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FTEC	
  422	
  Lab	
  Report	
  1	
  
	
  
Name:	
  	
  John	
  Schnettler	
  
Style	
  of	
  Brew:	
  	
  Kölsch	
  
Brew	
  Date:	
  	
  2/11/15	
  
Kegging	
  Date:	
  3/4/15	
  
Sensory	
  Evaluation	
  Date:	
  3/11/15	
  
Batch	
  Volume:	
  Target:	
  40.0	
  l	
  	
  
Original	
  Gravity:	
  Target=	
  12.140°	
  P	
  (Actual=	
  11.3°	
  P)	
  
Final	
  Gravity:	
  Target=	
  2.912°	
  P	
  (Actual=	
  2.02°	
  P)	
  
	
  
Material	
  Bill	
  
	
  
Water	
  Additives:	
  
	
  
Ingredient	
   Amount	
   Step	
   Time	
  
Calcium	
  Chloride	
   18.40	
  g	
   Mash	
  	
   60	
  minutes	
  
Lactic	
  Acid	
   13.10	
  ml	
   Mash	
   60	
  minutes	
  
	
  
Grist	
  Bill:	
  
	
  
Malt	
   Amount	
   Color	
  (European	
  Brewing	
  
Convention)	
  	
  
Breiss	
  Brewers	
  Malt	
  (2	
  
Row)	
  US	
  	
  
7.00	
  kg	
   4.0	
  EBC	
  
Munich	
  Malt	
  10L	
   0.83	
  kg	
   19.7	
  EBC	
  
White	
  Wheat	
  Malt	
   0.68	
  kg	
   4.7	
  EBC	
  
	
  
Boil	
  Ingredients:	
  
	
  
Ingredient	
   Amount	
   Time	
  
Merkur	
  (13.60%	
  alpha-­‐
acid):	
  Hop	
  addition	
  
11.0	
  g	
   60	
  minutes	
  
Sterling	
  2013	
  (6.70%	
  alpha-­‐
acid):	
  Hop	
  addition	
  
57.0	
  g	
   15	
  minutes	
  
Whirlfloc:	
  Clarification	
   1	
  Tablet	
   10	
  minutes	
  
Sterling	
  2013	
  (6.70%	
  alpha-­‐
acid):	
  Hop	
  addition	
  
39.0	
  g	
   5	
  minutes	
  
	
  
Yeast:	
  	
  German	
  Ale/Kölsch	
  (White	
  Labs	
  #WLP029)	
  
	
  
	
  
	
  
	
  
	
  
Water	
  Treatment	
  
	
  
Starting	
  Water:	
  
Fort	
  Collins	
  Water	
  analysis:	
  
	
  
1.	
  Hardness	
  =	
  100	
  ppm	
  
	
  
2.	
  Alkalinity	
  =	
  80	
  ppm	
  
	
  
3.	
  pH	
  =	
  6.9	
  
	
  
4.	
  Ca	
  =	
  17.3	
  ppm	
  
	
  
5.	
  Mg	
  =	
  1.6	
  ppm	
  
	
  
6.	
  Cl	
  =	
  2.9	
  ppm	
  
	
  
Criteria:	
  	
  Produce	
  a	
  light	
  to	
  medium	
  light	
  bodied,	
  clean,	
  crisp,	
  clear,	
  mildly	
  sweet	
  and	
  low	
  
ester	
  straw	
  to	
  gold	
  ale	
  with	
  low	
  hop	
  character.	
  	
  We	
  decided	
  as	
  a	
  class	
  to	
  increase	
  the	
  
hardness	
  of	
  the	
  beer	
  to	
  2:1	
  hardness	
  to	
  alkalinity	
  ratio	
  as	
  well	
  as	
  lower	
  the	
  mash	
  pH	
  of	
  the	
  
water	
  to	
  increase	
  wort	
  fermentability	
  by	
  providing	
  the	
  optimum	
  saccharification	
  
temperature.	
  	
  Therefore,	
  we	
  aimed	
  for	
  a	
  water	
  profile	
  with	
  a	
  calcium	
  content	
  of	
  80	
  ppm	
  
with	
  a	
  mash	
  pH	
  of	
  5.4.	
  	
  	
  
	
  
Determination:	
  	
  In	
  order	
  to	
  produce	
  the	
  desired	
  water	
  profile,	
  we	
  decided	
  as	
  a	
  class	
  to	
  
utilize	
  calcium	
  chloride	
  and	
  lactic	
  acid	
  to	
  treat	
  80.0	
  l	
  of	
  water	
  (approximately	
  1/3	
  mash	
  tun	
  
water	
  and	
  2/3	
  hot	
  liquor	
  tank	
  water).	
  	
  Calcium	
  ions	
  are	
  important	
  in	
  stabilizing	
  mash	
  alpha	
  
amylase	
  enzymes,	
  reducing	
  mash	
  pH	
  by	
  reacting	
  with	
  phosphates	
  to	
  create	
  insoluble	
  
compounds	
  releasing	
  H+	
  ions,	
  aiding	
  the	
  formation	
  of	
  hot	
  break	
  by	
  enhancing	
  protein	
  
coagulation,	
  and	
  increasing	
  clarity.	
  	
  Chloride	
  ions	
  are	
  known	
  to	
  balance	
  the	
  flavor	
  profile	
  of	
  
beer	
  and	
  also	
  influence	
  sweetness.	
  	
  Therefore,	
  we	
  calculated	
  that	
  we	
  would	
  use	
  18.40g	
  of	
  
calcium	
  chloride	
  in	
  order	
  to	
  contribute	
  these	
  benefits	
  of	
  each	
  ion	
  as	
  well	
  as	
  to	
  increase	
  
permanent	
  hardness	
  and	
  remove	
  alkaline	
  water’s	
  buffering	
  capacity.	
  	
  We	
  avoided	
  the	
  use	
  
of	
  magnesium	
  due	
  to	
  the	
  fact	
  that	
  although	
  it	
  shares	
  many	
  impacts	
  on	
  beer	
  as	
  calcium,	
  it	
  is	
  
much	
  less	
  effective	
  and	
  as	
  a	
  result	
  is	
  required	
  in	
  greater	
  amounts.	
  	
  We	
  also	
  chose	
  to	
  add	
  
permanent	
  hardness	
  in	
  the	
  form	
  of	
  chlorides	
  rather	
  than	
  sulfates	
  in	
  order	
  to	
  contribute	
  a	
  
subtle	
  sweetness	
  rather	
  than	
  enhance	
  hop	
  bitterness,	
  which	
  is	
  not	
  characteristic	
  of	
  the	
  
Kölsch	
  style.	
  	
  Using	
  18.40g	
  calcium	
  chloride	
  brought	
  us	
  to	
  our	
  desired	
  hardness	
  to	
  
alkalinity	
  ratio	
  and	
  80-­‐ppm	
  calcium	
  concentration;	
  however,	
  we	
  needed	
  to	
  further	
  reduce	
  
the	
  mash	
  pH	
  and	
  therefore	
  turned	
  to	
  lactic	
  acid.	
  	
  Our	
  classmate	
  Trent	
  calculated	
  13.10	
  ml	
  of	
  
lactic	
  acid	
  would	
  effectively	
  bring	
  our	
  mash	
  pH	
  down	
  to	
  5.4.	
  
	
  
Malt	
  Analysis	
  
	
  
Malt	
  Extract	
  Methods	
  for	
  DBFG	
  and	
  DBCG:	
  	
  First	
  we	
  tested	
  for	
  the	
  specific	
  gravity	
  (using	
  
ASBC	
  Method	
  of	
  Analysis)	
  of	
  our	
  Breiss	
  Brewer’s	
  Malt	
  dry	
  basis	
  fine	
  and	
  coarse	
  grinds	
  
using	
  a	
  laboratory	
  conducted	
  mash.	
  	
  By	
  testing	
  for	
  the	
  malt’s	
  extract	
  potentials,	
  we	
  
determined	
  the	
  Brewer’s	
  Malt	
  DBCG	
  to	
  have	
  a	
  specific	
  gravity	
  of	
  6.8°	
  P	
  and	
  the	
  Brewer’s	
  
Malt	
  DBFG	
  to	
  have	
  a	
  specific	
  gravity	
  of	
  7.8°	
  P.	
  	
