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Section	
  1	
  
	
  
Name:	
  	
  John	
  Schnettler	
  
Name	
  of	
  Brew:	
  	
  Study	
  Break	
  IPA	
  
Style	
  of	
  Brew:	
  	
  American	
  IPA	
  
Brew	
  Date:	
  	
  9/13/2014	
  
Bottling	
  Date:	
  10/3/2014	
  
Batch	
  Volume:	
  	
  40.00	
  l	
  (actual:	
  42.00	
  l)	
  
Original	
  Gravity:	
  	
  15.2°	
  P	
  
Final	
  Gravity:	
  	
  3.8°	
  P	
  
	
  
Calculation	
  #1	
  –	
  IBU’s	
  
	
  
37g	
  Columbus	
  (60	
  min):	
  	
  14.1°	
  Brix/1.04	
  =	
  13.558	
  Plato	
  	
  
SG	
  =	
  (4*13.558)/1000+1	
  =	
  1.054	
  
(37.00g	
  *0.135*0.221*1000)/49.2	
  l	
  =	
  22.437	
  IBU	
  
	
  
34g	
  Columbus	
  (45	
  min):	
  	
  14.1°	
  Brix/1.04	
  =	
  13.558	
  Plato	
  	
  
SG	
  =	
  (4*13.558)/1000+1	
  =	
  1.054	
  
(34.00g*0.135*0.171*1000)/49.2	
  l	
  =	
  15.953	
  IBU	
  
	
  
54g	
  Perle	
  (5	
  min):	
  	
  16.8°	
  Brix/1.04	
  =	
  16.154	
  Plato	
  
SG	
  =	
  (4*16.154)/1000+1	
  =	
  1.065	
  
(54.00g*0.092*0.073*1000)/45	
  l	
  =	
  8.059	
  IBU	
  
	
  
Total	
  IBU’s	
  =	
  22.437+15.953+8.059	
  =	
  46.449	
  IBU	
  
	
  
(I	
  chose	
  not	
  to	
  calculate	
  the	
  IBU’s	
  of	
  whirlpool	
  additions	
  despite	
  Beersmith’s	
  
calculations	
  of	
  the	
  5-­‐minute	
  whirlpool	
  additions	
  due	
  to	
  the	
  fact	
  that	
  the	
  hop	
  
utilization	
  chart	
  does	
  not	
  account	
  for	
  post-­‐boil	
  hop	
  additions)	
  
	
  
Calculation	
  #2	
  -­‐	
  %ABV	
  
	
  
(15.2°	
  Plato	
  –	
  3.8°	
  Plato)	
  *	
  0.516	
  =	
  5.88%	
  ABV	
  
	
  	
  
Calculation	
  #3	
  –	
  yeast	
  pitch	
  volume	
  
	
  
(15.2*106	
  mill/ml*	
  42	
  l)/1500*106	
  mill/ml	
  =	
  425.6	
  ml	
  
	
  
(Instructor	
  Jeff	
  Biegert	
  estimated	
  the	
  slurry	
  count)	
  
	
  
Calculation	
  #4	
  –	
  apparent	
  attenuation	
  
	
  
(15.2°	
  Plato	
  –	
  3.8°	
  Plato)/15.2°	
  Plato	
  =	
  75%	
  
	
  
	
  
Section	
  2	
  
	
  
Material	
  Bill	
  
	
  
Water	
  Additives:	
  
	
  
Ingredient	
   Amount	
   Step	
   Time	
  
Gypsum	
   20.00	
  g	
   Mash	
  	
   60	
  minutes	
  
Lactic	
  Acid	
   4.00	
  ml	
   Mash	
   60	
  minutes	
  
Epsom	
  Salt	
   1.50	
  g	
   Mash	
   60	
  minutes	
  
Salt	
   1.00	
  g	
   Mash	
   60	
  minutes	
  
	
  
Grist	
  Bill:	
  
	
  
Malt	
   Amount	
   Color	
  (European	
  Brewing	
  
Convention)	
  	
  
Colorado	
  Malting	
  Co.	
  	
  
2-­‐Row	
  
7.85	
  kg	
   2.3	
  EBC	
  
Vienna	
  Malt	
   3.55	
  kg	
   6.9	
  EBC	
  
Munich	
  Malt	
  –	
  10L	
   0.82	
  kg	
   19.7	
  EBC	
  
	
  
Hops:	
  
	
  
Hop	
  Varietal	
   Amount	
   Alpha-­‐Acid	
  
Content	
  
Step	
   Time	
  
Columbus	
   37.00	
  g	
   13.50%	
   Boil	
   60	
  minutes	
  
Columbus	
   34.00	
  g	
   13.50%	
   Boil	
   45	
  minutes	
  
Perle	
   54.00	
  g	
   9.20%	
   Boil	
   5	
  minutes	
  
Bravo	
   54.00	
  g	
   15.00%	
   Steep/Whirlpool	
   5	
  minutes	
  
Cascade	
   54.00	
  g	
   8.20%	
   Steep/Whirlpool	
   5	
  minutes	
  
Columbus	
   27.00	
  g	
   13.50%	
   Steep/Whirlpool	
   0	
  minutes	
  
Bravo	
   54.00	
  g	
   15.00%	
   Dry	
  Hop	
   2	
  days	
  
Columbus	
   54.00	
  g	
   13.50%	
   Dry	
  Hop	
   2	
  days	
  
Simcoe	
   54.00	
  g	
   15.00%	
   Dry	
  Hop	
   2	
  days	
  
	
  
Yeast:	
  	
  Odell	
  House	
  Yeast	
  
Other:	
  	
  Whirlfloc	
  (1	
  tablet)	
  
	
  
	
  
	
  
	
  
	
  
	
  
	
  
	
  
Equipment:	
  	
  	
  
A.	
  Gifford	
  Sabco	
  BrewMagic	
  Brewing	
  System:	
  
-­‐Hot	
  Liquor	
  Tank	
  (1/2	
  barrel	
  keg)	
  
-­‐Mash	
  Tun	
  (1/2	
  barrel	
  keg)	
  
-­‐Brew	
  Kettle	
  (`1/2	
  barrel	
  keg)	
  
-­‐Sabco	
  Pump	
  
-­‐Sabco	
  Frame	
  (V350MS	
  PLC,	
  USB	
  Port,	
  RTD	
  Sensor,	
  E-­‐Stop,	
  LP	
  Bottle	
  Rack,	
  3x	
  
Gas	
  Valves,	
  Locking	
  Front	
  Casters)	
  
B.	
  	
  Chill	
  Wizard	
  plate	
  chiller	
  
C.	
  	
  Chill	
  Wizard	
  pump	
  
D.	
  	
  Grain	
  mill	
  
E.	
  	
  Garden	
  hoses	
  
F.	
  	
  Food	
  grade	
  tri-­‐clamp	
  hoses	
  
G.	
  	
  Extension	
  cords	
  
H.	
  	
  Propane	
  tank	
  
I.	
  	
  	
  Oxygen	
  tank	
  with	
  tubing	
  and	
  filter	
  
J.	
  	
  	
  Metal	
  spoon	
  
K.	
  	
  Mash	
  thermometer	
  
L.	
  	
  Hot	
  gloves	
  
M.	
  Tool	
  bucket	
  
N.	
  	
  Iodophor	
  spray	
  bottle,	
  freshly	
  mixed	
  
O.	
  	
  Clean	
  rags	
  
P.	
  	
  Long	
  lighter	
  
Q.	
  	
  Box	
  of	
  extra	
  tri-­‐clamps	
  and	
  gaskets	
  
R.	
  	
  pH	
  meter	
  
S.	
  	
  Tub	
  for	
  spent	
  grain	
  
T.	
  	
  Kim-­‐wipes	
  
U.	
  	
  Refractometer	
  
V.	
  	
  Deionized	
  water	
  bottler	
  
W.	
  Hose	
  sprayer	
  nozzle	
  
X.	
  	
  	
  Slop	
  buckets	
  
Y.	
  	
  	
  PRONTO	
  cleaning	
  solution	
  
	
  
	
  
Procedure	
  
	
  
Pre-­‐Boil:	
  
	
  
9/12/2014	
  
1. We	
  measured	
  out	
  all	
  water	
  additives,	
  grains,	
  and	
  hops	
  and	
  used	
  the	
  grain	
  
mill	
  to	
  crush	
  all	
  grains	
  into	
  grist,	
  leaving	
  the	
  husk	
  still	
  intact.	
  	
  	
  
-­‐Colorado	
  Malting	
  Co.	
  2-­‐Row	
  malt	
  served	
  as	
  our	
  base	
  malt	
  and	
  primary	
  
source	
  of	
  fermentable	
  sugar.	
  	
  Vienna	
  malt	
  was	
  used	
  to	
  provide	
  
fermentable	
  sugars	
  and	
  coloring	
  and	
  Munich	
  malt	
  was	
  used	
  in	
  order	
  to	
  
add	
  sweetness	
  as	
  	
  	
  well	
  as	
  contribute	
  to	
  an	
  orange/golden	
  color.	
  	
  The	
  
grains	
  we	
  utilized	
  had	
  already	
  been	
  steeped,	
  germinated,	
  and	
  kilned	
  in	
  
order	
  to	
  develop	
  and	
  preserve	
  enzymes	
  for	
  the	
  mash	
  as	
  well	
  as	
  break	
  
down	
  grain	
  cell	
  walls	
  in	
  order	
  to	
  be	
  modified	
  for	
  an	
  effective	
  mash	
  and	
  
fermentation.	
  	
  In	
  addition,	
  the	
  kilning	
  process	
  affects	
  the	
  color	
  and	
  flavor	
  
of	
  the	
  grains.	
  	
  These	
  processes	
  constitute	
  the	
  malting	
  of	
  the	
  grain.	
  
-­‐We	
  used	
  Columbus	
  hops	
  for	
  bittering	
  due	
  to	
  the	
  fact	
  they	
  have	
  a	
  high	
  
alpha-­‐acid	
  content	
  of	
  13.5%.	
  	
  Alpha	
  acids	
  are	
  a	
  soft	
  resin	
  found	
  in	
  hops	
  
that	
  add	
  bitterness	
  to	
  the	
  beer	
  when	
  isomerized	
  during	
  the	
  boil.	
  	
  Perle	
  
hops,	
  normally	
  a	
  bittering	
  hop,	
  were	
  used	
  at	
  the	
  end	
  of	
  the	
  boil	
  to	
  
contribute	
  aroma.	
  	
  In	
  addition,	
  Bravo,	
  Cascade,	
  and	
  Columbus	
  hops	
  were	
  
used	
  post-­‐boil	
  during	
  whirlpool	
  to	
  contribute	
  a	
  variety	
  of	
  citrusy,	
  fruity	
  
and	
  floral	
  aromas	
  and	
  flavors	
  thanks	
  to	
  the	
  essential	
  oils	
  contained	
  within	
  
their	
  lupulin	
  glands.	
  	
  Finally,	
  Bravo,	
  Columbus,	
  and	
  Simcoe	
  hops	
  were	
  
used	
  for	
  two	
  days	
  of	
  dry	
  hopping	
  to	
  add	
  more	
  citrus,	
  pine,	
  and	
  aroma	
  
flavors	
  despite	
  their	
  high	
  alpha-­‐acid	
  contents.	
  
-­‐We	
  used	
  a	
  variety	
  of	
  water	
  additives	
  at	
  the	
  beginning	
  of	
  our	
  mash.	
  	
  We	
  
added	
  Gypsum	
  (calcium	
  sulphate)	
  in	
  order	
  to	
  increase	
  the	
  hardness	
  of	
  the	
  
water,	
  enhance	
  bitterness,	
  and	
  lower	
  pH.	
  	
  We	
  also	
  used	
  lactic	
  acid	
  in	
  
order	
  to	
  acidify	
  our	
  pH	
  to	
  the	
  5.3-­‐5.6	
  range	
  where	
  conversion	
  enzymes	
  
will	
  be	
  most	
  effective.	
  	
  Finally,	
  we	
  added	
  Epsom	
  Salt	
  (magnesium	
  
sulphate)	
  as	
  well	
  as	
  regular	
  salt	
  to	
  enhance	
  bitterness	
  and	
  slightly	
  lower	
  
pH.	
  	
  A	
  big	
  reason	
  for	
  using	
  several	
  pH-­‐lowering	
  additives	
  was	
  that	
  the	
  
lighter	
  malts	
  we	
  used	
  are	
  less	
  acidic.	
  
-­‐Grain	
  is	
  milled	
  in	
  order	
  to	
  reduce	
  and	
  control	
  the	
  size	
  of	
  the	
  grain	
  and	
  
break	
  up	
  the	
  endosperm	
  in	
  order	
  to	
  make	
  convertible	
  starches	
  more	
  
available	
  at	
  the	
  desired	
  extract	
  yield.	
  	
  	
  
	
  
9/13/2014	
  
1. The	
  teaching	
  assistants	
  cleaned	
  all	
  Sabco	
  brewing	
  system	
  equipment	
  and	
  
materials	
  thoroughly	
  using	
  Pronto	
  (0.5	
  cap	
  per	
  gallon	
  of	
  hot	
  water)	
  and	
  
rinse	
  with	
  hot	
  water.	
  
	
  	
  -­‐Cleaning	
  is	
  vital	
  in	
  removing	
  soil	
  and	
  a	
  majority	
  of	
  existing	
  
microorganisms	
  from	
  the	
  equipment	
  that	
  can	
  cause	
  inactivation	
  of	
  
sanitizer	
  and	
  potential	
  contamination	
  of	
  the	
  final	
  product.	
  
2. The	
  teaching	
  assistants	
  sanitized	
  all	
  equipment	
  and	
  materials	
  thoroughly	
  
using	
  Iodophor	
  and	
  cold	
  water.	
  
	
  	
  -­‐Iodophor	
  is	
  a	
  halogen	
  sanitizer	
  containing	
  surface-­‐active	
  agents	
  that	
  
inhibit	
  the	
  function	
  of	
  microbial	
  proteins	
  thus	
  removing	
  any	
  
microorganisms.	
  	
