This document discusses different circuit designs for non-dispersive infrared (NDIR) gas sensors. It describes sensors that use thermopile, pyroelectric, and bolometer detectors to measure infrared radiation absorbed by target gases. For thermopile detectors, the temperature difference between an active and reference junction creates a voltage proportional to gas concentration. Pyroelectric detectors use a scandium aluminum nitride layer to generate a voltage from temperature changes due to absorbed infrared light. Bolometer detectors measure infrared absorption by detecting temperature increases with a thermistor. The document also discusses driver circuits and components used to isolate the detector layers from thermal losses.
Thermal Detector
A resistive element which measures electromagnetic radiation by absorbing it and converting it into heat. The increase in its temperature is used to measure the radiant energy. Also called thermal sensor (1), or bolometer.
An instrument or device, such as a thermal detector (1), which senses heat. Also called thermal sensor (2).
An instrument or device, such as a thermocouple, which functions or is actuated when exposed to heat.
An instrument or device, such as a thermometer, which quantifies heat.
synonym thermal sensor
Uv-Vis spectroscopy: electronic spectroscopy, absorption and emission, Terms describing UV absorptions, absorbing species containing s,n and pi, absorbing species,sigma and pi orbitals, electronic transitions, Absorption: physical Basis and lineshape,UV-Spectra.
Thermal Detector
A resistive element which measures electromagnetic radiation by absorbing it and converting it into heat. The increase in its temperature is used to measure the radiant energy. Also called thermal sensor (1), or bolometer.
An instrument or device, such as a thermal detector (1), which senses heat. Also called thermal sensor (2).
An instrument or device, such as a thermocouple, which functions or is actuated when exposed to heat.
An instrument or device, such as a thermometer, which quantifies heat.
synonym thermal sensor
Uv-Vis spectroscopy: electronic spectroscopy, absorption and emission, Terms describing UV absorptions, absorbing species containing s,n and pi, absorbing species,sigma and pi orbitals, electronic transitions, Absorption: physical Basis and lineshape,UV-Spectra.
mercury analysis in AAS, by fayaz hussain chandio, Introduction of Atomic Absorption Spectroscopy
Mercury-Element information, properties and uses
Mercury contamination and Human health
Analytical methods for mercury analysis
Determination of mercury by Cold-vapor Atomic absorption spectroscopy
Conclusion
Acknowledgment
Atomic Spectroscopy
Atomic-absorption (AA) spectroscopy uses the absorption of light to measure the concentration of gas-phase atoms.
samples are usually liquids or solids
Analyte atoms or ions must be vaporized in a flame or graphite furnace
The atoms absorb ultraviolet or visible light and make transitions to higher electronic energy levels.
Discovered approximately 1500 BC
Group 12, Period 6, Block d, Atomic number 80, Boiling point 356.619 ℃.
Mercury is an element and a transition metal that is found in air, water, and soil.
It is liquid at room temperature
Mercury has long been known as quicksilver.
Elemental mercury is liquid at room temperature. (Hg)
Inorganic mercury compounds are formed when mercury combines with other elements, such as sulfur or oxygen, to form compounds or salts. inorganic Hg (Hg2+).
Organic mercury compounds are formed when mercury combines with carbon. (MMHg, CH3Hg+), (DMHg, CH3HgCH3).
Mercury is also used in dental applications.
Coatings for mirrors.
The most important use of mercury is in the preparation of chlorine.
Mercury thermometers
and barometers.
Mercuric arsenate used
as waterproofing paints.
Mercuric chloride, or
mercury bichloride, or corrosive sublimate (HgCl ):disinfectant, insecticide.
Vapors pass through the skin into the blood stream. Can also be inhaled, can also be swallowed.
Mercury chloride known as calomel was sometimes used as a poison to kill people.
Depression, nervousness, and personality changes.
Damage to the kidneys and muscles.
Most exposure to mercury comes from the ingestion of certain foods, such as fish, in which the mercury has accumulated at high levels.
According to US EPA, list of many of the regulatory methods that are available for use with today’s technologies.
Cold Vapour Atomic Absorption Spectroscopy (CVAAS):
Cold Vapour At omic Fluorescence Spectroscopy (CVAFS):
Direct Analysis by Thermal Decomposition:
ICP or ICP-MS:
SCOPE AND APPLICATION METHOD:
This procedure measures total mercury (organic + inorganic) in drinking, surface, ground, sea, brackish waters, industrial and domestic wastewater, fish and coal.
The range of the method is 0.2-10 μg Hg/L.
most modern CVAAS instruments are more sensitive, automated, smaller, faster, and less expensive than generic flame spectrometers with cold vapor devices attached.
