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Research Results and
Recommendations for
High RAP mixes in California
Mohamed Elkashef, UC Pavement Research Center
CalAPA conference, November 2019
High RAP defined as > 25% binder replacement.
Why RAP binder replacement ?
Use of Rejuvenators
 Type of rejuvenators.
 Rejuvenators Vs softening agents.
 How to account for the rejuvenator ?
2
RAP increases mix stiffness and reduces cracking/fatigue
resistance.
Partial to full blending occurs between RAP/Virgin binder.
Full blending is difficult to attain with increasing RAP
content and RAP stiffness.
Rejuvenators can mitigate the effect of using high RAP.
Effect of rejuvenators on durability and moisture sensitivity.
3
 Mixes between 30-50% RAP
 Proposed AASHTO standard of practice
 Pre-selection of materials
• RAP binder (PGH > 100 is not recommended to use in high RAP mixes)
• Virgin binder (limit on ΔTc )
• Intermediate temperature for binder evaluation
• Glover-Rowe parameter
• Crossover temperature (@ phase angle = 45oC)
• Intermediate temperature for mixes
• SCB: FI >= 7 after STOA
• High temp. blending charts can be used to estimate rejuvenator dose
• RAP binder availability factor dependent on mixing temperature and
PGH of RAP
4
NCAT
 Test sections containing 15-35% RAP
 1.5” surface lifts
 Different AC content, compaction density, binder types to yield
different expected cracking resistance.
 FI and IDEAL-CT ranked mixes similarly
 IDEAL-CT faster and easier to perform
MnROAD
 30-40% RAP mixes with different types of rejuvenators.
 10 different test sections.
 Assess long-term performance
5
Industry:
- Maximize binder replacement, aggregate replacement less important
- Limit use of extraction and recovery (except for greater than 25% binder
replacement)
Caltrans:
 Manage risks of effect of RAP binder on cracking resistance
 Have tests and specifications to assess and manage that risk
 Tests should balance providing actionable information with time, cost,
simplicity; variability needs to be appropriate for use in specifications
 Tests need to provide information/indicators about the property being
investigated of interest in California: stiffness and fatigue cracking
6
Routine mix design, QC/QA
Getting started on field use and spec development as
soon as possible
7
Blending charts
 High temperature PG restricts use of RAP compared to low and
intermediate temperatures
 RAP1 (Sacramento) PG 107-2
 RAP2 (SF Bay Area) PG 89-8
8
Based on
HT
Based on
IT
RAP1 18% 27%
RAP2 25% 32%
Based on
HT
Based on
IT
RAP1 6% 8%
RAP2 8% 10%
No change in virgin
binder
Using softer virgin
binder
 Not consistent.Varies based on RAP stiffness, test frequency (rate of
loading), and test temperature.
 R1 (Sacramento RAP)
 Continuous PG107-2
 R2 (Bay Area RAP)
 Continuous PG89-8
9
RAP binder blends using a PG64-16
 Effect measured by binder testing
does not truly represent mix
testing, mainly due to blending.
 Softer RAP2 (Bay Area region)
produced stiffer mixes because
RAP binder did not completely
blend with virgin binder
10
FAM mixes
11
 Dependent on time, temperature, RAP stiffness, and RAP binder
replacement.
 Higher RAP binder replacement and stiffer RAP require longer time
at high temperatures to get blending/diffusion.
 Sufficient time and temperature needed, but results in more aging.
 AC content – Overall binder properties.
 RAS does not blend effectively (tear offs)
 Predictive models (correlating binder and mix testing) need to
account for blending.
12
 Wafer composite binder specimens made of 1-mm thick virgin binder
placed on top of a 1-mm thick aged RAP binder
 Control wafer specimens made of 2-mm thick fully blended
RAP/virgin binder.
Wafer DSR specimen Change in modulus with time
13
RAP in RHMA Mixes
 Amount of RAP limited to 10
percent to maintain gap-gradation
and pass Superpave volumetric
requirements
 Reduced cracking resistance
negating benefit of RHMA-G as an
overlay to resist reflection
cracking.
