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ALD Vacuum Technologies
	 High Tech is our Business
Electro Slag Remelting (ESR)
Electro Slag Remelting Processes and Furnaces
02
Generally, the ESR process offers a very
high, consistent and predictable product
quality. Finely controlled solidification
improves soundness and structural
integrity. Ingot surface quality is
improved by the formation of a solidified
thin slag skin between ingot and mold
wall during the remelting operation.
This is why ESR is recognized as the
preferred production method for high-
performance superalloys that are used
today in industries such as aerospace
and nuclear engineering as well as for
heavy forgings.
ESR Technology
ESR is the continuous remelting of
a consumable electrode by means
of a resistance-heated slag.
The main process stages are:
OO A consumable ESR electrode is
	 generated by secondary metallurgy
	 or VIM
OO Process condition is established
	 (inert gas, vacuum, pressure)
OO Slag is added to the bottom of the
	 crystallizer (mold)
OO AC power heats the slag
OO The intense heat generated by slag
	 resistance melts the tip of the electrode
	 and a new ingot grows in the mold
OO De-oxidant or nitriding agents are
	added
OO The melt rate and the immersion of
	 the electrode is precisely regulated
	 by the ESR control system
OO Ingot cooling is controlled for
	 directional solidification
ALD has improved the basic design of
the ESR furnace in computer control and
regulation continuously over the years to
achieve:
OO Fully-automatic remelting processes
OO Improved reproducibility of the
	 metallurgy properties.
Electro Slag Remelting
ALD is one of the leading
suppliers of vacuum and inert
gas melting furnace technologies
for engineered metals.
03
ESR Materials/Alloys
OO Tool steels for milling cutters,
	 mining, etc.
OO Die steels for the glass, plastic
	 and automotive industries
OO Ball-bearing steels
OO Cold rolls
OO Stainless steels
OO Steels for turbine and generator shafts
OO Superalloys for aerospace and power
	turbines
OO Nickel-based alloys for the chemical
	industry
Fields of Application
OO Aerospace
OO Power generation/Heavy forgings
OO Chemical industry
OO Medical and nuclear industries
OO Tool and die industries
OO Construction industries
OO Automotive industry
Primary benefits of ESR
OO Homogenous, sound and a directionally
	 solidified structure
OO Achievement of directional solidification
	 of the ingot from bottom to top
OO Free of macro-segregation and
	 reduction of micro-segregation
OO High degree of cleanliness
OO Remaining inclusions are very small in
	 size and evenly spread
OO Excellent mechanical properties in
	 transversal and longitudinal directions
OO Free of internal flaws (e.g. hydrogen
	 flakes)
OO Smooth ingot surface resulting in high
	 ingot yield
OO Thin slag skin improves heat transfer
	 to the mold
Further Advantages
OO High material yield in ingot
OO No shrinkage cavities in ingot
OO No conditioning of ingot surface is
	 necessary prior to forging
OO Electrodes for remelting can be used
	 in the as-cast condition	
Courtesy of VDM Metals Intern. GmbH
Courtesy of VDM Metals Intern. GmbH
ESR Features &
Advantages
Electros Slag Remelting
is used wherever high quality
material is required.
04
ESR Process Technology
and Characteristics
ALD’s process expertise
guarantees high
process reproducibility
and material quality.
ALD ESR Features
OO Ingot weights from 100 kg to above
	 200 metric tons
OO AC-current used as remelting energy,
	 from 3 kA to 92 kA
OO Ingot diameters from 80 mm to >2000 mm,
	 depending on material being remelted
OO Round, square and rectangular ingot
	 shapes are possible
OO ALD offers systems for special processes
	 such as remelting under pressure,
	 protective inert gas or vacuum. A growing
	 market share is anticipated for these
	 processes, especially the ESR process
	 under inert gas atmosphere.
OO ESR configurations are available with
	 multiple heads and/or melt withdrawal
	 stations for faster preparation or
	 multiple electrode exchange techniques
	 for larger ingot.
Slags in ESR
Slag chemistries for ESR are usually based
on calcium fluoride (CaF2
), lime (CaO)
and alumina (Al2
O3
). Additions such as
magnesia (MgO), titanium dioxide/titania
(TiO2
) and silica (SiO22
) may also be
added, depending on the alloy to be
remelted. To perform its intended
functions, the slag must have some
well-defined properties, such as:
OO Its melting point must be lower than
	 that of the metal to be remelted
OO It must be electrically efficient
OO Its composition should be selected to
	 ensure the desired chemical reactions
OO It must have suitable viscosity at
	 remelting temperature
Inert ESR
OO Oxidation of electrode and slag is
	 completely avoided.