  Although	
  DGCG	
  is	
  a	
  more	
  realistic	
  
representation	
  of	
  the	
  actual	
  grist	
  used	
  in	
  brewing	
  due	
  to	
  the	
  need	
  of	
  a	
  certain	
  extent	
  of	
  
coarseness	
  to	
  preserve	
  the	
  husk	
  and	
  promote	
  filtration,	
  DBFG	
  is	
  useful	
  in	
  determining	
  the	
  
grain’s	
  ultimate	
  affinity	
  for	
  saccharification.	
  	
  This	
  is	
  why	
  the	
  DBFG	
  specific	
  gravity	
  is	
  higher	
  
than	
  the	
  DBCG.	
  
	
  
Malt	
  Moisture	
  Content:	
  	
  By	
  placing	
  roughly	
  10	
  grams	
  of	
  Brewer’s	
  Fine	
  into	
  the	
  Brainweight	
  
moisture	
  content	
  analyzer	
  we	
  were	
  able	
  to	
  calculate	
  a	
  moisture	
  content	
  of	
  roughly	
  3.4%,	
  
indicating	
  we	
  had	
  a	
  well	
  malted	
  barley	
  with	
  low	
  moisture	
  content.	
  	
  Having	
  malt	
  with	
  low	
  
moisture	
  content	
  is	
  essential	
  due	
  to	
  the	
  fact	
  that	
  it	
  greatly	
  reduces	
  the	
  likelihood	
  of	
  
microbial	
  spoilage	
  or	
  flavor/aroma	
  loss	
  over	
  time.	
  	
  	
  
	
  
	
  
Malt	
  Sieve	
  Analysis:	
  	
  (Brewer’s	
  Malt	
  DBCG	
  Grist=	
  115g)	
  
	
  
Sieve	
   Amount	
   Percentage	
  
#10	
   64	
  grams	
   56.19%	
  
#14	
   26.7	
  grams	
   23.44%	
  
#18	
   9.4	
  grams	
   8.25%	
  
#30	
   5.8	
  grams	
   5.09%	
  
#60	
   4.4	
  grams	
   3.86%	
  
#100	
   1.2	
  grams	
   1.05%	
  
Pan	
   2.4	
  grams	
   2.11%	
  
	
  
This	
  sieve	
  analysis	
  indicated	
  that	
  our	
  Brewer’s	
  Malt	
  DBCG	
  Grist	
  was	
  too	
  coarse	
  based	
  on	
  
the	
  percentages	
  of	
  retained	
  kernels	
  on	
  the	
  #10	
  and	
  #14	
  sieves	
  which,	
  combined	
  were	
  
higher	
  than	
  our	
  target	
  retention	
  of	
  55%.	
  	
  Therefore,	
  we	
  adjusted	
  our	
  mill	
  0.38	
  to	
  0.34	
  in	
  
order	
  to	
  slightly	
  decrease	
  the	
  coarseness	
  of	
  the	
  grain	
  for	
  the	
  proper	
  ratio	
  of	
  extractability	
  
vs.	
  husk	
  friability	
  lending	
  to	
  its	
  ability	
  to	
  act	
  as	
  a	
  filtration	
  bed	
  following	
  saccharification.	
  
	
  
Expected	
  SRM	
  of	
  Finished	
  Beer:	
  
	
  
°L	
  =	
  EBC	
  /	
  1.97	
  
Briess	
  Brewer’s	
  Malt=	
  4.0	
  EBC/1.97	
  =	
  2.03	
  °L	
  
Munich	
  Malt=	
  19.7	
  EBC/1.97	
  =	
  10	
  °L	
  
White	
  Wheat	
  Malt=	
  4.7	
  EBC/1.97	
  =	
  2.39°	
  L	
  
	
  
SRM	
  =	
  (Malt	
  Color	
  °L	
  x	
  Malt	
  Weight	
  lbs)	
  /	
  Total	
  Kettle	
  Volume	
  Gallons	
  
Briess	
  Brewer’s	
  Malt=	
  (2.03°	
  L	
  x	
  15.43lbs)/12	
  gallons	
  =	
  2.61	
  SRM	
  
Munich	
  Malt=	
  (10°L	
  x	
  1.83	
  lbs)/12	
  gallons	
  =	
  1.53	
  SRM	
  
White	
  Wheat	
  Malt=	
  (2.39°	
  L	
  x	
  1.38	
  lbs)/12	
  gallons	
  =	
  0.27	
  SRM	
  
	
  
Total	
  SRM	
  =	
  4.41	
  SRM	
  
 
Malt	
  Bill	
  Characteristics:	
  
• Briess	
  Brewer’s	
  Malt	
  (2-­‐Row)	
  was	
  chosen	
  as	
  our	
  base	
  malt	
  (82.2%	
  of	
  total	
  grist	
  bill).	
  	
  
Aside	
  from	
  lending	
  consistency	
  and	
  malty	
  flavors,	
  the	
  grain	
  had	
  high	
  potential	
  for	
  
extract	
  (>81%)	
  based	
  on	
  its	
  kernel	
  plumpness	
  and	
  starch	
  content,	
  acceptable	
  
protein	
  content	
  (11.63%),	
  high	
  diastatic	
  power	
  (154°	
  Lintner),	
  and	
  decent	
  friability.	
  	
  
Therefore,	
  this	
  malt	
  will	
  be	
  an	
  effective	
  base	
  malt	
  based	
  on	
  its	
  high	
  contribution	
  of	
  
fermentable	
  sugars	
  based	
  on	
  high	
  starch	
  and	
  low	
  protein	
  content	
  as	
  well	
  as	
  will	
  act	
  
as	
  an	
  effective	
  filtration	
  bed	
  based	
  on	
  its	
  low	
  total	
  and	
  soluble	
  protein	
  contents.	
  
• Munich	
  Malt	
  10°L	
  was	
  chosen	
  to	
  add	
  further	
  malty	
  fullness	
  and	
  a	
  golden,	
  orange	
  
color	
  to	
  the	
  beer.	
  	
  The	
  malt	
  has	
  high	
  melanoidin	
  levels	
  as	
  a	
  result	
  of	
  Malliard	
  
reactions,	
  which	
  will	
  contribute	
  to	
  its	
  color	
  and	
  flavor	
  enhancement.	
  	
  The	
  malt	
  
makes	
  up	
  a	
  small	
  portion	
  of	
  our	
  grist	
  (9.8%)	
  and	
  has	
  a	
  low	
  diastatic	
  power	
  (40°	
  
Lintner)	
  that	
  is	
  still	
  capable	
  of	
  saccharification.	
  	
  Ultimately,	
  the	
  grain	
  may	
  contribute	
  
fermentable	
  sugar	
  but	
  its	
  primary	
  purpose	
  is	
  color	
  and	
  flavor	
  enhancement.	
  
• White	
  Wheat	
  Malt	
  was	
  chosen	
  to	
  add	
  slightly	
  bready	
  malty	
  flavors	
  as	
  well	
  as	
  to	
  
improve	
  head	
  retention	
  based	
  on	
  its	
  higher	
  protein	
  content.	
  	
  The	
  malt	
  makes	
  up	
  a	
  
small	
  portion	
  of	
  our	
  grist	
  (8%)	
  and	
  has	
  a	
  high	
  diastatic	
  power	
  (160°	
  Lintner).	
  	
  This	
  
malt	
  will	
  contribute	
  little	
  color	
  based	
  on	
  its	
  low	
  SRM.	
  
	
  
Hypothesis	
  
-­‐	
  	
  Based	
  on	
  our	
  water	
  treatment	
  with	
  calcium	
  chloride	
  and	
  lactic	
  acid,	
  we	
  expect	
  a	
  final	
  
product	
  with	
  a	
  2:1	
  alkalinity	
  ratio	
  and	
  a	
  slight	
  amount	
  of	
  body	
  and	
  sweetness	
  that	
  
successfully	
  saccharified.	
  	
  Furthermore,	
  based	
  on	
  our	
  aforementioned	
  malt	
  analyses	
  and	
  
selections,	
  we	
  can	
  expect	
  a	
  sessionable	
  final	
  product	
  that	
  is	
  light	
  to	
  medium-­‐light	
  bodied,	
  
straw	
  to	
  light	
  golden	
  colored,	
  with	
  bready	
  malty	
  flavors.	
  	
  We	
  also	
  expect	
  a	
  beer	
  with	
  low	
  
hop	
  character,	
  low	
  ester	
  profile,	
  and	
  absence	
  of	
  chill	
  haze.	
  
