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D1.2Operational demo cases
CS9 - Kalundborg
KWB, Kalundborg Forsyning, Novozymes, Pentair X-Flow
2
The project leading to this application has received funding from the European Union’s
Horizon 2020 research and innovation programme under grant agreement No 869318
CS9: Kalundborg
Lead partner:
Other partners:
3
The project leading to this application has received funding from the European Union’s
Horizon 2020 research and innovation programme under grant agreement No 869318
CS9: Situation before Ultimate
- No water reclamation
from WWTP effluent
- Each WWTP has its
separate control system
- No high added value
product recovery from
wastewater so far
4
The project leading to this application has received funding from the European Union’s
Horizon 2020 research and innovation programme under grant agreement No 869318
CS9: Project objectives in Kalundborg:
- Production of fit-for-purpose water
using a novel membrane pre-
treatment for wastewater with high a
fraction of non-degradable organic
matter
- Energy efficiency increase through
a synergetic operation of two
WWTPs and concept study for heat
recovery
- Concept study for nutrient and/or
high-value product recovery
5
The project leading to this application has received funding from the European Union’s
Horizon 2020 research and innovation programme under grant agreement No 869318
Baseline technology
• no water reuse so far (discharge to the recipient)
Ultimate solution to foster circular economy
• nanofiltration (NF) or novel ultra-tight ultrafiltration
(UF) as pre-treatment for reverse osmosis (RO)
TRL 5  7
Capacity 2 m³/h
Ambition beyond the project
• > 70,000 m³/a fit-for-purpose water production
• > 40% reduction of surface water through reuse of
treated water
Status/progress
• Pilot plants in operation since June 2021
Novel ultra-tight ultrafiltration membrane
 Molecular weight cut off: 4 kDa
 Filtration: inside out
 Material: (modified) polyethersulphone with LbL
Fibre wall Fibre Module head
0.8 mm 1.54 m
Fibre wall Fibre Module head
CS9: Pilot plant: fit-for-purpose water production
Subtask: 1.2.7NovelmembranetreatmentforbiotechorbiotechandmunicipalWWTPeffluentforwaterreuse
6
The project leading to this application has received funding from the European Union’s
Horizon 2020 research and innovation programme under grant agreement No 869318
CS9: Specific challenges at the municipal WWTP
Subtask: 1.2.7NovelmembranetreatmentforbiotechorbiotechandmunicipalWWTPeffluentforwaterreuse
Parameter Unit Content
Electrical conductivity µS/cm 2800-8200
Total dissolved solids mg/L 3500-4200
TOC / COD mg/L 20-60 / 50-190*
Calcium mg/L 98-130
Hydrogen carbonate mg/L 1000-1100
Sulfate mg/L 440-510
* before ozonation for COD removal
Increases pressure in RO
High potential for scaling
High potential for organic
fouling
Increased operational costs
7
The project leading to this application has received funding from the European Union’s
Horizon 2020 research and innovation programme under grant agreement No 869318
Fouling prevention:
 Does the novel ultra tight membrane or nanofiltration membrane prevent better the RO from
fouling than a conventional UF?
 Conventional UF membrane, novel UF membrane and nanofiltration membrane are operated in
parallel in order to compare their performance in terms of fouling prevention
Production of fit-for-purpose water:
 Can we produce fit-for-purpose water for cooling towers and/or boilers?
 Which water quality is reached after UF and for which reuse purpose can the water be used (truck
or street cleaning)?
 Investigation of water quality after each treatment step
CS9: Operational procedures and methodologies
Subtask: 1.2.7NovelmembranetreatmentforbiotechorbiotechandmunicipalWWTPeffluentforwaterreuse
8
The project leading to this application has received funding from the European Union’s
Horizon 2020 research and innovation programme under grant agreement No 869318
Effluent from municipal WWTP:
CS9: Treatment trains
for water recovery
COD
DOC
NF
RO
UF
WWTP
Chemical oxygen demand
Dissolved organic carbon
Nanofiltration
Reverse Osmosis
Ultrafiltration
Wastewater treatment plant
DOC: 20 mg/L
COD: 70 mg/L
9
The project leading to this application has received funding from the European Union’s
Horizon 2020 research and innovation programme under grant agreement No 869318
CS9: Different variants of tested treatment trains
10
The project leading to this application has received funding from the European Union’s
Horizon 2020 research and innovation programme under grant agreement No 869318
CS9: Pictures of the pilot plants
Subtask: 1.2.7 Novel membrane treatment for biotech or biotech and municipal WWTP effluent for water reuse
Pilot A: conventional UF & RO Pilot B: novel ultra tight UF membrane & RO
Pilot B
Pilot A
11
The project leading to this application has received funding from the European Union’s
Horizon 2020 research and innovation programme under grant agreement No 869318
CS9: Pictures of the pilot plants
Subtask: 1.2.7 Novel membrane treatment for biotech or biotech and municipal WWTP effluent for water reuse
Reverse osmosis membranes
Pilot A (conventional UF membrane) Pilot B (novel UF membrane)
12
The project leading to this application has received funding from the European Union’s
Horizon 2020 research and innovation programme under grant agreement No 869318
CS9: Videos of the pilot plants in operation
Subtask: 1.2.7 Novel membrane treatment for biotech or biotech and municipal WWTP effluent for water reuse
Reverse osmosis membranes
Pilot A (conventional UF membrane) Pilot B (novel UF membrane)
These videos are accessible via the indicated links below this
presentation on the ULTIMATE webpage.