OO Oxidizing loss of elements such as
	 Ti, Zr, Al, Si, etc. is almost completely
	 avoided. This is especially important
	 when remelting high Al- and Ti-
	 containing alloys, like superalloys with
	 very narrow analytical ranges.
OO Better cleanliness in the ingot is
	achieved.
OO When using argon as the inert gas,
	 pick-up of nitrogen and hydrogen is
	 avoided; (when using nitrogen as the
	 inert gas, some pick-up of nitrogen
	 is possible.)
05
Design Features of
ALD ESR Furnaces
OO Stable or free-standing gantry design
	 of furnace head superstructure
	 features a simple platform installation,
	 with no flexing of the superstructure
	 under load, and provides a consistent
	 centering of the electrode.
OO Proven electro-mechanical, dual-
	 electrode drive system for very
	 precise control of slow ram speeds
	 during the remelting process and
	 faster speeds for charging procedures.
OO Remotely controlled, pneumatically
	 operated electrode/stub clamp with 	
	 maximum melting current transfer
	 to the electrode.
OO Fully coaxial design avoids stirring
	 action of the melt bath due to stray
	 magnetic fields.
OO Power supply with space saving
	 design, either thyristor or saturable
	 reactor control, designed specifically
	 for fast response, tight current control
	 and power control.
OO Sophisticated weight management
	 system including highly accurate,
	 fully temperature compensated load
	 cell system and statistical based melt
	 rate algorithm.
OO Completely automatic operation of
	 the furnace by the use of password-
	 protected preset melt recipes, stored
	 locally or downloaded from any host
	system.
OO Statistical Process Analysis (SPA) is
	 possible with the data acquisition
	 system of the Operator Interface PC
	 in combination with the optional
	 Supervision System PC.
Atmospheric Protection Systems
Two furnace concepts are available, one
with a protective hood system of relative
tightness, the other with a fully vacuum-
tight protective chamber that allows the
complete exchange of air against an inert
gas atmosphere prior to starting the
remelting process.
ALD ESR Furnace
Stationary Mold
Inert Electro Slag Remelting
06
ALD ESR Furnace
Special Designs 	
Pressure and Vacuum
Electro Slag Remelting
Electro Slag Remelting under
Pressure (PESR)
For the production of high nitrogen
steels, it is essential that a sufficiently
high amount of nitrogen above the
solubility limit under normal pressure
is introduced into the molten steel and
that nitrogen loss is prevented during
solidification.
PESR Features
OO Nitrogen content above the solubility
	 limit at atmospheric pressure
OO Continuous nitrogen feed into the
	 furnace interior
OO Operating pressures up to 42 bar in
	 production and 70 bar in laboratory
OO Pressure level depends on
	 composition of the alloy and desired
	 nitrogen content in ingot
OO Pressure prevents nitrogen loss
	 during solidification
OO Liquid solidifies under high pressure
Electro Slag Remelting under
Vacuum (VESR)
Remelting is carried out under vacuum
as in VAR, however, using a slag. The
advantages of both ESR and VAR are
combined in one process.
VESR Features
OO Combined process (VAR and ESR)
OO Avoid hydrogen and nitrogen pick up
OO No moisture from slag
OO No oxidation of the melt
OO Danger of white spots reduced to a
	minimum
07
ALD ESR Furnaces
Ingot Withdrawal
Whenever large dimensions
and heavy weights become
necessary
Ingot Withdrawal Systems
System configurations are available with
a central ingot withdrawal station and
electrode exchange capability, and two
outer stations for remelting in stationary
molds. The central station is particularly
suited for the remelting of large diameter
ingots. Smaller diameter ingots may
be remelted simultaneously in the outer
stations.
Special Design Features
OO 2 heads, 1 center withdrawal station
OO 2 optional outer stations for
	 simultaneous melting
OO Electrode pre-heating device
OO Short electrodes possible
OO Electrode exchange technique
	(automatic)
OO Long ingots in center station
OO Flexible in ingot length
OO Insulation of the ingot in center station
	 to maintain ingot bottom temperature
OO Fully enclosed electrode melting
ESR Process Control 	
ALD’s automatic melt control system (AMC) is unsurpassed
in the world for its accuracy, reproducible metallurgical quality
and ease of operation.