	
  
Brew	
  Method	
  (Brew	
  Date:	
  2/11/15)	
  
	
  
Mashing:	
  
1. After	
  adding	
  approximately	
  6.13g	
  calcium	
  chloride	
  and	
  4.37ml	
  of	
  lactic	
  acid	
  to	
  our	
  
mash	
  kettle	
  containing	
  25	
  liters	
  of	
  water	
  (and	
  approximately	
  12.27g	
  calcium	
  
chloride	
  and	
  8.73ml	
  of	
  lactic	
  acid	
  to	
  the	
  hot	
  liquor	
  tank	
  containing	
  55	
  liters	
  of	
  
water),	
  we	
  mashed	
  in	
  at	
  3:07pm.	
  
2. Our	
  strike	
  water	
  was	
  added	
  to	
  our	
  8.51kg	
  of	
  grist	
  at	
  73°	
  C	
  producing	
  a	
  mash	
  
temperature	
  of	
  62.5°C	
  (at	
  3:12pm)	
  which	
  was	
  quite	
  a	
  bit	
  lower	
  than	
  our	
  target	
  mash	
  
temperature	
  of	
  66.7°C.	
  	
  Therefore	
  we	
  re-­‐circulated	
  (rather	
  than	
  incorrectly	
  heating	
  
the	
  mash	
  tun	
  with	
  the	
  burner	
  as	
  someone	
  suggested)	
  the	
  heat	
  and	
  eventually	
  
achieved	
  a	
  mash	
  temperature	
  of	
  66.6°C	
  (at	
  3:36pm).	
  
3. During	
  recirculation,	
  the	
  mash	
  pH	
  was	
  determined	
  to	
  be	
  5.8	
  at	
  3:25pm,	
  higher	
  than	
  
our	
  expected	
  pH	
  of	
  5.4.	
  
4. After	
  thirty	
  minutes	
  of	
  mash	
  resting,	
  an	
  iodine	
  test	
  was	
  performed	
  yielding	
  a	
  
negative	
  result	
  at	
  3:37pm	
  and	
  began	
  vorlauf.	
  	
  This	
  indicated	
  saccharification	
  had	
  
successfully	
  occurred.	
  
 
Observations/Conclusions:	
  
-­‐	
  	
  The	
  initial	
  mash	
  temperature	
  was	
  too	
  long	
  which	
  has	
  a	
  negative	
  impact	
  on	
  the	
  enzymes’	
  
ability	
  to	
  effectively	
  convert	
  starch	
  to	
  fermentable	
  sugars.	
  	
  Inadequate	
  enzyme	
  activity	
  will	
  
lead	
  to	
  inability	
  to	
  saccharify	
  or	
  lower	
  fermentability	
  and	
  resulting	
  lower	
  attenuation	
  and	
  
higher	
  levels	
  of	
  residual	
  sugar.	
  	
  However,	
  we	
  were	
  able	
  to	
  increase	
  the	
  temperature	
  of	
  our	
  
mash	
  and	
  verified	
  that	
  saccharification	
  occurred	
  through	
  the	
  use	
  of	
  an	
  iodine	
  test.	
  	
  In	
  the	
  
future,	
  wind	
  and	
  cooler	
  conditions	
  (since	
  we	
  brew	
  outside	
  Gifford)	
  should	
  be	
  considered	
  
based	
  on	
  their	
  ability	
  to	
  lower	
  mash	
  pH	
  and	
  action	
  should	
  be	
  taken	
  to	
  prevent	
  this	
  from	
  
happening.	
  
-­‐	
  	
  Our	
  mash	
  temperature	
  of	
  66.6°C	
  incorporated	
  a	
  balance	
  of	
  both	
  alpha	
  amylase	
  and	
  beta	
  
amylase	
  enzymes.	
  	
  Alpha	
  amylase	
  favors	
  higher	
  temperatures	
  and	
  a	
  more	
  full-­‐bodied	
  beer	
  
and	
  beta	
  amylase	
  favors	
  lower	
  temperatures	
  and	
  a	
  lighter	
  bodied,	
  drier	
  beer.	
  	
  Since	
  a	
  
majority	
  of	
  the	
  mash	
  rest	
  was	
  spent	
  at	
  lower	
  temperatures	
  before	
  being	
  brought	
  to	
  this	
  
balanced	
  temperature,	
  the	
  final	
  product	
  should	
  be	
  more	
  light-­‐bodied.	
  
-­‐	
  	
  Our	
  higher	
  than	
  expected	
  mash	
  pH	
  of	
  5.8	
  indicated	
  that	
  we	
  probably	
  needed	
  to	
  add	
  more	
  
lactic	
  acid	
  to	
  further	
  acidify	
  our	
  mash.	
  	
  While	
  the	
  enzymes	
  still	
  seemed	
  to	
  function	
  properly	
  
at	
  this	
  pH	
  given	
  the	
  successful	
  thirty	
  minute	
  saccharification,	
  it	
  must	
  be	
  later	
  considered	
  
that	
  this	
  may	
  adversely	
  affect	
  our	
  final	
  product	
  based	
  on	
  inadequate	
  enzyme	
  activity.	
  
	
  
Lautering/Sparging:	
  
1. We	
  began	
  separating	
  our	
  wort	
  from	
  our	
  grain	
  bed	
  at	
  3:51pm.	
  
2. We	
  sparged	
  with	
  36.0l	
  at	
  78.3°C	
  until	
  we	
  completed	
  lautering	
  at	
  4:30	
  pm.	
  
	
  
Observations/Conclusions:	
  
-­‐	
  	
  Sparging	
  should	
  ideally	
  function	
  as	
  a	
  slow	
  rinsing	
  of	
  the	
  grains	
  with	
  warm	
  water	
  to	
  
gather	
  any	
  residual	
  sugar	
  not	
  separated	
  by	
  the	
  original	
  draining	
  of	
  mash	
  rest	
  water.	
  	
  
However,	
  we	
  mistakenly	
  added	
  the	
  sparge	
  water	
  too	
  quickly	
  which	
  could	
  potentially	
  lead	
  
to	
  lower	
  extraction	
  of	
  residual	
  sugars.	
  	
  This	
  was	
  a	
  big	
  mistake	
  to	
  be	
  learned	
  from	
  and	
  not	
  
made	
  again.	
  	
  This	
  event	
  necessitated	
  the	
  need	
  to	
  keep	
  an	
  eye	
  out	
  for	
  a	
  lower	
  starting	
  
gravity	
  than	
  expected.	
  
-­‐	
  	
  Our	
  change	
  in	
  mill	
  settings	
  previously	
  mentioned	
  didn’t	
  seem	
  to	
  negatively	
  impact	
  the	
  
effectiveness	
  of	
  the	
  grain	
  husks	
  acting	
  as	
  a	
  filtration	
  bed,	
  there	
  were	
  no	
  problems	
  with	
  the	
  
actual	
  separation	
  of	
  wort	
  from	
  grain	
  bed	
  process.	
  
	
  
Boil:	
  
1. At	
  4:33pm	
  we	
  reached	
  a	
  boil	
  with	
  a	
  pre-­‐boil	
  pH	
  of	
  5.6	
  and	
  gravity	
  of	
  9.7°	
  P.	
  	
  As	
  the	
  
boil	
  commenced,	
  we	
  added	
  11.0	
  grams	
  of	
  Merkur	
  hops	
  as	
  our	
  primary	
  bittering	
  hop	
  
addition.	
  
2. Forty-­‐five	
  minutes	
  later,	
  at	
  5:18pm,	
  we	
  performed	
  our	
  second	
  hop	
  addition	
  of	
  57.0	
  
grams	
  of	
  Sterling	
  hops	
  contributing	
  both	
  bitterness	
  and	
  aroma.	
  
3. At	
  5:23pm,	
  we	
  added	
  Whirlfloc	
  as	
  our	
  kettle	
  coagulant.	
  
4. At	
  5:33pm,	
  another	
  39.0	
  grams	
  of	
  Sterling	
  hops	
  were	
  added	
  as	
  our	
  primary	
  aroma	
  
hop	
  addition.	
  	
  In	
  addition,	
  we	
  began	
  our	
  whirlpool	
  at	
  this	
  time	
  as	
  well	
  as	
  ended	
  our	
  
boil.	
  	
  At	
  the	
  end	
  of	
  boil	
  we	
  had	
  45	
  liters	
  of	
  boiled	
  wort	
  and	
  a	
  pH	
  of	
  5.59.	
  	
  The	
  
whirlpool	
  was	
  ended	
  at	
  5:43pm.	
  
