1) The document describes the fabrication and characterization of silane-nanocrystalline cellulose bio-nanocomposites for removing arsenic from water.
2) Specifically, it details the functionalization of nanocrystalline cellulose with 3-aminopropyltrimethoxy silane and 3-mercaptopropyltrimethoxy silane to introduce amino and thiol groups with affinity for arsenic species.
3) Batch experiments were conducted to evaluate the sorption capacity of the composites for arsenic (III) and arsenic (V) under various conditions.
4. 100],
where, and are the initial and final concentrations of arsenic ions in solution. All the
investigations were carried out in triplicate to confirm reproducibility of the experimental results.
The reproducibility and relative deviation are considered at ±0.5% and ±2.5%, respectively. The
adsorption capacity (mg/g) was calculated from the following equation:
5. where
and represent the initial and final concentrations of the arsenic solutions, respectively. V and m
are the solution volumes and adsorbent dose.
2.6. Statistical and Error analysis
Batch experiments were conducted in triplicate (N=3) and data represents the mean value.
Mean values, correlation coefficients, and standard deviations were computerized. For inter-group
mean value differences, each parameter was subjected to the Student’s t-test for significance level
(p 0.05). For nonlinear fitting of kinetic data, the Standard Error (SE) analysis is used to evaluate
the applicability of the model. The SE is calculated as