ALD Vacuum Technologies GmbH
Otto-von-Guericke Platz 1
63457 Hanau, Germany
Phone +49 6181 307-0
Fax +49 6181 307-3290
E-Mail info@ald-vt.de
Internet www.ald-vt.de
USA/Canada
ALD Vacuum Technologies Inc.
18 Thomson Road
East Windsor, CT 06088, USA
Phone +1 (860) 386 7227
E-Mail info@ald-usa.com
Far East (Japan/Korea/Taiwan)
ALD Thermo Technologies
Far East Co., Ltd.
Shinjuku Nomura Bldg. 6F
1-26-2 Nishi Shinjuku
Shinjuku-ku
Tokyo 163-0558, Japan
Phone +81 (3) 3340 3726
E-Mail peter.lang@ald-vt.de
China
ALD-C&K Vacuum Technologies
(Suzhou) Co. Ltd.
333 Yegang Road
Wujiang Economic and
Technological Development Zone
Suzhou, 215200, P. R. China
Phone +86 512 6385 8833
E-Mail info@ald-cnk.com
Russia
ALD Vacuum Technologies GmbH
Daev per., 20
Moskau, Russia
Phone +7 (495) 787 6733
E-Mail ald@metallurg.com.ru
ALD provides precise control of all ESR
remelting parameters for the reproducible
production of homogenous ingots, which
are free of macro-segregation and show
a controlled solidification structure and
superior cleanliness.
Computer controlled process automation
used by ESR furnaces fulfill today’s most
stringent material quality specifications.
ALD’s ESR control system
handles
OO Logic control functions
OO Continuous weighing of the
	 consumable electrode
OO Closed loop control of process para-
	 meters (e.g. remelting rate, immersion
	 depth using resistance swing)
OO Data acquisition
OO Data management
OO Communication via field bus or
	 specific interfaces
Operator Interface PC (OIP)
OO Acts hierarchically as master of
	 the automatic melt control
	 system (AMC)
OO Utilized as interface between
	 operator and ESR process
OO Server for process visualization,
	 featuring parameter indication,
	 graphic displays and soft keys for
	 operator commands, editing and
	 handling of remelting recipes,
	 data acquisition and storage and
	 for generation of melt records
OO Can be optionally equipped with an
	 Ethernet network interface which
	 may be utilized for data transfer
	 to other computers connected to the
	 local area network (e.g. supervisory
	 PC, customer’s mainframe, etc.)
Melt Recipes
ALD furnaces work with established
remelting parameters stored as remelting
recipes on a hard disk, for the repeatable
ESR production of specific ingot sizes
and material grade combinations, and to
assure full metallurgical ingot quality.
MetaCom/ESR/09.16

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Electro Slag Melting Processes and Furnaces

  • 1. ALD Vacuum Technologies High Tech is our Business Electro Slag Remelting (ESR) Electro Slag Remelting Processes and Furnaces
  • 2. 02 Generally, the ESR process offers a very high, consistent and predictable product quality. Finely controlled solidification improves soundness and structural integrity. Ingot surface quality is improved by the formation of a solidified thin slag skin between ingot and mold wall during the remelting operation. This is why ESR is recognized as the preferred production method for high- performance superalloys that are used today in industries such as aerospace and nuclear engineering as well as for heavy forgings. ESR Technology ESR is the continuous remelting of a consumable electrode by means of a resistance-heated slag. The main process stages are: OO A consumable ESR electrode is generated by secondary metallurgy or VIM OO Process condition is established (inert gas, vacuum, pressure) OO Slag is added to the bottom of the crystallizer (mold) OO AC power heats the slag OO The intense heat generated by slag resistance melts the tip of the electrode and a new ingot grows in the mold OO De-oxidant or nitriding agents are added OO The melt rate and the immersion of the electrode is precisely regulated by the ESR control system OO Ingot cooling is controlled for directional solidification ALD has improved the basic design of the ESR furnace in computer control and regulation continuously over the years to achieve: OO Fully-automatic remelting processes OO Improved reproducibility of the metallurgy properties. Electro Slag Remelting ALD is one of the leading suppliers of vacuum and inert gas melting furnace technologies for engineered metals.
