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International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395 -0056
Volume: 04 Issue: 05 | May -2017 www.irjet.net p-ISSN: 2395-0072
© 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 2986
Flow time analysis of blended mixes using Marsh cone apparatus
Abdul Razak.B.H1,Rakesh.R2,Gaurav Ranjan3,Ashish Kumar Singh4,Uttkarsh Tyagi5
1 Assistant Professor, Dept.of Civil Engineering, JSS Academy of Technical Education, Karnataka, India
2,3,4,5UG scholar, Dept.of Civil Engineering, JSS Academy of Technical Education, Karnataka, India
---------------------------------------------------------------------***---------------------------------------------------------------------
Abstract -Admixture-Cement interaction in
concrete is a complex blend of chemical and physical
mechanism that are independent. Every admixture at
optimum dosage gives better results when used with
cement. The proposed research is aimed to study the
compatibility of super plasticizer with different types of
blended cements by investigatingflow time value. The
present work is to study the behaviour of blended mixes
(OPC+GGBS+ALCCOFINE) with the PCE (poly carboxylic
ether) based admixtures at various dosages of both
GGB,ALCCOFINE and chemical admixture. It was observed
that most of the blended mixes were compatible with PCE
based admixtures at dosages of around 3%. Increase in flow
time has been observed with the addition of ALCCOFINE.
Key Words: GGBS, ALCCOFINE, PCE based admixture,
Compatibility
1. INTRODUCTION
The hydration of cement involves series of reactions,
which mainly depend on the cement composition, the
water / cement ratio, surface area, particle size
distribution, temperature and admixtures. Admixtures
when added in small quantities make the hydration
process much more complex. In recent times, advances in
the field of cement products are related to the use of
admixtures particularly organic polymeric materials.
Many type of organic polymeric materials, known as
superplasticizers, are being used in construction
industries to alter the flow behaviour and the mechanical
properties of concretes. Among various types of chemical
admixtures, PCE based admixtures proved to enhance the
flow fresh and hardened properties of concrete at low
dosage.
2. Literature Review
The present investigation deals with the study of
compatibility of chemical admixtures with different mixes.
The study also deals with the fresh and hardened
properties of blended concrete. The relevant literature
available in this area has been critically studied and
discussed.
Anshuman Dogra and Richa Bhardwaj (1) investigated
the compatibility behaviour of superplasticizers with
cement containing mineral admixtures like fly ash,
alccofine. It was observed that Polycarboxylate Ether(PCE)
based super plasticizers show greater compatibility and
economical dosage as compared to sulphonated
Napthalene Formaldehyde(SNF) based superplasticizers.
M.K.Maroliya (2) studied the change in ingredients
contents of concrete like sand and cement under the
influence of plasticizers and superplasticizers at various
dosages level. It was also observed that plasticizers
enhanced the compressive strength at reduced water-
cement ratio in addition to improved workability at
constant water cement ratio. Reduction in cement content
was achieved with increase in sand content to overcome
bleeding and segregation.
Janardhana Maganti and V.Silva Prasada Raju(3)
studied compatibility of Sulphonated Naphthalene
Formaldehyde and Lignosulphonates based
superplasticizer with Portland slag cements. It was
observed that the different brands of cements behaved
differently even if the coarse and fine aggregates, water
and family of chemical admixture and the method of
concrete mix design were kept constant.
S.Sheela(4) studied the workability and strength behavior
of superplasticized concrete and conventional concrete
both in fresh and hardened states. It was also observed
that the use of superplasticizer can increase the
workability and strength without increasing the water
cement ratio. It was also concluded that non destructive
testing values were in good agreement with the strength
behavior of superplasticized concrete for destructive
testing.
Ravindra Gettu, Dr.Joana Roncero (5) studied some
aspects related to the dosage of superplasticizer using the
Marsh Cone test and the effect of the temperature in
superplasticized pastes are evaluated. The study also
included the loss of fluidity of cement paste with time. The
study revealed that polycarboxylic acid based
superplasticizers performed better than naphthalene and
melamine based admixtures.
