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Lubricant Film Thickness Estimation
   at the Mould Inlet Region of a                                                                                           Objectives
   Continuous Casting Process
                                                                                                                             To develop a thermal Reynolds equation applied
                                                                                                                            to different surfaces velocities and temperatures
                                                                                                                            condition

      Seminar Masyarakat Pemulas Indonesia (MASPI)                                                                           To implement the Thermal Reynolds equation to
                                                                                                                            the inlet mould region of the continuous casting
      Gedung BPPT Ruang Komisi 3                                                                                            process
      Jakarta, 27 Mei 2008
                                                                                                                            To estimate the mould inlet film thickness for
                                                                                                                            various parameters in continuous casting
                                                Dr. Barman Tambunan
                                                 Pusat Teknologi Material (PTM) -
                                Badan Pengkajian dan Penerapan Teknologi (BPPT)     Gedung BPPT II, Lt 22,
                                                                                    Jl. MH Thamrin No. 8
                                                                                    Jakarta 10340            barman@webmail.bppt.go.id




                Research Question                                                                                                              Introduction
                                                                                                             • Practically all metals, which are not used in cast form are reduced to
                  How does the hydrodynamic lubrication in the                                                 some standard shapes for subsequent processing.
                  mould region of a continuous casting process                                               • Manufacturing companies producing metals supply metals in form of
                  influence the casting product?                                                               ingots which are obtained by casting liquid metal into a square cross
                                                                                                               section.
                  How can the thermal Reynolds equation be                                                       – Slab (500-1800 mm wide and 50-300 mm thick)
                  developed and implemented in the continuous                                                    – Billets (40 to 150 sq mm)
                  casting process?
                                                                                                                 – Blooms (150 to 400 sq mm)
                  What are the influences of the various casting                                             • Sometimes continuous casting methods are also used to cast the
                  parameter to the lubrication in the continuous                                               liquid metal into slabs, billets or blooms.
                  casting process?                                                                           • These shapes are further processed through hot rolling, forging or
                                                                                                               extrusion, to produce materials in standard form such as plates,
                                                                                                               sheets, rods, tubes and structural sections.

barman@webmail.bppt.go.id




                                                                                                                                                                                        1
Sequence of operations for
       obtaining different shapes                                                                                          Steel Making Plant




                                                                                               barman@webmail.bppt.go.id




         STEEL MAKING PROCESS                                                                       Continuous Casting Process

                                                                                                                                 Area to be
                                                                                                                                 analyzed


 MELTING                SECONDARY                     CASTING             INSPECTION                                               End
                        METALLURGY                                                                                                 Product
• Charging ratio    • Alloying (chemical comp.)    • Temperature         • Surface quality
• Chemical comp.    • Desulfurisasi, deoksidasi,   • Chemical comp.      • Internal quality
• Temperature         dehidrogenisasi,             • Casting parameter     by sulphur print/
• Tap to tap time     decarburisasi                                        macro-etch
                    • Inclusion shaped control                           • Shape/dimensio
                    • Temperature                                          n



                                                                                               barman@webmail.bppt.go.id




                                                                                                                                                2
Mould Flux Infiltration                                                       Continuous Casting Mold Flux
                                                                               Performs Five Basic Functions :
                                                                               • Thermally insulates the molten steel meniscus to
                                                                                 prevent premature solidification.
                                                                               • Protects the molten steel in the mold from
                                                                                 reacting with atmospheric gases.
                                                                               • Absorbs products of de/reoxidation from the
                                                                                 molten steel.
                                                                               • Provides a lubricating film of molten slag to
                                                                                 prevent the steel from adhering to the mold wall
                                                                                 and to facilitate strand withdrawal.
                                                                               • Modifies thermal heat removal in the mold.
barman@webmail.bppt.go.id




                            Thermal Heat Transfer                              Provides Liquid Lubrication in
                                 in the Mold                                      Gap Between Mold and
                                           Solid Flux Film
                                                                                     Solidifying Shell
     • The slag between the steel
       shell significantly affects heat                                     Liquid slag is drawn down              Solid   Liquid     Steel
                                                      Heat Flux
       transfer.                                                            into the gap along the                 Flux     Slag      Shell
                                                         Liquid
                                          MOLD                              steel shell. The liquid is a
     • The mold wall is very cold,        WALL
                                                          Slag

       and causes the slag to freeze                                        lubricant, allowing the
       into a solid. The solid greatly                                      steel to be withdrawn                           Flux
       reduces heat transfer.                                 Solidifying   without sticking to the                        Velocity

     • The slag along the shell stays                         Shell         mold wall. If the steel         Mold
       hot, and in liquid form. It                                          sticks to the wall, it causes   Wall

       lubricates.                                                          a breakout.