  • 3. 03 ESR Materials/Alloys OO Tool steels for milling cutters, mining, etc. OO Die steels for the glass, plastic and automotive industries OO Ball-bearing steels OO Cold rolls OO Stainless steels OO Steels for turbine and generator shafts OO Superalloys for aerospace and power turbines OO Nickel-based alloys for the chemical industry Fields of Application OO Aerospace OO Power generation/Heavy forgings OO Chemical industry OO Medical and nuclear industries OO Tool and die industries OO Construction industries OO Automotive industry Primary benefits of ESR OO Homogenous, sound and a directionally solidified structure OO Achievement of directional solidification of the ingot from bottom to top OO Free of macro-segregation and reduction of micro-segregation OO High degree of cleanliness OO Remaining inclusions are very small in size and evenly spread OO Excellent mechanical properties in transversal and longitudinal directions OO Free of internal flaws (e.g. hydrogen flakes) OO Smooth ingot surface resulting in high ingot yield OO Thin slag skin improves heat transfer to the mold Further Advantages OO High material yield in ingot OO No shrinkage cavities in ingot OO No conditioning of ingot surface is necessary prior to forging OO Electrodes for remelting can be used in the as-cast condition Courtesy of VDM Metals Intern. GmbH Courtesy of VDM Metals Intern. GmbH ESR Features & Advantages Electros Slag Remelting is used wherever high quality material is required.
  • 4. 04 ESR Process Technology and Characteristics ALD’s process expertise guarantees high process reproducibility and material quality. ALD ESR Features OO Ingot weights from 100 kg to above 200 metric tons OO AC-current used as remelting energy, from 3 kA to 92 kA OO Ingot diameters from 80 mm to >2000 mm, depending on material being remelted OO Round, square and rectangular ingot shapes are possible OO ALD offers systems for special processes such as remelting under pressure, protective inert gas or vacuum. A growing market share is anticipated for these processes, especially the ESR process under inert gas atmosphere. OO ESR configurations are available with multiple heads and/or melt withdrawal stations for faster preparation or multiple electrode exchange techniques for larger ingot. Slags in ESR Slag chemistries for ESR are usually based on calcium fluoride (CaF2 ), lime (CaO) and alumina (Al2 O3 ). Additions such as magnesia (MgO), titanium dioxide/titania (TiO2 ) and silica (SiO22 ) may also be added, depending on the alloy to be remelted. To perform its intended functions, the slag must have some well-defined properties, such as: OO Its melting point must be lower than that of the metal to be remelted OO It must be electrically efficient OO Its composition should be selected to ensure the desired chemical reactions OO It must have suitable viscosity at remelting temperature Inert ESR OO Oxidation of electrode and slag is completely avoided. OO Oxidizing loss of elements such as Ti, Zr, Al, Si, etc. is almost completely avoided. This is especially important when remelting high Al- and Ti- containing alloys, like superalloys with very narrow analytical ranges. OO Better cleanliness in the ingot is achieved. OO When using argon as the inert gas, pick-up of nitrogen and hydrogen is avoided; (when using nitrogen as the inert gas, some pick-up of nitrogen is possible.)
  • 5. 05 Design Features of ALD ESR Furnaces OO Stable or free-standing gantry design of furnace head superstructure features a simple platform installation, with no flexing of the superstructure under load, and provides a consistent centering of the electrode. OO Proven electro-mechanical, dual- electrode drive system for very precise control of slow ram speeds during the remelting process and faster speeds for charging procedures. OO Remotely controlled, pneumatically operated electrode/stub clamp with maximum melting current transfer to the electrode. OO Fully coaxial design avoids stirring action of the melt bath due to stray magnetic fields. OO Power supply with space saving design, either thyristor or saturable reactor control, designed specifically for fast response, tight current control and power control. OO Sophisticated weight management system including highly accurate, fully temperature compensated load cell system and statistical based melt rate algorithm. OO Completely automatic operation of the furnace by the use of password- protected preset melt recipes, stored locally or downloaded from any host system. OO Statistical Process Analysis (SPA) is possible with the data acquisition system of the Operator Interface PC in combination with the optional Supervision System PC. Atmospheric Protection Systems Two furnace concepts are available, one with a protective hood system of relative tightness, the other with a fully vacuum- tight protective chamber that allows the complete exchange of air against an inert gas atmosphere prior to starting the remelting process. ALD ESR Furnace Stationary Mold Inert Electro Slag Remelting
