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Reactor Internals and solid/liquid filtration
for the Refining & Petrochemical Industry
1
Wedge wire screens
Trislot®
manufactures reactor internals using wedge wire screens (V-wire
screens). Such a screen consists of surface wires that are welded onto
support profiles. The distance between the surface profiles is controlled
very accurately, as it forms the continuous slot opening (aperture) through
which the process liquid or gas flows and by which the media (catalyst or
resin) is retained in its position.
	 Strong Self-Supporting Construction
	 In many applications the wedge wire screen is selfsupporting due to a
strong weld at each surface wire to support profile intersection. Mesh
tends to tear, especially when changing the catalyst.
	 Non-Clogging
	 The continuous slot opening formed by the triangularshaped (‘V’) sur-
face wires ensures a two-point contact between particles and the slot,
which minimises clogging.
	 High-Precision Slot Sizes
	 Precise slot sizes are available to meet customer’s requirements. Slot
openings down to 25μm.
	 Low Pressure Drop and High Open Area
	 To optimise your process output.
	 Smooth Screen Interface
	 The low friction between the screen and expensive medium is a result
of the smooth continuous slot openings, which run in one direction
allowing the media to move in that direction with a low friction force.
All these advantages result in a low maintenance cost and a minimal operational
cost for the petrochemical and refining plants.
Trislot®
has many different profiles available in most stainless steel alloys, Duplex and
Super Duplex alloys, Inconel 600, Titanium, Hastelloy C-276, AISI 310, 348, etc.
For available profiles and materials, please refer to the end of this brochure or our
website www.trislot.be
Compared with
conventional wire mesh
internals, the wedge
wire reactor internals
have the following
advantages:
2
The refining process
feedstock filtration
axial flow internals
radial flow internals
To Black Oil
Hydrocracking
Light
Naphtha
Gasoline
Treating
Heavy
Naphtha
Atmospheric
Gas Oil
Kerosene
Middle Distillate
Desalted
Crude Oil
Vacuum
Distillation
Crude
Distillation
Light Naphtha
Isomerization
Kero/Jet Fuel
Sweetening
Catalytic
Condensation
Gasoline
Treating
Selective
Hydrotreating
Lube Base Oil
Upgrading
Lube
Base Oils
Diesel
Kerosene
& Jet Fuel
Gasoline
C4
Isomerization
Hydrotreating
Hydrotreating
Hydrotreating
Hydrotreating
SHP
Alkylation
LPG Treating
FCC
Hydrocracking
Reforming
RF
RF
AF
AF
AF
AF
AF
AF
AF
AF
AF
AF
AF
F
F F
F
F
F
F
3
Typical Applications
in the refining
and petrochemical process
Trislot®
has a wide range of wedge wire reactor internals available for your
media retention and solid-liquid separation processes that have been used
in many types of vessels and reactors. The wedge wire reactor internals
are mainly used in two types of reactor processes.
	 Axial flow (down or up) reactors, whereby the flow of the process
liquid/gas through the catalyst is from top to bottom.
	 Radial flow reactors, whereby the flow of the process liquid/gas
through the catalyst is from outside to the centre of the reactor and
vice versa.
	 Bubble column reactors, where the catalyst freely moves in the reac-
tor. Catalyst is retained by means of slot tubes.
Refining
	Hydrotreating
	Hydrocracking
	 Hydrodesulphurisation (HDS)
	 Molecular Sieve
	 Sulphur Recovery Units
	Alkylation
	 Continuous Catalyst
Regeneration (CCR)
Petrochemical
	 Purified Terephthalic Acid
(PTA)
	 Styrene Monomer
Dehydrogenation
	 Ammonia Conversion
	 Mercury Removal
	 Sulphur Recovery
	Ethylene
	Merox
	 Gas Dehydration
Natural Gas
	 Molecular Sieves (Hydrogen)
	 Activated Carbon
	 Silica Gel
	Amine
	 Mercury Removal
Trislot®
wedge wire reactor internals are commonly found in the following processes:
4
Shell Global Solutions (SGS)
	UOP
	 IFP / Axens
	 Haldor Topsoe (HTAS)
	 ABB Lummus
	Uhde
	Linde
	Snamprogretti
	 Air Products
	Chevron
	BOC
	Sasol
Trislot®
has been working with worldwide Process Licensors including the following:
Wedge wire advantages
Needless to say that the maintenance cost and risk of defects need
to be minimised in refining & petrochemical applications.