3. OBJECTIVE
 Study of characteristics of different series of
cement mixes (double blended) with different
types of chemical admixtures.
 Study the flow time values of blended cements for
optimum dosage of chemical admixtures.
 Impart additional guidelines for the usage of
ALCCOFINE in preparing flowable concrete.
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395 -0056
Volume: 04 Issue: 05 | May -2017 www.irjet.net p-ISSN: 2395-0072
© 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 2987
4. MATERIALS USED
 Cement: Ordinary Portland Cement (OPC),
Ground Granulated Blast furnace slag(GGBS),
ALCCOFINE
 Chemical Admixtures: Polycarboxylic acid
based.
 Water: Potable water
5. METHODOLOGY
 Study on properties of different types of blended
cement and cementitious materials.
 Study on flow time using Marsh Cone Apparatus.
 Mix design of concrete using IS method.
6. EXPERIMENTAL WORK
 Study on properties of ingredients
Cement:
The following tests have been carried out for the
OPC
Specific gravity test
Fineness of cement
Mineral admixture(GGBS,ALCCOFINE)
Specific Gravity test has been carried out for GGBS and
ALCCOFINE
Chemical Admixtures
Specific Gravity test has been carried out for Chemical
Admixture
 Study on flow time(Marsh Cone Test)
The test is carried to check the flow time for 1000 ml
of cement paste to completely pass through nozzle of the
Marsh cone is determined for various dosages of chemical
admixture and for various percentages of cement
replacement by GGBS and ALCCOFINE.
Preparation of cement paste
 Cement paste of 1200 ml is prepared by keeping
the w/c cement ratio of 0.5.
 Mixing is done for 4 minutes in the mortar
mixer(2 minutes at high speed and 2 minutes at
low speed).
7.RESULTS
TEST ON INGREDIENTS
Specific Gravity
SL NO MATERIAL SPECIFIC GRAVITY
1 Cement (OPC) 3.05
2 GGBS 2.86
3 ALCCOFINE 3.44
Fineness
SL NO MATERIAL FINENESS
1 OPC 4%
GRAPHS OF FLOW TIME TEST
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395 -0056
Volume: 04 Issue: 05 | May -2017 www.irjet.net p-ISSN: 2395-0072
© 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 2988
TESTS ON CEMENT PASTE (Flow Time Test)
Sl. No Cement
Content,
grams
GGBS,
grams
ALCCOFINE,
grams
W/C
ratio
Water
Content,
ml
Chemical
Admixture
Dosage in
%
Chemical
Admixture
Content,
ml
Flow
Time
, Sec
80% = OPC, 10% = GGBS, 10% = ALCCOFINE
1 1114.2 139.27 139.27 0.4 557.1 0% - 316
2 1102.3 137.8 137.8 0.4 551.1 1% 12.86 95
3 1086.18 135.77 135.7 0.4 543.09 2% 25.143 53
4 1072.89 134.13 134.13 0.4 536.96 3% 36.79 55
5 1059.5 132.4 132.4 0.4 529.77 4% 49.05 62
70% = OPC, 20% = GGBS, 10% = ALCCOFINE
1 970.57 277.3 138.65 0.4 554.61 0% - 380
2 957.88 273. 136.79 0.4 547.21 1% 12.5 101
3 946.27 270.36 135.18 0.4 540.73 2% 25.03 58
4 935.88 266.73 133.34 0.4 533.91 3% 37.1 53
5 923.17 263.76 131.88 0.4 527.52 4% 49 64
60% = OPC, 30% = GGBS, 10% = ALCCOFINE
1 828 414 138 0.4 552 0% - 413
2 817.75 408.95 136.45 0.4 544.8 1% 13.45 110
3 807.56 403.8 134.9 0.4 538.4 2% 26.91 59
4 797.1 398.8 133.1 0.4 531.8 3% 40.21 51
5 787.9 393.9 131.32 0.4 525.3 4% 52.53 63
50% = OPC, 40% = GGBS, 10% = ALCCOFINE
1 687.1 549.68 137.42 0.4 549.7 0% - 482
2 678.56 542.23 135.17 0.4 542.1 1% 13.4 123
3 669.77 535.8 133.95 0.4 535.8 2% 26.8 84
4 661.66 529.4 132.28 0.4 529.4 3% 40.1 67
5 653.56 522.9 130.71 0.4 522.9 4% 52.3 75
40% = OPC, 50% = GGBS, 10% = ALCCOFINE
1 547.32 684.1 136.83 0.4 547.2 0% - 520
2 540.35 675.4 135.09 0.4 540.35 1% 13.35 228
3 533.38 666.7 133.34 0.4 533.38 2% 26.7 64
4 527.06 658.55 131.67 0.4 527.06 3% 39.95 57
5 520.74 650.4 130 0.4 520.3 4% 52.03 58
CONCLUSION
 ALCCOFINE can also be utilized as a high range
water reducer to improve compressive strength
or as a super workability aid to improve flow.