Ongoing study
 Using Coarse RAP to limit binder
replacement
14
0
0.5
1
1.5
2
2.5
3
3.5
4
4.5
0 1 2 3 4 5
Load(kN)
Deformation (mm)
Peak load
Slope(Spp)
P1= peak load
P2= peak load
Work of
fracture (Wf)
Slope(Sasc)
 Uses a notched semi-circular
specimen.
 Parameters calculated from
SCB test results.
• FI = Fracture Energy/Spp
• Front slope (Sasc)
• Stress-Intensity factor (KIC)
 Mixes containing different RAP percentages and binder types
tested using SCB and Beam Fatigue.
 Flexibility index was found not to correlate well with fatigue results.
15
R
2
= 0.32
200
400
600
800
0.0 2.5 5.0 7.5 10.0 12.5
FI
StrainlevelwhenNf=1M
MIX
0% RAP with AR binder
12%RAP with PM binder
15%RAP with neat binder
15%RAP with PG+X binder
15%RAP with PM binder
25%RAP with neat binder
25%RAP with PM binder
SCB fracture toughness & beam fatigue
16
R
2
= 0.61
2500
5000
7500
10000
12500
5 10
Sasc
E50
MIX
0% RAP with AR binder
12%RAP with PMbinder
15%RAP with neat binder
15%RAP with PG+Xbinder
15%RAP with PMbinder
25%RAP with neat binder
25%RAP with PMbinder
R
2
= 0.72
-5
-4
-3
-2
-1
0
-1.0 -0.5 0.0
ln(KIC)
ln(StrainlevelwhenNf=1M/E50)
MIX
0% RAP
12%RAP
15%RAP
15%RAP
15%RAP
25%RAP
25%RAP
SCB stiffness & beam stiffness
17
 Both bio-based and petroleum-based rejuvenators were added at 10%
dose of RAP binder.
 Effect of rejuvenator can be assessed using critical temperatures and
ΔTc
RAP RAP+PetR RAP+BioR
High Temp. (oC) 95.1 82.1 70.5
Intermediate Temp. (oC) 49.7 42.2 28.1
Low Temp. (oC) -4.2 -9.4 -21.5
ΔTc -1.2 0.8 2
18
 Colloidal Instability Index (CII):
Saturates+Asphaltenes /Aromatics+ Resins
CII = 0.67
CII = 0.58
CII = 0.52
 Rejuvenation enhance low temperature properties of the RAP binder.
 Rejuvenation improves stress relaxation properties of the RAP binder.
19
RAP
20
Rejuvenated RAP
 Work with industry to test and evaluate plant mixes and raw
materials for HMA with more than 25% RAP.
 Objectives:
 Evaluate ability of simple mix testing to flag high RAP mixes.
 Evaluate effect of time/temperature on blending, aging and overall mix
properties.
 Assess suitability of blending charts to produce well-performing mixes.
 Approach:
 Document the approach and assumptions, analyze performance-
related test results; binder extraction/blending results if available
 Combine results with lab study underway
Deliverables
 Initial specification limits for mix tests, effectiveness of blending
charts and parameters to limit risk for cracking
21
 4 plant mixes from different plants.
 Mixes collected at 2 aging conditions:
 a) No silo time, b) >= 6 hours silo time
 Mixes compacted at UCPRC and tested for:
 Stiffness using beam bending frequency sweeps.
 Fatigue using beam bending fatigue.
 Repeated load triaxial test using AMPT
 Simple tests include SCB and IDEAL-CT to assess stiffness/fatigue.
 Raw materials collected and tested:
 Binder Testing.
 Fine Aggregate Matrix (FAM) testing.
22
 Performance-related tests include SCB , IDEAL-CT, Beam fatigue and
flexural stiffness, Hamburg, and FAM
23
Mix RAP RAS Virgin
Binder
AC
Content
Rejuvenator Silo Times (hrs)
A 50% - PG64-10 5.1% Aromatic
10%
0, 6
B 40% - PG58-28 5.3% - 0, 16
C 20% 3% PG58-22 5% - 0, 5
D 35% - PG64-10 5.8% Bio-derived 0,6
 Flexibility index dropped
significantly with silo time.
 More silo time promotes
blending and induce aging.
 Mix B not containing rejuvenator
also exhibited same effect.
 High FI at 0 hours despite high
RAP content (possible indication
of poor blending).
24
 Fine portion of the asphalt mix passing
#8.
 Tested in a DSR under oscillatory
sinusoidal loading.