                                                    Air Gap




                                                                                                                                              3
Mould Flux Infiltration Analysis
  Temperature Distribution of the
                                                                                                                                                                      Top of the Mould
  Slab                                                                                                                                                 Mould
                                                                                                                                                                                      Meniscus Region
                                                                                                                                                                                                            Center line

                                                                                                                                                                          z
                                                                                                                                                                          Lubricant
                                                                                                                                                                     x                              Molten
                                                                                                                                                                                                    Steel Pool
                                                                                                                                              x0                          h

                                                                                                                                                                     ho
                                                                                                                                                                                              Ferrostatic
                                                                                                                                                                                              Pressure
                                                                                                                                                                              T2
                                                                                                                             Film thickness
                                                                                                                                                                                         u2
                                                                                                                                                                                                   Centre of the
                                                                                                                                                                                                   Mould
                                                                                                                                                           ±u1

                                                                                                                                                            T1
                                                                                                                                                                                        Solidified Steel
                                                                                                                                                                                        Strand

                                                                                                  H : Non-
                                                                                                  dimensional film
                                                                                                  thickness                           H=
                                                                                                                                              q ⎢
                                                                                                                                                ln
                                                                                                                                                   ⎡
                                                                                                                                                          x
                                                                                                                                                                    ⎤                  ⎛             ⎞
                                                                                                                                                                    ⎥ − 2 q 2 − x 2 + q⎜1 + ln 2 − 1 ⎟                    (   )
                                                                                                                                               2 ⎢ 2 q2 − 2 q2 − x2 ⎥                  ⎜       2 ⎟
                            Temperature Distribution of the Transverse Slice at the Mould Exit                                                     ⎣                ⎦                  ⎝             ⎠
                                                                                                  equation in the                                                                                                                                1
                                                   (time t = 39.4 sec)                                                                                                                                                              ⎛ 2γ ⎞           2
                                                                                                  meniscus region                                                                                                                   ⎜
                                                                                                                                                                                                                                  q=⎜        ⎟
                                                                                                                                                                                                                                             ⎟
                                                                                                                                                                                                    (Ref. Jimbo et al. (1991))      ⎝ (Δρ )g ⎠
                                                                                                 barman@webmail.bppt.go.id




   Thermal Reynolds Equation                                                                              Thermal Reynolds Equation

    ∂P ∂τ  ∂ ⎛ ∂u ⎞
                                                                                                                                                               p 'h 3                                       Non-dimensional Pressure
                                                              The Pressure                                                          R =
                                                                                                                                                               (Uh − Q                    )
          = ⎜μ ⎟
                                                                                                                                              12 μ
      =                                                                                                                                                    s
                                                                                                                                                                                                            Gradient
                                                              Gradient =
    ∂x ∂z ∂z ⎝ ∂z ⎠                                           Shear Stress                                                          F =
                                                                                                                                              μ s α (Uh − Q )2
                                                                                                                                                                      2
                                                                                                                                                                                                            Non-dimensional Thermal
                                                                                                                                                                                                            Backflow parameter
                                                                                                                                                               kh

                                       The viscosity                                                                                D = α (T2 − T1 )
                                                                                                                                                                                                             Non-dimensional
                   ⎧    ⎛      T2 − T1 ⎞⎫
       μ = μs exp⎨−α ⎜T −              ⎟⎬of
                                          the mould                                                                                                                                                          Temperature difference
                   ⎩    ⎝         2 ⎠⎭
                                       lubricant                    ∂ 2T                                                                      μ s α (u 1 − u 2 )2
                                                                k             = E                                                   S =                                                                      Non-dimensional Velocity
                                                                    ∂z 2                                                                                         k
                               h
                                   2
                                                                      Constant Energy                                                                  Eα h                       2                         Non-dimensional Energy
                       Q=      ∫ u dz The Flow Rate                   Dissipation
                                                                                                                                    E   *
                                                                                                                                              =
                                                                                                                                                         k                                                  Dissipation
                              −h
                                   2


                                                                                                                                                   μ        α u
                                                                                                                                                                              2                              Non-dimensional Thermal
                                                                                                                                    L =                0
                                                                                                                                                                                                             Loading Parameter
                                                                                                                                                               k
barman@webmail.bppt.go.id                                                                        barman@webmail.bppt.go.id




                                                                                                                                                                                                                                                         4
Applying Thermal Reynolds
                                                                                                 Results and Discussion
                                                                                                                  3.5