  • 6. 06 ALD ESR Furnace Special Designs Pressure and Vacuum Electro Slag Remelting Electro Slag Remelting under Pressure (PESR) For the production of high nitrogen steels, it is essential that a sufficiently high amount of nitrogen above the solubility limit under normal pressure is introduced into the molten steel and that nitrogen loss is prevented during solidification. PESR Features OO Nitrogen content above the solubility limit at atmospheric pressure OO Continuous nitrogen feed into the furnace interior OO Operating pressures up to 42 bar in production and 70 bar in laboratory OO Pressure level depends on composition of the alloy and desired nitrogen content in ingot OO Pressure prevents nitrogen loss during solidification OO Liquid solidifies under high pressure Electro Slag Remelting under Vacuum (VESR) Remelting is carried out under vacuum as in VAR, however, using a slag. The advantages of both ESR and VAR are combined in one process. VESR Features OO Combined process (VAR and ESR) OO Avoid hydrogen and nitrogen pick up OO No moisture from slag OO No oxidation of the melt OO Danger of white spots reduced to a minimum
  • 7. 07 ALD ESR Furnaces Ingot Withdrawal Whenever large dimensions and heavy weights become necessary Ingot Withdrawal Systems System configurations are available with a central ingot withdrawal station and electrode exchange capability, and two outer stations for remelting in stationary molds. The central station is particularly suited for the remelting of large diameter ingots. Smaller diameter ingots may be remelted simultaneously in the outer stations. Special Design Features OO 2 heads, 1 center withdrawal station OO 2 optional outer stations for simultaneous melting OO Electrode pre-heating device OO Short electrodes possible OO Electrode exchange technique (automatic) OO Long ingots in center station OO Flexible in ingot length OO Insulation of the ingot in center station to maintain ingot bottom temperature OO Fully enclosed electrode melting
  • 8. ESR Process Control ALD’s automatic melt control system (AMC) is unsurpassed in the world for its accuracy, reproducible metallurgical quality and ease of operation. ALD Vacuum Technologies GmbH Otto-von-Guericke Platz 1 63457 Hanau, Germany Phone +49 6181 307-0 Fax +49 6181 307-3290 E-Mail info@ald-vt.de Internet www.ald-vt.de USA/Canada ALD Vacuum Technologies Inc. 18 Thomson Road East Windsor, CT 06088, USA Phone +1 (860) 386 7227 E-Mail info@ald-usa.com Far East (Japan/Korea/Taiwan) ALD Thermo Technologies Far East Co., Ltd. Shinjuku Nomura Bldg. 6F 1-26-2 Nishi Shinjuku Shinjuku-ku Tokyo 163-0558, Japan Phone +81 (3) 3340 3726 E-Mail peter.lang@ald-vt.de China ALD-C&K Vacuum Technologies (Suzhou) Co. Ltd. 333 Yegang Road Wujiang Economic and Technological Development Zone Suzhou, 215200, P. R. China Phone +86 512 6385 8833 E-Mail info@ald-cnk.com Russia ALD Vacuum Technologies GmbH Daev per., 20 Moskau, Russia Phone +7 (495) 787 6733 E-Mail ald@metallurg.com.ru ALD provides precise control of all ESR remelting parameters for the reproducible production of homogenous ingots, which are free of macro-segregation and show a controlled solidification structure and superior cleanliness. Computer controlled process automation used by ESR furnaces fulfill today’s most stringent material quality specifications. ALD’s ESR control system handles OO Logic control functions OO Continuous weighing of the consumable electrode OO Closed loop control of process para- meters (e.g. remelting rate, immersion depth using resistance swing) OO Data acquisition OO Data management OO Communication via field bus or specific interfaces Operator Interface PC (OIP) OO Acts hierarchically as master of the automatic melt control system (AMC) OO Utilized as interface between operator and ESR process OO Server for process visualization, featuring parameter indication, graphic displays and soft keys for operator commands, editing and handling of remelting recipes, data acquisition and storage and for generation of melt records OO Can be optionally equipped with an Ethernet network interface which may be utilized for data transfer to other computers connected to the local area network (e.g. supervisory PC, customer’s mainframe, etc.) Melt Recipes ALD furnaces work with established remelting parameters stored as remelting recipes on a hard disk, for the repeatable ESR production of specific ingot sizes and material grade combinations, and to assure full metallurgical ingot quality. MetaCom/ESR/09.16