 Due to lower hydration rate of GGBS, curing time
should be prolonged than portland cement
concrete.
 The addition of ALCCOFINE in cement mixes
increases the self compatibility characteristic like
filling ability ,passing ability and .resistance to
segregation.
 The relative cost of Alccofine is cheaper than
cement hence it is also economic with higher
strength.
 Usage of mineral admixtures reduces the cost of
concrete production.
International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395 -0056
Volume: 04 Issue: 05 | May -2017 www.irjet.net p-ISSN: 2395-0072
© 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 2989
9. REFERENCES
[1]Anshuman Dogra and Richa Bhardwaj “Study of the
admixture-cement compatibility for the economic
production of special concretes” International Journal of
Civil Engineering Research”, Vol.5, No.1, 2014, pp 43-
48,ISSN 2278-3652
[2]M.K.Maroliya “Influence of type of chemical admixtures
on sand and cement content of ordinary grade concrete”,
International Journal of advances in Engineering &
Technology, Nov 2012,pp298-302.
[3]Janardhana Maganti,V.Silva Prasada Raju “Compatibility
of Sulphonated Naphthalene Formaldehyde and
Lignosulphonates based Superplasticizer with Portland
Slag Cements”, Third international conference on
sustainable construction materials and technologies.
[4]S.Sheela “Study on workability and strengthBehaviour
of concrete by the additionOf different admixtures”
Proceedings of the INCONTEST 2003 on 10 –12,
September 2003.
[5] L.Ferrari,J.Kaufmann,F.Winnefeld,J.Plank “Multi
method approach to study influence of superplasticizers
on cement suspensions”, Cement and Concrete
Composites,ELSEVIER, Vol.41,2011, pp.1058-1066.
[6] Anatol Zingg, Frank Winnefeld, Lorenz Holder, Joachin
Pakusch, Stefan Becker, Renato Figi, Ludwig Gauckler.,
“Interaction of polycarboxylate-based superplasticizers
with cements containing different C3A amounts”, Cement
and Concrete Composites,ELSEVIER, Vol.31,2009, pp.153-
162.
BIOGRAPHIES
Prof. Abdul Razak.B.H. is
working as Assistant
Professor at department
of civil engineering, JSS
Academy of Technical
Education, Bangalore,
Karnataka, India. He has
published several
technical papers in the
reputed journals and also
authored handbooks in
Civil Engineering.
