SlideShare a Scribd company logo
1 of 12
Determining Water Separation of Aviation
Turbine Fuel as per ASTM D3948
By
Aamir Shahzad Butt
SCOPE & SIGNIFICANCE
The instrument provides a quick, portable means for
field and laboratory use to rate the ability of aviation
turbine fuels to release entrained or emulsified water
when passed through fiberglass coalescence material.
The test provides a measure of surface active materials
in aviation turbine fuels. These are known to affect the
ability of filter separators to separate free water from
fuel.
APPARATUS
Micro-Separometer Six Pack Micro-Separometer kit Micropipette
Wire Aid
PREPARATION OF APPARATUS
• Unlock the box of WSIM apparatus by putting “000” on the lock and press
• Locate the instrument in an area where the temperature is between 18 °C and
29°C ± 3°C. Test performed outside of these temperature limits may not meet
ASTM repeatability/reproducibility criteria.
• Open the case and remove the Six-Pack box from the lid. Insert your finger into the
hole in the right panel and raise the panel until completely vertical and locked in
place. If power is available, check to be certain the source voltage (220-260 volt
power cord) matches the power cord label and connect the power cord.
• Open a new six pack “syringe, ALUMICEL COALESCER, vial, plug, pipette tip, and a
container for clean water.
• If the instrument is to be operated in a location where an AC outlet is not available,
the instrument should be charged for approximately 16 hours before testing. The
unit will function properly for approximately 25 tests before battery recharging is
necessary.
PREPARATION OF SAMPLE
• Obtain and handle the samples with the utmost care and cleanliness as required in
the ASTM Procedure D-3948. Before pouring the test sample from container, wipe
the container outlet thoroughly with a clean, lintless wipe. Then pour the test
sample into a clean beaker or directly into the syringe.
• If the sample for test is not within the test temperature limits (18°C to 29°C) let the
container stand or preferably put sample in a clean beaker and let it come to
operating temperature.
PROCEDURE
• Press “ON” switch and warm up for at least 30 minutes.
• Momentarily depress the "ON" switch. The annunciator lamps located on switches A
through G in the TEST SELECT section will then be scanning for your selection.
Depress switch "A". This will initiate the standard automatic program for Jet A fuel.
• Note: Only JP 4 requires Mode B operation
• Remove a plunger from a new 50-mL syringe and wipe the tip using a clean, lintless
wipe to remove any sheen caused by excess lubricant. Insert a plug into the exit hole
of the syringe barrel, add 50 ± 1 mL of fuel, and place the syringe barrel on the
emulsifier mount, turning to lock in place. Ensure that the syringe barrel is properly
aligned concentrically with the mixer shaft and is not touching the propeller.
Emulsifier mount
plug
Syringe Barrel
plunger
vial
ALUMICEL COALESCER
pipette tip
Micropipette
Wire Aid
clean water
PROCEDURE
• Add about 15 to 20 mL of the fuel to be tested into a new vial. Wipe the outside of the
vial with a clean, lintless wiper and insert the vial into the turbidimeter well aligning
the black mark on the vial with the line on the front panel.
• Initiate the CLEAN cycle by depressing the “START” pushbutton as designated by the
annunciator light.
• Warnings—do not operate the mixer without having a syringe with fuel in place.
Turbidimeter
Emulsifier mount and syringe barrel with fuel / Mixer
PROCEDURE
• At the end of the first clean cycle, when the mixer motor stops, press the RESET
push-button, remove the syringe barrel from the emulsifier, discard the fuel, and
drain the syringe thoroughly. Add 50 ± 1 mL of fresh fuel into the syringe and place
the syringe barrel on the emulsifier mount (turn to lock in place). Visually inspect that
the syringe barrel is properly aligned concentrically with the mixer shaft and is not
touching the propeller. Select Test Mode A by pressing A push-button
• Initiate the second CLEAN cycle by depressing the “START” pushbutton as
designated by the annunciator light.
• At the end of the clean cycle, when the mixer motor stops, remove the syringe barrel
from the emulsifier, discard the fuel, and drain the syringe thoroughly. Add 50 ± 1 mL
of fresh fuel into the syringe, add 50 μL of distilled water to the fuel sample. Place
the syringe barrel on the emulsifier mount, With the syringe in place, depress the
START push-button.
Water Addition
depress the START push-button.
PROCEDURE
• The automatic program starts with a read meter indication followed by a 10-s full-
scale adjustment period. During this period, the ARROWED pushbuttons will
illuminate and can be depressed to adjust the meter to read 100. If the adjustment
cannot be completed at this time, final adjustment can be accomplished during the
second meter adjust period occurring later in the test sequence.
• After the full-scale adjustment period the mixer motor activates and the emulsion
process is initiated.
• When the mixer stops (after emulsification), remove the syringe barrel from the
emulsifier and partially insert the. plunger to seal the open end of the syringe. Invert
the syringe (exit hole up), remove the plug, and exhaust the entrapped air in the
syringe barrel without significant fuel loss by carefully inserting plunger to the 50 mL
mark. (Use a clean wipe over the exit hole to capture the small amounts of fuel which
may be extruded as foam. Affix a new Alumicel coalescer to the end of the syringe
barrel.
PROCEDURE
• Place the entire syringe assembly into the syringe drive mechanism. To minimize the effect of
plunger resistance (drag) in the syringe barrel, align the syringe assembly vertically in the
syringe drive mechanism with the end of the syringe plunger parallel with pushbar of the
syringe drive mechanism. Position a waste container beneath the Alumicel coalescer to collect
the unwanted portion of the processed fuel sample during the coalescing period.
Pushbar
• Collect the last 15 mL of fuel sample being processed from the Alumicel coalesce, when the
collect sample annunciator lamp (marked C/S) illuminates and a pulsed tone of short duration
sounds. To lessen the amount of air introduced into the fuel during this operation, position the
vial at a slight angle and allow the fuel to flow down the inner surface. Remove the vial just
prior to when the last amount of sample is expelled from the Alumicel coalescer.
Collect the last 15 mL of fuel sample
PROCEDURE
• Wipe the outside of the vial with a clean, lintless wiper to remove any fingerprints
and fuel. Place the sample vial into the turbidimeter well aligning the marks on the
vial and on the control panel in front of the well. At the end of the settling time (1
min), a steady (4-s duration) tone will alert the operator that the meter is about to
activate
• At the end of the tone, the METER will automatically activate for approximately 10 s.
• MSEP ratings are read at the midpoint of the 10-s meter read cycle indicated by a
short 1-s tone.
• Report the results obtained in hole number.
WSIM Presentation 30072015