 Sample dimensions 12.5 mm x 50 mm
 FAM mixes provided a good alternative
to testing full-graded mixes to get
complete stiffness curves and fatigue;
only research use at this point
25
 Increase in stiffness with silo time
evident at all test frequencies
(i.e. temperatures)
26
 Linear amplitude sweep: Modulus is measured with increasing strain
amplitudes.
 Aged mix start at a higher stiffness but fails at a lower strain level
27
Fatigue Life Modulus vs strain level
 Effect of rejuvenators on properties of binders and mixes with aging
 Assess rejuvenators’ effectiveness without extraction and recovery
 Understand blending/diffusion between RAP and virgin binders with
and without rejuvenators.
 Effect of silo time and temperature on blending and aging
 Assess suitability of current tests; SCB and IDEAL-CT, to get strong
indicators of stiffness and fatigue performance
 Review panel: A. Epps Martin, E. Arambula
28
 Testing include FAM and full-graded mixes
 Long term aging of mixes to study durability of rejuvenated mixes.
 Stiffness (Frequency sweeps)
 Cracking (Beam fatigue, SCB, IDEAL-CT)
29
Factor Number Variables
RAP sources
RAP content (%)
Virgin binders
Rejuvenators
Rejuvenator dosages
3
3
2
3
2
Central Valley, Bay Area, Southern California
0, 25, 50
PG58-22, PG64-16
Aromatic extract, bio-based, tall oil
Dependent on product
 Selection of projects for pilots using draft specifications
 Build pilots, collect plant mix, cores and beams, and raw materials, perform
full set of binder and mix tests
 Run CalME using properties of tested mixes assuming different conditions
(climates, traffic, etc.) to look at effects of specification and whether higher
stiffnesses in some structures are appropriate
 Provide recommendations on suitability of high RAP mixes for different
applications, including different specs for thicker layers, and updated
specifications
 Establish long-term monitoring, periodic review for pilot sections
 Deliverables: updated specifications for different structures and climates
30
Any Questions ?
melkashef@ucdavis.edu
http://www.ucprc.ucdavis.edu/
Director: Prof. John Harvey
Associate Director: Dr. David Jones
31

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Evaluating High Reclaimed Asphalt Pavement (RAP) Mixes

  • 1. Research Results and Recommendations for High RAP mixes in California Mohamed Elkashef, UC Pavement Research Center CalAPA conference, November 2019
  • 2. High RAP defined as > 25% binder replacement. Why RAP binder replacement ? Use of Rejuvenators  Type of rejuvenators.  Rejuvenators Vs softening agents.  How to account for the rejuvenator ? 2
  • 3. RAP increases mix stiffness and reduces cracking/fatigue resistance. Partial to full blending occurs between RAP/Virgin binder. Full blending is difficult to attain with increasing RAP content and RAP stiffness. Rejuvenators can mitigate the effect of using high RAP. Effect of rejuvenators on durability and moisture sensitivity. 3
  • 4.  Mixes between 30-50% RAP  Proposed AASHTO standard of practice  Pre-selection of materials • RAP binder (PGH > 100 is not recommended to use in high RAP mixes) • Virgin binder (limit on ΔTc ) • Intermediate temperature for binder evaluation • Glover-Rowe parameter • Crossover temperature (@ phase angle = 45oC) • Intermediate temperature for mixes • SCB: FI >= 7 after STOA • High temp. blending charts can be used to estimate rejuvenator dose • RAP binder availability factor dependent on mixing temperature and PGH of RAP 4
  • 5. NCAT  Test sections containing 15-35% RAP  1.5” surface lifts  Different AC content, compaction density, binder types to yield different expected cracking resistance.  FI and IDEAL-CT ranked mixes similarly  IDEAL-CT faster and easier to perform MnROAD  30-40% RAP mixes with different types of rejuvenators.  10 different test sections.  Assess long-term performance 5