  Iodophor	
  does	
  not	
  require	
  rinsing	
  degrades	
  to	
  
flavorless,	
  odorless,	
  and	
  non-­‐toxic	
  compounds	
  which	
  volatize.	
  
3. We	
  started	
  by	
  heating	
  54	
  l	
  strike	
  in	
  the	
  hot	
  liquor	
  tank	
  and	
  34.9	
  l	
  of	
  strike	
  
water	
  in	
  the	
  mash	
  tun.	
  	
  In	
  addition,	
  we	
  began	
  heating	
  water	
  in	
  the	
  kettle	
  
to	
  be	
  used	
  in	
  sterilizing	
  the	
  plate	
  chiller.	
  
4. Once	
  the	
  mash	
  tun	
  water	
  reached	
  73.7°C,	
  we	
  added	
  the	
  culmination	
  of	
  
our	
  2-­‐Row,	
  Vienna,	
  and	
  Munich	
  malts	
  to	
  the	
  mash	
  tun	
  at	
  a	
  steady	
  rate	
  
while	
  simultaneously	
  stirring	
  to	
  avoid	
  clumping	
  of	
  grain,	
  which	
  can	
  
decrease	
  the	
  efficiency	
  of	
  the	
  mash	
  in	
  converting	
  starches	
  to	
  fermentable	
  
sugars.	
  	
  	
  We	
  also	
  added	
  our	
  20.00g	
  Gypsum,	
  4.0	
  ml	
  lactic	
  acid,	
  1.5g	
  of	
  
Epsom	
  salt,	
  and	
  1.00	
  g	
  of	
  salt	
  at	
  the	
  beginning	
  of	
  the	
  mash.	
  
	
  	
  -­‐We	
  utilized	
  a	
  downward	
  infusion	
  mash	
  consisting	
  of	
  an	
  insulated	
  mash	
  
tun	
  and	
  stainless	
  steel	
  false	
  bottom	
  allowing	
  for	
  effective	
  separation	
  of	
  
wort	
  from	
  grain	
  that	
  is	
  unstirred	
  and	
  facilitates	
  starch	
  conversion	
  at	
  a	
  
single	
  temperature.	
  	
  	
  
	
  	
  	
   	
  	
  -­‐The	
  mash-­‐in	
  occurred	
  at	
  9:16am	
  and	
  the	
  strike	
  water	
  brought	
  the	
  mash	
  
to	
  64.8°C	
  for	
  one	
  hour	
  which	
  we	
  closely	
  monitored.	
  	
  At	
  this	
  temperature,	
  
although	
  both	
  alpha	
  and	
  beta	
  amylase	
  enzymes	
  were	
  functioning,	
  beta-­‐
amylase	
  was	
  predominant	
  thus	
  creating	
  chemical	
  conditions	
  lending	
  to	
  a	
  
lower	
  extract	
  yield	
  but	
  higher	
  fermentability.	
  	
  This	
  higher	
  fermentability	
  
will	
  occur	
  based	
  on	
  beta-­‐amylase’s	
  creation	
  of	
  maltose	
  which	
  is	
  a	
  less	
  
complex	
  carbohydrate	
  and	
  thus	
  easier	
  to	
  break	
  down	
  during	
  
fermentation.	
  	
  This	
  lower	
  mash	
  temp	
  will	
  ultimately	
  contribute	
  to	
  a	
  drier	
  
beer.	
  
	
  	
  	
   	
  	
  -­‐We	
  took	
  a	
  pH	
  reading	
  during	
  the	
  mash	
  and	
  observed	
  a	
  pH	
  of	
  5.4,	
  a	
  great	
  
pH	
  for	
  amylase	
  to	
  effectively	
  function.	
  
5.	
   While	
  we	
  allowed	
  conversion	
  to	
  occur	
  in	
  our	
  mash	
  tun,	
  we	
  began	
  
sterilizing	
  our	
  plate	
  chiller	
  in	
  preparation	
  for	
  post-­‐boil.	
  
	
   	
  	
  -­‐The	
  plate	
  chiller	
  was	
  sterilized	
  by	
  running	
  hot	
  water	
  that	
  had	
  been	
  
heated	
  in	
  the	
  boil	
  kettle	
  to	
  temperatures	
  above	
  82°C.	
  	
  This	
  removed	
  all	
  
residue	
  and	
  microorganisms	
  in	
  order	
  to	
  avoid	
  contaminating	
  our	
  wort	
  
during	
  cooling	
  after	
  the	
  boil.	
  
	
  6.	
  	
  We	
  started	
  our	
  vorlauf	
  at	
  10:15am,	
  delaying	
  it	
  five	
  minutes	
  from	
  our	
  
desired	
  vorlauf	
  time.	
  	
  We	
  would	
  normally	
  allow	
  the	
  vorlauf	
  to	
  occur	
  for	
  
fifteen	
  minutes;	
  however,	
  we	
  extended	
  the	
  process	
  an	
  extra	
  five	
  minutes.	
  
	
   	
  	
  -­‐Vorlauf	
  is	
  the	
  German	
  word	
  for	
  “pre-­‐run”	
  and	
  is	
  utilized	
  in	
  brewing	
  to	
  
draw	
  off	
  and	
  recirculate	
  the	
  wort	
  throughout	
  the	
  mash	
  tun	
  without	
  
running	
  off	
  into	
  the	
  boil	
  kettle.	
  
	
   	
  	
  -­‐Vorlauf	
  is	
  important	
  in	
  clarifying	
  the	
  wort	
  being	
  drawn	
  out	
  of	
  the	
  mash	
  
tun	
  and	
  establishing	
  a	
  good	
  filtration	
  system	
  through	
  the	
  grain	
  bed.	
  	
  The	
  
first	
  runnings	
  will	
  appear	
  hazy	
  and	
  contain	
  some	
  milled	
  grain	
  particles	
  
but	
  will	
  eventually	
  clear	
  up.	
  
	
   	
  	
  -­‐We	
  delayed	
  the	
  vorlauf	
  due	
  to	
  the	
  fact	
  that	
  the	
  plate	
  chiller	
  was	
  leaking	
  
and	
  the	
  boil	
  kettle	
  hadn’t	
  fully	
  drained	
  due	
  to	
  the	
  fact	
  the	
  kettle	
  burner	
  
wasn’t	
  properly	
  working	
  so	
  we	
  wanted	
  to	
  be	
  sure	
  the	
  kettle	
  was	
  drained	
  
before	
  runoff.	
  	
  Because	
  the	
  kettle	
  burner	
  wasn’t	
  properly	
  working,	
  we	
  
changed	
  interchanged	
  the	
  kettle	
  burner	
  and	
  mash	
  tun	
  burner.	
  	
  
7.	
  	
  After	
  clarifying	
  our	
  wort,	
  we	
  began	
  our	
  runoff	
  into	
  the	
  boil	
  kettle	
  at	
  
10:37am.	
  	
  At	
  10:40am	
  we	
  began	
  sparging	
  using	
  31	
  l	
  of	
  water	
  at	
  78°C.	
  	
  
During	
  the	
  sparge,	
  we	
  made	
  sure	
  to	
  adjust	
  the	
  sparge	
  pump	
  so	
  that	
  the	
  
liquid	
  level	
  was	
  about	
  2-­‐3	
  cm	
  above	
  the	
  grain	
  level	
  in	
  order	
  to	
  ensure	
  a	
  
steady	
  rinsing	
  of	
  the	
  grains.	
  	
  While	
  we	
  ran	
  off	
  into	
  the	
  kettle,	
  we	
  
simultaneously	
  heated	
  the	
  boil	
  kettle	
  and	
  held	
  at	
  a	
  temperature	
  just	
  
before	
  boiling	
  in	
  order	
  to	
  be	
  able	
  to	
  begin	
  boiling	
  quickly	
  after	
  finishing	
  
runoff.	
  
  	
  	
  -­‐The	
  technical	
  term	
  for	
  the	
  runoff	
  is	
  lautering,	
  where	
  wort	
  is	
  separated	
  
from	
  grains.	
  	
  Our	
  mash	
  tun	
  also	
  acted	
  as	
  a	
  lauter	
  tun	
  due	
  to	
  the	
  fact	
  that	
  it	
  
has	
  a	
  false	
  bottom	
  that	
  effectively	
  filters	
  the	
  wort	
  without	
  letting	
  the	
  
grain	
  drain	
  off	
  in	
  to	
  the	
  kettle.	
  
	
   	
  	
  -­‐We	
  sparged	
  in	
  order	
  to	
  give	
  the	
  grain	
  an	
  extra	
  rinse	
  to	
  drain	
  off	
  any	
  
residual	
  fermentable	
  sugars	
  on	
  the	
  grain	
  bed	
  into	
  our	
  boil	
  kettle.	
  	
  To	
  
avoid	
  extracting	
  tannins	
  from	
  the	
  grains,	
  we	
  sparged	
  using	
  water	
  at	
  a	
  
temperature	
  that	
  wasn’t	
  too	
  hot,	
  avoided	
  over	
  sparging,	
  and	
  avoided	
  
sparging	
  above	
  a	
  pH	
  of	
  5.8.	
  
8.	
  	
  	
  We	
  finished	
  sparging	
  at	
  10:59am	
  and	
  ended	
  our	
  runoff	
  into	
  the	
  boil	
  kettle	
  
at	
  11:07am.	
  	
  Our	
  pre-­‐boil	
  volume	
  was	
  49.2	
  l	
  and	
  had	
  a	
  pre-­‐boil	
  gravity	
  
reading	
  of	
  14.1°	
  Brix	
  measured	
  using	
  a	
  refractometer.	
  
	
   	
  	
  -­‐Our	
  pH	
  just	
  prior	
  to	
  boiling	
  was	
  5.3,	
  indicating	
  we	
  had	
  a	
  good	
  acidity	
  
and	
  hadn’t	
  extracted	
  tannins	
  based	
  on	
  pH	
  during	
  the	
  sparge.	
  
	
   	
  	
  -­‐Our	
  actual	
  pre-­‐boil	
  volume	
  of	
  49.2	
  l	
  was	
  right	
  on	
  our	
  estimated	
  pre-­‐boil	
  
volume	
  of	
  49.21	
  l	
  and	
  our	
  actual	
  pre-­‐boil	
  gravity	
  of	
  14.1°	
  Brix	
  was	
  also	
  
very	
  close	
  to	
  our	
  estimated	
  pre-­‐boil	
  volume	
  of	
  14.411°	
  Plato	
  which	
  
converts	
  to	
  13.857°	
  Brix.	
  
	
   	
  	
  -­‐It	
  is	
  important	
  to	
  note	
  that	
  refractometers	
  are	
  fairly	
  inaccurate	
  when	
  
measuring	
  alcohol	
  and	
  typically	
  shouldn’t	
  be	
  used	
  for	
  beer.	
  	
  However,	
  we	
  
use	
  a	
  refractometer	
  anyway	
  to	
  obtain	
  a	
  rough	
  estimate	
  of	
  numerous	
  
gravity	
  measurements.	
  
	
   	
  	
  -­‐We	
  monitor	
  the	
  gravity	
  of	
  our	
  wort	
  throughout	
  the	
  brewing	
  process	
  
because	
  gravity	
  is	
  a	
  measurement	
  of	
  sugar	
  concentration	
  in	
  wort/beer,	
  
which	
  allows	
  us	
  to	
  know	
  the	
  fermentation	
  capacity	
  of	
  our	
  brew	
  and	
  how	
  
much	
  alcohol	
  will	
  ultimately	
  be	
  produced	
  during	
  fermentation.	
  
	
   -­‐We	
  also	
  made	
  the	
  decision	
  to	
  end	
  runoff	
  based	
  on	
  our	
  monitoring	
  of	
  the	
  
gravity	
  throughout	
  and	
  once	
  we	
  had	
  reached	
  our	
  estimated	
  pre-­‐boil	
  
gravity	
  we	
  ended	
  runoff.	
  
	
  
The	
  Boil:	
  
	
  
9/13/2014	
  (Same	
  day)	
  
1. We	
  began	
  our	
  boil	
  time	
  at	
  11:28am	
  after	
  achieving	
  a	
  rolling	
  boil.	
  	
  At	
  this	
  
time	
  we	
  momentarily	
  shut	
  off	
  the	
  burner	
  and	
  added	
  our	
  first	
  hop	
  
addition,	
  32.0	
  g	
  of	
  Columbus	
  hops,	
  which	
  would	
  last	
  the	
  duration	
  of	
  our	
  
sixty-­‐minute	
  boil.	
  
	
  	
  -­‐We	
  boil	
  our	
  wort	
  (unfermented	
  beer)	
  in	
  order	
  to	
  evaporate	
  water	
  thus	
  
concentrating	
  the	
  wort’s	
  fermentable	
  sugars,	
  boil	
  off	
  any	
  volatiles	
  such	
  as	
  
dimethyl	
  sulfide,	
  and	
  extract	
  bitterness	
  from	
  hops	
  via	
  isomerization.	
  	
  In	
  
addition,	
  boiling	
  wort	
  is	
  essential	
  in	
  stabilizing	
  the	
  wort	
  by	
  denaturing	
  
amylase	
  enzymes	
  from	
  mash	
  as	
  well	
  as	
  killing	
  any	
  microorganisms	
  
present	
  in	
  the	
  beer.	
  	
  Furthermore,	
  boiling	
  helps	
  to	
  react	
  simple	
  sugars	
  
with	
  amino	
  acids	
  to	
  form	
  melanoidins	
  and	
  flavor	
  compounds.	
  	
  Finally,	
  
boiling	
  denatures	
  proteins,	
  causing	
  the	
  formation	
  and	
  precipitation	
  of	
  
undesirable	
  protein-­‐polyphenol	
  complexes.	
  	
  
 	
  -­‐Hops	
  added	
  toward	
  the	
  beginning	
  of	
  the	
  boil	
  are	
  known	
  as	
  bittering	
  
hops	
  because	
  the	
  heat	
  of	
  the	
  boil	
  isomerizes	
  (changes	
  the	
  6-­‐carbon	
  ring	
  
to	
  a	
  5-­‐carbon	
  ring)	
  alpha-­‐acids	
  making	
  them	
  soluble	
  in	
  water	
  and	
  bitter	
  
when	
  they	
  were	
  previously	
  insoluble	
  in	
  water	
  prior	
  to	
  boiling.	
  	