 
Observations/Conclusions:	
  
-­‐	
  	
  As	
  previously	
  mentioned,	
  we	
  were	
  not	
  trying	
  to	
  produce	
  a	
  beer	
  with	
  a	
  prominent	
  hop	
  
character	
  based	
  on	
  the	
  parameters	
  of	
  the	
  Kölsch	
  style.	
  	
  However,	
  we	
  still	
  utilized	
  Merkur	
  
hops,	
  whose	
  high	
  alpha	
  acid	
  content	
  (13.6%)	
  and	
  low	
  co-­‐humulone	
  content	
  contributed	
  
mild	
  bitterness	
  via	
  isomerization	
  to	
  balance	
  the	
  light-­‐bodied	
  beer.	
  	
  In	
  addition,	
  we	
  also	
  
utilized	
  Sterling	
  hops,	
  which	
  lend	
  herbal,	
  spicy,	
  and	
  slightly	
  floral	
  and	
  citrusy	
  aromas	
  when	
  
added	
  at	
  the	
  end	
  of	
  boil.	
  	
  Not	
  only	
  were	
  we	
  attempting	
  to	
  correctly	
  match	
  the	
  Kölsch	
  style,	
  
but	
  this	
  minimal	
  hop	
  character	
  beer	
  also	
  allowed	
  for	
  greater	
  focus	
  on	
  water	
  treatment	
  and	
  
grain	
  analysis	
  and	
  selection,	
  the	
  major	
  topics	
  of	
  this	
  brew	
  in	
  particular.	
  
-­‐	
  	
  Whirlfloc	
  (an	
  Irish	
  moss/carrageenan	
  blend)	
  was	
  added	
  to	
  the	
  boil	
  in	
  order	
  to	
  assist	
  the	
  
formation	
  of	
  hot	
  break	
  (in	
  addition	
  to	
  the	
  whirlpool)	
  by	
  precipitating	
  haze-­‐causing	
  proteins	
  
and	
  beta-­‐glucans.	
  	
  This	
  is	
  especially	
  desirable	
  in	
  a	
  Kölsch	
  where	
  clarity	
  is	
  an	
  important	
  
parameter	
  of	
  the	
  style.	
  
	
  
Knockout/Yeast	
  Pitch:	
  
1. At	
  5:45pm	
  we	
  began	
  knockout	
  into	
  a	
  keg	
  at	
  14°C	
  using	
  oxygen	
  at	
  psi.	
  	
  	
  
2. The	
  initial	
  gravity	
  of	
  our	
  wort	
  prior	
  to	
  fermentation	
  was	
  measured	
  to	
  be	
  11.3°	
  P.	
  	
  We	
  
decided	
  to	
  pitch	
  three	
  packages	
  of	
  German	
  Ale	
  Kölsch	
  Yeast	
  (WLP029)	
  due	
  to	
  the	
  
fact	
  that	
  each	
  vial	
  of	
  yeast	
  contains	
  roughly	
  150	
  billion	
  cells	
  and	
  the	
  following	
  
calculation,	
  1.5	
  million	
  cells	
  (lager	
  yeast)	
  x	
  45.4	
  l	
  x	
  11.3°	
  P	
  =	
  769,869,000,000	
  cells,	
  
indicates	
  three	
  packages	
  is	
  close	
  enough	
  (450	
  billion	
  cells).	
  
	
  
Observations/Conclusions:	
  
-­‐	
  	
  The	
  knockout	
  occurred	
  quickly	
  reducing	
  the	
  risk	
  of	
  aldehyde	
  and/or	
  dimethyl	
  sulfide	
  
formation	
  in	
  the	
  wort.	
  
-­‐	
  	
  Our	
  initial	
  gravity	
  of	
  11.3°	
  P	
  (at	
  45.4	
  l)	
  was	
  lower	
  than	
  our	
  expected	
  gravity	
  of	
  12.140°	
  P	
  
(at	
  40.0	
  l)	
  due	
  to	
  the	
  fact	
  that	
  our	
  actual	
  total	
  volume	
  was	
  also	
  higher	
  and	
  therefore	
  the	
  
wort	
  and	
  its	
  fermentable	
  sugars	
  weren’t	
  as	
  condensed	
  as	
  expected.	
  	
  In	
  addition,	
  our	
  
accidental	
  rapid	
  sparging	
  also	
  may	
  have	
  contributed	
  to	
  this	
  lower	
  than	
  expected	
  initial	
  
gravity.	
  
-­‐	
  	
  This	
  Kölsch	
  Ale	
  Yeast	
  was	
  ideal	
  for	
  our	
  beer	
  due	
  to	
  its	
  clean,	
  low-­‐ester	
  profile,	
  which	
  matched	
  
our	
  quality	
  parameters	
  for	
  what	
  we	
  were	
  trying	
  to	
  brew.	
  	
  The	
  yeast	
  strain	
  is	
  also	
  fittingly	
  
attenuable	
  and	
  lends	
  to	
  the	
  fermentation	
  into	
  a	
  light-­‐bodied	
  beer.	
  
	
  
Fermentation/Conditioning/Packaging:	
  
Date:	
   Gravity:	
   Temperature	
   Step	
  
2/11/15	
   11.3°P	
   14°C	
   Pitch	
  
2/13/15	
   5.9°P	
   24°C	
   Fermentation	
  
2/16/15	
   2.22°P	
   20°C	
   Fermentation	
  
2/18/15	
   2.02°P	
   -­‐-­‐-­‐	
   Cold	
  Crash	
  
2/27/15	
   2.02°P	
   -­‐-­‐-­‐	
   Racked	
  	
  
3/4/15	
   2.02°P	
   -­‐-­‐-­‐	
   Kegged	
  
 
Observations/Conclusions:	
  
-­‐Fermentation	
  proceeded	
  rather	
  quickly,	
  which	
  came	
  as	
  a	
  bit	
  of	
  a	
  surprise	
  based	
  on	
  the	
  
yeast	
  quantity	
  pitched.	
  	
  Although	
  we	
  thought	
  three	
  packages	
  of	
  yeast	
  containing	
  a	
  total	
  of	
  
450	
  billion	
  cells	
  (which	
  it	
  seemingly	
  was),	
  this	
  came	
  up	
  fairly	
  short	
  of	
  our	
  calculated	
  yeast	
  
quantity	
  of	
  nearly	
  770	
  billion	
  cells	
  meaning	
  we	
  under	
  pitched.	
  	
  This	
  could’ve	
  led	
  to	
  a	
  slow	
  
or	
  even	
  uncompleted	
  fermentation	
  and	
  could’ve	
  also	
  stressed	
  the	
  yeast	
  leading	
  to	
  a	
  
number	
  of	
  off	
  flavors	
  such	
  as	
  fusel	
  alcohols	
  and	
  undesirable	
  sulfurous	
  flavors.	
  	
  Again,	
  
although	
  it	
  seemed	
  fermentation	
  was	
  facilitated	
  with	
  ease	
  by	
  our	
  yeast	
  (based	
  on	
  time	
  and	
  
our	
  actual	
  final	
  gravity	
  that	
  was	
  lower	
  than	
  our	
  theoretical	
  final	
  gravity)	
  at	
  this	
  point	
  we	
  
still	
  out	
  to	
  be	
  mindful	
  of	
  potential	
  off	
  flavors	
  that	
  may	
  have	
  been	
  produced	
  during	
  this	
  
fermentation.	
  
-­‐	
  	
  The	
  fermentation	
  temperature	
  fluctuated	
  quite	
  a	
  bit	
  likely	
  due	
  to	
  our	
  inability	
  to	
  
temperature	
  control	
  the	
  brew	
  lab	
  during	
  winter	
  where	
  the	
  heat	
  was	
  being	
  turned	
  on	
  and	
  
off.	
  	
  Ideally	
  we	
  wanted	
  to	
  ferment	
  just	
  below	
  ale	
  temperatures	
  (roughly	
  14-­‐17°C),	
  but	
  we	
  
ended	
  up	
  as	
  high	
  as	
  24°C.	
  	
  While	
  this	
  shouldn’t	
  kill	
  off	
  the	
  yeast,	
  the	
  warmer	
  fermentation	
  
may	
  lend	
  some	
  esters	
  to	
  our	
  beer	
  to	
  be	
  considered	
  when	
  sampling	
  our	
  final	
  product.	
  
-­‐	
  	
  We	
  kegged	
  this	
  beer	
  into	
  two	
  1/6	
  barrels	
  to	
  make	
  packaging	
  quicker	
  and	
  less	
  labor	
  
intensive.	
  	
