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PELLETIZING TECHNOLOGY
             EXTRUSION AND SPHERONIZATION




BEPEX · BEPEX · BEPEX · BEPEX · BEPEX · BEPEX · BEPEX · BEPEX · BEPEX · BEPEX · BEPEX
BEPEX Pelletizing Technology
Extrusion and Spheronization




With the BEPEX technologies of low        Materials of Construction, Finishes        Drives/Electrics
pressure extrusion and spheronization,    Although all of the product contact        For the drives usually gear motors with
cylindrical, rounded and spherical        parts of the gear pelletizer series, the   frequency converters are used. The
pellets are produced for versatile        BEXTRUDER series and the                   standard design of the motors is IP 54/
applications in the fields of             BEXROLLER series are constructed           IP65.
   Pharmaceutical                         from stainless steel, you can request
   Food                                   custom construction from other             For hazardous areas all types of
   Chemical                               materials such as Hastelloy.               protection are available.
Powdery or pasty feed materials are       The following finishes are available:
softly transformed to dust-free pellets       Bead blasted finish
with the required apprearance.                Brush finished
                                              Mechanically and electropolished

2
Gear Pelletizer GCS/GMS
Extrusion of stable cylindrical pellets   Applications
   Conical feed chamber                      Improvement of handling and
   Counter rotating gear tooth               metering properties
   type rolls                                Dust-free cylindrical pellets
   Nozzle bores between the teeth            Smooth surface
   with various sizes and profiles           High pellet stability
   Even product integrity


Pages 4 - 5


BEXTRUDER BX
Soft product densification                Applications
   Cylindrical extrusion chamber             Improvement of handling and
   Counter rotating rotors                   dosing properties
   Mixing and densification                  Low dust cylindrical pellets with
   Screen baskets with different             large surface
   perforations and wall thicknesses         Good deformation properties
                                             Low densification
                                             Loose structure, good solubility
Pages 6 - 7


BEXROLLER BR
                                          Applications
Rounding from pellet to sphere
                                             Optimum flowing, dosing and
   Spheronization                            handling properties
   Rotating disc with various surface        Rounding of pellets or forming of
   Intense rolling movement of               spheres
   granules                                  Pellets of uniform size, shape and
   Gap purge air                             surface
                                             Dust-free, attrition resistant
                                             product
                                             Narrow particle size distribution
Pages 8 - 9


Pelletizing Processes                     BEPEX Technology                        Product Types
   Batch process                             Technical testing center               Flakes
   Continuous process                        Customer site visits and seminars      Granules
   Batch-continuous process                  Manufacturing                          Briquettes
   Multiple-stage arrangements               Research and design                    Pellets
   Process with aeration and size            Systems design                         Spherical granules
   reduction                                 Feedback and control systems
                                             Automation
                                             Validation

Page 10                                   Page 11                                 Page 12

                                                                                                         3
Gear Pelletizer GCS/GMS
Extrusion of stable cylindrical Pellets


Gear pelletizer with cantilevered shafts and
gasketed cover for dust-free operation

                                               The Working Principle
                                               Below the feeding hopper a pair of gear
                                               type toothed rolls are counter rotating.
                                               Product is pulled in by the rolls and
                                               pressed through nozzle bores which are
                                               situated between the teeth. In the press
                                               channels the product is densified into
                                               cylinder shaped pellets. The pellets
                                               emerge at the inside of the hollow gear
                                               type toothed rolls.