  These	
  
alpha-­‐acids	
  are	
  soft	
  resins	
  known	
  as	
  humulones	
  found	
  within	
  the	
  lupulin	
  
glands	
  of	
  hops	
  along	
  with	
  essential	
  oils.	
  
	
  	
  -­‐When	
  adding	
  hops	
  to	
  the	
  boil	
  it	
  is	
  important	
  to	
  monitor	
  the	
  level	
  of	
  
liquid	
  in	
  the	
  kettle	
  in	
  order	
  to	
  avoid	
  a	
  boil	
  over.	
  	
  When	
  adding	
  ingredients	
  
to	
  the	
  Sabco	
  system	
  we	
  turned	
  off	
  the	
  burner	
  to	
  avoid	
  boil	
  over	
  and	
  also	
  
kept	
  a	
  hose	
  nearby	
  to	
  spray	
  any	
  erupting	
  wort.	
  
2. Fifteen	
  minutes	
  later,	
  at	
  11:43am,	
  we	
  added	
  our	
  second	
  hop	
  addition	
  of	
  
34.0	
  g	
  of	
  Columbus	
  hops	
  also	
  for	
  bittering	
  purposes.	
  	
  	
  
3. Thirty-­‐six	
  minutes	
  later,	
  at	
  12:19pm,	
  we	
  added	
  one	
  Whirlfloc	
  tablet	
  in	
  
order	
  to	
  help	
  clarify	
  the	
  wort	
  by	
  precipitating	
  proteins	
  and	
  beta	
  glucans	
  
that	
  contribute	
  haze	
  in	
  the	
  final	
  product.	
  
4. At	
  12:23pm,	
  we	
  added	
  54.00g	
  of	
  Perle	
  hops	
  with	
  five	
  minutes	
  left	
  to	
  boil.	
  	
  	
  
	
  	
  -­‐Although	
  Perle	
  hops	
  have	
  a	
  fairly	
  high	
  alpha	
  acid	
  content	
  and	
  still	
  
contribute	
  some	
  bitterness	
  to	
  the	
  beer	
  due	
  to	
  the	
  fact	
  they	
  are	
  being	
  
isomerized	
  with	
  heat,	
  their	
  primary	
  role	
  in	
  this	
  brew	
  was	
  to	
  contribute	
  
flavor	
  and	
  aroma	
  to	
  the	
  beer	
  based	
  on	
  their	
  short	
  boiling	
  time	
  of	
  five	
  
minutes.	
  	
  Perle	
  hops	
  are	
  known	
  for	
  contributing	
  slightly	
  spicy	
  and	
  minty	
  
flavors	
  and	
  aromas.	
  
5. At	
  12:28pm	
  we	
  turned	
  off	
  the	
  heat	
  ending	
  the	
  boil,	
  a	
  process	
  known	
  as	
  
flameout.	
  	
  Although	
  cleaning	
  and	
  sanitation	
  are	
  emphasized	
  throughout	
  
the	
  entire	
  brewing	
  process,	
  it	
  is	
  absolutely	
  vital	
  that	
  anything	
  that	
  comes	
  
in	
  contact	
  with	
  the	
  wort	
  from	
  this	
  point	
  forward	
  is	
  clean	
  and	
  sanitized	
  to	
  
avoid	
  contamination	
  due	
  to	
  the	
  fact	
  that	
  the	
  major	
  antibacterial	
  step,	
  the	
  
boil,	
  is	
  finished.	
  
	
  
Post	
  Boil:	
  
	
  
9/13/2014	
  (Same	
  day)	
  
1. After	
  turning	
  the	
  kettle	
  burner	
  off,	
  we	
  simultaneously	
  initiated	
  the	
  
whirlpool	
  and	
  prepared	
  the	
  Chill	
  Wizard	
  plate	
  chiller	
  for	
  knockout	
  at	
  
12:28pm.	
  	
  To	
  initiate	
  the	
  whirlpool,	
  we	
  used	
  a	
  clean	
  and	
  sanitized	
  spoon	
  
to	
  vigorously	
  stir	
  the	
  wort	
  into	
  centrifugal	
  motion.	
  	
  After	
  ten	
  minutes	
  of	
  
whirlpooling,	
  we	
  added	
  54.0g	
  of	
  Bravo	
  hops	
  and	
  54.0g	
  of	
  Cascade	
  hops	
  at	
  
12:38pm.	
  	
  	
  
-­‐The	
  purpose	
  of	
  the	
  whirlpool	
  is	
  to	
  collect	
  hop	
  residues	
  and	
  hot	
  break	
  
(denatured	
  protein-­‐polyphenol	
  complexes)	
  at	
  the	
  center	
  and	
  bottom	
  of	
  
the	
  kettle	
  via	
  centrifugal	
  motion.	
  	
  This	
  helps	
  to	
  clarify	
  the	
  wort	
  and	
  make	
  
it	
  easier	
  to	
  separate	
  from	
  the	
  trub	
  settled	
  at	
  the	
  bottom	
  of	
  the	
  kettle.	
  
-­‐Bravo	
  and	
  Cascade	
  hops	
  are	
  used	
  as	
  flavoring	
  and	
  aroma	
  hops	
  during	
  
the	
  whirlpool,	
  yet	
  still	
  impart	
  a	
  small	
  amount	
  of	
  bitterness	
  to	
  the	
  beer	
  due	
  
to	
  the	
  fact	
  the	
  wort	
  is	
  still	
  at	
  high	
  enough	
  temperatures	
  to	
  isomerize	
  
alpha-­‐acids.	
  	
  Bravo	
  hops	
  contribute	
  fruity	
  and	
  floral	
  aromas	
  and	
  flavors	
  
while	
  Cascade	
  hops	
  contribute	
  citrusy,	
  fruity,	
  floral,	
  and	
  spicy	
  aromas	
  and	
  
flavors.	
  
2. During	
  the	
  whirlpool,	
  we	
  prepared	
  for	
  knockout	
  (running	
  off	
  wort	
  into	
  
the	
  fermenter)	
  by	
  connecting	
  the	
  hose	
  to	
  the	
  cold	
  water	
  inlet	
  of	
  the	
  
sterilized	
  plate	
  chiller,	
  connecting	
  a	
  second	
  hose	
  to	
  the	
  warm	
  water	
  
outlet,	
  and	
  connecting	
  the	
  oxygen	
  tank	
  (set	
  to	
  5	
  psi	
  but	
  not	
  yet	
  turned	
  on)	
  
to	
  the	
  oxygen	
  inlet.	
  	
  In	
  addition,	
  we	
  measured	
  the	
  post-­‐boil	
  gravity	
  to	
  be	
  
16.8°	
  Brix,	
  the	
  post-­‐boil	
  pH	
  to	
  be	
  5.3,	
  and	
  the	
  post-­‐boil	
  volume	
  to	
  be	
  45	
  l.	
  
	
  	
  -­‐Our	
  estimated	
  post-­‐boil	
  gravity	
  was	
  16.433°	
  Plato.	
  	
  When	
  we	
  convert	
  or	
  
actual	
  gravity	
  to	
  Plato,	
  we	
  get	
  a	
  value	
  of	
  16.154°	
  Plato,	
  which	
  is	
  pretty	
  
close	
  to	
  our	
  estimated	
  gravity.	
  	
  In	
  addition,	
  our	
  estimated	
  post	
  boil	
  
volume	
  was	
  44.51	
  l,	
  which	
  was	
  also	
  very	
  close	
  to	
  our	
  actual	
  post-­‐boil	
  
volume.	
  
3. First,	
  we	
  connected	
  a	
  clean	
  and	
  sanitized	
  tri-­‐clamp	
  hose	
  from	
  the	
  kettle	
  to	
  
the	
  plate	
  chiller	
  and	
  a	
  clean	
  and	
  sanitized	
  tri-­‐clamp	
  hose	
  form	
  the	
  plate	
  
chiller	
  to	
  the	
  fermenter.	
  	
  Next,	
  we	
  turned	
  on	
  the	
  water	
  supply	
  facilitating	
  
cooling	
  of	
  the	
  wort	
  as	
  it	
  passed	
  through	
  the	
  chiller	
  into	
  the	
  fermenter.	
  	
  In	
  
addition,	
  we	
  opened	
  the	
  oxygen	
  tank	
  connected	
  to	
  the	
  chiller	
  to	
  facilitate	
  
a	
  steady	
  bubbling	
  and	
  aeration	
  of	
  the	
  wort.	
  	
  We	
  began	
  knockout	
  at	
  
12:46pm	
  by	
  opening	
  the	
  kettle	
  and	
  allowing	
  the	
  wort	
  to	
  pass	
  through	
  the	
  
chiller	
  system	
  and	
  into	
  the	
  fermenter.	
  	
  This	
  process	
  occurred	
  at	
  a	
  
temperature	
  of	
  23°C.	
  
-­‐Cooling	
  the	
  wort	
  to	
  approximately	
  16°	
  C	
  is	
  absolutely	
  vital	
  in	
  order	
  to	
  
provide	
  the	
  ale	
  yeast	
  we	
  were	
  using	
  the	
  proper	
  fermentation	
  
environment	
  in	
  terms	
  of	
  temperature.	
  	
  Both	
  ale	
  and	
  lager	
  yeast	
  will	
  not	
  
survive	
  if	
  pitched	
  into	
  non-­‐cooled	
  wort.	
  	
  The	
  wort	
  should	
  be	
  rapidly	
  
cooled	
  in	
  order	
  to	
  avoid	
  oxidation,	
  formation	
  of	
  sulfur	
  compounds,	
  
contamination,	
  and	
  also	
  in	
  order	
  to	
  form	
  the	
  cold	
  break	
  (trub	
  settled	
  out	
  
after	
  cooling).	
  
	
  	
  -­‐We	
  use	
  oxygen	
  to	
  aerate	
  the	
  wort	
  due	
  to	
  the	
  fact	
  that	
  yeast	
  need	
  oxygen	
  
in	
  the	
  lag	
  and	
  growth	
  phase	
  in	
  order	
  to	
  produce	
  lipids	
  and	
  ultimately	
  
grow	
  and	
  multiply.	
  	
  This	
  ensures	
  a	
  healthy,	
  steady	
  fermentation.	
  
	
  	
  -­‐Ideally,	
  we	
  want	
  to	
  cool	
  the	
  wort	
  to	
  16°	
  C,	
  however,	
  we	
  were	
  only	
  able	
  
to	
  get	
  our	
  heat	
  exchanger	
  down	
  to	
  a	
  temperature	
  of	
  23°	
  C.	
  	
  Therefore,	
  we	
  
planned	
  on	
  placing	
  the	
  fermenter	
  in	
  the	
  cooler	
  following	
  the	
  end	
  of	
  
knockout.	
  
4. Midway	
  through	
  knockout,	
  at	
  12:54	
  pm,	
  we	
  added	
  27.0g	
  of	
  Columbus	
  
hops	
  to	
  the	
  kettle.	
  
	
  	
  -­‐This	
  hop	
  addition	
  was	
  once	
  again	
  an	
  aroma	
  hop	
  addition,	
  which	
  did	
  not	
  
contribute	
  bitterness	
  due	
  to	
  the	
  fact	
  the	
  wort	
  was	
  cooling	
  and	
  
isomerization	
  of	
  alpha	
  acids	
  did	
  not	
  occur.	
  	
  Columbus	
  is	
  known	
  for	
  
contributing	
  citrusy,	
  spicy,	
  and	
  resiny	
  aroma	
  and	
  flavor	
  characteristics.	
  
5. At	
  1:07	
  pm,	
  we	
  finished	
  knockout	
  into	
  the	
  cylindroconical	
  fermenter.	
  	
  The	
  
rapid	
  chilling	
  of	
  the	
  wort	
  formed	
  a	
  cold	
  break	
  (trub	
  settled	
  out	
  after	
  
cooling),	
  which	
  we	
  drained	
  into	
  a	
  slop	
  bucket	
  and	
  discarded.	
  As	
  we	
  rolled	
  
the	
  fermenter	
  up	
  to	
  the	
  2nd	
  floor	
  Gifford	
  lab,	
  we	
  noticed	
  a	
  small	
  leak	
  in	
  the	
  
cylindroconical	
  vessel.	
  	
  In	
  response	
  cleaned	
  a	
  keg	
  style	
  fermenter	
  using	
  
pronto	
  and	
  sanitized	
  a	
  keg-­‐style	
  fermenter,	
  which	
  we	
  then	
  transferred	
  
our	
  cooled	
  wort	
  into.	
  	
  	
  
	
  	
  -­‐Our	
  post	
  boil	
  volume,	
  as	
  previously	
  noted,	
  was	
  measured	
  at	
  
approximately	
  45	
  l;	
  however,	
  after	
  transfer	
  and	
  cooling	
  we	
  measure	
  
approximately	
  42	
  l	
  of	
  cool	
  wort.	
  	
  This	
  discrepancy	
  likely	
  occurred	
  due	
  to	
  
formation	
  of	
  cold	
  break	
  as	
  well	
  as	
  losses	
  from	
  the	
  leaking	
  cylindroconical	
  
and/or	
  transferring	
  between	
  fermenters.	
  
	
  	
  -­‐Our	
  fermenter	
  after	
  cooling	
  was	
  at	
  21°C	
  and	
  therefore	
  we	
  put	
  the	
  keg-­‐
style	
  fermenter	
  into	
  the	
  cooler	
  after	
  slightly	
  pressurizing	
  with	
  oxygen	
  and	
  
brought	
  it	
  down	
  to	
  16°C,	
  our	
  desired	
  fermentation	
  temperature.	
  	
  
6. As	
  part	
  of	
  the	
  class	
  handled	
  transferring	
  between	
  fermenters,	
  we	
  also	
  
began	
  cleaning	
  the	
  Sabco	
  Brew	
  Magic	
  System	
  and	
  its	
  components.	
  	