Mr.Rakesh.R is an under
graduate scholar in the
department of Civil
Engineering in JSS
ACADEMY OF TECHNICAL
EDUCATION,
BANGALORE, INDIA
Mr.Gaurav Ranjan is an
under graduate scholar in
the department of Civil
Engineering in JSS
ACADEMY OF TECHNICAL
EDUCATION,
BANGALORE, INDIA
Ashish Kumar Singh is an
under graduate scholar in
the department of Civil
Engineering in JSS
ACADEMY OF TECHNICAL
EDUCATION,
BANGALORE, INDIA
Uttkarsh Tyagi is an
under graduate scholar in
the department of Civil
Engineering in JSS
ACADEMY OF TECHNICAL
EDUCATION,
BANGALORE, INDIA

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  • 1. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395 -0056 Volume: 04 Issue: 05 | May -2017 www.irjet.net p-ISSN: 2395-0072 © 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 2986 Flow time analysis of blended mixes using Marsh cone apparatus Abdul Razak.B.H1,Rakesh.R2,Gaurav Ranjan3,Ashish Kumar Singh4,Uttkarsh Tyagi5 1 Assistant Professor, Dept.of Civil Engineering, JSS Academy of Technical Education, Karnataka, India 2,3,4,5UG scholar, Dept.of Civil Engineering, JSS Academy of Technical Education, Karnataka, India ---------------------------------------------------------------------***--------------------------------------------------------------------- Abstract -Admixture-Cement interaction in concrete is a complex blend of chemical and physical mechanism that are independent. Every admixture at optimum dosage gives better results when used with cement. The proposed research is aimed to study the compatibility of super plasticizer with different types of blended cements by investigatingflow time value. The present work is to study the behaviour of blended mixes (OPC+GGBS+ALCCOFINE) with the PCE (poly carboxylic ether) based admixtures at various dosages of both GGB,ALCCOFINE and chemical admixture. It was observed that most of the blended mixes were compatible with PCE based admixtures at dosages of around 3%. Increase in flow time has been observed with the addition of ALCCOFINE. Key Words: GGBS, ALCCOFINE, PCE based admixture, Compatibility 1. INTRODUCTION The hydration of cement involves series of reactions, which mainly depend on the cement composition, the water / cement ratio, surface area, particle size distribution, temperature and admixtures. Admixtures when added in small quantities make the hydration process much more complex. In recent times, advances in the field of cement products are related to the use of admixtures particularly organic polymeric materials. Many type of organic polymeric materials, known as superplasticizers, are being used in construction industries to alter the flow behaviour and the mechanical properties of concretes. Among various types of chemical admixtures, PCE based admixtures proved to enhance the flow fresh and hardened properties of concrete at low dosage. 2. Literature Review The present investigation deals with the study of compatibility of chemical admixtures with different mixes. The study also deals with the fresh and hardened properties of blended concrete. The relevant literature available in this area has been critically studied and discussed. Anshuman Dogra and Richa Bhardwaj (1) investigated the compatibility behaviour of superplasticizers with cement containing mineral admixtures like fly ash, alccofine. It was observed that Polycarboxylate Ether(PCE) based super plasticizers show greater compatibility and economical dosage as compared to sulphonated Napthalene Formaldehyde(SNF) based superplasticizers. M.K.Maroliya (2) studied the change in ingredients contents of concrete like sand and cement under the influence of plasticizers and superplasticizers at various dosages level. It was also observed that plasticizers enhanced the compressive strength at reduced water- cement ratio in addition to improved workability at constant water cement ratio. Reduction in cement content was achieved with increase in sand content to overcome bleeding and segregation. Janardhana Maganti and V.Silva Prasada Raju(3) studied compatibility of Sulphonated Naphthalene Formaldehyde and Lignosulphonates based superplasticizer with Portland slag cements. It was observed that the different brands of cements behaved differently even if the coarse and fine aggregates, water and family of chemical admixture and the method of concrete mix design were kept constant. S.Sheela(4) studied the workability and strength behavior of superplasticized concrete and conventional concrete both in fresh and hardened states. It was also observed that the use of superplasticizer can increase the workability and strength without increasing the water cement ratio. It was also concluded that non destructive testing values were in good agreement with the strength behavior of superplasticized concrete for destructive testing. Ravindra Gettu, Dr.Joana Roncero (5) studied some aspects related to the dosage of superplasticizer using the Marsh Cone test and the effect of the temperature in superplasticized pastes are evaluated. The study also included the loss of fluidity of cement paste with time. The study revealed that polycarboxylic acid based superplasticizers performed better than naphthalene and melamine based admixtures. 3. OBJECTIVE  Study of characteristics of different series of cement mixes (double blended) with different types of chemical admixtures.  Study the flow time values of blended cements for optimum dosage of chemical admixtures.  Impart additional guidelines for the usage of ALCCOFINE in preparing flowable concrete.