Heating the sample in the presence of different combinations of mineral acids such as nitric, hydrochloric, sulfuric and per chloric acids and also other oxidizing agents such as hydrogen peroxide.
Atomic spectroscopy plays a major role as the basis of a wide range of analytical techniques that contribute data on elemental concentrations and isotope ratios .These analytical data provide the raw material on which progress in geochemistry depends.
The main advantages of AAS & AES are that it is relatively inexpensive and easy to use, while still offering high throughput, quantitative analysis of the metal content of solids or liquids. This makes it suitable for use in a wide range of applications.
A short lecture about Atomic Spectroscopy: Flame Photometry, Atomic Absorption, and Atomic Emission with Coupled Plasma (FP, AA and ICP-AES). Presented at 28.03.2011, Faculty of Agriculture, Hebrew University of Jerusalem, by Vasiliy Rosen, M.Sc.
This article discusses the principle of interferometry. The definition of the term along with its applications are stated in this article. Five most common type of interferometers viz. Michelson Interferometer, Mach-Zahnder Interferometer, Fabry Perot Interferometer, Sagnac Interferometer and Fiber Interferometer are discussed in detial in this article.
mercury analysis in AAS, by fayaz hussain chandio, Introduction of Atomic Absorption Spectroscopy
Mercury-Element information, properties and uses
Mercury contamination and Human health
Analytical methods for mercury analysis
Determination of mercury by Cold-vapor Atomic absorption spectroscopy
Conclusion
Acknowledgment
Atomic Spectroscopy
Atomic-absorption (AA) spectroscopy uses the absorption of light to measure the concentration of gas-phase atoms.
samples are usually liquids or solids
Analyte atoms or ions must be vaporized in a flame or graphite furnace
The atoms absorb ultraviolet or visible light and make transitions to higher electronic energy levels.
Discovered approximately 1500 BC
Group 12, Period 6, Block d, Atomic number 80, Boiling point 356.619 ℃.
Mercury is an element and a transition metal that is found in air, water, and soil.
It is liquid at room temperature
Mercury has long been known as quicksilver.
Elemental mercury is liquid at room temperature. (Hg)
Inorganic mercury compounds are formed when mercury combines with other elements, such as sulfur or oxygen, to form compounds or salts. inorganic Hg (Hg2+).
Organic mercury compounds are formed when mercury combines with carbon. (MMHg, CH3Hg+), (DMHg, CH3HgCH3).
Mercury is also used in dental applications.
Coatings for mirrors.
The most important use of mercury is in the preparation of chlorine.
Mercury thermometers
and barometers.
Mercuric arsenate used
as waterproofing paints.
Mercuric chloride, or
mercury bichloride, or corrosive sublimate (HgCl ):disinfectant, insecticide.
Vapors pass through the skin into the blood stream. Can also be inhaled, can also be swallowed.
Mercury chloride known as calomel was sometimes used as a poison to kill people.
Depression, nervousness, and personality changes.
Damage to the kidneys and muscles.
Most exposure to mercury comes from the ingestion of certain foods, such as fish, in which the mercury has accumulated at high levels.
According to US EPA, list of many of the regulatory methods that are available for use with today’s technologies.
Cold Vapour Atomic Absorption Spectroscopy (CVAAS):
Cold Vapour At omic Fluorescence Spectroscopy (CVAFS):
Direct Analysis by Thermal Decomposition:
ICP or ICP-MS:
SCOPE AND APPLICATION METHOD:
This procedure measures total mercury (organic + inorganic) in drinking, surface, ground, sea, brackish waters, industrial and domestic wastewater, fish and coal.
The range of the method is 0.2-10 μg Hg/L.
most modern CVAAS instruments are more sensitive, automated, smaller, faster, and less expensive than generic flame spectrometers with cold vapor devices attached.
Heating the sample in the presence of different combinations of mineral acids such as nitric, hydrochloric, sulfuric and per chloric acids and also other oxidizing agents such as hydrogen peroxide.
Atomic spectroscopy plays a major role as the basis of a wide range of analytical techniques that contribute data on elemental concentrations and isotope ratios .These analytical data provide the raw material on which progress in geochemistry depends.
The main advantages of AAS & AES are that it is relatively inexpensive and easy to use, while still offering high throughput, quantitative analysis of the metal content of solids or liquids. This makes it suitable for use in a wide range of applications.
A short lecture about Atomic Spectroscopy: Flame Photometry, Atomic Absorption, and Atomic Emission with Coupled Plasma (FP, AA and ICP-AES). Presented at 28.03.2011, Faculty of Agriculture, Hebrew University of Jerusalem, by Vasiliy Rosen, M.Sc.