  
	
  	
  -­‐To	
  clean	
  the	
  brew	
  system,	
  we	
  first	
  emptied	
  the	
  mash	
  tun	
  into	
  buckets	
  
that	
  we	
  dumped	
  into	
  Gifford’s	
  outdoor	
  compost.	
  	
  In	
  addition,	
  we	
  drained	
  
the	
  trub	
  from	
  the	
  boil	
  kettle	
  and	
  cleaned	
  manually	
  aka	
  cleaned	
  out	
  of	
  
place	
  (COP).	
  
	
  	
  -­‐Next,	
  we	
  cleaned	
  all	
  of	
  the	
  components	
  of	
  the	
  Brew	
  Magic	
  System	
  by	
  
utilizing	
  the	
  system’s	
  CIP	
  (clean-­‐in-­‐place)	
  loop.	
  	
  This	
  was	
  accomplished	
  
by	
  first	
  connecting	
  a	
  tri-­‐clamp	
  hose	
  between	
  the	
  mash	
  tun	
  inlet	
  and	
  chill	
  
wizard	
  outlet,	
  attaching	
  a	
  second	
  tri-­‐clamp	
  hose	
  to	
  the	
  chill-­‐wizard	
  outlet,	
  
and	
  placing	
  the	
  open	
  end	
  of	
  the	
  second	
  tri-­‐clamp	
  hose	
  into	
  a	
  slop	
  bucket.	
  	
  
Next,	
  we	
  filled	
  the	
  hot	
  liquor	
  tank	
  with	
  Pronto	
  cleaner	
  and	
  used	
  the	
  Sabco	
  
pump	
  to	
  propel	
  cleaning	
  solution	
  through	
  the	
  system	
  while	
  periodically	
  
venting	
  oxygen	
  in	
  the	
  chill	
  wizard	
  to	
  be	
  cleaned	
  as	
  well.	
  	
  After	
  the	
  water	
  
runs	
  clear	
  into	
  slop	
  buckets	
  from	
  both	
  the	
  hot	
  liquor	
  tank	
  and	
  mash	
  tun,	
  
we	
  emptied	
  any	
  remaining	
  water	
  in	
  both	
  vessels	
  into	
  the	
  slop	
  buckets.	
  
	
  	
  -­‐Following	
  cleaning,	
  we	
  rinsed	
  the	
  system	
  by	
  filling	
  the	
  mash	
  tun	
  with	
  
cold	
  water	
  and	
  circulating	
  throughout	
  the	
  system.	
  	
  Finally,	
  we	
  drained	
  all	
  
vessels	
  after	
  rinsing	
  and	
  brought	
  the	
  system	
  piece	
  by	
  piece	
  back	
  up	
  to	
  the	
  
2nd	
  floor	
  Gifford	
  lab.	
  
7. Once	
  our	
  fermenter	
  had	
  cooled	
  to	
  16°	
  C,	
  we	
  took	
  a	
  gravity	
  reading	
  using	
  a	
  
hydrometer	
  and	
  measured	
  a	
  gravity	
  of	
  15.2°	
  Plato.	
  	
  We	
  sanitized	
  the	
  
opening	
  of	
  our	
  fermenter	
  containing	
  42	
  l	
  cooled	
  wort	
  and	
  poured	
  290	
  ml	
  
of	
  Odell	
  house	
  yeast	
  slurry	
  into	
  the	
  fermenter	
  at	
  2:24pm	
  and	
  closed.	
  	
  We	
  
ran	
  a	
  blow	
  off	
  hose	
  from	
  the	
  fermenter	
  into	
  a	
  bucket	
  of	
  Iodophor.	
  
	
  	
  -­‐We	
  calculated	
  the	
  volume	
  of	
  yeast	
  to	
  be	
  pitched	
  as	
  425.6	
  ml;	
  however,	
  
we	
  only	
  had	
  290	
  ml	
  slurry	
  from	
  Odell.	
  	
  
	
  	
  	
  -­‐As	
  previously	
  mentioned,	
  cleaning	
  and	
  sanitation	
  is	
  vital	
  post	
  boil	
  
therefore	
  we	
  exercised	
  extreme	
  caution	
  when	
  handling	
  our	
  cooled	
  wort.	
  
	
  	
  -­‐We	
  use	
  a	
  blow	
  off	
  hose	
  to	
  allow	
  carbon	
  dioxide,	
  a	
  product	
  of	
  
fermentation,	
  to	
  escape	
  our	
  fermentation	
  vessel.	
  	
  We	
  placed	
  the	
  blow	
  off	
  
in	
  sanitizer	
  to	
  avoid	
  contamination	
  and	
  oxygen	
  from	
  entering	
  the	
  
fermenter.	
  
	
  	
  -­‐Our	
  estimated	
  batch	
  volume	
  was	
  40	
  l	
  according	
  to	
  Beersmith	
  whereas	
  
our	
  actual	
  batch	
  volume	
  in	
  the	
  fermenter	
  was	
  42	
  l.	
  	
  This	
  might	
  explain	
  
why	
  our	
  actual	
  original	
  gravity	
  of	
  15.2°	
  Plato	
  was	
  less	
  than	
  our	
  estimated	
  
original	
  gravity	
  of	
  16.433	
  Plato	
  because	
  our	
  actual	
  batch	
  volume	
  was	
  less	
  
concentrated	
  than	
  our	
  estimated	
  batch	
  volume.	
  	
  
8. After	
  pitching	
  the	
  yeast,	
  we	
  stored	
  the	
  fermenter	
  at	
  room	
  temperature	
  
until	
  it	
  was	
  time	
  to	
  cold	
  crash.	
  
-­‐During	
  storage	
  at	
  room	
  temperature,	
  the	
  yeast	
  we	
  pitched	
  were	
  in	
  an	
  
anaerobic	
  environment	
  which	
  facilitated	
  the	
  metabolism	
  of	
  sugars	
  
(primarily	
  maltose	
  and	
  maltotriose)	
  by	
  yeast	
  creating	
  ethanol,	
  carbon	
  
dioxide,	
  and	
  various	
  other	
  flavor	
  components/byproducts	
  in	
  a	
  process	
  
known	
  as	
  fermentation.	
  
9/19/2014	
  
1. Jeff	
  Biegert	
  informed	
  us	
  in	
  class	
  that	
  our	
  beer	
  was	
  at	
  a	
  gravity	
  of	
  7.2°	
  
Plato	
  and	
  therefore	
  we	
  hadn’t	
  finished	
  fermenting	
  based	
  on	
  our	
  
estimated	
  final	
  gravity	
  of	
  3.569	
  Plato.	
  	
  He	
  also	
  noticed	
  some	
  acetaldehyde	
  
in	
  the	
  beer,	
  which	
  is	
  to	
  be	
  expected	
  during	
  fermentation	
  due	
  to	
  the	
  fact	
  it	
  
is	
  a	
  fermentation	
  intermediate.	
  
	
  	
  -­‐Jeff	
  mentioned	
  the	
  beer	
  should’ve	
  fully	
  fermented	
  in	
  about	
  five	
  days.	
  	
  
However,	
  the	
  beer	
  was	
  not	
  fully	
  fermented	
  likely	
  due	
  to	
  the	
  fact	
  that	
  our	
  
volume	
  of	
  yeast	
  pitched	
  was	
  290	
  ml	
  instead	
  of	
  our	
  calculated	
  value	
  of	
  
425.6	
  ml	
  and	
  therefore	
  there	
  weren’t	
  enough	
  yeast	
  to	
  successfully	
  
metabolize	
  the	
  amount	
  of	
  fermentable	
  sugar	
  in	
  our	
  wort.	
  	
  In	
  addition,	
  the	
  
pitch	
  rate	
  could’ve	
  also	
  adversely	
  affected	
  our	
  speed	
  of	
  fermentation.	
  
	
  	
  -­‐We	
  pushed	
  back	
  our	
  dry	
  hop	
  until	
  the	
  beer	
  had	
  further	
  fermented.	
  
9/21/2014	
  
1. We	
  measured	
  our	
  gravity	
  as	
  4.6°	
  Plato	
  and	
  continued	
  fermenting.	
  
	
  
9/23/2014	
  
1. We	
  cold	
  crashed	
  our	
  beer	
  at	
  this	
  time	
  and	
  also	
  added	
  a	
  sanitary	
  mesh	
  hop	
  
bag	
  containing	
  54.0	
  g	
  of	
  Bravo	
  hops,	
  54.0	
  g	
  of	
  Columbus	
  hops,	
  and	
  54.0	
  g	
  
of	
  Simcoe	
  hops	
  for	
  our	
  two	
  day	
  dry	
  hop.	
  	
  These	
  processes	
  constitute	
  
secondary	
  fermentation.	
  
	
  	
  -­‐We	
  cold	
  crashed	
  our	
  beer	
  in	
  order	
  to	
  ultimately	
  clarify	
  our	
  beer.	
  	
  This	
  
occurs	
  due	
  to	
  the	
  fact	
  that	
  when	
  cold	
  crashed	
  at	
  near	
  freezing	
  
temperatures,	
  yeast	
  and	
  other	
  sediments	
  undesirable	
  in	
  the	
  final	
  product	
  
will	
  group	
  together	
  (flocculate)	
  and	
  fall	
  to	
  the	
  bottom	
  of	
  the	
  vessel.	
  	
  	
  
	
  	
  -­‐Dry	
  hopping	
  solely	
  contributes	
  flavor	
  and	
  aroma	
  to	
  beer	
  due	
  to	
  the	
  fact	
  
the	
  hops’	
  alpha	
  acids	
  are	
  not	
  being	
  isomerized	
  due	
  to	
  heat.	
  	
  The	
  dry	
  hop	
  
addition	
  added	
  a	
  variety	
  of	
  flavors	
  and	
  aromas	
  including	
  citrus,	
  pine,	
  
fruit,	
  floral,	
  and	
  spicy	
  notes.	
  	
  We	
  allowed	
  the	
  dry	
  hop	
  to	
  occur	
  for	
  two	
  
days	
  in	
  order	
  to	
  effectively	
  obtain	
  flavor	
  and	
  aroma	
  characteristics	
  
without	
  obtaining	
  the	
  grassy	
  flavors	
  commonly	
  associated	
  with	
  a	
  longer	
  
dry	
  hop.	
  
	
  
9/25/2014	
  
1. We	
  ended	
  cold	
  crash	
  on	
  this	
  day.	
  	
  New	
  Belgium	
  lab	
  analysis	
  from	
  
9/22/14	
  indicated	
  a	
  back	
  calculated	
  original	
  gravity	
  (BCOG)	
  of	
  15.17°	
  
Plato,	
  a	
  final	
  gravity	
  (FG)	
  of	
  3.67°	
  Plato,	
  19.3	
  EBC	
  (European	
  Brewing	
  
Convention:	
  measure	
  of	
  color),	
  and	
  6.26%	
  ABV.	
  	
  We	
  used	
  a	
  hydrometer	
  to	
  
observe	
  a	
  final	
  gravity	
  3.8°	
  Plato.	
  	
  	
  
-­‐The	
  lab	
  report	
  indicated	
  both	
  our	
  original	
  and	
  final	
  gravity	
  
measurements	
  using	
  a	
  hydrometer	
  were	
  fairly	
  accurate.	
  
2. We	
  cleaned	
  (using	
  Pronto)	
  and	
  sanitized	
  (using	
  Iodophor)	
  or	
  maturation	
  
keg	
  where	
  we	
  would	
  be	
  transferring	
  our	
  green	
  beer,	
  or	
  non-­‐matured	
  
fermented	
  beer.	
  
3. We	
  racked	
  from	
  our	
  keg-­‐style	
  fermenter	
  into	
  our	
  clean	
  and	
  sanitized	
  
maturation	
  keg	
  using	
  carbon	
  dioxide	
  to	
  transfer.	
  	
  Once	
  we	
  had	
  racked	
  
into	
  our	
  maturation	
  keg	
  we	
  returned	
  the	
  green	
  beer	
  to	
  the	
  cooler	
  to	
  be	
  
further	
  matured	
  and	
  stabilized.	
  
	
  
Packaging:	
  
	
  
10/3/2014	
  
1. Our	
  teaching	
  assistants	
  had	
  the	
  bottles	
  cleaned	
  and	
  sanitized	
  when	
  we	
  
showed	
  up	
  to	
  class	
  and	
  we	
  also	
  tossed	
  our	
  crowns	
  (bottle	
  caps)	
  into	
  
Iodophor	
  prior	
  to	
  bottling.	
  	
  With	
  all	
  of	
  our	
  equipment	
  cleaned	
  and	
  
sanitized	
  we	
  were	
  ready	
  to	
  bottle.	
  
2. Next,	
  we	
  added	
  200g	
  of	
  corn	
  sugar	
  for	
  the	
  40	
  l	
  of	
  beer	
  we	
  had	
  collected	
  in	
  
the	
  maturation	
  tank.	
  	
  Jeff	
  Biegert	
  calculated	
  this	
  amount	
  of	
  corn	
  sugar	
  
using	
  Beersmith,	
  which	
  he	
  mentioned	
  considered	
  a	
  wide	
  variety	
  of	
  
aspects	
  of	
  the	
  beer.	
  
	
  	
  -­‐We	
  used	
  corn	
  sugar	
  for	
  bottling	
  due	
  to	
  the	
  fact	
  that	
  it	
  is	
  a	
  simple	
  sugar	
  
(dextrose),	
  which	
  will	
  be	
  metabolized	
  for	
  a	
  “mini”	
  fermentation	
  within	
  
the	
  bottle.	
  	
  This	
  mini	
  fermentation	
  will	
  contribute	
  an	
  insignificant	
  amount	
  
of	
  ethanol	
  but	
  more	
  importantly	
  it	
  will	
  produce	
  carbon	
  dioxide,	
  thus	
  
carbonating	
  our	
  beer.	
  
	
  	
  	
  -­‐We	
  carbonate	
  beer	
  because	
  carbonation	
  is	
  very	
  important	
  in	
  
contributing	
  to	
  mouthfeel,	
  consistency	
  and	
  stability	
  of	
  the	
  foamy	
  head,	
  
and	
  overall	
  flavor.	
  