                                               The Construction
                                               In most cases, gravity force feeding is
                                               sufficient. For extremely bad flowing
                                               products agitating elements are
                                               installed in the feed hopper. A special
                                               feed hopper with an agitator designed
                                               like a screw is used for viscoplastic feed
                                               materials.
                                               The rolls are sealed at both sides by
                                               cheek plates against lateral material
                                               escape. For the same working principle
                                               according to the case of application the
                                               optimum roll bearing is used. The
                                               model GMS uses mill shafts, and the
                                               model GCS has cantilevered shafts.
                                               For improvement of product discharge
                                               inside the hollow rolls, adjustable
      a
                                               cutting knives are installed, which are
                                               easily accessible.
                                               A gasketed cover ensures dust-free
                                               operation and is especially suitable
                                               when purging is done with inert gas or
                                               solvents are present.




              b




                                               a Pair of rolls with press nozzles bored in
                                                 solid extrusion rolls
                                               b Pair of rolls with nozzle inserts

4
Usual nozzle design
                                            1 Press nozzles bored in solid extrusion rolls
                                            2 Press nozzles bored in solid extrusion
                                              rolls, shortened by counterbores
                                            3 Nozzle inserts with short length
                                              (small L/D ratio)
                                            4 Nozzle inserts with large length
                                              (high L/D ratio)

Toothed Rolls and Nozzle Plates
Press rolls can be designed with nozzles
bored in solid extrusion rolls or with
exchangeable nozzle inserts. If at
product changeover a different nozzle
geometry is necessary, the nozzle
inserts are easily and quickly changed.
Densification is determined by the
relation of nozzle diameter to nozzle
length. Through counterbores the
nozzle length can be shortened. The                   1                      2               3   4
appropriate choice of the press rolls,
tooth shape, nozzle diameter and nozzle
length depends on the charged material
and on the required product properties.

The Product
The pellet diameter is determined by the
diameter of the press channel. With gear
type pelletizing machines stable
cylindrical pellets with a diameter range
of 1 to 10 mm can be produced. The
cylindrical pellets dispose of a smooth
surface, a constant diameter and are
only rarely bent. Often the length of the
single pellets is very uniform.

Technical Data
Model         Drive          Rolls
                       ø       Width
               kW     mm        mm
GCS 200      4,0 -7,5 200     40 - 100
GCS 300        18,5 300       80 - 120
GMS 200        11,0 200       80 - 100
GMS 300        22,0 300         200
GMS 300        30,0 300       2 x 200




                                                                                                     5
BEXTRUDER BX
Soft Product Densification



BEXTRUDER with vibration discharge chute
                                           Principle of Operation
                                           In the product chamber of the machine
                                           two rotors are counter rotating. The
                                           upper rotor with inclined positioned
                                           baffle plates provides for a good
                                           mixture and conveys the material
                                           evenly downwards. The lower rotor is
                                           designed with bent arms. This rotor
                                           densifies the material and conveys it
                                           through the cylindrical screen basket.

                                           Machine and Construction
                                           The speeds of the rotors are adjustable,
                                           independent from each other. For the
                                           optimum process adjustment the lower
                                           rotor is equipped with a measurement of
                                           torque.
                                           The drive is situated according to the
                                           application below or above the product
                                           chamber in a closed housing. When the
                                           drive is positioned below the extrusion
                                           chamber, the product discharge can be
                                           effected with a vibrating chute or with a
                                           rotating disc. With a drive above the
                                           product chamber the product falls freely
                                           downwards to the next process step.

                                           Rotor Exchange and Cleaning
                                           The rotors have plug connections to the
                                           drive shafts. Rotors and basket screen
                                           cylinders are very accessible and can be
                                           easily changed. The BEXTRUDER can
                                           be cleaned and retrofitted in a very short
                                           time.




6
BEXTRUDER with free product discharge
Accessories
  Different rotors
  Screen baskets with different hole
  diameters and different wall
  thicknesses
  Outside rotating cutting knife
  Vibration discharge chute
  Rotation disc for product discharge
  Blow-off ring for product cooling
  and separation

The Product
Product extruded with the BEX-
TRUDER has a loose structure with
large surface area and good defor-
mation properties. The diameter of the
cylindrical pellets can range from 0,3 to
3 mm. The product exhibits good
dispersion, compression and dissolu-
tion properties.

