nickel and Chromium rich borides.  Corrosion resistance increases as eutectic width decreases. Microstructure of Joint with No Eutectic RESULTS & DISCUSSIONS  Eutectic width decreases as hold time increases. Brazed NE BM Brazed WE HNO3 80oC Financial support from NSERC is gratefully acknowledged ACKNOWLEDGEMENT Fig. 1: Jet turbine engine [1] M. France, FRANCE-METALLURGIE, 2015 (2015) MATERIALS AND METHODS  Nickel-base single crystal superalloy IN738 was used as the base material.  Ni-base Chromium bearing and Chromium free inter-fillers were used.  Bonding was done in a vacuum furnace for different gaps sizes, bonding temperatures and holding time.  Test coupons were mounted on bakelite and surface prepared according to ASTM G5 for electrochemical polarization. Substrate Substrate Fig. 2: Joint microstructure with Chromium distribution across joint Uneven Cr peaks Joint Electrochemical Polarization Fig. 5: Effect of Chromium in the filler Chromium Free Filler Chromium Bearing Filler HNO3 Fig. 6: Variation of Eutectic Width with Corrosion Resistance 400µm<EW<1000µm EW<50µm 200EW>400µm 50µm>EW<200µm EW CR HNO3 25oC It is possible to produce eutectic free joint by a new method using powder mixture as filler Substrate SubstrateJoint Cr Distribution NE Fairly uniform Cr peaks Fig. 7: Joint microstructure with Chromium distribution across joint Brazed NE BM BrazedWE HNO3 25oC Brazed NE BM Brazed WE H2SO4 25oC Fig. 8: Brazed with eutectic and with no eutectic in HNO3 and H2SO4  No eutectic joint shows comparable corrosion resistance with the base material in both HNO3 and H2SO4. Electrochemical Polarization Brazed Joint with Eutectic vs without Eutectic  As temperature increases from 25-80oC,the corrosion resistance generally reduces but that of the joint with no eutectic remains comparable to that of the base material. Fig. 6: Effect of Temperature on Corrosion Resistance of Brazed joints Cr 20 wt % Cr 16 wt %  Chromium bearing filler shows better corrosion resistance than Chromium free filler Electrochemical Polarization Electrochemical Polarization