More Related Content

What's hot

diesel index aniline point and pour point of lubricating oil
diesel index aniline point and pour point of lubricating oildiesel index aniline point and pour point of lubricating oil
diesel index aniline point and pour point of lubricating oilAlina Waheed
 
Troubleshooting in Distillation Columns
Troubleshooting in Distillation ColumnsTroubleshooting in Distillation Columns
Troubleshooting in Distillation ColumnsGerard B. Hawkins
 
WQD2011 - KAIZEN - EMAL - Core Cutting Machine (Tech. Lab.) Safety Modification
WQD2011 - KAIZEN - EMAL - Core Cutting Machine (Tech. Lab.) Safety ModificationWQD2011 - KAIZEN - EMAL - Core Cutting Machine (Tech. Lab.) Safety Modification
WQD2011 - KAIZEN - EMAL - Core Cutting Machine (Tech. Lab.) Safety ModificationDubai Quality Group
 
Berol® ENV226 Plus - a formulator’s delight
Berol® ENV226 Plus - a formulator’s delightBerol® ENV226 Plus - a formulator’s delight
Berol® ENV226 Plus - a formulator’s delightSorel Muresan
 
Balance calibration.pptx
Balance calibration.pptxBalance calibration.pptx
Balance calibration.pptxLalitKumar970
 