Technical Data
Model       Drive    Throughput kg/h
             kW       Min.    Max.
BX 150       2,8      1...3     300
BX 300       8,0        25      600
BX 450      15,0       100    1500
BX 600      22,0       200    2400




                                                                                    7
BEXROLLER BR
Rounding from Pellet to Sphere




                                 The Machine
                                 In the cylindrical product chamber a
                                 horizontal disc is rotating. The drive
                                 with frequency converter and electric
                                 control enables exact speed regulation.
                                 For fast cleaning the disc can easily be
                                 exchanged. A gap air purge prevents the
                                 product from reaching the area below
                                 the disc. The purge air quantity is
                                 adjustable and can be adapted to assist
                                 optimum product movement.

                                 Accessories
                                   Discs with different surfaces and
                                   profiles
                                   Jacketed product chamber
                                   Profiled product chamber wall
                                   Pneumatically operated discharge
                                   Height adjustable weir for
                                   continuous product discharge
                                   Cascade arrangement
                                   PLC




8
The Product
The pellets perform intense rotating and
rolling movements in the product                                                              Ideal Sphere
                                                              1,0
chamber. With increasing spheroni-
zation time the pellets round off and are
transformed, if the material disposes of                                                      Pharma
                                                [-]




good deformation properties, to perfect
                                                              0,9
spheres with smooth surface and
                                                2
                                                =4 A / U




narrow particle size distribution. The
product is dust-free.
                                                                                              Food
                                                              0,8
Technical Data                                                                                Instant
                                                2




Model       Drive            Quantity                                                         Chemicals
             kW             appr. dm3 *
                                                Form factor




BR 150       0,55            0,1 - 0,4                        0,7
BR 300       1,5             0,3 - 2,5
BR 450       1,5               2-9
BR 600       3,0               7 - 23
BR 900       5,5              20 - 70
* depend on product                                           0,6
                                                                    0   60       120       180          240   300

                                                                        Spheronization time t [ s ]
Alteration of the pellet shape during sphero-
nization dependent on time

                                                                                                                    9
Pelletizing Processes
Versatile Process Technology




                                   Batch                   Continuous            Batch-Continuous

 Dosing


 Mixing
 Humidification



 Extrusion
    BEXTRUDER
    GCS
 Spheronization
   BEXROLLER


 Drying
 Coating
   AGGLOMASTER




     Production of cylindrical pellets with short length                   Spheronization 3-step
     of temperature sensitive product                                      continuous and batch




                                                                                       1. Pellet breakage
                                                                                          Dust agglomeration
                                                                                          Spheronization
                                                    Pelletizing
                                                        GCS

                                                                                       2. Spheronization
     Dust                                           Cooling, separating,                  Dust agglomeration
     recovery                                       aeration

                                                    Size reduction
                                                        BEXMILL                        3. Spheronization
                                                                                          Polishing


                                                    Screening




10
BEPEX Technology
... more than just machines




The BEPEX Test Center
Extensive know-how is available in the
BEPEX test center to provide technical
and economical solutions.
Customer tests are performed daily in
our testing facilities - a laboratory for
pharmaceutical applications as well as a
test center providing both the complete
machine equipment and a pilot plant
used for scale-up of processing plants.
Our analytical lab can quickly analyse
the product. The results of our tests are
not only the production of samples or
machine configurations but also an
individual system design and complete
process engineering for your needs.

Development and Design
To accommodate our technology to
your application we use modern CAD
and our own fabrication. We develop
and manufacture new machines, plants
and processes to be able to produce
granules with specially tailored
properties. Due to the intensive and
world-wide co-operation especially
with sister companies and research
institutes we have a high development
potential at our disposal, which we can
offer for your application.

Control and Automation
Process Logic Control (PLC) is
standard and can easily be interfaced
with other main process control and
data logging systems on your plant. Our
COMPACT CONTROL enables
process automation and visualisation
including process monitoring, data
gathering and diagnosis of errors.

Validation
We can validate both machines and
plants according to your given
standards (IQ and OQ validation).