  We	
  carbonated	
  it	
  in	
  the	
  cooler	
  for	
  6	
  days	
  at	
  16	
  psi	
  until	
  the	
  day	
  before	
  sensory	
  
evaluation	
  in	
  which	
  we	
  increased	
  the	
  pressure	
  to	
  25	
  psi.	
  
	
  
Sensory	
  Analysis	
  (Date:	
  3/11/15)	
  
	
  
Visual:	
  	
  	
  
• The	
  beer	
  was	
  light	
  yellow	
  as	
  a	
  result	
  of	
  the	
  light	
  (low	
  SRM)	
  malts	
  we	
  utilized.	
  
• The	
  beer	
  was	
  slightly	
  opaque	
  indicating	
  slight	
  chill	
  haze	
  and	
  inadequate	
  reduction	
  of	
  
proteins	
  or	
  beta-­‐glucans.	
  
• The	
  beer	
  had	
  only	
  slight	
  head	
  retention,	
  which	
  comes	
  as	
  a	
  bit	
  of	
  surprise	
  based	
  on	
  
our	
  use	
  of	
  high	
  alpha-­‐acid	
  hops	
  and	
  residual	
  protein	
  in	
  the	
  beer.	
  	
  	
  Perhaps	
  this	
  
occurred	
  based	
  on	
  our	
  somewhat	
  low	
  protein	
  malt	
  bill	
  (white	
  wheat	
  malt	
  was	
  used	
  
sparingly)	
  or	
  the	
  low	
  carbonation	
  of	
  the	
  beer.	
  
• The	
  beer	
  also	
  had	
  decent	
  lacing	
  that	
  could’ve	
  been	
  affected	
  by	
  a	
  number	
  of	
  factors	
  
such	
  as	
  hop	
  and	
  protein	
  content	
  or	
  the	
  cleanness	
  of	
  the	
  glass	
  being	
  sampled	
  from.	
  
	
  
Aroma:	
  
• The	
  beer	
  had	
  slight	
  fruit	
  esters	
  likely	
  due	
  to	
  fermentation	
  at	
  warmer	
  temperatures.	
  	
  
In	
  addition,	
  we	
  noted	
  a	
  pear,	
  apple	
  like	
  aroma,	
  which	
  is	
  indicative	
  of	
  acetaldehyde.	
  	
  
Normally,	
  the	
  presence	
  of	
  acetaldehyde	
  indicates	
  an	
  incomplete	
  fermentation,	
  but	
  
this	
  seems	
  unlikely	
  due	
  to	
  the	
  high	
  attenuation	
  of	
  our	
  beer	
  and	
  resulting	
  lower	
  final	
  
gravity	
  than	
  expected.	
  	
  Perhaps	
  these	
  aromas	
  were	
  more	
  attributed	
  to	
  ester	
  
production	
  during	
  fermentation.	
  
• The	
  beer	
  had	
  slight	
  aromas	
  of	
  honey,	
  which	
  can	
  be	
  directly	
  attributed	
  to	
  our	
  use	
  of	
  
Munich	
  malt.	
  	
  There	
  were	
  also	
  some	
  bready	
  aromas	
  that	
  were	
  also	
  either	
  
attributable	
  to	
  our	
  malt	
  selection	
  or	
  even	
  yeast.	
  
• The	
  beer	
  had	
  some	
  slightly	
  floral	
  (geraniol)	
  and	
  grassy	
  hop	
  aromas,	
  which	
  can	
  be	
  
directly	
  attributed	
  to	
  our	
  use	
  of	
  Sterling	
  aroma	
  hop	
  additions.	
  
	
  
Flavor:	
  
• The	
  beer	
  had	
  a	
  light	
  caramelly	
  maltiness,	
  which	
  can	
  be	
  attributed	
  to	
  our	
  use	
  of	
  
Munich	
  malt.	
  
• The	
  beer	
  also	
  had	
  slight	
  hop	
  bitterness	
  resulting	
  from	
  our	
  hop	
  additions,	
  especially	
  
the	
  addition	
  of	
  Merkur.	
  
• The	
  beer	
  had	
  a	
  slight	
  fruity	
  sweetness,	
  which	
  can	
  most	
  likely	
  be	
  attributed	
  to	
  ester	
  
production	
  during	
  fermentation.	
  	
  Perhaps	
  some	
  of	
  the	
  perception	
  of	
  sweetness	
  came	
  
from	
  our	
  use	
  of	
  calcium	
  chloride.	
  
	
  
Mouthfeel:	
  
• The	
  beer	
  was	
  medium-­‐light	
  bodied	
  based	
  on	
  our	
  malt	
  selection,	
  attenuative	
  
fermentation,	
  and	
  mash	
  temperature	
  choice	
  balancing	
  alpha	
  and	
  beta	
  amylase	
  
enzymes.	
  	
  Despite	
  a	
  slight	
  chill	
  haze,	
  there	
  was	
  low	
  overall	
  viscosity	
  due	
  to	
  low	
  
protein	
  content	
  of	
  our	
  beer.	
  
• The	
  beer	
  was	
  smooth,	
  coating,	
  clean,	
  and	
  balanced	
  based	
  on	
  our	
  water	
  treatment	
  
with	
  calcium	
  chloride.	
  
• The	
  beer	
  had	
  low	
  carbonation	
  thus	
  lacking	
  a	
  biting	
  bitterness,	
  which	
  ultimately	
  led	
  
to	
  a	
  palatable	
  beer	
  with	
  greater	
  focus	
  on	
  flavor.	
  
	
  
Overall:	
  
• The	
  beer	
  met	
  BJCP	
  guidelines	
  to	
  a	
  tee	
  in	
  terms	
  of	
  appearance,	
  aroma,	
  flavor,	
  and	
  
mouthfeel.	
  	
  We	
  successfully	
  brewed	
  a	
  clean,	
  sessionable	
  Kölsch	
  that	
  was	
  medium-­‐
light	
  bodied,	
  had	
  low	
  esters,	
  low	
  hop	
  flavor,	
  and	
  slight	
  hop	
  bitterness.	
  
	
  
Conclusion	
  
-­‐	
  	
  Based	
  on	
  our	
  water	
  treatment,	
  malt	
  analyses,	
  malt	
  selection,	
  and	
  other	
  brewing	
  
parameters	
  aforementioned,	
  we	
  ultimately	
  came	
  pretty	
  close	
  to	
  completely	
  verifying	
  our	
  
expectations	
  and	
  hypothesis.	
  	
  We	
  produced	
  a	
  medium-­‐light	
  bodied	
  beer	
  based	
  on	
  our	
  use	
  
of	
  calcium	
  chloride,	
  our	
  malt	
  selection,	
  and	
  mash	
  regimen.	
  	
  The	
  beer	
  also	
  was	
  light	
  golden	
  
in	
  color	
  and	
  had	
  bready	
  and	
  honey	
  malty	
  aromas	
  and	
  flavors,	
  all	
  of	
  which	
  can	
  be	
  directly	
  
attributed	
  to	
  our	
  malt	
  selection.	
  	
  In	
  addition,	
  the	
  beer	
  had	
  a	
  slight	
  sweetness	
  as	
  a	
  result	
  of	
  
our	
  manipulation	
  of	
  body	
  and	
  use	
  of	
  calcium	
  chloride.	
  	
  The	
  final	
  product	
  slightly	
  strayed	
  
from	
  the	
  hypothesis	
  based	
  on	
  the	
  fact	
  that	
  esters	
  were	
  present	
  likely	
  as	
  a	
  result	
  of	
  warmer	
  
fermentation	
  temperatures.	
  	
  In	
  addition,	
  the	
  beer	
  had	
  a	
  slight	
  chill	
  haze	
  based	
  on	
  haze-­‐
forming	
  proteins	
  and	
  beta-­‐glucans,	
  which	
  wasn’t	
  expected	
  or	
  desired	
  based	
  on	
  Kölsch	
  style	
  
guidelines.	
  	
  Overall,	
  our	
  water	
  treatment	
  and	
  malt	
  selection	
  as	
  well	
  as	
  other,	
  less	
  
emphasized	
  brewing	
  parameters,	
  contributed	
  to	
  an	
  ale	
  both	
  consistent	
  with	
  our	
  hypothesis	
  
and	
  expectations	
  as	
  well	
  as	
  the	
  BJCP	
  guidelines.	
  	