QC CASE STUDY: PREVENT OR REDUCE CHOCKING OF RC FEEDER#G AND MILL#G CENTRE PIPE
QC CASE STUDY: PREVENT OR REDUCE CHOCKING OF RC FEEDER#G AND MILL#G CENTRE PIPEQC CASE STUDY: PREVENT OR REDUCE CHOCKING OF RC FEEDER#G AND MILL#G CENTRE PIPE
QC CASE STUDY: PREVENT OR REDUCE CHOCKING OF RC FEEDER#G AND MILL#G CENTRE PIPERAVI PAL SINGH
 
Qualification of INFARED SPECTROSCOPY BY HIMAJA.D
Qualification of INFARED SPECTROSCOPY BY HIMAJA.DQualification of INFARED SPECTROSCOPY BY HIMAJA.D
Qualification of INFARED SPECTROSCOPY BY HIMAJA.Dhimaja donthula
 
Qualification of gc equipment by manoj kumar
Qualification of gc equipment by manoj kumarQualification of gc equipment by manoj kumar
Qualification of gc equipment by manoj kumarhimaja donthula
 
Aspen Plus Tutorial - LHHW - reverse propane cycle
Aspen Plus Tutorial - LHHW - reverse propane cycleAspen Plus Tutorial - LHHW - reverse propane cycle
Aspen Plus Tutorial - LHHW - reverse propane cycleHamed Hoorijani
 
Determination of Residue and Oil in Anhydrous Ammonia
Determination of Residue and Oil in Anhydrous AmmoniaDetermination of Residue and Oil in Anhydrous Ammonia
Determination of Residue and Oil in Anhydrous AmmoniaGerard B. Hawkins
 
Trouble shooting
Trouble shootingTrouble shooting
Trouble shootingVishYenare1
 
Methanol Plant - Theory of Distillation
Methanol Plant - Theory of DistillationMethanol Plant - Theory of Distillation
Methanol Plant - Theory of DistillationGerard B. Hawkins
 
ASTM Distillation D86: A Standard Test Method for Distillation of Petroleum P...
ASTM Distillation D86: A Standard Test Method for Distillation of Petroleum P...ASTM Distillation D86: A Standard Test Method for Distillation of Petroleum P...
ASTM Distillation D86: A Standard Test Method for Distillation of Petroleum P...IRJESJOURNAL
 
Analytical Method Validation.pdf
Analytical Method Validation.pdfAnalytical Method Validation.pdf
Analytical Method Validation.pdfHiteshGajjar7
 
Calibration and Qualification of Analytical Instruments
Calibration and Qualification of Analytical InstrumentsCalibration and Qualification of Analytical Instruments
Calibration and Qualification of Analytical InstrumentsISF COLLEGE OF PHARMACY MOGA
 
Deyab a. aspen hysys 2013 workbook
Deyab a.  aspen hysys 2013   workbookDeyab a.  aspen hysys 2013   workbook
Deyab a. aspen hysys 2013 workbookLito Aguirre
 
Ensuring the validity of results
Ensuring the validity of resultsEnsuring the validity of results
Ensuring the validity of resultsGH Yeoh
 

What's hot (20)

diesel index aniline point and pour point of lubricating oil
diesel index aniline point and pour point of lubricating oildiesel index aniline point and pour point of lubricating oil
diesel index aniline point and pour point of lubricating oil
 
Troubleshooting in Distillation Columns
Troubleshooting in Distillation ColumnsTroubleshooting in Distillation Columns
Troubleshooting in Distillation Columns
 
WQD2011 - KAIZEN - EMAL - Core Cutting Machine (Tech. Lab.) Safety Modification
WQD2011 - KAIZEN - EMAL - Core Cutting Machine (Tech. Lab.) Safety ModificationWQD2011 - KAIZEN - EMAL - Core Cutting Machine (Tech. Lab.) Safety Modification
WQD2011 - KAIZEN - EMAL - Core Cutting Machine (Tech. Lab.) Safety Modification
 