3. To	
  bottle,	
  we	
  connected	
  a	
  “beer	
  gun”	
  to	
  the	
  sankey	
  coupler	
  which	
  allows	
  
for	
  transfer	
  of	
  beer	
  out	
  of	
  a	
  keg.	
  	
  The	
  beer	
  gun	
  is	
  used	
  not	
  only	
  to	
  purge	
  
the	
  air	
  out	
  of	
  each	
  and	
  every	
  empty	
  bottle	
  to	
  avoid	
  oxygen	
  ending	
  up	
  in	
  
the	
  bottle	
  and	
  producing	
  off	
  flavors,	
  but	
  also	
  to	
  dispense	
  beer	
  filling	
  each	
  
and	
  every	
  bottle.	
  	
  The	
  beer	
  gun	
  displaces	
  the	
  amount	
  of	
  liquid	
  in	
  each	
  
bottle	
  so	
  that	
  there’s	
  about	
  an	
  inch	
  of	
  air	
  between	
  the	
  liquid	
  and	
  the	
  
crown.	
  	
  	
  
4. As	
  the	
  bottles	
  were	
  being	
  rinsed	
  using	
  the	
  bottle	
  cleaner	
  that	
  attaches	
  to	
  
the	
  sink	
  faucet	
  and	
  purged	
  and	
  filled	
  using	
  the	
  beer	
  gun,	
  we	
  
simultaneously	
  began	
  capping	
  each	
  bottle	
  using	
  the	
  sanitized	
  crowns	
  and	
  
a	
  bottle	
  capper.	
  
5. Finally,	
  we	
  stored	
  yield	
  of	
  approximately	
  three	
  and	
  a	
  half	
  cases	
  of	
  beer	
  at	
  
room	
  temperature	
  (a	
  favorable	
  temperature	
  for	
  residual	
  yeast)	
  and	
  
allowed	
  carbonation	
  to	
  occur	
  via	
  fermentation.	
  	
  We	
  tasted	
  our	
  first	
  
sample	
  of	
  finished	
  beer	
  on	
  October	
  16,	
  2014.	
  
	
  
Sensory	
  Evaluation	
  
	
  
	
   After	
  completing	
  tasting	
  and	
  a	
  BJCP	
  score	
  sheet	
  of	
  our	
  Study	
  Break	
  IPA	
  on	
  
10/16/2014,	
  my	
  total	
  score	
  for	
  our	
  brew	
  was	
  35/50.	
  	
  Here	
  was	
  the	
  breakdown:	
  
	
  
Aroma	
  (8/12):	
  
	
   -­‐The	
  combination	
  of	
  end	
  of	
  boil,	
  whirlpool,	
  and	
  dry	
  hop	
  additions	
  of	
  Perle,	
  
Bravo,	
  Cascade,	
  Columbus,	
  and	
  Simcoe	
  hops	
  provided	
  a	
  variety	
  of	
  pleasant	
  hop	
  
aromas	
  including	
  citrus,	
  pine,	
  fruity,	
  floral,	
  and	
  slightly	
  spicy	
  notes.	
  	
  There	
  were	
  also	
  
malty	
  sweet,	
  caramel	
  aromas	
  that	
  could’ve	
  been	
  attributed	
  to	
  our	
  Munich	
  malt	
  or	
  
perhaps	
  residual	
  priming	
  sugar	
  that	
  hadn’t	
  been	
  completely	
  metabolized	
  by	
  yeast	
  
(the	
  beer	
  wasn’t	
  fully	
  carbonated).	
  	
  There	
  were	
  slight	
  green-­‐apple	
  like	
  aromas	
  that	
  
were	
  likely	
  a	
  result	
  of	
  acetaldehyde.	
  	
  Although	
  the	
  acetaldehyde	
  aroma	
  was	
  slightly	
  
off-­‐putting,	
  it	
  is	
  fairly	
  normal	
  those	
  aromas	
  would	
  be	
  present	
  due	
  to	
  the	
  fact	
  that	
  
acetaldehyde	
  is	
  a	
  fermentation	
  intermediate	
  and	
  the	
  process	
  of	
  carbonation	
  is	
  in	
  
essence	
  a	
  “mini”	
  fermentation.	
  	
  Overall,	
  there	
  were	
  pleasant	
  hop	
  aromas	
  but	
  the	
  
sweet	
  malt	
  and	
  acetaldehyde	
  aromas	
  were	
  slightly	
  off	
  putting.	
  
	
  
Appearance	
  (2.5/3):	
  
	
   -­‐The	
  beer	
  had	
  a	
  nice	
  golden-­‐orange	
  and	
  slightly	
  copper	
  color	
  as	
  a	
  result	
  of	
  
the	
  combination	
  of	
  2-­‐row	
  malt	
  with	
  Vienna	
  and	
  Munich,	
  both	
  known	
  for	
  
contributing	
  an	
  orange	
  color	
  to	
  the	
  beer.	
  	
  In	
  addition,	
  the	
  beer	
  had	
  pretty	
  good	
  
clarity,	
  which	
  can	
  be	
  attributed	
  to	
  the	
  use	
  of	
  Whirlfloc,	
  whirlpooling,	
  formation	
  and	
  
separation	
  of	
  cold	
  break,	
  and	
  cold	
  crashing.	
  	
  The	
  beer	
  had	
  a	
  nice	
  thin,	
  lasting	
  head	
  
with	
  good	
  lacing.	
  	
  Overall,	
  the	
  finished	
  beer	
  had	
  a	
  great	
  appearance	
  but	
  could’ve	
  
benefited	
  from	
  further	
  clarity.	
  
	
  
Flavor	
  (14/20):	
  
	
   -­‐Again,	
  the	
  culmination	
  of	
  hop	
  additions	
  added	
  some	
  great	
  flavors.	
  	
  Early	
  
Columbus	
  additions	
  contributed	
  a	
  decent,	
  lasting	
  bitterness	
  and	
  the	
  numerous	
  
aroma	
  additions	
  during	
  the	
  boil,	
  whirlpool,	
  and	
  dry	
  hop	
  contributed	
  mostly	
  citrus	
  
and	
  pine	
  notes	
  with	
  some	
  slight	
  spiciness.	
  	
  The	
  malt	
  character	
  was	
  fairly	
  sweet	
  and	
  
had	
  hints	
  of	
  caramel	
  and	
  biscuit.	
  	
  The	
  aftertaste	
  was	
  bitter	
  with	
  malt	
  sweetness.	
  	
  
Fermentation	
  didn’t	
  seem	
  to	
  add	
  any	
  distinguishable	
  flavor	
  characteristics.	
  	
  Overall,	
  
the	
  hop	
  flavor	
  and	
  bitterness	
  of	
  this	
  beer	
  are	
  enjoyable;	
  however,	
  the	
  malty	
  
sweetness	
  seems	
  overpowering	
  and	
  takes	
  the	
  beer	
  out	
  of	
  balance.	
  	
  Again,	
  this	
  malty	
  
sweetness	
  is	
  subjective	
  to	
  my	
  palate	
  and	
  likely	
  a	
  result	
  of	
  either	
  Munich	
  malt	
  or	
  
residual	
  priming	
  sugar.	
  
	
  
Mouthfeel	
  (3.5/5):	
  
	
   The	
  beer	
  is	
  smooth	
  and	
  medium-­‐bodied.	
  	
  The	
  beer	
  is	
  barely	
  astringent	
  and	
  
may	
  just	
  be	
  a	
  result	
  of	
  hop	
  bitterness.	
  	
  Although	
  the	
  beer	
  had	
  a	
  thin,	
  decent	
  head,	
  a	
  
number	
  of	
  students	
  including	
  myself	
  perceived	
  it	
  as	
  slightly	
  flat.	
  	
  Overall,	
  the	
  
mouthfeel	
  is	
  decent	
  but	
  the	
  lack	
  of	
  full	
  carbonation	
  is	
  slightly	
  offputting.	
  
	
  
Overall	
  Impression	
  (7/10)	
  
	
   -­‐As	
  evident	
  by	
  my	
  overall	
  impressions	
  of	
  aroma,	
  appearance,	
  flavor,	
  and	
  
mouthfeel,	
  there	
  were	
  a	
  lot	
  of	
  enjoyable	
  characteristics	
  of	
  this	
  beer	
  including	
  hop	
  
aroma	
  and	
  flavor,	
  the	
  color,	
  clarity,	
  and	
  overall	
  appearance,	
  and	
  the	
  smooth,	
  
medium-­‐bodied	
  mouthfeel.	
  	
  However,	
  the	
  malty	
  sweetness	
  of	
  the	
  beer	
  was	
  fairly	
  off	
  
putting	
  in	
  terms	
  of	
  aroma	
  and	
  flavor.	
  	
  The	
  acetaldehyde	
  aroma	
  was	
  also	
  undesirable	
  
as	
  was	
  the	
  lack	
  of	
  full	
  carbonation.	
  	
  The	
  beer	
  could	
  be	
  improved	
  with	
  more	
  time	
  for	
  
bottle	
  conditioning	
  and	
  if	
  the	
  sweetness	
  doesn’t	
  mellow	
  out	
  perhaps	
  adjusting	
  the	
  
grain	
  bill	
  to	
  have	
  less	
  residual	
  sweetness.	
  	
  Overall,	
  our	
  first	
  attempt	
  at	
  the	
  Study	
  
Break	
  IPA	
  was	
  a	
  decent	
  beer	
  but	
  not	
  outstanding.	
  
	
  
Reflection	
  of	
  Results	
  
	
  
	
   Although	
  we	
  ran	
  into	
  a	
  few	
  problems	
  throughout	
  our	
  brewing	
  process,	
  we	
  
ultimately	
  had	
  a	
  fairly	
  smooth	
  experience	
  brewing	
  the	
  Study	
  Break	
  IPA.	
  	
  One	
  of	
  our	
  
first	
  mistakes	
  was	
  spilling	
  about	
  a	
  handful	
  of	
  grain	
  during	
  the	
  milling	
  process,	
  which	
  
we	
  replaced	
  with	
  roughly	
  the	
  same	
  amount.	
  	
  In	
  addition,	
  as	
  previously	
  mentioned,	
  
we	
  had	
  some	
  equipment	
  difficulties	
  such	
  as	
  a	
  faulty	
  kettle	
  burner	
  and	
  leaking	
  
cylindroconical	
  fermenter.	
  	
  We	
  dealt	
  with	
  these	
  issues	
  by	
  swapping	
  the	
  kettle	
  
burner	
  with	
  the	
  mash	
  tun	
  burner	
  and	
  transferring	
  our	
  cooled	
  wort	
  in	
  the	
  
cylindroconical	
  into	
  a	
  new,	
  keg-­‐style	
  fermenter.	
  	
  We	
  also	
  experienced	
  a	
  longer	
  than	
  
expected	
  fermentation	
  which	
  was	
  likely	
  a	
  result	
  of	
  having	
  too	
  small	
  a	
  volume	
  of	
  
yeast	
  to	
  pitch.	
  	
  Other	
  than	
  these	
  minor	
  issues	
  than	
  we	
  were	
  able	
  to	
  easily	
  resolve,	
  
the	
  brewing	
  experience	
  went	
  well.	
  	
  We	
  had	
  no	
  trouble	
  milling,	
  mashing,	
  sparging	
  or	
  
boiling,	
  little	
  to	
  no	
  trouble	
  with	
  fermentation,	
  maturation,	
  or	
  packaging,	
  and	
  our	
  
finished	
  beer	
  came	
  out	
  pretty	
  good.	
  
	
   Another	
  positive	
  aspect	
  of	
  our	
  brewing	
  experience	
  was	
  the	
  fact	
  that	
  our	
  
Beersmith	
  estimated,	
  actual,	
  calculated,	
  and	
  New	
  Belgium	
  lab	
  tested	
  measurements	
  
and	
  values	
  were	
  all	
  fairly	
  consistent.	
  	
  Our	
  estimated	
  and	
  actual	
  pre-­‐boil	
  gravity	
  and	
  
volumes,	
  post-­‐boil	
  gravity	
  and	
  volumes,	
  and	
  overall	
  batch	
  volume	
  and	
  gravity	
  were	
  
all	
  fairly	
  consistent.	
  	
  There	
  were	
  some	
  minor	
  discrepancies	
  between	
  estimated,	
  
calculated,	
  and	
  actual	
  ABV	
  and	
  IBUs	
  but	
  these	
  were	
  likely	
  the	
  result	
  of	
  minor	
  
differences	
  in	
  gravities	
  and	
  volumes	
  of	
  each	
  step.	
  	
  Overall,	
  we	
  yielded	
  consistent	
  
results	
  based	
  on	
  our	
  Beersmith	
  estimations	
  and	
  actual	
  results	
  indicating	
  that	
  we	
  
were	
  efficient	
  in	
  our	
  brewing	
  processes.	
  
	
   As	
  mentioned	
  previously	
  in	
  the	
  sensory	
  evaluation,	
  our	
  beer	
  was	
  almost	
  spot	
  
on	
  with	
  the	
  BJCP	
  style	
  guidelines	
  for	
  an	
  American	
  IPA.	
  	
  We	
  produced	
  an	
  orange-­‐
gold,	
  smooth,	
  medium-­‐bodied	
  ale	
  which	
  had	
  great	
  hoppy	
  flavors	
  and	
  aromas	
  
including	
  citrus,	
  fruit,	
  pine,	
  floral,	
  and	
  slightly	
  spicy	
  characteristics	
  with	
  a	
  lasting	
  
bitterness.	
  	
  The	
  only	
  changes	
  I	
  would	
  make	
  to	
  the	
  beer	
  next	
  time	
  would	
  be	
  to	
  adjust	
  
the	
  overly	
  sweet	
  malt	
  backbone	
  which	
  I	
  believe	
  negatively	
  affects	
  the	
  balance	
  of	
  the	
  
beer,	
  make	
  sure	
  the	
  beer	
  is	
  fully	
  carbonated	
  (some	
  class	
  members’	
  samples	
  were,	
  
some	
  weren’t,	
  may	
  have	
  been	
  an	
  issue	
  of	
  fully	
  homogenizing	
  the	
  priming	
  sugar	
  in	
  
the	
  maturation	
  keg),	
  and	
  allow	
  the	
  acetaldehyde	
  to	
  be	
  fully	
  converted	
  to	
  its	
  
negligible	
  form.	
  	
