This document describes procedures for determining aflatoxins and arsenic in samples. For aflatoxins, it outlines sample preparation using extraction and a multifunctional column, followed by HPLC analysis to detect four main aflatoxin compounds. For arsenic, it describes preparing a test solution from the sample, generating arsine gas, and using a colorimetric reaction to detect arsenic at levels below the limit. Key steps include extraction, column chromatography, HPLC, and colorimetric comparisons to standards.