         Thermal Reynolds equation with the non-                                                                                    G=1                                                G=5
         dimensional film thickness parameter H                                                                    3                G=2
                                                                                                                                    G=3
                                                                                                                                                                                       G=4


                    G (H − 1)
                                                                                                                  2.5               G=4
                                                                                                                                    G=5

               dB                                                                                   Film

                  =                                                                                 Thicknes       2

                               R                                                                    s Ho.L(1/6)
                                                                                                                                                                                       G=3



               d x H0 A0 2 H 3                                                                                    1.5                                                                   G=2


                                                                                                                   1
                                                                                                                                                                                       G=1

        The thermal Reynolds equation with the                                                                    0.5

        correction factor R was integrated numerically
        using a Fourth order Runge-Kutta program                                                                   0
                                                                                                                        0   0.1   0.2   0.3   0.4   0.5   0.6   0.7    0.8   0.9   1    1.1   1.2   1.3   1.4   1.5   1.6   1.7   1.8   1.9


                                                                                                                                                                      Thermal Loading L(1/6)

                                          1                                 2                                                                 Film thickness variation for D = 2, S = 0 and
                       ⎛              ⎞              2 ⎛                ⎞
                                           3                                    3
                             PFer                              PFer
G = γ P Fer                                    A0 = xtot ⎜                                                                                                     various G
                                                         ⎜ 12 μ U x 2 ⎟
              H 0 = h0 ⎜                                                                  − γp
                       ⎜ 12 μ U x 2 ⎟                                               B=e
                                                 2
                                      ⎟                                 ⎟
                       ⎝     0    tot ⎠                  ⎝     0    tot ⎠




          The Continuous Casting Rig                                                               Modelling
     •Mould cylinder 32.5 mm
     •Outer diameter 74 mm                                                                                                                          Copper                                                                                    LVDT
     •Length 400 mm          Oscillating                         Plate                                                                              Mould



                                                             Lubricant Reservoir
                                                                                                                                                                                                                            MLP-50 Load Cell
                                                                                                 molten
                                                                                                 bismuth
                                                                                                 based
                                                                                                 alloy
                                  Withdrawal Motor




                                                                                                                                                                                                                                                     5
Evaluation of Continuous Casting                                     Lubricant
                         Lubricant Applied                                   Produced Round        Lubricant :
                         during Casting: • Castrol GTX2 oil                  Billet Shaped Cast    Castrol GTX2 oil
                                         • Castor oil                                              Castor oil
                                         • Propar 1800                                             Propar 1800          The viscosity measured at 40 ºC
                                                                                                                        η1(40ºC)=165 P
              Casting Withdrawal speed: 3.7 m/sec.
              Mould amplitude (Oscillated): 10 mm
                                                                                                                        η2(40ºC)=263 cP
              Mould velocity: 0 to +36.77 / -36.77                                                                      η3(40ºC) = 12330 cP.
              mm/sec                                                                                                    At 40 ºC it shows that η3 which is
                                                                                                                        the Propar 1800, has the highest
       Lubricant film thickness between                       Molten Bismuth Alloy                                      viscosity of 12339 cP.
       the strand and the mould wall                          (Bi=50%, Pb=25%,
       were measured for various                              Sn=12.5%, Cd=12.5%)
       lubricants                                             in Boiled Water




                         Film Thickness Variation                                                 Result and Discussion
                   0.3

                               Propar 1800

                               Castor Oil
                                                                                                  Castrol GTX 2       Castor GTX 2       Propar 1800
                  0.25         Castrol GTX
F T ic n s (m )
 ilm h k e s m




                   0.2




                  0.15




                   0.1
                         1             10         100              1000        10000
                                             Viscosity (cp)



                              Film thickness variation at various
                             lubricant viscosities applied during
                                      continuous casting




                                                                                                                                                             6
Conclusions
•   Low melting point material i.e. Bismuth based alloy material
    was successfully used in this continuous casting experimental
    rig to study the film layer formation of hydrodynamic
    lubrication at the strand mould interface.

•   The initial film thickness variation occurring during continuous
    casting as shown here is influenced by the viscosity of the
    lubricant.