13
The project leading to this application has received funding from the European Union’s
Horizon 2020 research and innovation programme under grant agreement No 869318
Legend
Task/Subtask
Activity as planned
Postponed activity
Delay of activity
M1
M2
M3
M4
M5
M6
M7
M8
M9
M10
M11
M12
M1
M2
M3
M4
M5
M6
M7
M8
M9
M10
M11
M12
M1
M2
M3
M4
M5
M6
M7
M8
M9
M10
M11
M12
M1
M2
M3
M4
M5
M6
M7
M8
M9
M10
M11
M12
M1
M2
M3
M4
M5
YEAR 5
YEAR 4
YEAR 1 YEAR 2 YEAR 3
T1.2.7 - Novel membrane treatment for biotech or biotech +
municipal WWTP effluent for water reuse in Kalundborg
Baseline conditions assessed MS05 D1.1
Design of pilot system MS09
Pilot system operational MS15 D1.2
Start-up & results MS19 D1.9
Best practices for water recycling D1.3
CS9: Task 1.2.7 is in time
Subtask: 1.2.7NovelmembranetreatmentforbiotechorbiotechandmunicipalWWTPeffluentforwaterreuse
 Pilot is operational & results obtained: task is in time
 Due to the energy crises, the ozonation facility at the municipal WWTP was shut
down. Hence, ozonation as a pre-treatment option for the water recovery treatment
train cannot be investigated.
 In addition to the foreseen Dynasand filter, a dual media filter was installed
alternatively and is being investigated as pre-treatment option.
The project leading to this application has received funding from the European Union’s
Horizon 2020 research and innovation programme under grant agreement No 869318
anne.kleyboecker@kompetenz-wasser.de
Contacts
jeannette.jaehrig@kompetenz-wasser.de
leo.vredenbregt@pentair.com
lirm@kalfor.dk
prth@kalfor.dk

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D1.2-Demonstrator Case Study Kalundborg

  • 1. D1.2Operational demo cases CS9 - Kalundborg KWB, Kalundborg Forsyning, Novozymes, Pentair X-Flow
  • 2. 2 The project leading to this application has received funding from the European Union’s Horizon 2020 research and innovation programme under grant agreement No 869318 CS9: Kalundborg Lead partner: Other partners:
  • 3. 3 The project leading to this application has received funding from the European Union’s Horizon 2020 research and innovation programme under grant agreement No 869318 CS9: Situation before Ultimate - No water reclamation from WWTP effluent - Each WWTP has its separate control system - No high added value product recovery from wastewater so far
  • 4. 4 The project leading to this application has received funding from the European Union’s Horizon 2020 research and innovation programme under grant agreement No 869318 CS9: Project objectives in Kalundborg: - Production of fit-for-purpose water using a novel membrane pre- treatment for wastewater with high a fraction of non-degradable organic matter - Energy efficiency increase through a synergetic operation of two WWTPs and concept study for heat recovery - Concept study for nutrient and/or high-value product recovery
  • 5. 5 The project leading to this application has received funding from the European Union’s Horizon 2020 research and innovation programme under grant agreement No 869318 Baseline technology • no water reuse so far (discharge to the recipient) Ultimate solution to foster circular economy • nanofiltration (NF) or novel ultra-tight ultrafiltration (UF) as pre-treatment for reverse osmosis (RO) TRL 5  7 Capacity 2 m³/h Ambition beyond the project • > 70,000 m³/a fit-for-purpose water production • > 40% reduction of surface water through reuse of treated water Status/progress • Pilot plants in operation since June 2021 Novel ultra-tight ultrafiltration membrane  Molecular weight cut off: 4 kDa  Filtration: inside out  Material: (modified) polyethersulphone with LbL Fibre wall Fibre Module head 0.8 mm 1.54 m Fibre wall Fibre Module head CS9: Pilot plant: fit-for-purpose water production Subtask: 1.2.7NovelmembranetreatmentforbiotechorbiotechandmunicipalWWTPeffluentforwaterreuse
  • 6. 6 The project leading to this application has received funding from the European Union’s Horizon 2020 research and innovation programme under grant agreement No 869318 CS9: Specific challenges at the municipal WWTP Subtask: 1.2.7NovelmembranetreatmentforbiotechorbiotechandmunicipalWWTPeffluentforwaterreuse Parameter Unit Content Electrical conductivity µS/cm 2800-8200 Total dissolved solids mg/L 3500-4200 TOC / COD mg/L 20-60 / 50-190* Calcium mg/L 98-130 Hydrogen carbonate mg/L 1000-1100 Sulfate mg/L 440-510 * before ozonation for COD removal Increases pressure in RO High potential for scaling High potential for organic fouling Increased operational costs