  The	
  brewing	
  of	
  this	
  beer	
  ultimately	
  proved	
  
successful	
  despite	
  some	
  issues	
  (higher	
  mash	
  temperature,	
  too	
  quick	
  of	
  sparge,	
  non-­‐
temperature	
  controlled	
  fermentation)	
  based	
  on	
  the	
  fact	
  we	
  produced	
  a	
  drinkable,	
  
sessionable	
  Kölsch	
  ale.	
  

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FTEC 422 Lab Report 1

  • 1. FTEC  422  Lab  Report  1     Name:    John  Schnettler   Style  of  Brew:    Kölsch   Brew  Date:    2/11/15   Kegging  Date:  3/4/15   Sensory  Evaluation  Date:  3/11/15   Batch  Volume:  Target:  40.0  l     Original  Gravity:  Target=  12.140°  P  (Actual=  11.3°  P)   Final  Gravity:  Target=  2.912°  P  (Actual=  2.02°  P)     Material  Bill     Water  Additives:     Ingredient   Amount   Step   Time   Calcium  Chloride   18.40  g   Mash     60  minutes   Lactic  Acid   13.10  ml   Mash   60  minutes     Grist  Bill:     Malt   Amount   Color  (European  Brewing   Convention)     Breiss  Brewers  Malt  (2   Row)  US     7.00  kg   4.0  EBC   Munich  Malt  10L   0.83  kg   19.7  EBC   White  Wheat  Malt   0.68  kg   4.7  EBC     Boil  Ingredients:     Ingredient   Amount   Time   Merkur  (13.60%  alpha-­‐ acid):  Hop  addition   11.0  g   60  minutes   Sterling  2013  (6.70%  alpha-­‐ acid):  Hop  addition   57.0  g   15  minutes   Whirlfloc:  Clarification   1  Tablet   10  minutes   Sterling  2013  (6.70%  alpha-­‐ acid):  Hop  addition   39.0  g   5  minutes     Yeast:    German  Ale/Kölsch  (White  Labs  #WLP029)            
  • 2. Water  Treatment     Starting  Water:   Fort  Collins  Water  analysis:     1.  Hardness  =  100  ppm     2.  Alkalinity  =  80  ppm     3.  pH  =  6.9     4.  Ca  =  17.3  ppm     5.  Mg  =  1.6  ppm     6.  Cl  =  2.9  ppm     Criteria:    Produce  a  light  to  medium  light  bodied,  clean,  crisp,  clear,  mildly  sweet  and  low   ester  straw  to  gold  ale  with  low  hop  character.    We  decided  as  a  class  to  increase  the   hardness  of  the  beer  to  2:1  hardness  to  alkalinity  ratio  as  well  as  lower  the  mash  pH  of  the   water  to  increase  wort  fermentability  by  providing  the  optimum  saccharification   temperature.    Therefore,  we  aimed  for  a  water  profile  with  a  calcium  content  of  80  ppm   with  a  mash  pH  of  5.4.         Determination:    In  order  to  produce  the  desired  water  profile,  we  decided  as  a  class  to   utilize  calcium  chloride  and  lactic  acid  to  treat  80.0  l  of  water  (approximately  1/3  mash  tun   water  and  2/3  hot  liquor  tank  water).    Calcium  ions  are  important  in  stabilizing  mash  alpha   amylase  enzymes,  reducing  mash  pH  by  reacting  with  phosphates  to  create  insoluble   compounds  releasing  H+  ions,  aiding  the  formation  of  hot  break  by  enhancing  protein   coagulation,  and  increasing  clarity.    Chloride  ions  are  known  to  balance  the  flavor  profile  of   beer  and  also  influence  sweetness.    Therefore,  we  calculated  that  we  would  use  18.40g  of   calcium  chloride  in  order  to  contribute  these  benefits  of  each  ion  as  well  as  to  increase   permanent  hardness  and  remove  alkaline  water’s  buffering  capacity.    We  avoided  the  use   of  magnesium  due  to  the  fact  that  although  it  shares  many  impacts  on  beer  as  calcium,  it  is   much  less  effective  and  as  a  result  is  required  in  greater  amounts.    We  also  chose  to  add   permanent  hardness  in  the  form  of  chlorides  rather  than  sulfates  in  order  to  contribute  a   subtle  sweetness  rather  than  enhance  hop  bitterness,  which  is  not  characteristic  of  the   Kölsch  style.    Using  18.40g  calcium  chloride  brought  us  to  our  desired  hardness  to   alkalinity  ratio  and  80-­‐ppm  calcium  concentration;  however,  we  needed  to  further  reduce   the  mash  pH  and  therefore  turned  to  lactic  acid.    Our  classmate  Trent  calculated  13.10  ml  of   lactic  acid  would  effectively  bring  our  mash  pH  down  to  5.4.     Malt  Analysis     Malt  Extract  Methods  for  DBFG  and  DBCG:    First  we  tested  for  the  specific  gravity  (using   ASBC  Method  of  Analysis)  of  our  Breiss  Brewer’s  Malt  dry  basis  fine  and  coarse  grinds  
  • 3. using  a  laboratory  conducted  mash.    By  testing  for  the  malt’s  extract  potentials,  we   determined  the  Brewer’s  Malt  DBCG  to  have  a  specific  gravity  of  6.8°  P  and  the  Brewer’s   Malt  DBFG  to  have  a  specific  gravity  of  7.8°  P.    Although  DGCG  is  a  more  realistic   representation  of  the  actual  grist  used  in  brewing  due  to  the  need  of  a  certain  extent  of   coarseness  to  preserve  the  husk  and  promote  filtration,  DBFG  is  useful  in  determining  the   grain’s  ultimate  affinity  for  saccharification.    This  is  why  the  DBFG  specific  gravity  is  higher   than  the  DBCG.     Malt  Moisture  Content:    By  placing  roughly  10  grams  of  Brewer’s  Fine  into  the  Brainweight   moisture  content  analyzer  we  were  able  to  calculate  a  moisture  content  of  roughly  3.4%,   indicating  we  had  a  well  malted  barley  with  low  moisture  content.    Having  malt  with  low   moisture  content  is  essential  due  to  the  fact  that  it  greatly  reduces  the  likelihood  of   microbial  spoilage  or  flavor/aroma  loss  over  time.           Malt  Sieve  Analysis:    (Brewer’s  Malt  DBCG  Grist=  115g)     Sieve   Amount   Percentage   #10   64  grams   56.19%   #14   26.7  grams   23.44%   #18   9.4  grams   8.25%   #30   5.8  grams   5.09%   #60   4.4  grams   3.86%   #100   1.2  grams   1.05%   Pan   2.4  grams   2.11%     This  sieve  analysis  indicated  that  our  Brewer’s  Malt  DBCG  Grist  was  too  coarse  based  on   the  percentages  of  retained  kernels  on  the  #10  and  #14  sieves  which,  combined  were   higher  than  our  target  retention  of  55%.    Therefore,  we  adjusted  our  mill  0.38  to  0.34  in   order  to  slightly  decrease  the  coarseness  of  the  grain  for  the  proper  ratio  of  extractability   vs.  husk  friability  lending  to  its  ability  to  act  as  a  filtration  bed  following  saccharification.     Expected  SRM  of  Finished  Beer:     °L  =  EBC  /  1.97   Briess  Brewer’s  Malt=  4.0  EBC/1.97  =  2.03  °L   Munich  Malt=  19.7  EBC/1.97  =  10  °L   White  Wheat  Malt=  4.7  EBC/1.97  =  2.39°  L     SRM  =  (Malt  Color  °L  x  Malt  Weight  lbs)  /  Total  Kettle  Volume  Gallons   Briess  Brewer’s  Malt=  (2.03°  L  x  15.43lbs)/12  gallons  =  2.61  SRM   Munich  Malt=  (10°L  x  1.83  lbs)/12  gallons  =  1.53  SRM   White  Wheat  Malt=  (2.39°  L  x  1.38  lbs)/12  gallons  =  0.27  SRM     Total  SRM  =  4.41  SRM  