  • 2. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395 -0056 Volume: 04 Issue: 05 | May -2017 www.irjet.net p-ISSN: 2395-0072 © 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 2987 4. MATERIALS USED  Cement: Ordinary Portland Cement (OPC), Ground Granulated Blast furnace slag(GGBS), ALCCOFINE  Chemical Admixtures: Polycarboxylic acid based.  Water: Potable water 5. METHODOLOGY  Study on properties of different types of blended cement and cementitious materials.  Study on flow time using Marsh Cone Apparatus.  Mix design of concrete using IS method. 6. EXPERIMENTAL WORK  Study on properties of ingredients Cement: The following tests have been carried out for the OPC Specific gravity test Fineness of cement Mineral admixture(GGBS,ALCCOFINE) Specific Gravity test has been carried out for GGBS and ALCCOFINE Chemical Admixtures Specific Gravity test has been carried out for Chemical Admixture  Study on flow time(Marsh Cone Test) The test is carried to check the flow time for 1000 ml of cement paste to completely pass through nozzle of the Marsh cone is determined for various dosages of chemical admixture and for various percentages of cement replacement by GGBS and ALCCOFINE. Preparation of cement paste  Cement paste of 1200 ml is prepared by keeping the w/c cement ratio of 0.5.  Mixing is done for 4 minutes in the mortar mixer(2 minutes at high speed and 2 minutes at low speed). 7.RESULTS TEST ON INGREDIENTS Specific Gravity SL NO MATERIAL SPECIFIC GRAVITY 1 Cement (OPC) 3.05 2 GGBS 2.86 3 ALCCOFINE 3.44 Fineness SL NO MATERIAL FINENESS 1 OPC 4% GRAPHS OF FLOW TIME TEST
  • 3. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395 -0056 Volume: 04 Issue: 05 | May -2017 www.irjet.net p-ISSN: 2395-0072 © 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 2988 TESTS ON CEMENT PASTE (Flow Time Test) Sl. No Cement Content, grams GGBS, grams ALCCOFINE, grams W/C ratio Water Content, ml Chemical Admixture Dosage in % Chemical Admixture Content, ml Flow Time , Sec 80% = OPC, 10% = GGBS, 10% = ALCCOFINE 1 1114.2 139.27 139.27 0.4 557.1 0% - 316 2 1102.3 137.8 137.8 0.4 551.1 1% 12.86 95 3 1086.18 135.77 135.7 0.4 543.09 2% 25.143 53 4 1072.89 134.13 134.13 0.4 536.96 3% 36.79 55 5 1059.5 132.4 132.4 0.4 529.77 4% 49.05 62 70% = OPC, 20% = GGBS, 10% = ALCCOFINE 1 970.57 277.3 138.65 0.4 554.61 0% - 380 2 957.88 273. 136.79 0.4 547.21 1% 12.5 101 3 946.27 270.36 135.18 0.4 540.73 2% 25.03 58 4 935.88 266.73 133.34 0.4 533.91 3% 37.1 53 5 923.17 263.76 131.88 0.4 527.52 4% 49 64 60% = OPC, 30% = GGBS, 10% = ALCCOFINE 1 828 414 138 0.4 552 0% - 413 2 817.75 408.95 136.45 0.4 544.8 1% 13.45 110 3 807.56 403.8 134.9 0.4 538.4 2% 26.91 59 4 797.1 398.8 133.1 0.4 531.8 3% 40.21 51 5 787.9 393.9 131.32 0.4 525.3 4% 52.53 63 50% = OPC, 40% = GGBS, 10% = ALCCOFINE 1 687.1 549.68 137.42 0.4 549.7 0% - 482 2 678.56 542.23 135.17 0.4 542.1 1% 13.4 123 3 669.77 535.8 133.95 0.4 535.8 2% 26.8 84 4 661.66 529.4 132.28 0.4 529.4 3% 40.1 67 5 653.56 522.9 130.71 0.4 522.9 4% 52.3 75 40% = OPC, 50% = GGBS, 10% = ALCCOFINE 1 547.32 684.1 136.83 0.4 547.2 0% - 520 2 540.35 675.4 135.09 0.4 540.35 1% 13.35 228 3 533.38 666.7 133.34 0.4 533.38 2% 26.7 64 4 527.06 658.55 131.67 0.4 527.06 3% 39.95 57 5 520.74 650.4 130 0.4 520.3 4% 52.03 58 CONCLUSION  ALCCOFINE can also be utilized as a high range water reducer to improve compressive strength or as a super workability aid to improve flow.  