This article discusses the principle of interferometry. The definition of the term along with its applications are stated in this article. Five most common type of interferometers viz. Michelson Interferometer, Mach-Zahnder Interferometer, Fabry Perot Interferometer, Sagnac Interferometer and Fiber Interferometer are discussed in detial in this article.
Carbon Nanotubes Based Sensor for Detection of Traces of Gas Molecules- A ReviewIJEEE
In this review paper, we discuss various gas sensors based on technique and sensing materials used in there fabrication. Various sensors are designed making use of salient features of carbon nanotubes and its electrical, mechanical, and electromechanical properties. Effect of using nano-composites on sensitivity and selectivity of gas sensor have been studied.
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Indigenized remote control interface card suitable for MAFI system CCR equipment. Compatible for IDM8000 CCR. Backplane mounted serial and TCP/Ethernet communication module for CCR remote access. IDM 8000 CCR remote control on serial and TCP protocol.
• Remote control: Parallel or serial interface.
• Compatible with MAFI CCR system.
• Compatible with IDM8000 CCR.
• Compatible with Backplane mount serial communication.
• Compatible with commercial and Defence aviation CCR system.
• Remote control system for accessing CCR and allied system over serial or TCP.
• Indigenized local Support/presence in India.
• Easy in configuration using DIP switches.
Technical Specifications
Indigenized remote control interface card suitable for MAFI system CCR equipment. Compatible for IDM8000 CCR. Backplane mounted serial and TCP/Ethernet communication module for CCR remote access. IDM 8000 CCR remote control on serial and TCP protocol.
Key Features
Indigenized remote control interface card suitable for MAFI system CCR equipment. Compatible for IDM8000 CCR. Backplane mounted serial and TCP/Ethernet communication module for CCR remote access. IDM 8000 CCR remote control on serial and TCP protocol.
• Remote control: Parallel or serial interface
• Compatible with MAFI CCR system
• Copatiable with IDM8000 CCR
• Compatible with Backplane mount serial communication.
• Compatible with commercial and Defence aviation CCR system.
• Remote control system for accessing CCR and allied system over serial or TCP.
• Indigenized local Support/presence in India.
Application
• Remote control: Parallel or serial interface.
• Compatible with MAFI CCR system.
• Compatible with IDM8000 CCR.
• Compatible with Backplane mount serial communication.
• Compatible with commercial and Defence aviation CCR system.
• Remote control system for accessing CCR and allied system over serial or TCP.
• Indigenized local Support/presence in India.
• Easy in configuration using DIP switches.
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5. Cont….
• Since, in case of a thermopile detector ( usually, series connection of
thermocouples), the temperature difference between the active and the reference
junction creates a potential difference, and if the later quantity is measured with a
voltmeter and if we measure the temperature of reference junction using
thermistor, we can calculate the concentration of the target gas.
• Ex- If IR light is applied to a dual thermopile detector fitted with a pair of optical
filters so that one filter is centered on 4260 nm and the other on 3910 nm, the
concentration of carbon dioxide can be measured from the ratios of the two
thermopile voltages.
9. Cont….
Fig. 1a shows a schematic of the ScAlN-based pyroelectric detector
that we use. The pyroelectric detector consists of a pyroelectric sensing
layer with area ~ 500 μm x 500 μm. We use 12 %-doped ScAlN with
thickness of ~1 μm as the pyroelectric sensing layer. On top and below the
ScAlN sensing layer is the top and bottom electrodes respectively. Tita-
nium nitride (TiN) is used as the top electrode and molybdenum (Mo) as
the bottom electrode. Above TiN top electrode is a dielectric stack of
silicon dioxide – silicon nitride – silicon dioxide (SiO2-SiN-SiO2) which
acts as the absorber to help enhance light absorption into the device. This
absorber stack is used to help broaden the absorption bandwidth with 3
layers of dielectric films and create destructive light wave interference in
the stack for more efficient absorption.
10. Cont….
• The top and bottom electrodes are connected to aluminium metal pads
which act as metal contacts for electrical connections. Below the bottom
electrode is a ~1 μm thick SiO2 layer with waffle-like structures. The SiO2
material helps to thermally isolate the thermal energy received by the
pyroelectric detector sensing layer, slowing down thermal conduction to
the medium below. In addition, the Si substrate is released from the
backside to form an air cavity area under the pyroelectric sensing region
to further reduce thermal losses as air is a poor thermal conductor. The
SiO2 ribs help to increase the mechanical stiffness of the pyroelectric
sensing region which is in membrane form.