  • 4.   Malt  Bill  Characteristics:   • Briess  Brewer’s  Malt  (2-­‐Row)  was  chosen  as  our  base  malt  (82.2%  of  total  grist  bill).     Aside  from  lending  consistency  and  malty  flavors,  the  grain  had  high  potential  for   extract  (>81%)  based  on  its  kernel  plumpness  and  starch  content,  acceptable   protein  content  (11.63%),  high  diastatic  power  (154°  Lintner),  and  decent  friability.     Therefore,  this  malt  will  be  an  effective  base  malt  based  on  its  high  contribution  of   fermentable  sugars  based  on  high  starch  and  low  protein  content  as  well  as  will  act   as  an  effective  filtration  bed  based  on  its  low  total  and  soluble  protein  contents.   • Munich  Malt  10°L  was  chosen  to  add  further  malty  fullness  and  a  golden,  orange   color  to  the  beer.    The  malt  has  high  melanoidin  levels  as  a  result  of  Malliard   reactions,  which  will  contribute  to  its  color  and  flavor  enhancement.    The  malt   makes  up  a  small  portion  of  our  grist  (9.8%)  and  has  a  low  diastatic  power  (40°   Lintner)  that  is  still  capable  of  saccharification.    Ultimately,  the  grain  may  contribute   fermentable  sugar  but  its  primary  purpose  is  color  and  flavor  enhancement.   • White  Wheat  Malt  was  chosen  to  add  slightly  bready  malty  flavors  as  well  as  to   improve  head  retention  based  on  its  higher  protein  content.    The  malt  makes  up  a   small  portion  of  our  grist  (8%)  and  has  a  high  diastatic  power  (160°  Lintner).    This   malt  will  contribute  little  color  based  on  its  low  SRM.     Hypothesis   -­‐    Based  on  our  water  treatment  with  calcium  chloride  and  lactic  acid,  we  expect  a  final   product  with  a  2:1  alkalinity  ratio  and  a  slight  amount  of  body  and  sweetness  that   successfully  saccharified.    Furthermore,  based  on  our  aforementioned  malt  analyses  and   selections,  we  can  expect  a  sessionable  final  product  that  is  light  to  medium-­‐light  bodied,   straw  to  light  golden  colored,  with  bready  malty  flavors.    We  also  expect  a  beer  with  low   hop  character,  low  ester  profile,  and  absence  of  chill  haze.     Brew  Method  (Brew  Date:  2/11/15)     Mashing:   1. After  adding  approximately  6.13g  calcium  chloride  and  4.37ml  of  lactic  acid  to  our   mash  kettle  containing  25  liters  of  water  (and  approximately  12.27g  calcium   chloride  and  8.73ml  of  lactic  acid  to  the  hot  liquor  tank  containing  55  liters  of   water),  we  mashed  in  at  3:07pm.   2. Our  strike  water  was  added  to  our  8.51kg  of  grist  at  73°  C  producing  a  mash   temperature  of  62.5°C  (at  3:12pm)  which  was  quite  a  bit  lower  than  our  target  mash   temperature  of  66.7°C.    Therefore  we  re-­‐circulated  (rather  than  incorrectly  heating   the  mash  tun  with  the  burner  as  someone  suggested)  the  heat  and  eventually   achieved  a  mash  temperature  of  66.6°C  (at  3:36pm).   3. During  recirculation,  the  mash  pH  was  determined  to  be  5.8  at  3:25pm,  higher  than   our  expected  pH  of  5.4.   4. After  thirty  minutes  of  mash  resting,  an  iodine  test  was  performed  yielding  a   negative  result  at  3:37pm  and  began  vorlauf.    This  indicated  saccharification  had   successfully  occurred.  
  • 5.   Observations/Conclusions:   -­‐    The  initial  mash  temperature  was  too  long  which  has  a  negative  impact  on  the  enzymes’   ability  to  effectively  convert  starch  to  fermentable  sugars.    Inadequate  enzyme  activity  will   lead  to  inability  to  saccharify  or  lower  fermentability  and  resulting  lower  attenuation  and   higher  levels  of  residual  sugar.    However,  we  were  able  to  increase  the  temperature  of  our   mash  and  verified  that  saccharification  occurred  through  the  use  of  an  iodine  test.    In  the   future,  wind  and  cooler  conditions  (since  we  brew  outside  Gifford)  should  be  considered   based  on  their  ability  to  lower  mash  pH  and  action  should  be  taken  to  prevent  this  from   happening.   -­‐    Our  mash  temperature  of  66.6°C  incorporated  a  balance  of  both  alpha  amylase  and  beta   amylase  enzymes.    Alpha  amylase  favors  higher  temperatures  and  a  more  full-­‐bodied  beer   and  beta  amylase  favors  lower  temperatures  and  a  lighter  bodied,  drier  beer.    Since  a   majority  of  the  mash  rest  was  spent  at  lower  temperatures  before  being  brought  to  this   balanced  temperature,  the  final  product  should  be  more  light-­‐bodied.   -­‐    Our  higher  than  expected  mash  pH  of  5.8  indicated  that  we  probably  needed  to  add  more   lactic  acid  to  further  acidify  our  mash.    While  the  enzymes  still  seemed  to  function  properly   at  this  pH  given  the  successful  thirty  minute  saccharification,  it  must  be  later  considered   that  this  may  adversely  affect  our  final  product  based  on  inadequate  enzyme  activity.     Lautering/Sparging:   1. We  began  separating  our  wort  from  our  grain  bed  at  3:51pm.   2. We  sparged  with  36.0l  at  78.3°C  until  we  completed  lautering  at  4:30  pm.     Observations/Conclusions:   -­‐    Sparging  should  ideally  function  as  a  slow  rinsing  of  the  grains  with  warm  water  to   gather  any  residual  sugar  not  separated  by  the  original  draining  of  mash  rest  water.     However,  we  mistakenly  added  the  sparge  water  too  quickly  which  could  potentially  lead   to  lower  extraction  of  residual  sugars.    This  was  a  big  mistake  to  be  learned  from  and  not   made  again.    This  event  necessitated  the  need  to  keep  an  eye  out  for  a  lower  starting   gravity  than  expected.   -­‐    Our  change  in  mill  settings  previously  mentioned  didn’t  seem  to  negatively  impact  the   effectiveness  of  the  grain  husks  acting  as  a  filtration  bed,  there  were  no  problems  with  the   actual  separation  of  wort  from  grain  bed  process.     Boil:   1. At  4:33pm  we  reached  a  boil  with  a  pre-­‐boil  pH  of  5.6  and  gravity  of  9.7°  P.    As  the   boil  commenced,  we  added  11.0  grams  of  Merkur  hops  as  our  primary  bittering  hop   addition.   2. Forty-­‐five  minutes  later,  at  5:18pm,  we  performed  our  second  hop  addition  of  57.0   grams  of  Sterling  hops  contributing  both  bitterness  and  aroma.   3. At  5:23pm,  we  added  Whirlfloc  as  our  kettle  coagulant.   4. At  5:33pm,  another  39.0  grams  of  Sterling  hops  were  added  as  our  primary  aroma   hop  addition.    In  addition,  we  began  our  whirlpool  at  this  time  as  well  as  ended  our   boil.    At  the  end  of  boil  we  had  45  liters  of  boiled  wort  and  a  pH  of  5.59.    The   whirlpool  was  ended  at  5:43pm.  
  • 6.   Observations/Conclusions:   -­‐    As  previously  mentioned,  we  were  not  trying  to  produce  a  beer  with  a  prominent  hop   character  based  on  the  parameters  of  the  Kölsch  style.    However,  we  still  utilized  Merkur   hops,  whose  high  alpha  acid  content  (13.6%)  and  low  co-­‐humulone  content  contributed   mild  bitterness  via  isomerization  to  balance  the  light-­‐bodied  beer.    In  addition,  we  also   utilized  Sterling  hops,  which  lend  herbal,  spicy,  and  slightly  floral  and  citrusy  aromas  when   added  at  the  end  of  boil.    Not  only  were  we  attempting  to  correctly  match  the  Kölsch  style,   but  this  minimal  hop  character  beer  also  allowed  for  greater  focus  on  water  treatment  and   grain  analysis  and  selection,  the  major  topics  of  this  brew  in  particular.   -­‐    Whirlfloc  (an  Irish  moss/carrageenan  blend)  was  added  to  the  boil  in  order  to  assist  the   formation  of  hot  break  (in  addition  to  the  whirlpool)  by  precipitating  haze-­‐causing  proteins   and  beta-­‐glucans.    This  is  especially  desirable  in  a  Kölsch  where  clarity  is  an  important   parameter  of  the  style.     Knockout/Yeast  Pitch:   1. At  5:45pm  we  began  knockout  into  a  keg  at  14°C  using  oxygen  at  psi.       2. The  initial  gravity  of  our  wort  prior  to  fermentation  was  measured  to  be  11.3°  P.    We   decided  to  pitch  three  packages  of  German  Ale  Kölsch  Yeast  (WLP029)  due  to  the   fact  that  each  vial  of  yeast  contains  roughly  150  billion  cells  and  the  following   calculation,  1.5  million  cells  (lager  yeast)  x  45.4  l  x  11.3°  P  =  769,869,000,000  cells,   indicates  three  packages  is  close  enough  (450  billion  cells).     