Berol® ENV226 Plus - a formulator’s delight
Berol® ENV226 Plus - a formulator’s delightBerol® ENV226 Plus - a formulator’s delight
Berol® ENV226 Plus - a formulator’s delight
 
Balance calibration.pptx
Balance calibration.pptxBalance calibration.pptx
Balance calibration.pptx
 
Tpm ppt
Tpm pptTpm ppt
Tpm ppt
 
QC CASE STUDY: PREVENT OR REDUCE CHOCKING OF RC FEEDER#G AND MILL#G CENTRE PIPE
QC CASE STUDY: PREVENT OR REDUCE CHOCKING OF RC FEEDER#G AND MILL#G CENTRE PIPEQC CASE STUDY: PREVENT OR REDUCE CHOCKING OF RC FEEDER#G AND MILL#G CENTRE PIPE
QC CASE STUDY: PREVENT OR REDUCE CHOCKING OF RC FEEDER#G AND MILL#G CENTRE PIPE
 
Qualification of INFARED SPECTROSCOPY BY HIMAJA.D
Qualification of INFARED SPECTROSCOPY BY HIMAJA.DQualification of INFARED SPECTROSCOPY BY HIMAJA.D
Qualification of INFARED SPECTROSCOPY BY HIMAJA.D
 
Qualification of gc equipment by manoj kumar
Qualification of gc equipment by manoj kumarQualification of gc equipment by manoj kumar
Qualification of gc equipment by manoj kumar
 
Aspen Plus Tutorial - LHHW - reverse propane cycle
Aspen Plus Tutorial - LHHW - reverse propane cycleAspen Plus Tutorial - LHHW - reverse propane cycle
Aspen Plus Tutorial - LHHW - reverse propane cycle
 
Determination of Residue and Oil in Anhydrous Ammonia
Determination of Residue and Oil in Anhydrous AmmoniaDetermination of Residue and Oil in Anhydrous Ammonia
Determination of Residue and Oil in Anhydrous Ammonia
 
Trouble shooting
Trouble shootingTrouble shooting
Trouble shooting
 
Qualification of gc equipment
Qualification of gc equipmentQualification of gc equipment
Qualification of gc equipment
 
Methanol Plant - Theory of Distillation
Methanol Plant - Theory of DistillationMethanol Plant - Theory of Distillation
Methanol Plant - Theory of Distillation
 
ASTM Distillation D86: A Standard Test Method for Distillation of Petroleum P...
ASTM Distillation D86: A Standard Test Method for Distillation of Petroleum P...ASTM Distillation D86: A Standard Test Method for Distillation of Petroleum P...
ASTM Distillation D86: A Standard Test Method for Distillation of Petroleum P...
 
Analytical Method Validation.pdf
Analytical Method Validation.pdfAnalytical Method Validation.pdf
Analytical Method Validation.pdf
 
Calibration and Qualification of Analytical Instruments
Calibration and Qualification of Analytical InstrumentsCalibration and Qualification of Analytical Instruments
Calibration and Qualification of Analytical Instruments
 
Deyab a. aspen hysys 2013 workbook
Deyab a.  aspen hysys 2013   workbookDeyab a.  aspen hysys 2013   workbook
Deyab a. aspen hysys 2013 workbook
 
Tpm
TpmTpm
Tpm
 
Ensuring the validity of results
Ensuring the validity of resultsEnsuring the validity of results
Ensuring the validity of results
 

Similar to WSIM Presentation 30072015

Operating procedure of Agitated Nutsch Filter
Operating procedure of Agitated Nutsch FilterOperating procedure of Agitated Nutsch Filter
Operating procedure of Agitated Nutsch FilterKamlesh Hariyani
 
Fueling
FuelingFueling
Fuelingenafla
 
Maa sharda pharmacy college ayodhya SOP
Maa sharda pharmacy college ayodhya SOPMaa sharda pharmacy college ayodhya SOP
Maa sharda pharmacy college ayodhya SOPJitendraKumarChauhan3
 