•   The highest viscosity lubricant applied during casting
    produces the thickest lubricant film. A higher estimate of film             Pusat Teknologi Material
    thickness was obtained for continuous casting where Propar                    Deputi TIEM - BPPT       MASPI
    1800 lubricant was used. Castrol GTX2 with the lowest
    viscosity gave the lowest estimated film thickness during                     Gedung BPPT II, Lt
                                                                                  22, Jl. MH Thamrin
    casting                                                                       No. 8 Jakarta 10340




                                                                       barman@webmail.bppt.go.id




                                                                                                                   7

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Bahan barman bppt

  • 1. Lubricant Film Thickness Estimation at the Mould Inlet Region of a Objectives Continuous Casting Process To develop a thermal Reynolds equation applied to different surfaces velocities and temperatures condition Seminar Masyarakat Pemulas Indonesia (MASPI) To implement the Thermal Reynolds equation to the inlet mould region of the continuous casting Gedung BPPT Ruang Komisi 3 process Jakarta, 27 Mei 2008 To estimate the mould inlet film thickness for various parameters in continuous casting Dr. Barman Tambunan Pusat Teknologi Material (PTM) - Badan Pengkajian dan Penerapan Teknologi (BPPT) Gedung BPPT II, Lt 22, Jl. MH Thamrin No. 8 Jakarta 10340 barman@webmail.bppt.go.id Research Question Introduction • Practically all metals, which are not used in cast form are reduced to How does the hydrodynamic lubrication in the some standard shapes for subsequent processing. mould region of a continuous casting process • Manufacturing companies producing metals supply metals in form of influence the casting product? ingots which are obtained by casting liquid metal into a square cross section. How can the thermal Reynolds equation be – Slab (500-1800 mm wide and 50-300 mm thick) developed and implemented in the continuous – Billets (40 to 150 sq mm) casting process? – Blooms (150 to 400 sq mm) What are the influences of the various casting • Sometimes continuous casting methods are also used to cast the parameter to the lubrication in the continuous liquid metal into slabs, billets or blooms. casting process? • These shapes are further processed through hot rolling, forging or extrusion, to produce materials in standard form such as plates, sheets, rods, tubes and structural sections. barman@webmail.bppt.go.id 1
  • 2. Sequence of operations for obtaining different shapes Steel Making Plant barman@webmail.bppt.go.id STEEL MAKING PROCESS Continuous Casting Process Area to be analyzed MELTING SECONDARY CASTING INSPECTION End METALLURGY Product • Charging ratio • Alloying (chemical comp.) • Temperature • Surface quality • Chemical comp. • Desulfurisasi, deoksidasi, • Chemical comp. • Internal quality • Temperature dehidrogenisasi, • Casting parameter by sulphur print/ • Tap to tap time decarburisasi macro-etch • Inclusion shaped control • Shape/dimensio • Temperature n barman@webmail.bppt.go.id 2
  • 3. Mould Flux Infiltration Continuous Casting Mold Flux Performs Five Basic Functions : • Thermally insulates the molten steel meniscus to prevent premature solidification. • Protects the molten steel in the mold from reacting with atmospheric gases. • Absorbs products of de/reoxidation from the molten steel. • Provides a lubricating film of molten slag to prevent the steel from adhering to the mold wall and to facilitate strand withdrawal. • Modifies thermal heat removal in the mold. barman@webmail.bppt.go.id Thermal Heat Transfer Provides Liquid Lubrication in in the Mold Gap Between Mold and Solid Flux Film Solidifying Shell • The slag between the steel shell significantly affects heat Liquid slag is drawn down Solid Liquid Steel Heat Flux transfer. into the gap along the Flux Slag Shell Liquid MOLD steel shell. The liquid is a • The mold wall is very cold, WALL Slag and causes the slag to freeze lubricant, allowing the into a solid. The solid greatly steel to be withdrawn Flux reduces heat transfer. Solidifying without sticking to the Velocity • The slag along the shell stays Shell mold wall. If the steel Mold hot, and in liquid form. It sticks to the wall, it causes Wall lubricates. a breakout. Air Gap 3