                                            11
BEPEX Agglomeration Technology
We bring your powder into shape




HOSOKAWA BEPEX GmbH                            The BEPEX Technologies
P.O. Box 1152                                  Machines and complete plants for
D-74207 Leingarten / Germany                     Compaction
Tel.: 0049 (0)7131 / 907 - 0                     Briquetting
Fax: 0049 (0)7131 / 907 - 301                    Granulation
                                                 Size reduction
E-Mail:
                                                 Fluid bed agglomeration
compaction@bepex.hosokawa.com
                                                 Granule drying
Delivery address:                                Coating
Daimlerstr. 8                                    Pelletizing
D-74211 Leingarten / Germany                     Extrusion
                                                 Spheronization
                                                                                                                               Pellets B GB - Oe - PE - 5011 - Printed in Germany




                                                                                               Internet
                                                                                               http://www.hosokawamicron.com
Hosokawa Bepex GmbH is a member of the Hosokawa Micron Group, responding to
global needs through emphasis on materials science and engineering. The Group is an
international provider of equipment and technology for powder and particle processing,
product recovery, plastics processing and confectionery products. The Group maintains
facilities for research, engineering, manufacturing and service in each of the world’s major
industrial markets.

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Pelletizing e[1]

  • 1. PELLETIZING TECHNOLOGY EXTRUSION AND SPHERONIZATION BEPEX · BEPEX · BEPEX · BEPEX · BEPEX · BEPEX · BEPEX · BEPEX · BEPEX · BEPEX · BEPEX
  • 2. BEPEX Pelletizing Technology Extrusion and Spheronization With the BEPEX technologies of low Materials of Construction, Finishes Drives/Electrics pressure extrusion and spheronization, Although all of the product contact For the drives usually gear motors with cylindrical, rounded and spherical parts of the gear pelletizer series, the frequency converters are used. The pellets are produced for versatile BEXTRUDER series and the standard design of the motors is IP 54/ applications in the fields of BEXROLLER series are constructed IP65. Pharmaceutical from stainless steel, you can request Food custom construction from other For hazardous areas all types of Chemical materials such as Hastelloy. protection are available. Powdery or pasty feed materials are The following finishes are available: softly transformed to dust-free pellets Bead blasted finish with the required apprearance. Brush finished Mechanically and electropolished 2
  • 3. Gear Pelletizer GCS/GMS Extrusion of stable cylindrical pellets Applications Conical feed chamber Improvement of handling and Counter rotating gear tooth metering properties type rolls Dust-free cylindrical pellets Nozzle bores between the teeth Smooth surface with various sizes and profiles High pellet stability Even product integrity Pages 4 - 5 BEXTRUDER BX Soft product densification Applications Cylindrical extrusion chamber Improvement of handling and Counter rotating rotors dosing properties Mixing and densification Low dust cylindrical pellets with Screen baskets with different large surface perforations and wall thicknesses Good deformation properties Low densification Loose structure, good solubility Pages 6 - 7 BEXROLLER BR Applications Rounding from pellet to sphere Optimum flowing, dosing and Spheronization handling properties Rotating disc with various surface Rounding of pellets or forming of Intense rolling movement of spheres granules Pellets of uniform size, shape and Gap purge air surface Dust-free, attrition resistant product Narrow particle size distribution Pages 8 - 9 Pelletizing Processes BEPEX Technology Product Types Batch process Technical testing center Flakes Continuous process Customer site visits and seminars Granules Batch-continuous process Manufacturing Briquettes Multiple-stage arrangements Research and design Pellets Process with aeration and size Systems design Spherical granules reduction Feedback and control systems Automation Validation Page 10 Page 11 Page 12 3