Mori Seiki Maintenance Guide
Mori Seiki Maintenance GuideMori Seiki Maintenance Guide
Mori Seiki Maintenance Guidescojetinc
 
Step 5 equipment setup
Step 5 equipment setupStep 5 equipment setup
Step 5 equipment setupfqf383
 
LECTURE 4- SUCTION MACHINE.pptx
LECTURE 4- SUCTION MACHINE.pptxLECTURE 4- SUCTION MACHINE.pptx
LECTURE 4- SUCTION MACHINE.pptxYUSUPHUMZEE
 
Checking piston valve clearance
Checking piston valve clearanceChecking piston valve clearance
Checking piston valve clearanceJomer Almozara
 
nothing but awesome
nothing but awesome nothing but awesome
nothing but awesome zeth111
 
Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)
Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)
Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)fjskekmdm
 
Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)
Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)
Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)udjfjjskekkem
 
Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)
Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)
Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)fjseolseksmem
 
Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)
Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)
Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)fusjefjskekemm
 
Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)
Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)
Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)udfjjssekkemm
 
Air content test for fresh concrete
Air content test for fresh concreteAir content test for fresh concrete
Air content test for fresh concreteAyaz khan
 
Basic laboratory techniques
Basic laboratory techniquesBasic laboratory techniques
Basic laboratory techniquesYhanzieCapilitan
 
Pentair #320 chlorinator manual
Pentair #320 chlorinator manualPentair #320 chlorinator manual
Pentair #320 chlorinator manualDavid Hackney
 
Anastasia machine reparing
Anastasia machine reparingAnastasia machine reparing
Anastasia machine reparingRABAH ABUABKER
 
Tegramin is a High Quality Specimen Preparation system
Tegramin is a High Quality Specimen Preparation systemTegramin is a High Quality Specimen Preparation system
Tegramin is a High Quality Specimen Preparation systemAimil Ltd
 
Clark c500(y) 30 55 forklift service repair manual
Clark c500(y) 30 55 forklift service repair manualClark c500(y) 30 55 forklift service repair manual
Clark c500(y) 30 55 forklift service repair manualfujsjekskem
 

Similar to WSIM Presentation 30072015 (20)

Operating procedure of Agitated Nutsch Filter
Operating procedure of Agitated Nutsch FilterOperating procedure of Agitated Nutsch Filter
Operating procedure of Agitated Nutsch Filter
 
Fueling
FuelingFueling
Fueling
 
Maa sharda pharmacy college ayodhya SOP
Maa sharda pharmacy college ayodhya SOPMaa sharda pharmacy college ayodhya SOP
Maa sharda pharmacy college ayodhya SOP
 
Mori Seiki Maintenance Guide
Mori Seiki Maintenance GuideMori Seiki Maintenance Guide
Mori Seiki Maintenance Guide
 
Step 5 equipment setup
Step 5 equipment setupStep 5 equipment setup
Step 5 equipment setup
 
Leak Tests.pptx
Leak Tests.pptxLeak Tests.pptx
Leak Tests.pptx
 
LECTURE 4- SUCTION MACHINE.pptx
LECTURE 4- SUCTION MACHINE.pptxLECTURE 4- SUCTION MACHINE.pptx
LECTURE 4- SUCTION MACHINE.pptx
 
Checking piston valve clearance
Checking piston valve clearanceChecking piston valve clearance
Checking piston valve clearance
 
nothing but awesome
nothing but awesome nothing but awesome
nothing but awesome
 
Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)
Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)
Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)
 
Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)
Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)
Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)
 
Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)
Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)
Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)
 
Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)
Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)
Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)
 
Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)
Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)
Jcb 1 t 1 high tip dumper service repair manual (sn 2561001 and up)
 
Air content test for fresh concrete
Air content test for fresh concreteAir content test for fresh concrete
Air content test for fresh concrete
 
Basic laboratory techniques
Basic laboratory techniquesBasic laboratory techniques
Basic laboratory techniques
 
Pentair #320 chlorinator manual
Pentair #320 chlorinator manualPentair #320 chlorinator manual
Pentair #320 chlorinator manual
 