  • 4. Mould Flux Infiltration Analysis Temperature Distribution of the Top of the Mould Slab Mould Meniscus Region Center line z Lubricant x Molten Steel Pool x0 h ho Ferrostatic Pressure T2 Film thickness u2 Centre of the Mould ±u1 T1 Solidified Steel Strand H : Non- dimensional film thickness H= q ⎢ ln ⎡ x ⎤ ⎛ ⎞ ⎥ − 2 q 2 − x 2 + q⎜1 + ln 2 − 1 ⎟ ( ) 2 ⎢ 2 q2 − 2 q2 − x2 ⎥ ⎜ 2 ⎟ Temperature Distribution of the Transverse Slice at the Mould Exit ⎣ ⎦ ⎝ ⎠ equation in the 1 (time t = 39.4 sec) ⎛ 2γ ⎞ 2 meniscus region ⎜ q=⎜ ⎟ ⎟ (Ref. Jimbo et al. (1991)) ⎝ (Δρ )g ⎠ barman@webmail.bppt.go.id Thermal Reynolds Equation Thermal Reynolds Equation ∂P ∂τ ∂ ⎛ ∂u ⎞ p 'h 3 Non-dimensional Pressure The Pressure R = (Uh − Q ) = ⎜μ ⎟ 12 μ = s Gradient Gradient = ∂x ∂z ∂z ⎝ ∂z ⎠ Shear Stress F = μ s α (Uh − Q )2 2 Non-dimensional Thermal Backflow parameter kh The viscosity D = α (T2 − T1 ) Non-dimensional ⎧ ⎛ T2 − T1 ⎞⎫ μ = μs exp⎨−α ⎜T − ⎟⎬of the mould Temperature difference ⎩ ⎝ 2 ⎠⎭ lubricant ∂ 2T μ s α (u 1 − u 2 )2 k = E S = Non-dimensional Velocity ∂z 2 k h 2 Constant Energy Eα h 2 Non-dimensional Energy Q= ∫ u dz The Flow Rate Dissipation E * = k Dissipation −h 2 μ α u 2 Non-dimensional Thermal L = 0 Loading Parameter k barman@webmail.bppt.go.id barman@webmail.bppt.go.id 4
  • 5. Applying Thermal Reynolds Results and Discussion 3.5 Thermal Reynolds equation with the non- G=1 G=5 dimensional film thickness parameter H 3 G=2 G=3 G=4 G (H − 1) 2.5 G=4 G=5 dB Film = Thicknes 2 R s Ho.L(1/6) G=3 d x H0 A0 2 H 3 1.5 G=2 1 G=1 The thermal Reynolds equation with the 0.5 correction factor R was integrated numerically using a Fourth order Runge-Kutta program 0 0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1 1.1 1.2 1.3 1.4 1.5 1.6 1.7 1.8 1.9 Thermal Loading L(1/6) 1 2 Film thickness variation for D = 2, S = 0 and ⎛ ⎞ 2 ⎛ ⎞ 3 3 PFer PFer G = γ P Fer A0 = xtot ⎜ various G ⎜ 12 μ U x 2 ⎟ H 0 = h0 ⎜ − γp ⎜ 12 μ U x 2 ⎟ B=e 2 ⎟ ⎟ ⎝ 0 tot ⎠ ⎝ 0 tot ⎠ The Continuous Casting Rig Modelling •Mould cylinder 32.5 mm •Outer diameter 74 mm Copper LVDT •Length 400 mm Oscillating Plate Mould Lubricant Reservoir MLP-50 Load Cell molten bismuth based alloy Withdrawal Motor 5
  • 6. Evaluation of Continuous Casting Lubricant Lubricant Applied Produced Round Lubricant : during Casting: • Castrol GTX2 oil Billet Shaped Cast Castrol GTX2 oil • Castor oil Castor oil • Propar 1800 Propar 1800 The viscosity measured at 40 ºC η1(40ºC)=165 P Casting Withdrawal speed: 3.7 m/sec. Mould amplitude (Oscillated): 10 mm η2(40ºC)=263 cP Mould velocity: 0 to +36.77 / -36.77 η3(40ºC) = 12330 cP. mm/sec At 40 ºC it shows that η3 which is the Propar 1800, has the highest Lubricant film thickness between Molten Bismuth Alloy viscosity of 12339 cP. the strand and the mould wall (Bi=50%, Pb=25%, were measured for various Sn=12.5%, Cd=12.5%) lubricants in Boiled Water Film Thickness Variation Result and Discussion 0.3 Propar 1800 Castor Oil Castrol GTX 2 Castor GTX 2 Propar 1800 0.25 Castrol GTX F T ic n s (m ) ilm h k e s m 0.2 0.15 0.1 1 10 100 1000 10000 Viscosity (cp) Film thickness variation at various lubricant viscosities applied during continuous casting 6
  • 7. Conclusions • Low melting point material i.e. Bismuth based alloy material was successfully used in this continuous casting experimental rig to study the film layer formation of hydrodynamic lubrication at the strand mould interface. • The initial film thickness variation occurring during continuous casting as shown here is influenced by the viscosity of the lubricant. • The highest viscosity lubricant applied during casting produces the thickest lubricant film. A higher estimate of film Pusat Teknologi Material thickness was obtained for continuous casting where Propar Deputi TIEM - BPPT MASPI 1800 lubricant was used. Castrol GTX2 with the lowest viscosity gave the lowest estimated film thickness during Gedung BPPT II, Lt 22, Jl. MH Thamrin casting No. 8 Jakarta 10340 barman@webmail.bppt.go.id 7