  • 4. Gear Pelletizer GCS/GMS Extrusion of stable cylindrical Pellets Gear pelletizer with cantilevered shafts and gasketed cover for dust-free operation The Working Principle Below the feeding hopper a pair of gear type toothed rolls are counter rotating. Product is pulled in by the rolls and pressed through nozzle bores which are situated between the teeth. In the press channels the product is densified into cylinder shaped pellets. The pellets emerge at the inside of the hollow gear type toothed rolls. The Construction In most cases, gravity force feeding is sufficient. For extremely bad flowing products agitating elements are installed in the feed hopper. A special feed hopper with an agitator designed like a screw is used for viscoplastic feed materials. The rolls are sealed at both sides by cheek plates against lateral material escape. For the same working principle according to the case of application the optimum roll bearing is used. The model GMS uses mill shafts, and the model GCS has cantilevered shafts. For improvement of product discharge inside the hollow rolls, adjustable a cutting knives are installed, which are easily accessible. A gasketed cover ensures dust-free operation and is especially suitable when purging is done with inert gas or solvents are present. b a Pair of rolls with press nozzles bored in solid extrusion rolls b Pair of rolls with nozzle inserts 4
  • 5. Usual nozzle design 1 Press nozzles bored in solid extrusion rolls 2 Press nozzles bored in solid extrusion rolls, shortened by counterbores 3 Nozzle inserts with short length (small L/D ratio) 4 Nozzle inserts with large length (high L/D ratio) Toothed Rolls and Nozzle Plates Press rolls can be designed with nozzles bored in solid extrusion rolls or with exchangeable nozzle inserts. If at product changeover a different nozzle geometry is necessary, the nozzle inserts are easily and quickly changed. Densification is determined by the relation of nozzle diameter to nozzle length. Through counterbores the nozzle length can be shortened. The 1 2 3 4 appropriate choice of the press rolls, tooth shape, nozzle diameter and nozzle length depends on the charged material and on the required product properties. The Product The pellet diameter is determined by the diameter of the press channel. With gear type pelletizing machines stable cylindrical pellets with a diameter range of 1 to 10 mm can be produced. The cylindrical pellets dispose of a smooth surface, a constant diameter and are only rarely bent. Often the length of the single pellets is very uniform. Technical Data Model Drive Rolls ø Width kW mm mm GCS 200 4,0 -7,5 200 40 - 100 GCS 300 18,5 300 80 - 120 GMS 200 11,0 200 80 - 100 GMS 300 22,0 300 200 GMS 300 30,0 300 2 x 200 5
  • 6. BEXTRUDER BX Soft Product Densification BEXTRUDER with vibration discharge chute Principle of Operation In the product chamber of the machine two rotors are counter rotating. The upper rotor with inclined positioned baffle plates provides for a good mixture and conveys the material evenly downwards. The lower rotor is designed with bent arms. This rotor densifies the material and conveys it through the cylindrical screen basket. Machine and Construction The speeds of the rotors are adjustable, independent from each other. For the optimum process adjustment the lower rotor is equipped with a measurement of torque. The drive is situated according to the application below or above the product chamber in a closed housing. When the drive is positioned below the extrusion chamber, the product discharge can be effected with a vibrating chute or with a rotating disc. With a drive above the product chamber the product falls freely downwards to the next process step. Rotor Exchange and Cleaning The rotors have plug connections to the drive shafts. Rotors and basket screen cylinders are very accessible and can be easily changed. The BEXTRUDER can be cleaned and retrofitted in a very short time. 6
  • 7. BEXTRUDER with free product discharge Accessories Different rotors Screen baskets with different hole diameters and different wall thicknesses Outside rotating cutting knife Vibration discharge chute Rotation disc for product discharge Blow-off ring for product cooling and separation The Product Product extruded with the BEX- TRUDER has a loose structure with large surface area and good defor- mation properties. The diameter of the cylindrical pellets can range from 0,3 to 3 mm. The product exhibits good dispersion, compression and dissolu- tion properties. Technical Data Model Drive Throughput kg/h kW Min. Max. BX 150 2,8 1...3 300 BX 300 8,0 25 600 BX 450 15,0 100 1500 BX 600 22,0 200 2400 7