Anastasia machine reparing
Anastasia machine reparingAnastasia machine reparing
Anastasia machine reparing
 
Tegramin is a High Quality Specimen Preparation system
Tegramin is a High Quality Specimen Preparation systemTegramin is a High Quality Specimen Preparation system
Tegramin is a High Quality Specimen Preparation system
 
Clark c500(y) 30 55 forklift service repair manual
Clark c500(y) 30 55 forklift service repair manualClark c500(y) 30 55 forklift service repair manual
Clark c500(y) 30 55 forklift service repair manual
 

More from Aamir Shahzad Butt (8)

Moisture
MoistureMoisture
Moisture
 
Centifuge
CentifugeCentifuge
Centifuge
 
NSX
NSXNSX
NSX
 
Shimazdu UV-Spectrophotometer Certificate
Shimazdu UV-Spectrophotometer CertificateShimazdu UV-Spectrophotometer Certificate
Shimazdu UV-Spectrophotometer Certificate
 
Shimazdu RGA Certificate
Shimazdu RGA CertificateShimazdu RGA Certificate
Shimazdu RGA Certificate
 
JET FUEL THERMAL OXIDATION TESTER 09062015
JET FUEL THERMAL OXIDATION TESTER 09062015JET FUEL THERMAL OXIDATION TESTER 09062015
JET FUEL THERMAL OXIDATION TESTER 09062015
 