  • 6. Industry: - Maximize binder replacement, aggregate replacement less important - Limit use of extraction and recovery (except for greater than 25% binder replacement) Caltrans:  Manage risks of effect of RAP binder on cracking resistance  Have tests and specifications to assess and manage that risk  Tests should balance providing actionable information with time, cost, simplicity; variability needs to be appropriate for use in specifications  Tests need to provide information/indicators about the property being investigated of interest in California: stiffness and fatigue cracking 6
  • 7. Routine mix design, QC/QA Getting started on field use and spec development as soon as possible 7
  • 8. Blending charts  High temperature PG restricts use of RAP compared to low and intermediate temperatures  RAP1 (Sacramento) PG 107-2  RAP2 (SF Bay Area) PG 89-8 8 Based on HT Based on IT RAP1 18% 27% RAP2 25% 32% Based on HT Based on IT RAP1 6% 8% RAP2 8% 10% No change in virgin binder Using softer virgin binder
  • 9.  Not consistent.Varies based on RAP stiffness, test frequency (rate of loading), and test temperature.  R1 (Sacramento RAP)  Continuous PG107-2  R2 (Bay Area RAP)  Continuous PG89-8 9 RAP binder blends using a PG64-16
  • 10.  Effect measured by binder testing does not truly represent mix testing, mainly due to blending.  Softer RAP2 (Bay Area region) produced stiffer mixes because RAP binder did not completely blend with virgin binder 10 FAM mixes
  • 11. 11  Dependent on time, temperature, RAP stiffness, and RAP binder replacement.  Higher RAP binder replacement and stiffer RAP require longer time at high temperatures to get blending/diffusion.  Sufficient time and temperature needed, but results in more aging.  AC content – Overall binder properties.  RAS does not blend effectively (tear offs)  Predictive models (correlating binder and mix testing) need to account for blending.
  • 12. 12  Wafer composite binder specimens made of 1-mm thick virgin binder placed on top of a 1-mm thick aged RAP binder  Control wafer specimens made of 2-mm thick fully blended RAP/virgin binder. Wafer DSR specimen Change in modulus with time
  • 13. 13 RAP in RHMA Mixes  Amount of RAP limited to 10 percent to maintain gap-gradation and pass Superpave volumetric requirements  Reduced cracking resistance negating benefit of RHMA-G as an overlay to resist reflection cracking. Ongoing study  Using Coarse RAP to limit binder replacement
  • 14. 14 0 0.5 1 1.5 2 2.5 3 3.5 4 4.5 0 1 2 3 4 5 Load(kN) Deformation (mm) Peak load Slope(Spp) P1= peak load P2= peak load Work of fracture (Wf) Slope(Sasc)  Uses a notched semi-circular specimen.  Parameters calculated from SCB test results. • FI = Fracture Energy/Spp • Front slope (Sasc) • Stress-Intensity factor (KIC)
  • 15.  Mixes containing different RAP percentages and binder types tested using SCB and Beam Fatigue.  Flexibility index was found not to correlate well with fatigue results. 15 R 2 = 0.32 200 400 600 800 0.0 2.5 5.0 7.5 10.0 12.5 FI StrainlevelwhenNf=1M MIX 0% RAP with AR binder 12%RAP with PM binder 15%RAP with neat binder 15%RAP with PG+X binder 15%RAP with PM binder 25%RAP with neat binder 25%RAP with PM binder
  • 16. SCB fracture toughness & beam fatigue 16 R 2 = 0.61 2500 5000 7500 10000 12500 5 10 Sasc E50 MIX 0% RAP with AR binder 12%RAP with PMbinder 15%RAP with neat binder 15%RAP with PG+Xbinder 15%RAP with PMbinder 25%RAP with neat binder 25%RAP with PMbinder R 2 = 0.72 -5 -4 -3 -2 -1 0 -1.0 -0.5 0.0 ln(KIC) ln(StrainlevelwhenNf=1M/E50) MIX 0% RAP 12%RAP 15%RAP 15%RAP 15%RAP 25%RAP 25%RAP SCB stiffness & beam stiffness
  • 17. 17  Both bio-based and petroleum-based rejuvenators were added at 10% dose of RAP binder.  Effect of rejuvenator can be assessed using critical temperatures and ΔTc RAP RAP+PetR RAP+BioR High Temp. (oC) 95.1 82.1 70.5 Intermediate Temp. (oC) 49.7 42.2 28.1 Low Temp. (oC) -4.2 -9.4 -21.5 ΔTc -1.2 0.8 2
  • 18. 18  Colloidal Instability Index (CII): Saturates+Asphaltenes /Aromatics+ Resins CII = 0.67 CII = 0.58 CII = 0.52
  • 19.  Rejuvenation enhance low temperature properties of the RAP binder.  Rejuvenation improves stress relaxation properties of the RAP binder. 19