  • 8. BEXROLLER BR Rounding from Pellet to Sphere The Machine In the cylindrical product chamber a horizontal disc is rotating. The drive with frequency converter and electric control enables exact speed regulation. For fast cleaning the disc can easily be exchanged. A gap air purge prevents the product from reaching the area below the disc. The purge air quantity is adjustable and can be adapted to assist optimum product movement. Accessories Discs with different surfaces and profiles Jacketed product chamber Profiled product chamber wall Pneumatically operated discharge Height adjustable weir for continuous product discharge Cascade arrangement PLC 8
  • 9. The Product The pellets perform intense rotating and rolling movements in the product Ideal Sphere 1,0 chamber. With increasing spheroni- zation time the pellets round off and are transformed, if the material disposes of Pharma [-] good deformation properties, to perfect 0,9 spheres with smooth surface and 2 =4 A / U narrow particle size distribution. The product is dust-free. Food 0,8 Technical Data Instant 2 Model Drive Quantity Chemicals kW appr. dm3 * Form factor BR 150 0,55 0,1 - 0,4 0,7 BR 300 1,5 0,3 - 2,5 BR 450 1,5 2-9 BR 600 3,0 7 - 23 BR 900 5,5 20 - 70 * depend on product 0,6 0 60 120 180 240 300 Spheronization time t [ s ] Alteration of the pellet shape during sphero- nization dependent on time 9
  • 10. Pelletizing Processes Versatile Process Technology Batch Continuous Batch-Continuous Dosing Mixing Humidification Extrusion BEXTRUDER GCS Spheronization BEXROLLER Drying Coating AGGLOMASTER Production of cylindrical pellets with short length Spheronization 3-step of temperature sensitive product continuous and batch 1. Pellet breakage Dust agglomeration Spheronization Pelletizing GCS 2. Spheronization Dust Cooling, separating, Dust agglomeration recovery aeration Size reduction BEXMILL 3. Spheronization Polishing Screening 10
  • 11. BEPEX Technology ... more than just machines The BEPEX Test Center Extensive know-how is available in the BEPEX test center to provide technical and economical solutions. Customer tests are performed daily in our testing facilities - a laboratory for pharmaceutical applications as well as a test center providing both the complete machine equipment and a pilot plant used for scale-up of processing plants. Our analytical lab can quickly analyse the product. The results of our tests are not only the production of samples or machine configurations but also an individual system design and complete process engineering for your needs. Development and Design To accommodate our technology to your application we use modern CAD and our own fabrication. We develop and manufacture new machines, plants and processes to be able to produce granules with specially tailored properties. Due to the intensive and world-wide co-operation especially with sister companies and research institutes we have a high development potential at our disposal, which we can offer for your application. Control and Automation Process Logic Control (PLC) is standard and can easily be interfaced with other main process control and data logging systems on your plant. Our COMPACT CONTROL enables process automation and visualisation including process monitoring, data gathering and diagnosis of errors. Validation We can validate both machines and plants according to your given standards (IQ and OQ validation). 11
  • 12. BEPEX Agglomeration Technology We bring your powder into shape HOSOKAWA BEPEX GmbH The BEPEX Technologies P.O. Box 1152 Machines and complete plants for D-74207 Leingarten / Germany Compaction Tel.: 0049 (0)7131 / 907 - 0 Briquetting Fax: 0049 (0)7131 / 907 - 301 Granulation Size reduction E-Mail: Fluid bed agglomeration compaction@bepex.hosokawa.com Granule drying Delivery address: Coating Daimlerstr. 8 Pelletizing D-74211 Leingarten / Germany Extrusion Spheronization Pellets B GB - Oe - PE - 5011 - Printed in Germany Internet http://www.hosokawamicron.com Hosokawa Bepex GmbH is a member of the Hosokawa Micron Group, responding to global needs through emphasis on materials science and engineering. The Group is an international provider of equipment and technology for powder and particle processing, product recovery, plastics processing and confectionery products. The Group maintains facilities for research, engineering, manufacturing and service in each of the world’s major industrial markets.