scan0003
scan0003scan0003
scan0003
 
Sheikh Sons Letter
Sheikh Sons LetterSheikh Sons Letter
Sheikh Sons Letter
 

WSIM Presentation 30072015

  • 1. Determining Water Separation of Aviation Turbine Fuel as per ASTM D3948 By Aamir Shahzad Butt
  • 2. SCOPE & SIGNIFICANCE The instrument provides a quick, portable means for field and laboratory use to rate the ability of aviation turbine fuels to release entrained or emulsified water when passed through fiberglass coalescence material. The test provides a measure of surface active materials in aviation turbine fuels. These are known to affect the ability of filter separators to separate free water from fuel.
  • 3. APPARATUS Micro-Separometer Six Pack Micro-Separometer kit Micropipette Wire Aid
  • 4. PREPARATION OF APPARATUS • Unlock the box of WSIM apparatus by putting “000” on the lock and press • Locate the instrument in an area where the temperature is between 18 °C and 29°C ± 3°C. Test performed outside of these temperature limits may not meet ASTM repeatability/reproducibility criteria. • Open the case and remove the Six-Pack box from the lid. Insert your finger into the hole in the right panel and raise the panel until completely vertical and locked in place. If power is available, check to be certain the source voltage (220-260 volt power cord) matches the power cord label and connect the power cord. • Open a new six pack “syringe, ALUMICEL COALESCER, vial, plug, pipette tip, and a container for clean water. • If the instrument is to be operated in a location where an AC outlet is not available, the instrument should be charged for approximately 16 hours before testing. The unit will function properly for approximately 25 tests before battery recharging is necessary.
  • 5. PREPARATION OF SAMPLE • Obtain and handle the samples with the utmost care and cleanliness as required in the ASTM Procedure D-3948. Before pouring the test sample from container, wipe the container outlet thoroughly with a clean, lintless wipe. Then pour the test sample into a clean beaker or directly into the syringe. • If the sample for test is not within the test temperature limits (18°C to 29°C) let the container stand or preferably put sample in a clean beaker and let it come to operating temperature.
  • 6. PROCEDURE • Press “ON” switch and warm up for at least 30 minutes. • Momentarily depress the "ON" switch. The annunciator lamps located on switches A through G in the TEST SELECT section will then be scanning for your selection. Depress switch "A". This will initiate the standard automatic program for Jet A fuel. • Note: Only JP 4 requires Mode B operation • Remove a plunger from a new 50-mL syringe and wipe the tip using a clean, lintless wipe to remove any sheen caused by excess lubricant. Insert a plug into the exit hole of the syringe barrel, add 50 ± 1 mL of fuel, and place the syringe barrel on the emulsifier mount, turning to lock in place. Ensure that the syringe barrel is properly aligned concentrically with the mixer shaft and is not touching the propeller. Emulsifier mount plug Syringe Barrel plunger vial ALUMICEL COALESCER pipette tip Micropipette Wire Aid clean water
  • 7. PROCEDURE • Add about 15 to 20 mL of the fuel to be tested into a new vial. Wipe the outside of the vial with a clean, lintless wiper and insert the vial into the turbidimeter well aligning the black mark on the vial with the line on the front panel. • Initiate the CLEAN cycle by depressing the “START” pushbutton as designated by the annunciator light. • Warnings—do not operate the mixer without having a syringe with fuel in place. Turbidimeter Emulsifier mount and syringe barrel with fuel / Mixer
  • 8. PROCEDURE • At the end of the first clean cycle, when the mixer motor stops, press the RESET push-button, remove the syringe barrel from the emulsifier, discard the fuel, and drain the syringe thoroughly. Add 50 ± 1 mL of fresh fuel into the syringe and place the syringe barrel on the emulsifier mount (turn to lock in place). Visually inspect that the syringe barrel is properly aligned concentrically with the mixer shaft and is not touching the propeller. Select Test Mode A by pressing A push-button • Initiate the second CLEAN cycle by depressing the “START” pushbutton as designated by the annunciator light. • At the end of the clean cycle, when the mixer motor stops, remove the syringe barrel from the emulsifier, discard the fuel, and drain the syringe thoroughly. Add 50 ± 1 mL of fresh fuel into the syringe, add 50 μL of distilled water to the fuel sample. Place the syringe barrel on the emulsifier mount, With the syringe in place, depress the START push-button. Water Addition depress the START push-button.
  • 9. PROCEDURE • The automatic program starts with a read meter indication followed by a 10-s full- scale adjustment period. During this period, the ARROWED pushbuttons will illuminate and can be depressed to adjust the meter to read 100. If the adjustment cannot be completed at this time, final adjustment can be accomplished during the second meter adjust period occurring later in the test sequence. • After the full-scale adjustment period the mixer motor activates and the emulsion process is initiated. • When the mixer stops (after emulsification), remove the syringe barrel from the emulsifier and partially insert the. plunger to seal the open end of the syringe. Invert the syringe (exit hole up), remove the plug, and exhaust the entrapped air in the syringe barrel without significant fuel loss by carefully inserting plunger to the 50 mL mark. (Use a clean wipe over the exit hole to capture the small amounts of fuel which may be extruded as foam. Affix a new Alumicel coalescer to the end of the syringe barrel.
  • 10. PROCEDURE • Place the entire syringe assembly into the syringe drive mechanism. To minimize the effect of plunger resistance (drag) in the syringe barrel, align the syringe assembly vertically in the syringe drive mechanism with the end of the syringe plunger parallel with pushbar of the syringe drive mechanism. Position a waste container beneath the Alumicel coalescer to collect the unwanted portion of the processed fuel sample during the coalescing period. Pushbar • Collect the last 15 mL of fuel sample being processed from the Alumicel coalesce, when the collect sample annunciator lamp (marked C/S) illuminates and a pulsed tone of short duration sounds. To lessen the amount of air introduced into the fuel during this operation, position the vial at a slight angle and allow the fuel to flow down the inner surface. Remove the vial just prior to when the last amount of sample is expelled from the Alumicel coalescer. Collect the last 15 mL of fuel sample
  • 11. PROCEDURE • Wipe the outside of the vial with a clean, lintless wiper to remove any fingerprints and fuel. Place the sample vial into the turbidimeter well aligning the marks on the vial and on the control panel in front of the well. At the end of the settling time (1 min), a steady (4-s duration) tone will alert the operator that the meter is about to activate • At the end of the tone, the METER will automatically activate for approximately 10 s. • MSEP ratings are read at the midpoint of the 10-s meter read cycle indicated by a short 1-s tone. • Report the results obtained in hole number.