  • 21.  Work with industry to test and evaluate plant mixes and raw materials for HMA with more than 25% RAP.  Objectives:  Evaluate ability of simple mix testing to flag high RAP mixes.  Evaluate effect of time/temperature on blending, aging and overall mix properties.  Assess suitability of blending charts to produce well-performing mixes.  Approach:  Document the approach and assumptions, analyze performance- related test results; binder extraction/blending results if available  Combine results with lab study underway Deliverables  Initial specification limits for mix tests, effectiveness of blending charts and parameters to limit risk for cracking 21
  • 22.  4 plant mixes from different plants.  Mixes collected at 2 aging conditions:  a) No silo time, b) >= 6 hours silo time  Mixes compacted at UCPRC and tested for:  Stiffness using beam bending frequency sweeps.  Fatigue using beam bending fatigue.  Repeated load triaxial test using AMPT  Simple tests include SCB and IDEAL-CT to assess stiffness/fatigue.  Raw materials collected and tested:  Binder Testing.  Fine Aggregate Matrix (FAM) testing. 22
  • 23.  Performance-related tests include SCB , IDEAL-CT, Beam fatigue and flexural stiffness, Hamburg, and FAM 23 Mix RAP RAS Virgin Binder AC Content Rejuvenator Silo Times (hrs) A 50% - PG64-10 5.1% Aromatic 10% 0, 6 B 40% - PG58-28 5.3% - 0, 16 C 20% 3% PG58-22 5% - 0, 5 D 35% - PG64-10 5.8% Bio-derived 0,6
  • 24.  Flexibility index dropped significantly with silo time.  More silo time promotes blending and induce aging.  Mix B not containing rejuvenator also exhibited same effect.  High FI at 0 hours despite high RAP content (possible indication of poor blending). 24
  • 25.  Fine portion of the asphalt mix passing #8.  Tested in a DSR under oscillatory sinusoidal loading.  Sample dimensions 12.5 mm x 50 mm  FAM mixes provided a good alternative to testing full-graded mixes to get complete stiffness curves and fatigue; only research use at this point 25
  • 26.  Increase in stiffness with silo time evident at all test frequencies (i.e. temperatures) 26
  • 27.  Linear amplitude sweep: Modulus is measured with increasing strain amplitudes.  Aged mix start at a higher stiffness but fails at a lower strain level 27 Fatigue Life Modulus vs strain level
  • 28.  Effect of rejuvenators on properties of binders and mixes with aging  Assess rejuvenators’ effectiveness without extraction and recovery  Understand blending/diffusion between RAP and virgin binders with and without rejuvenators.  Effect of silo time and temperature on blending and aging  Assess suitability of current tests; SCB and IDEAL-CT, to get strong indicators of stiffness and fatigue performance  Review panel: A. Epps Martin, E. Arambula 28
  • 29.  Testing include FAM and full-graded mixes  Long term aging of mixes to study durability of rejuvenated mixes.  Stiffness (Frequency sweeps)  Cracking (Beam fatigue, SCB, IDEAL-CT) 29 Factor Number Variables RAP sources RAP content (%) Virgin binders Rejuvenators Rejuvenator dosages 3 3 2 3 2 Central Valley, Bay Area, Southern California 0, 25, 50 PG58-22, PG64-16 Aromatic extract, bio-based, tall oil Dependent on product
  • 30.  Selection of projects for pilots using draft specifications  Build pilots, collect plant mix, cores and beams, and raw materials, perform full set of binder and mix tests  Run CalME using properties of tested mixes assuming different conditions (climates, traffic, etc.) to look at effects of specification and whether higher stiffnesses in some structures are appropriate  Provide recommendations on suitability of high RAP mixes for different applications, including different specs for thicker layers, and updated specifications  Establish long-term monitoring, periodic review for pilot sections  Deliverables: updated specifications for different structures and climates 30
  • 31. Any Questions ? melkashef@ucdavis.edu http://www.ucprc.ucdavis.edu/ Director: Prof. John Harvey Associate Director: Dr. David Jones 31