  In	
  conclusion,	
  we	
  had	
  a	
  great,	
  relatively	
  problem-­‐free	
  first	
  brewing	
  
experience	
  brewing	
  the	
  Study	
  Break	
  IPA	
  in	
  which	
  we	
  learned	
  a	
  great	
  deal	
  and	
  
ultimately	
  created	
  a	
  quality	
  final	
  product.	
  
	
   	
  
	
  
	
  
	
  
	
  
	
  
	
  
	
  
	
  
	
  
	
  
	
  
	
  

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Brew Lab #1

  • 1. Section  1     Name:    John  Schnettler   Name  of  Brew:    Study  Break  IPA   Style  of  Brew:    American  IPA   Brew  Date:    9/13/2014   Bottling  Date:  10/3/2014   Batch  Volume:    40.00  l  (actual:  42.00  l)   Original  Gravity:    15.2°  P   Final  Gravity:    3.8°  P     Calculation  #1  –  IBU’s     37g  Columbus  (60  min):    14.1°  Brix/1.04  =  13.558  Plato     SG  =  (4*13.558)/1000+1  =  1.054   (37.00g  *0.135*0.221*1000)/49.2  l  =  22.437  IBU     34g  Columbus  (45  min):    14.1°  Brix/1.04  =  13.558  Plato     SG  =  (4*13.558)/1000+1  =  1.054   (34.00g*0.135*0.171*1000)/49.2  l  =  15.953  IBU     54g  Perle  (5  min):    16.8°  Brix/1.04  =  16.154  Plato   SG  =  (4*16.154)/1000+1  =  1.065   (54.00g*0.092*0.073*1000)/45  l  =  8.059  IBU     Total  IBU’s  =  22.437+15.953+8.059  =  46.449  IBU     (I  chose  not  to  calculate  the  IBU’s  of  whirlpool  additions  despite  Beersmith’s   calculations  of  the  5-­‐minute  whirlpool  additions  due  to  the  fact  that  the  hop   utilization  chart  does  not  account  for  post-­‐boil  hop  additions)     Calculation  #2  -­‐  %ABV     (15.2°  Plato  –  3.8°  Plato)  *  0.516  =  5.88%  ABV       Calculation  #3  –  yeast  pitch  volume     (15.2*106  mill/ml*  42  l)/1500*106  mill/ml  =  425.6  ml     (Instructor  Jeff  Biegert  estimated  the  slurry  count)     Calculation  #4  –  apparent  attenuation     (15.2°  Plato  –  3.8°  Plato)/15.2°  Plato  =  75%      
  • 2. Section  2     Material  Bill     Water  Additives:     Ingredient   Amount   Step   Time   Gypsum   20.00  g   Mash     60  minutes   Lactic  Acid   4.00  ml   Mash   60  minutes   Epsom  Salt   1.50  g   Mash   60  minutes   Salt   1.00  g   Mash   60  minutes     Grist  Bill:     Malt   Amount   Color  (European  Brewing   Convention)     Colorado  Malting  Co.     2-­‐Row   7.85  kg   2.3  EBC   Vienna  Malt   3.55  kg   6.9  EBC   Munich  Malt  –  10L   0.82  kg   19.7  EBC     Hops:     Hop  Varietal   Amount   Alpha-­‐Acid   Content   Step   Time   Columbus   37.00  g   13.50%   Boil   60  minutes   Columbus   34.00  g   13.50%   Boil   45  minutes   Perle   54.00  g   9.20%   Boil   5  minutes   Bravo   54.00  g   15.00%   Steep/Whirlpool   5  minutes   Cascade   54.00  g   8.20%   Steep/Whirlpool   5  minutes   Columbus   27.00  g   13.50%   Steep/Whirlpool   0  minutes   Bravo   54.00  g   15.00%   Dry  Hop   2  days   Columbus   54.00  g   13.50%   Dry  Hop   2  days   Simcoe   54.00  g   15.00%   Dry  Hop   2  days     Yeast:    Odell  House  Yeast   Other:    Whirlfloc  (1  tablet)                  
  • 3. Equipment:       A.  Gifford  Sabco  BrewMagic  Brewing  System:   -­‐Hot  Liquor  Tank  (1/2  barrel  keg)   -­‐Mash  Tun  (1/2  barrel  keg)   -­‐Brew  Kettle  (`1/2  barrel  keg)   -­‐Sabco  Pump   -­‐Sabco  Frame  (V350MS  PLC,  USB  Port,  RTD  Sensor,  E-­‐Stop,  LP  Bottle  Rack,  3x   Gas  Valves,  Locking  Front  Casters)   B.    Chill  Wizard  plate  chiller   C.    Chill  Wizard  pump   D.    Grain  mill   E.    Garden  hoses   F.    Food  grade  tri-­‐clamp  hoses   G.    Extension  cords   H.    Propane  tank   I.      Oxygen  tank  with  tubing  and  filter   J.      Metal  spoon   K.    Mash  thermometer   L.    Hot  gloves   M.  Tool  bucket   N.    Iodophor  spray  bottle,  freshly  mixed   O.    Clean  rags   P.    Long  lighter   Q.    Box  of  extra  tri-­‐clamps  and  gaskets   R.    pH  meter   S.    Tub  for  spent  grain   T.    Kim-­‐wipes   U.    Refractometer   V.    Deionized  water  bottler   W.  Hose  sprayer  nozzle   X.      Slop  buckets   Y.      PRONTO  cleaning  solution       Procedure     Pre-­‐Boil:     9/12/2014   1. We  measured  out  all  water  additives,  grains,  and  hops  and  used  the  grain   mill  to  crush  all  grains  into  grist,  leaving  the  husk  still  intact.       -­‐Colorado  Malting  Co.  2-­‐Row  malt  served  as  our  base  malt  and  primary   source  of  fermentable  sugar.    Vienna  malt  was  used  to  provide   fermentable  sugars  and  coloring  and  Munich  malt  was  used  in  order  to   add  sweetness  as      well  as  contribute  to  an  orange/golden  color.    The   grains  we  utilized  had  already  been  steeped,  germinated,  and  kilned  in  
  • 4. order  to  develop  and  preserve  enzymes  for  the  mash  as  well  as  break   down  grain  cell  walls  in  order  to  be  modified  for  an  effective  mash  and   fermentation.    In  addition,  the  kilning  process  affects  the  color  and  flavor   of  the  grains.    These  processes  constitute  the  malting  of  the  grain.   -­‐We  used  Columbus  hops  for  bittering  due  to  the  fact  they  have  a  high   alpha-­‐acid  content  of  13.5%.    Alpha  acids  are  a  soft  resin  found  in  hops   that  add  bitterness  to  the  beer  when  isomerized  during  the  boil.    Perle   hops,  normally  a  bittering  hop,  were  used  at  the  end  of  the  boil  to   contribute  aroma.    In  addition,  Bravo,  Cascade,  and  Columbus  hops  were   used  post-­‐boil  during  whirlpool  to  contribute  a  variety  of  citrusy,  fruity   and  floral  aromas  and  flavors  thanks  to  the  essential  oils  contained  within   their  lupulin  glands.    Finally,  Bravo,  Columbus,  and  Simcoe  hops  were   used  for  two  days  of  dry  hopping  to  add  more  citrus,  pine,  and  aroma   flavors  despite  their  high  alpha-­‐acid  contents.   -­‐We  used  a  variety  of  water  additives  at  the  beginning  of  our  mash.    We   added  Gypsum  (calcium  sulphate)  in  order  to  increase  the  hardness  of  the   water,  enhance  bitterness,  and  lower  pH.    We  also  used  lactic  acid  in   order  to  acidify  our  pH  to  the  5.3-­‐5.6  range  where  conversion  enzymes   will  be  most  effective.    Finally,  we  added  Epsom  Salt  (magnesium   sulphate)  as  well  as  regular  salt  to  enhance  bitterness  and  slightly  lower   pH.    A  big  reason  for  using  several  pH-­‐lowering  additives  was  that  the   lighter  malts  we  used  are  less  acidic.   -­‐Grain  is  milled  in  order  to  reduce  and  control  the  size  of  the  grain  and   break  up  the  endosperm  in  order  to  make  convertible  starches  more   available  at  the  desired  extract  yield.         9/13/2014   1. The  teaching  assistants  cleaned  all  Sabco  brewing  system  equipment  and   materials  thoroughly  using  Pronto  (0.5  cap  per  gallon  of  hot  water)  and   rinse  with  hot  water.      -­‐Cleaning  is  vital  in  removing  soil  and  a  majority  of  existing   microorganisms  from  the  equipment  that  can  cause  inactivation  of   sanitizer  and  potential  contamination  of  the  final  product.   2. The  teaching  assistants  sanitized  all  equipment  and  materials  thoroughly   using  Iodophor  and  cold  water.      -­‐Iodophor  is  a  halogen  sanitizer  containing  surface-­‐active  agents  that   inhibit  the  function  of  microbial  proteins  thus  removing  any   microorganisms.    Iodophor  does  not  require  rinsing  degrades  to   flavorless,  odorless,  and  non-­‐toxic  compounds  which  volatize.   3. We  started  by  heating  54  l  strike  in  the  hot  liquor  tank  and  34.9  l  of  strike   water  in  the  mash  tun.    In  addition,  we  began  heating  water  in  the  kettle   to  be  used  in  sterilizing  the  plate  chiller.   4. Once  the  mash  tun  water  reached  73.7°C,  we  added  the  culmination  of   our  2-­‐Row,  Vienna,  and  Munich  malts  to  the  mash  tun  at  a  steady  rate   while  simultaneously  stirring  to  avoid  clumping  of  grain,  which  can   decrease  the  efficiency  of  the  mash  in  converting  starches  to  fermentable  
  • 5. sugars.      We  also  added  our  20.00g  Gypsum,  4.0  ml  lactic  acid,  1.5g  of   Epsom  salt,  and  1.00  g  of  salt  at  the  beginning  of  the  mash.      -­‐We  utilized  a  downward  infusion  mash  consisting  of  an  insulated  mash   tun  and  stainless  steel  false  bottom  allowing  for  effective  separation  of   wort  from  grain  that  is  unstirred  and  facilitates  starch  conversion  at  a   single  temperature.                -­‐The  mash-­‐in  occurred  at  9:16am  and  the  strike  water  brought  the  mash   to  64.8°C  for  one  hour  which  we  closely  monitored.    At  this  temperature,   although  both  alpha  and  beta  amylase  enzymes  were  functioning,  beta-­‐ amylase  was  predominant  thus  creating  chemical  conditions  lending  to  a   lower  extract  yield  but  higher  fermentability.    This  higher  fermentability   will  occur  based  on  beta-­‐amylase’s  creation  of  maltose  which  is  a  less   complex  carbohydrate  and  thus  easier  to  break  down  during   fermentation.    This  lower  mash  temp  will  ultimately  contribute  to  a  drier   beer.            -­‐We  took  a  pH  reading  during  the  mash  and  observed  a  pH  of  5.4,  a  great   pH  for  amylase  to  effectively  function.   5.   While  we  allowed  conversion  to  occur  in  our  mash  tun,  we  began   sterilizing  our  plate  chiller  in  preparation  for  post-­‐boil.        -­‐The  plate  chiller  was  sterilized  by  running  hot  water  that  had  been   heated  in  the  boil  kettle  to  temperatures  above  82°C.    This  removed  all   residue  and  microorganisms  in  order  to  avoid  contaminating  our  wort   during  cooling  after  the  boil.    6.    We  started  our  vorlauf  at  10:15am,  delaying  it  five  minutes  from  our   desired  vorlauf  time.    We  would  normally  allow  the  vorlauf  to  occur  for   fifteen  minutes;  however,  we  extended  the  process  an  extra  five  minutes.        -­‐Vorlauf  is  the  German  word  for  “pre-­‐run”  and  is  utilized  in  brewing  to   draw  off  and  recirculate  the  wort  throughout  the  mash  tun  without   running  off  into  the  boil  kettle.        -­‐Vorlauf  is  important  in  clarifying  the  wort  being  drawn  out  of  the  mash   tun  and  establishing  a  good  filtration  system  through  the  grain  bed.    The   first  runnings  will  appear  hazy  and  contain  some  milled  grain  particles   but  will  eventually  clear  up.        -­‐We  delayed  the  vorlauf  due  to  the  fact  that  the  plate  chiller  was  leaking   and  the  boil  kettle  hadn’t  fully  drained  due  to  the  fact  the  kettle  burner   wasn’t  properly  working  so  we  wanted  to  be  sure  the  kettle  was  drained   before  runoff.    Because  the  kettle  burner  wasn’t  properly  working,  we   changed  interchanged  the  kettle  burner  and  mash  tun  burner.     7.    After  clarifying  our  wort,  we  began  our  runoff  into  the  boil  kettle  at   10:37am.    At  10:40am  we  began  sparging  using  31  l  of  water  at  78°C.     During  the  sparge,  we  made  sure  to  adjust  the  sparge  pump  so  that  the   liquid  level  was  about  2-­‐3  cm  above  the  grain  level  in  order  to  ensure  a   steady  rinsing  of  the  grains.    While  we  ran  off  into  the  kettle,  we   simultaneously  heated  the  boil  kettle  and  held  at  a  temperature  just   before  boiling  in  order  to  be  able  to  begin  boiling  quickly  after  finishing   runoff.  