  • 7. 7 The project leading to this application has received funding from the European Union’s Horizon 2020 research and innovation programme under grant agreement No 869318 Fouling prevention:  Does the novel ultra tight membrane or nanofiltration membrane prevent better the RO from fouling than a conventional UF?  Conventional UF membrane, novel UF membrane and nanofiltration membrane are operated in parallel in order to compare their performance in terms of fouling prevention Production of fit-for-purpose water:  Can we produce fit-for-purpose water for cooling towers and/or boilers?  Which water quality is reached after UF and for which reuse purpose can the water be used (truck or street cleaning)?  Investigation of water quality after each treatment step CS9: Operational procedures and methodologies Subtask: 1.2.7NovelmembranetreatmentforbiotechorbiotechandmunicipalWWTPeffluentforwaterreuse
  • 8. 8 The project leading to this application has received funding from the European Union’s Horizon 2020 research and innovation programme under grant agreement No 869318 Effluent from municipal WWTP: CS9: Treatment trains for water recovery COD DOC NF RO UF WWTP Chemical oxygen demand Dissolved organic carbon Nanofiltration Reverse Osmosis Ultrafiltration Wastewater treatment plant DOC: 20 mg/L COD: 70 mg/L
  • 9. 9 The project leading to this application has received funding from the European Union’s Horizon 2020 research and innovation programme under grant agreement No 869318 CS9: Different variants of tested treatment trains
  • 10. 10 The project leading to this application has received funding from the European Union’s Horizon 2020 research and innovation programme under grant agreement No 869318 CS9: Pictures of the pilot plants Subtask: 1.2.7 Novel membrane treatment for biotech or biotech and municipal WWTP effluent for water reuse Pilot A: conventional UF & RO Pilot B: novel ultra tight UF membrane & RO Pilot B Pilot A
  • 11. 11 The project leading to this application has received funding from the European Union’s Horizon 2020 research and innovation programme under grant agreement No 869318 CS9: Pictures of the pilot plants Subtask: 1.2.7 Novel membrane treatment for biotech or biotech and municipal WWTP effluent for water reuse Reverse osmosis membranes Pilot A (conventional UF membrane) Pilot B (novel UF membrane)
  • 12. 12 The project leading to this application has received funding from the European Union’s Horizon 2020 research and innovation programme under grant agreement No 869318 CS9: Videos of the pilot plants in operation Subtask: 1.2.7 Novel membrane treatment for biotech or biotech and municipal WWTP effluent for water reuse Reverse osmosis membranes Pilot A (conventional UF membrane) Pilot B (novel UF membrane) These videos are accessible via the indicated links below this presentation on the ULTIMATE webpage.
  • 13. 13 The project leading to this application has received funding from the European Union’s Horizon 2020 research and innovation programme under grant agreement No 869318 Legend Task/Subtask Activity as planned Postponed activity Delay of activity M1 M2 M3 M4 M5 M6 M7 M8 M9 M10 M11 M12 M1 M2 M3 M4 M5 M6 M7 M8 M9 M10 M11 M12 M1 M2 M3 M4 M5 M6 M7 M8 M9 M10 M11 M12 M1 M2 M3 M4 M5 M6 M7 M8 M9 M10 M11 M12 M1 M2 M3 M4 M5 YEAR 5 YEAR 4 YEAR 1 YEAR 2 YEAR 3 T1.2.7 - Novel membrane treatment for biotech or biotech + municipal WWTP effluent for water reuse in Kalundborg Baseline conditions assessed MS05 D1.1 Design of pilot system MS09 Pilot system operational MS15 D1.2 Start-up & results MS19 D1.9 Best practices for water recycling D1.3 CS9: Task 1.2.7 is in time Subtask: 1.2.7NovelmembranetreatmentforbiotechorbiotechandmunicipalWWTPeffluentforwaterreuse  Pilot is operational & results obtained: task is in time  Due to the energy crises, the ozonation facility at the municipal WWTP was shut down. Hence, ozonation as a pre-treatment option for the water recovery treatment train cannot be investigated.  In addition to the foreseen Dynasand filter, a dual media filter was installed alternatively and is being investigated as pre-treatment option.
  • 14. The project leading to this application has received funding from the European Union’s Horizon 2020 research and innovation programme under grant agreement No 869318 anne.kleyboecker@kompetenz-wasser.de Contacts jeannette.jaehrig@kompetenz-wasser.de leo.vredenbregt@pentair.com lirm@kalfor.dk prth@kalfor.dk