Observations/Conclusions:   -­‐    The  knockout  occurred  quickly  reducing  the  risk  of  aldehyde  and/or  dimethyl  sulfide   formation  in  the  wort.   -­‐    Our  initial  gravity  of  11.3°  P  (at  45.4  l)  was  lower  than  our  expected  gravity  of  12.140°  P   (at  40.0  l)  due  to  the  fact  that  our  actual  total  volume  was  also  higher  and  therefore  the   wort  and  its  fermentable  sugars  weren’t  as  condensed  as  expected.    In  addition,  our   accidental  rapid  sparging  also  may  have  contributed  to  this  lower  than  expected  initial   gravity.   -­‐    This  Kölsch  Ale  Yeast  was  ideal  for  our  beer  due  to  its  clean,  low-­‐ester  profile,  which  matched   our  quality  parameters  for  what  we  were  trying  to  brew.    The  yeast  strain  is  also  fittingly   attenuable  and  lends  to  the  fermentation  into  a  light-­‐bodied  beer.     Fermentation/Conditioning/Packaging:   Date:   Gravity:   Temperature   Step   2/11/15   11.3°P   14°C   Pitch   2/13/15   5.9°P   24°C   Fermentation   2/16/15   2.22°P   20°C   Fermentation   2/18/15   2.02°P   -­‐-­‐-­‐   Cold  Crash   2/27/15   2.02°P   -­‐-­‐-­‐   Racked     3/4/15   2.02°P   -­‐-­‐-­‐   Kegged  
  • 7.   Observations/Conclusions:   -­‐Fermentation  proceeded  rather  quickly,  which  came  as  a  bit  of  a  surprise  based  on  the   yeast  quantity  pitched.    Although  we  thought  three  packages  of  yeast  containing  a  total  of   450  billion  cells  (which  it  seemingly  was),  this  came  up  fairly  short  of  our  calculated  yeast   quantity  of  nearly  770  billion  cells  meaning  we  under  pitched.    This  could’ve  led  to  a  slow   or  even  uncompleted  fermentation  and  could’ve  also  stressed  the  yeast  leading  to  a   number  of  off  flavors  such  as  fusel  alcohols  and  undesirable  sulfurous  flavors.    Again,   although  it  seemed  fermentation  was  facilitated  with  ease  by  our  yeast  (based  on  time  and   our  actual  final  gravity  that  was  lower  than  our  theoretical  final  gravity)  at  this  point  we   still  out  to  be  mindful  of  potential  off  flavors  that  may  have  been  produced  during  this   fermentation.   -­‐    The  fermentation  temperature  fluctuated  quite  a  bit  likely  due  to  our  inability  to   temperature  control  the  brew  lab  during  winter  where  the  heat  was  being  turned  on  and   off.    Ideally  we  wanted  to  ferment  just  below  ale  temperatures  (roughly  14-­‐17°C),  but  we   ended  up  as  high  as  24°C.    While  this  shouldn’t  kill  off  the  yeast,  the  warmer  fermentation   may  lend  some  esters  to  our  beer  to  be  considered  when  sampling  our  final  product.   -­‐    We  kegged  this  beer  into  two  1/6  barrels  to  make  packaging  quicker  and  less  labor   intensive.    We  carbonated  it  in  the  cooler  for  6  days  at  16  psi  until  the  day  before  sensory   evaluation  in  which  we  increased  the  pressure  to  25  psi.     Sensory  Analysis  (Date:  3/11/15)     Visual:       • The  beer  was  light  yellow  as  a  result  of  the  light  (low  SRM)  malts  we  utilized.   • The  beer  was  slightly  opaque  indicating  slight  chill  haze  and  inadequate  reduction  of   proteins  or  beta-­‐glucans.   • The  beer  had  only  slight  head  retention,  which  comes  as  a  bit  of  surprise  based  on   our  use  of  high  alpha-­‐acid  hops  and  residual  protein  in  the  beer.      Perhaps  this   occurred  based  on  our  somewhat  low  protein  malt  bill  (white  wheat  malt  was  used   sparingly)  or  the  low  carbonation  of  the  beer.   • The  beer  also  had  decent  lacing  that  could’ve  been  affected  by  a  number  of  factors   such  as  hop  and  protein  content  or  the  cleanness  of  the  glass  being  sampled  from.     Aroma:   • The  beer  had  slight  fruit  esters  likely  due  to  fermentation  at  warmer  temperatures.     In  addition,  we  noted  a  pear,  apple  like  aroma,  which  is  indicative  of  acetaldehyde.     Normally,  the  presence  of  acetaldehyde  indicates  an  incomplete  fermentation,  but   this  seems  unlikely  due  to  the  high  attenuation  of  our  beer  and  resulting  lower  final   gravity  than  expected.    Perhaps  these  aromas  were  more  attributed  to  ester   production  during  fermentation.   • The  beer  had  slight  aromas  of  honey,  which  can  be  directly  attributed  to  our  use  of   Munich  malt.    There  were  also  some  bready  aromas  that  were  also  either   attributable  to  our  malt  selection  or  even  yeast.  
  • 8. • The  beer  had  some  slightly  floral  (geraniol)  and  grassy  hop  aromas,  which  can  be   directly  attributed  to  our  use  of  Sterling  aroma  hop  additions.     Flavor:   • The  beer  had  a  light  caramelly  maltiness,  which  can  be  attributed  to  our  use  of   Munich  malt.   • The  beer  also  had  slight  hop  bitterness  resulting  from  our  hop  additions,  especially   the  addition  of  Merkur.   • The  beer  had  a  slight  fruity  sweetness,  which  can  most  likely  be  attributed  to  ester   production  during  fermentation.    Perhaps  some  of  the  perception  of  sweetness  came   from  our  use  of  calcium  chloride.     Mouthfeel:   • The  beer  was  medium-­‐light  bodied  based  on  our  malt  selection,  attenuative   fermentation,  and  mash  temperature  choice  balancing  alpha  and  beta  amylase   enzymes.    Despite  a  slight  chill  haze,  there  was  low  overall  viscosity  due  to  low   protein  content  of  our  beer.   • The  beer  was  smooth,  coating,  clean,  and  balanced  based  on  our  water  treatment   with  calcium  chloride.   • The  beer  had  low  carbonation  thus  lacking  a  biting  bitterness,  which  ultimately  led   to  a  palatable  beer  with  greater  focus  on  flavor.     Overall:   • The  beer  met  BJCP  guidelines  to  a  tee  in  terms  of  appearance,  aroma,  flavor,  and   mouthfeel.    We  successfully  brewed  a  clean,  sessionable  Kölsch  that  was  medium-­‐ light  bodied,  had  low  esters,  low  hop  flavor,  and  slight  hop  bitterness.     Conclusion   -­‐    Based  on  our  water  treatment,  malt  analyses,  malt  selection,  and  other  brewing   parameters  aforementioned,  we  ultimately  came  pretty  close  to  completely  verifying  our   expectations  and  hypothesis.    We  produced  a  medium-­‐light  bodied  beer  based  on  our  use   of  calcium  chloride,  our  malt  selection,  and  mash  regimen.    The  beer  also  was  light  golden   in  color  and  had  bready  and  honey  malty  aromas  and  flavors,  all  of  which  can  be  directly   attributed  to  our  malt  selection.    In  addition,  the  beer  had  a  slight  sweetness  as  a  result  of   our  manipulation  of  body  and  use  of  calcium  chloride.    The  final  product  slightly  strayed   from  the  hypothesis  based  on  the  fact  that  esters  were  present  likely  as  a  result  of  warmer   fermentation  temperatures.    In  addition,  the  beer  had  a  slight  chill  haze  based  on  haze-­‐ forming  proteins  and  beta-­‐glucans,  which  wasn’t  expected  or  desired  based  on  Kölsch  style   guidelines.    Overall,  our  water  treatment  and  malt  selection  as  well  as  other,  less   emphasized  brewing  parameters,  contributed  to  an  ale  both  consistent  with  our  hypothesis   and  expectations  as  well  as  the  BJCP  guidelines.    The  brewing  of  this  beer  ultimately  proved   successful  despite  some  issues  (higher  mash  temperature,  too  quick  of  sparge,  non-­‐ temperature  controlled  fermentation)  based  on  the  fact  we  produced  a  drinkable,   sessionable  Kölsch  ale.