  • 6.      -­‐The  technical  term  for  the  runoff  is  lautering,  where  wort  is  separated   from  grains.    Our  mash  tun  also  acted  as  a  lauter  tun  due  to  the  fact  that  it   has  a  false  bottom  that  effectively  filters  the  wort  without  letting  the   grain  drain  off  in  to  the  kettle.        -­‐We  sparged  in  order  to  give  the  grain  an  extra  rinse  to  drain  off  any   residual  fermentable  sugars  on  the  grain  bed  into  our  boil  kettle.    To   avoid  extracting  tannins  from  the  grains,  we  sparged  using  water  at  a   temperature  that  wasn’t  too  hot,  avoided  over  sparging,  and  avoided   sparging  above  a  pH  of  5.8.   8.      We  finished  sparging  at  10:59am  and  ended  our  runoff  into  the  boil  kettle   at  11:07am.    Our  pre-­‐boil  volume  was  49.2  l  and  had  a  pre-­‐boil  gravity   reading  of  14.1°  Brix  measured  using  a  refractometer.        -­‐Our  pH  just  prior  to  boiling  was  5.3,  indicating  we  had  a  good  acidity   and  hadn’t  extracted  tannins  based  on  pH  during  the  sparge.        -­‐Our  actual  pre-­‐boil  volume  of  49.2  l  was  right  on  our  estimated  pre-­‐boil   volume  of  49.21  l  and  our  actual  pre-­‐boil  gravity  of  14.1°  Brix  was  also   very  close  to  our  estimated  pre-­‐boil  volume  of  14.411°  Plato  which   converts  to  13.857°  Brix.        -­‐It  is  important  to  note  that  refractometers  are  fairly  inaccurate  when   measuring  alcohol  and  typically  shouldn’t  be  used  for  beer.    However,  we   use  a  refractometer  anyway  to  obtain  a  rough  estimate  of  numerous   gravity  measurements.        -­‐We  monitor  the  gravity  of  our  wort  throughout  the  brewing  process   because  gravity  is  a  measurement  of  sugar  concentration  in  wort/beer,   which  allows  us  to  know  the  fermentation  capacity  of  our  brew  and  how   much  alcohol  will  ultimately  be  produced  during  fermentation.     -­‐We  also  made  the  decision  to  end  runoff  based  on  our  monitoring  of  the   gravity  throughout  and  once  we  had  reached  our  estimated  pre-­‐boil   gravity  we  ended  runoff.     The  Boil:     9/13/2014  (Same  day)   1. We  began  our  boil  time  at  11:28am  after  achieving  a  rolling  boil.    At  this   time  we  momentarily  shut  off  the  burner  and  added  our  first  hop   addition,  32.0  g  of  Columbus  hops,  which  would  last  the  duration  of  our   sixty-­‐minute  boil.      -­‐We  boil  our  wort  (unfermented  beer)  in  order  to  evaporate  water  thus   concentrating  the  wort’s  fermentable  sugars,  boil  off  any  volatiles  such  as   dimethyl  sulfide,  and  extract  bitterness  from  hops  via  isomerization.    In   addition,  boiling  wort  is  essential  in  stabilizing  the  wort  by  denaturing   amylase  enzymes  from  mash  as  well  as  killing  any  microorganisms   present  in  the  beer.    Furthermore,  boiling  helps  to  react  simple  sugars   with  amino  acids  to  form  melanoidins  and  flavor  compounds.    Finally,   boiling  denatures  proteins,  causing  the  formation  and  precipitation  of   undesirable  protein-­‐polyphenol  complexes.    
  • 7.    -­‐Hops  added  toward  the  beginning  of  the  boil  are  known  as  bittering   hops  because  the  heat  of  the  boil  isomerizes  (changes  the  6-­‐carbon  ring   to  a  5-­‐carbon  ring)  alpha-­‐acids  making  them  soluble  in  water  and  bitter   when  they  were  previously  insoluble  in  water  prior  to  boiling.    These   alpha-­‐acids  are  soft  resins  known  as  humulones  found  within  the  lupulin   glands  of  hops  along  with  essential  oils.      -­‐When  adding  hops  to  the  boil  it  is  important  to  monitor  the  level  of   liquid  in  the  kettle  in  order  to  avoid  a  boil  over.    When  adding  ingredients   to  the  Sabco  system  we  turned  off  the  burner  to  avoid  boil  over  and  also   kept  a  hose  nearby  to  spray  any  erupting  wort.   2. Fifteen  minutes  later,  at  11:43am,  we  added  our  second  hop  addition  of   34.0  g  of  Columbus  hops  also  for  bittering  purposes.       3. Thirty-­‐six  minutes  later,  at  12:19pm,  we  added  one  Whirlfloc  tablet  in   order  to  help  clarify  the  wort  by  precipitating  proteins  and  beta  glucans   that  contribute  haze  in  the  final  product.   4. At  12:23pm,  we  added  54.00g  of  Perle  hops  with  five  minutes  left  to  boil.          -­‐Although  Perle  hops  have  a  fairly  high  alpha  acid  content  and  still   contribute  some  bitterness  to  the  beer  due  to  the  fact  they  are  being   isomerized  with  heat,  their  primary  role  in  this  brew  was  to  contribute   flavor  and  aroma  to  the  beer  based  on  their  short  boiling  time  of  five   minutes.    Perle  hops  are  known  for  contributing  slightly  spicy  and  minty   flavors  and  aromas.   5. At  12:28pm  we  turned  off  the  heat  ending  the  boil,  a  process  known  as   flameout.    Although  cleaning  and  sanitation  are  emphasized  throughout   the  entire  brewing  process,  it  is  absolutely  vital  that  anything  that  comes   in  contact  with  the  wort  from  this  point  forward  is  clean  and  sanitized  to   avoid  contamination  due  to  the  fact  that  the  major  antibacterial  step,  the   boil,  is  finished.     Post  Boil:     9/13/2014  (Same  day)   1. After  turning  the  kettle  burner  off,  we  simultaneously  initiated  the   whirlpool  and  prepared  the  Chill  Wizard  plate  chiller  for  knockout  at   12:28pm.    To  initiate  the  whirlpool,  we  used  a  clean  and  sanitized  spoon   to  vigorously  stir  the  wort  into  centrifugal  motion.    After  ten  minutes  of   whirlpooling,  we  added  54.0g  of  Bravo  hops  and  54.0g  of  Cascade  hops  at   12:38pm.       -­‐The  purpose  of  the  whirlpool  is  to  collect  hop  residues  and  hot  break   (denatured  protein-­‐polyphenol  complexes)  at  the  center  and  bottom  of   the  kettle  via  centrifugal  motion.    This  helps  to  clarify  the  wort  and  make   it  easier  to  separate  from  the  trub  settled  at  the  bottom  of  the  kettle.   -­‐Bravo  and  Cascade  hops  are  used  as  flavoring  and  aroma  hops  during   the  whirlpool,  yet  still  impart  a  small  amount  of  bitterness  to  the  beer  due   to  the  fact  the  wort  is  still  at  high  enough  temperatures  to  isomerize   alpha-­‐acids.    Bravo  hops  contribute  fruity  and  floral  aromas  and  flavors  
  • 8. while  Cascade  hops  contribute  citrusy,  fruity,  floral,  and  spicy  aromas  and   flavors.   2. During  the  whirlpool,  we  prepared  for  knockout  (running  off  wort  into   the  fermenter)  by  connecting  the  hose  to  the  cold  water  inlet  of  the   sterilized  plate  chiller,  connecting  a  second  hose  to  the  warm  water   outlet,  and  connecting  the  oxygen  tank  (set  to  5  psi  but  not  yet  turned  on)   to  the  oxygen  inlet.    In  addition,  we  measured  the  post-­‐boil  gravity  to  be   16.8°  Brix,  the  post-­‐boil  pH  to  be  5.3,  and  the  post-­‐boil  volume  to  be  45  l.      -­‐Our  estimated  post-­‐boil  gravity  was  16.433°  Plato.    When  we  convert  or   actual  gravity  to  Plato,  we  get  a  value  of  16.154°  Plato,  which  is  pretty   close  to  our  estimated  gravity.    In  addition,  our  estimated  post  boil   volume  was  44.51  l,  which  was  also  very  close  to  our  actual  post-­‐boil   volume.   3. First,  we  connected  a  clean  and  sanitized  tri-­‐clamp  hose  from  the  kettle  to   the  plate  chiller  and  a  clean  and  sanitized  tri-­‐clamp  hose  form  the  plate   chiller  to  the  fermenter.    Next,  we  turned  on  the  water  supply  facilitating   cooling  of  the  wort  as  it  passed  through  the  chiller  into  the  fermenter.    In   addition,  we  opened  the  oxygen  tank  connected  to  the  chiller  to  facilitate   a  steady  bubbling  and  aeration  of  the  wort.    We  began  knockout  at   12:46pm  by  opening  the  kettle  and  allowing  the  wort  to  pass  through  the   chiller  system  and  into  the  fermenter.    This  process  occurred  at  a   temperature  of  23°C.   -­‐Cooling  the  wort  to  approximately  16°  C  is  absolutely  vital  in  order  to   provide  the  ale  yeast  we  were  using  the  proper  fermentation   environment  in  terms  of  temperature.    Both  ale  and  lager  yeast  will  not   survive  if  pitched  into  non-­‐cooled  wort.    The  wort  should  be  rapidly   cooled  in  order  to  avoid  oxidation,  formation  of  sulfur  compounds,   contamination,  and  also  in  order  to  form  the  cold  break  (trub  settled  out   after  cooling).      -­‐We  use  oxygen  to  aerate  the  wort  due  to  the  fact  that  yeast  need  oxygen   in  the  lag  and  growth  phase  in  order  to  produce  lipids  and  ultimately   grow  and  multiply.    This  ensures  a  healthy,  steady  fermentation.      -­‐Ideally,  we  want  to  cool  the  wort  to  16°  C,  however,  we  were  only  able   to  get  our  heat  exchanger  down  to  a  temperature  of  23°  C.    Therefore,  we   planned  on  placing  the  fermenter  in  the  cooler  following  the  end  of   knockout.   4. Midway  through  knockout,  at  12:54  pm,  we  added  27.0g  of  Columbus   hops  to  the  kettle.      -­‐This  hop  addition  was  once  again  an  aroma  hop  addition,  which  did  not   contribute  bitterness  due  to  the  fact  the  wort  was  cooling  and   isomerization  of  alpha  acids  did  not  occur.    Columbus  is  known  for   contributing  citrusy,  spicy,  and  resiny  aroma  and  flavor  characteristics.   5. At  1:07  pm,  we  finished  knockout  into  the  cylindroconical  fermenter.    The   rapid  chilling  of  the  wort  formed  a  cold  break  (trub  settled  out  after   cooling),  which  we  drained  into  a  slop  bucket  and  discarded.  As  we  rolled   the  fermenter  up  to  the  2nd  floor  Gifford  lab,  we  noticed  a  small  leak  in  the  
  • 9. cylindroconical  vessel.    In  response  cleaned  a  keg  style  fermenter  using   pronto  and  sanitized  a  keg-­‐style  fermenter,  which  we  then  transferred   our  cooled  wort  into.          -­‐Our  post  boil  volume,  as  previously  noted,  was  measured  at   approximately  45  l;  however,  after  transfer  and  cooling  we  measure   approximately  42  l  of  cool  wort.    This  discrepancy  likely  occurred  due  to   formation  of  cold  break  as  well  as  losses  from  the  leaking  cylindroconical   and/or  transferring  between  fermenters.      -­‐Our  fermenter  after  cooling  was  at  21°C  and  therefore  we  put  the  keg-­‐ style  fermenter  into  the  cooler  after  slightly  pressurizing  with  oxygen  and   brought  it  down  to  16°C,  our  desired  fermentation  temperature.     6. As  part  of  the  class  handled  transferring  between  fermenters,  we  also   began  cleaning  the  Sabco  Brew  Magic  System  and  its  components.        -­‐To  clean  the  brew  system,  we  first  emptied  the  mash  tun  into  buckets   that  we  dumped  into  Gifford’s  outdoor  compost.    In  addition,  we  drained   the  trub  from  the  boil  kettle  and  cleaned  manually  aka  cleaned  out  of   place  (COP).      -­‐Next,  we  cleaned  all  of  the  components  of  the  Brew  Magic  System  by   utilizing  the  system’s  CIP  (clean-­‐in-­‐place)  loop.    This  was  accomplished   by  first  connecting  a  tri-­‐clamp  hose  between  the  mash  tun  inlet  and  chill   wizard  outlet,  attaching  a  second  tri-­‐clamp  hose  to  the  chill-­‐wizard  outlet,   and  placing  the  open  end  of  the  second  tri-­‐clamp  hose  into  a  slop  bucket.     Next,  we  filled  the  hot  liquor  tank  with  Pronto  cleaner  and  used  the  Sabco   pump  to  propel  cleaning  solution  through  the  system  while  periodically   venting  oxygen  in  the  chill  wizard  to  be  cleaned  as  well.    After  the  water   runs  clear  into  slop  buckets  from  both  the  hot  liquor  tank  and  mash  tun,   we  emptied  any  remaining  water  in  both  vessels  into  the  slop  buckets.      -­‐Following  cleaning,  we  rinsed  the  system  by  filling  the  mash  tun  with   cold  water  and  circulating  throughout  the  system.    Finally,  we  drained  all   vessels  after  rinsing  and  brought  the  system  piece  by  piece  back  up  to  the   2nd  floor  Gifford  lab.   7. Once  our  fermenter  had  cooled  to  16°  C,  we  took  a  gravity  reading  using  a   hydrometer  and  measured  a  gravity  of  15.2°  Plato.    We  sanitized  the   opening  of  our  fermenter  containing  42  l  cooled  wort  and  poured  290  ml   of  Odell  house  yeast  slurry  into  the  fermenter  at  2:24pm  and  closed.    We   ran  a  blow  off  hose  from  the  fermenter  into  a  bucket  of  Iodophor.      -­‐We  calculated  the  volume  of  yeast  to  be  pitched  as  425.6  ml;  however,   we  only  had  290  ml  slurry  from  Odell.          -­‐As  previously  mentioned,  cleaning  and  sanitation  is  vital  post  boil   therefore  we  exercised  extreme  caution  when  handling  our  cooled  wort.      -­‐We  use  a  blow  off  hose  to  allow  carbon  dioxide,  a  product  of   fermentation,  to  escape  our  fermentation  vessel.    We  placed  the  blow  off   in  sanitizer  to  avoid  contamination  and  oxygen  from  entering  the   fermenter.      -­‐Our  estimated  batch  volume  was  40  l  according  to  Beersmith  whereas   our  actual  batch  volume  in  the  fermenter  was  42  l.    This  might  explain  