Due to lower hydration rate of GGBS, curing time should be prolonged than portland cement concrete.  The addition of ALCCOFINE in cement mixes increases the self compatibility characteristic like filling ability ,passing ability and .resistance to segregation.  The relative cost of Alccofine is cheaper than cement hence it is also economic with higher strength.  Usage of mineral admixtures reduces the cost of concrete production.
  • 4. International Research Journal of Engineering and Technology (IRJET) e-ISSN: 2395 -0056 Volume: 04 Issue: 05 | May -2017 www.irjet.net p-ISSN: 2395-0072 © 2017, IRJET | Impact Factor value: 5.181 | ISO 9001:2008 Certified Journal | Page 2989 9. REFERENCES [1]Anshuman Dogra and Richa Bhardwaj “Study of the admixture-cement compatibility for the economic production of special concretes” International Journal of Civil Engineering Research”, Vol.5, No.1, 2014, pp 43- 48,ISSN 2278-3652 [2]M.K.Maroliya “Influence of type of chemical admixtures on sand and cement content of ordinary grade concrete”, International Journal of advances in Engineering & Technology, Nov 2012,pp298-302. [3]Janardhana Maganti,V.Silva Prasada Raju “Compatibility of Sulphonated Naphthalene Formaldehyde and Lignosulphonates based Superplasticizer with Portland Slag Cements”, Third international conference on sustainable construction materials and technologies. [4]S.Sheela “Study on workability and strengthBehaviour of concrete by the additionOf different admixtures” Proceedings of the INCONTEST 2003 on 10 –12, September 2003. [5] L.Ferrari,J.Kaufmann,F.Winnefeld,J.Plank “Multi method approach to study influence of superplasticizers on cement suspensions”, Cement and Concrete Composites,ELSEVIER, Vol.41,2011, pp.1058-1066. [6] Anatol Zingg, Frank Winnefeld, Lorenz Holder, Joachin Pakusch, Stefan Becker, Renato Figi, Ludwig Gauckler., “Interaction of polycarboxylate-based superplasticizers with cements containing different C3A amounts”, Cement and Concrete Composites,ELSEVIER, Vol.31,2009, pp.153- 162. BIOGRAPHIES Prof. Abdul Razak.B.H. is working as Assistant Professor at department of civil engineering, JSS Academy of Technical Education, Bangalore, Karnataka, India. He has published several technical papers in the reputed journals and also authored handbooks in Civil Engineering. Mr.Rakesh.R is an under graduate scholar in the department of Civil Engineering in JSS ACADEMY OF TECHNICAL EDUCATION, BANGALORE, INDIA Mr.Gaurav Ranjan is an under graduate scholar in the department of Civil Engineering in JSS ACADEMY OF TECHNICAL EDUCATION, BANGALORE, INDIA Ashish Kumar Singh is an under graduate scholar in the department of Civil Engineering in JSS ACADEMY OF TECHNICAL EDUCATION, BANGALORE, INDIA Uttkarsh Tyagi is an under graduate scholar in the department of Civil Engineering in JSS ACADEMY OF TECHNICAL EDUCATION, BANGALORE, INDIA