  • 10. why  our  actual  original  gravity  of  15.2°  Plato  was  less  than  our  estimated   original  gravity  of  16.433  Plato  because  our  actual  batch  volume  was  less   concentrated  than  our  estimated  batch  volume.     8. After  pitching  the  yeast,  we  stored  the  fermenter  at  room  temperature   until  it  was  time  to  cold  crash.   -­‐During  storage  at  room  temperature,  the  yeast  we  pitched  were  in  an   anaerobic  environment  which  facilitated  the  metabolism  of  sugars   (primarily  maltose  and  maltotriose)  by  yeast  creating  ethanol,  carbon   dioxide,  and  various  other  flavor  components/byproducts  in  a  process   known  as  fermentation.   9/19/2014   1. Jeff  Biegert  informed  us  in  class  that  our  beer  was  at  a  gravity  of  7.2°   Plato  and  therefore  we  hadn’t  finished  fermenting  based  on  our   estimated  final  gravity  of  3.569  Plato.    He  also  noticed  some  acetaldehyde   in  the  beer,  which  is  to  be  expected  during  fermentation  due  to  the  fact  it   is  a  fermentation  intermediate.      -­‐Jeff  mentioned  the  beer  should’ve  fully  fermented  in  about  five  days.     However,  the  beer  was  not  fully  fermented  likely  due  to  the  fact  that  our   volume  of  yeast  pitched  was  290  ml  instead  of  our  calculated  value  of   425.6  ml  and  therefore  there  weren’t  enough  yeast  to  successfully   metabolize  the  amount  of  fermentable  sugar  in  our  wort.    In  addition,  the   pitch  rate  could’ve  also  adversely  affected  our  speed  of  fermentation.      -­‐We  pushed  back  our  dry  hop  until  the  beer  had  further  fermented.   9/21/2014   1. We  measured  our  gravity  as  4.6°  Plato  and  continued  fermenting.     9/23/2014   1. We  cold  crashed  our  beer  at  this  time  and  also  added  a  sanitary  mesh  hop   bag  containing  54.0  g  of  Bravo  hops,  54.0  g  of  Columbus  hops,  and  54.0  g   of  Simcoe  hops  for  our  two  day  dry  hop.    These  processes  constitute   secondary  fermentation.      -­‐We  cold  crashed  our  beer  in  order  to  ultimately  clarify  our  beer.    This   occurs  due  to  the  fact  that  when  cold  crashed  at  near  freezing   temperatures,  yeast  and  other  sediments  undesirable  in  the  final  product   will  group  together  (flocculate)  and  fall  to  the  bottom  of  the  vessel.          -­‐Dry  hopping  solely  contributes  flavor  and  aroma  to  beer  due  to  the  fact   the  hops’  alpha  acids  are  not  being  isomerized  due  to  heat.    The  dry  hop   addition  added  a  variety  of  flavors  and  aromas  including  citrus,  pine,   fruit,  floral,  and  spicy  notes.    We  allowed  the  dry  hop  to  occur  for  two   days  in  order  to  effectively  obtain  flavor  and  aroma  characteristics   without  obtaining  the  grassy  flavors  commonly  associated  with  a  longer   dry  hop.     9/25/2014   1. We  ended  cold  crash  on  this  day.    New  Belgium  lab  analysis  from   9/22/14  indicated  a  back  calculated  original  gravity  (BCOG)  of  15.17°  
  • 11. Plato,  a  final  gravity  (FG)  of  3.67°  Plato,  19.3  EBC  (European  Brewing   Convention:  measure  of  color),  and  6.26%  ABV.    We  used  a  hydrometer  to   observe  a  final  gravity  3.8°  Plato.       -­‐The  lab  report  indicated  both  our  original  and  final  gravity   measurements  using  a  hydrometer  were  fairly  accurate.   2. We  cleaned  (using  Pronto)  and  sanitized  (using  Iodophor)  or  maturation   keg  where  we  would  be  transferring  our  green  beer,  or  non-­‐matured   fermented  beer.   3. We  racked  from  our  keg-­‐style  fermenter  into  our  clean  and  sanitized   maturation  keg  using  carbon  dioxide  to  transfer.    Once  we  had  racked   into  our  maturation  keg  we  returned  the  green  beer  to  the  cooler  to  be   further  matured  and  stabilized.     Packaging:     10/3/2014   1. Our  teaching  assistants  had  the  bottles  cleaned  and  sanitized  when  we   showed  up  to  class  and  we  also  tossed  our  crowns  (bottle  caps)  into   Iodophor  prior  to  bottling.    With  all  of  our  equipment  cleaned  and   sanitized  we  were  ready  to  bottle.   2. Next,  we  added  200g  of  corn  sugar  for  the  40  l  of  beer  we  had  collected  in   the  maturation  tank.    Jeff  Biegert  calculated  this  amount  of  corn  sugar   using  Beersmith,  which  he  mentioned  considered  a  wide  variety  of   aspects  of  the  beer.      -­‐We  used  corn  sugar  for  bottling  due  to  the  fact  that  it  is  a  simple  sugar   (dextrose),  which  will  be  metabolized  for  a  “mini”  fermentation  within   the  bottle.    This  mini  fermentation  will  contribute  an  insignificant  amount   of  ethanol  but  more  importantly  it  will  produce  carbon  dioxide,  thus   carbonating  our  beer.        -­‐We  carbonate  beer  because  carbonation  is  very  important  in   contributing  to  mouthfeel,  consistency  and  stability  of  the  foamy  head,   and  overall  flavor.   3. To  bottle,  we  connected  a  “beer  gun”  to  the  sankey  coupler  which  allows   for  transfer  of  beer  out  of  a  keg.    The  beer  gun  is  used  not  only  to  purge   the  air  out  of  each  and  every  empty  bottle  to  avoid  oxygen  ending  up  in   the  bottle  and  producing  off  flavors,  but  also  to  dispense  beer  filling  each   and  every  bottle.    The  beer  gun  displaces  the  amount  of  liquid  in  each   bottle  so  that  there’s  about  an  inch  of  air  between  the  liquid  and  the   crown.       4. As  the  bottles  were  being  rinsed  using  the  bottle  cleaner  that  attaches  to   the  sink  faucet  and  purged  and  filled  using  the  beer  gun,  we   simultaneously  began  capping  each  bottle  using  the  sanitized  crowns  and   a  bottle  capper.   5. Finally,  we  stored  yield  of  approximately  three  and  a  half  cases  of  beer  at   room  temperature  (a  favorable  temperature  for  residual  yeast)  and  
  • 12. allowed  carbonation  to  occur  via  fermentation.    We  tasted  our  first   sample  of  finished  beer  on  October  16,  2014.     Sensory  Evaluation       After  completing  tasting  and  a  BJCP  score  sheet  of  our  Study  Break  IPA  on   10/16/2014,  my  total  score  for  our  brew  was  35/50.    Here  was  the  breakdown:     Aroma  (8/12):     -­‐The  combination  of  end  of  boil,  whirlpool,  and  dry  hop  additions  of  Perle,   Bravo,  Cascade,  Columbus,  and  Simcoe  hops  provided  a  variety  of  pleasant  hop   aromas  including  citrus,  pine,  fruity,  floral,  and  slightly  spicy  notes.    There  were  also   malty  sweet,  caramel  aromas  that  could’ve  been  attributed  to  our  Munich  malt  or   perhaps  residual  priming  sugar  that  hadn’t  been  completely  metabolized  by  yeast   (the  beer  wasn’t  fully  carbonated).    There  were  slight  green-­‐apple  like  aromas  that   were  likely  a  result  of  acetaldehyde.    Although  the  acetaldehyde  aroma  was  slightly   off-­‐putting,  it  is  fairly  normal  those  aromas  would  be  present  due  to  the  fact  that   acetaldehyde  is  a  fermentation  intermediate  and  the  process  of  carbonation  is  in   essence  a  “mini”  fermentation.    Overall,  there  were  pleasant  hop  aromas  but  the   sweet  malt  and  acetaldehyde  aromas  were  slightly  off  putting.     Appearance  (2.5/3):     -­‐The  beer  had  a  nice  golden-­‐orange  and  slightly  copper  color  as  a  result  of   the  combination  of  2-­‐row  malt  with  Vienna  and  Munich,  both  known  for   contributing  an  orange  color  to  the  beer.    In  addition,  the  beer  had  pretty  good   clarity,  which  can  be  attributed  to  the  use  of  Whirlfloc,  whirlpooling,  formation  and   separation  of  cold  break,  and  cold  crashing.    The  beer  had  a  nice  thin,  lasting  head   with  good  lacing.    Overall,  the  finished  beer  had  a  great  appearance  but  could’ve   benefited  from  further  clarity.     Flavor  (14/20):     -­‐Again,  the  culmination  of  hop  additions  added  some  great  flavors.    Early   Columbus  additions  contributed  a  decent,  lasting  bitterness  and  the  numerous   aroma  additions  during  the  boil,  whirlpool,  and  dry  hop  contributed  mostly  citrus   and  pine  notes  with  some  slight  spiciness.    The  malt  character  was  fairly  sweet  and   had  hints  of  caramel  and  biscuit.    The  aftertaste  was  bitter  with  malt  sweetness.     Fermentation  didn’t  seem  to  add  any  distinguishable  flavor  characteristics.    Overall,   the  hop  flavor  and  bitterness  of  this  beer  are  enjoyable;  however,  the  malty   sweetness  seems  overpowering  and  takes  the  beer  out  of  balance.    Again,  this  malty   sweetness  is  subjective  to  my  palate  and  likely  a  result  of  either  Munich  malt  or   residual  priming  sugar.     Mouthfeel  (3.5/5):     The  beer  is  smooth  and  medium-­‐bodied.    The  beer  is  barely  astringent  and   may  just  be  a  result  of  hop  bitterness.    Although  the  beer  had  a  thin,  decent  head,  a  
  • 13. number  of  students  including  myself  perceived  it  as  slightly  flat.    Overall,  the   mouthfeel  is  decent  but  the  lack  of  full  carbonation  is  slightly  offputting.     Overall  Impression  (7/10)     -­‐As  evident  by  my  overall  impressions  of  aroma,  appearance,  flavor,  and   mouthfeel,  there  were  a  lot  of  enjoyable  characteristics  of  this  beer  including  hop   aroma  and  flavor,  the  color,  clarity,  and  overall  appearance,  and  the  smooth,   medium-­‐bodied  mouthfeel.    However,  the  malty  sweetness  of  the  beer  was  fairly  off   putting  in  terms  of  aroma  and  flavor.    The  acetaldehyde  aroma  was  also  undesirable   as  was  the  lack  of  full  carbonation.    The  beer  could  be  improved  with  more  time  for   bottle  conditioning  and  if  the  sweetness  doesn’t  mellow  out  perhaps  adjusting  the   grain  bill  to  have  less  residual  sweetness.    Overall,  our  first  attempt  at  the  Study   Break  IPA  was  a  decent  beer  but  not  outstanding.     Reflection  of  Results       Although  we  ran  into  a  few  problems  throughout  our  brewing  process,  we   ultimately  had  a  fairly  smooth  experience  brewing  the  Study  Break  IPA.    One  of  our   first  mistakes  was  spilling  about  a  handful  of  grain  during  the  milling  process,  which   we  replaced  with  roughly  the  same  amount.    In  addition,  as  previously  mentioned,   we  had  some  equipment  difficulties  such  as  a  faulty  kettle  burner  and  leaking   cylindroconical  fermenter.    We  dealt  with  these  issues  by  swapping  the  kettle   burner  with  the  mash  tun  burner  and  transferring  our  cooled  wort  in  the   cylindroconical  into  a  new,  keg-­‐style  fermenter.    We  also  experienced  a  longer  than   expected  fermentation  which  was  likely  a  result  of  having  too  small  a  volume  of   yeast  to  pitch.    Other  than  these  minor  issues  than  we  were  able  to  easily  resolve,   the  brewing  experience  went  well.    We  had  no  trouble  milling,  mashing,  sparging  or   boiling,  little  to  no  trouble  with  fermentation,  maturation,  or  packaging,  and  our   finished  beer  came  out  pretty  good.     Another  positive  aspect  of  our  brewing  experience  was  the  fact  that  our   Beersmith  estimated,  actual,  calculated,  and  New  Belgium  lab  tested  measurements   and  values  were  all  fairly  consistent.    Our  estimated  and  actual  pre-­‐boil  gravity  and   volumes,  post-­‐boil  gravity  and  volumes,  and  overall  batch  volume  and  gravity  were   all  fairly  consistent.    There  were  some  minor  discrepancies  between  estimated,   calculated,  and  actual  ABV  and  IBUs  but  these  were  likely  the  result  of  minor   differences  in  gravities  and  volumes  of  each  step.    Overall,  we  yielded  consistent   results  based  on  our  Beersmith  estimations  and  actual  results  indicating  that  we   were  efficient  in  our  brewing  processes.     As  mentioned  previously  in  the  sensory  evaluation,  our  beer  was  almost  spot   on  with  the  BJCP  style  guidelines  for  an  American  IPA.    We  produced  an  orange-­‐ gold,  smooth,  medium-­‐bodied  ale  which  had  great  hoppy  flavors  and  aromas   including  citrus,  fruit,  pine,  floral,  and  slightly  spicy  characteristics  with  a  lasting   bitterness.    The  only  changes  I  would  make  to  the  beer  next  time  would  be  to  adjust   the  overly  sweet  malt  backbone  which  I  believe  negatively  affects  the  balance  of  the   beer,  make  sure  the  beer  is  fully  carbonated  (some  class  members’  samples  were,   some  weren’t,  may  have  been  an  issue  of  fully  homogenizing  the  priming  sugar  in  
  • 14. the  maturation  keg),  and  allow  the  acetaldehyde  to  be  fully  converted  to  its   negligible  form.    In  conclusion,  we  had  a  great,  relatively  problem-­‐free  first  brewing   experience  brewing  the  Study  Break  IPA  in  which  we  learned  a  great  deal  and   ultimately  created  a  quality  final  product.