Wedge wire holds the advantages that have a larger return on invest-
ment than any other filter medium:
	 Strong mechanical
construction
	 Non-clogging surface
	 No maintenance or
replacement costs
5
Axial Flow Reactor Internals
These reactor internals are employed for their high ability to safely retain your expensive catalyst media from
migration. Wedge wire screens allow the collection of process flow across the entire reactor/vessel diameter or
length.
Employing the advantages of wedge wire, Trislot®
offers a wide range of reactor internals designed by our engi-
neers to your specific requirements. All screen internals are designed to fit through the reactor manway and are
commonly manufactured from Stainless Steel AISI 304 / 304L / 316L / 321 / 348 / 310.
1
Inlet Distributors
(Feed Diffusers)
	 Manufactured from either
wedge wire screen or from
plate.
	 Used to evenly distribute the
process flow over the top
surface of the catalyst bed
or onto the adjacent reactor
internal (e.g. distribution
tray).
	 Designs vary depending on
the Process Licensor.
Support Grids
	 A welded flat screen
with or without additional
support bars.
	 Used for supporting and
directly retaining media.
	 Made in several sections
to pass through the vessel
manway.
	 Designed to a calculated
design load, which includes
the bed weight and pressure
drop through a catalyst/
resin bed.
	 Can be easily accommodated
with vessel support beams.
	 Common slot openings:
0.25 – 1.0 mm.
Filter Elements
(Scale Traps)
	 A series of cylindrical
screens arrayed at the top
of the upper catalyst bed.
	 Used to collect metallic
contaminants or scale from
plugging the top surface of
the upper catalyst bed.
	 Will also increase the total
surface area of the upper
catalyst bed to extend the
bed’s useful life.
	 Common slot openings: 0.5
– 1.5 mm.
Outlet Collectors
(Bottom Baskets)
	 A cylindrical screen with or
without a screen top section.
	 Used for direct media
retention and as a safety
screen to prevent migration
of catalyst through the outlet
nozzle.
	 Designed to a calculated
design load, which includes
the bed weight and pressure
drop through a catalyst/
resin bed.
	 Fixed to the reactor/vessel
bottom head via bolts; lugs
with wedge-pins; or fully
welded.
	 Common slot openings:
0.25 – 4.0 mm.
6
Axial Flow Reactor Internals (cont.)
Trislot®
has designed and manufactured axial flow reactor internals to many customers worldwide.
Catalyst Support Grid with Support Beams
4 sets of Scale Trap Baskets
Molecular Sieve Bed Support Grid for a horizontal vessel
Large Catalyst Support Grid (4000 mm dia.) with Beams and
Anti-Buckling Combs
Outlet Collectors
Scale Trap Baskets
7
Radial Flow Reactor Internals
These reactor internals are employed for their high-volume flow capacity with minimal pressure drop. Normally ar-
ranged with two types of concentric-positioned screens, which create an annulus filled with either static or flowing
catalyst media.
Also employing the advantages of wedge wire, Trislot®
offers a wide range of screen internals designed by our
engineers to your specific requirements. All screen internals are designed to fit through the reactor manway and
are commonly manufactured from Stainless Steel AISI 316L and 321/321H / Inconel.
Cover Plates and Riser Plates
	Trislot®
also offers the
centrepipe cover plates and
scallop riser seal plates.
Other types of internals can
also be supplied.
Centrepipes
	 A large cylindrical screen
wrapped around a strong
perforated tube.
	 The slot openings run in
the axial direction (up to
down) to provide a smooth
interface to eliminate the
abrasion of expensive
catalyst and thus minimising
fines.
	 Centrepipes or centre
screens are designed to a
calculated design load, which
includes the bed load and
pressure drop through the
catalyst bed.
	 Slot openings vary depending
on the Process Licensor.
Commonly 0.61 mm.
Scallops
	 ’D’-shaped screens
manufactured from either
wedge wire screen or
perforated plate.
	 Scallops are located around
the reactor wall and held into
position by expander rings.
	 Provides a higher surface
area than a traditional outer
basket.
	 Installation and repair can
be much faster and simpler
with these individual screens.
	 Slot openings/perforation
openings vary depending
on the Process Licensor.
Commonly 1.02 x 12.57
mm perforated slots.
	 Spare Scallops are generally
held in stock by many
refiners for emergency
shutdowns.
2
8
Radial Flow Reactor Internals (cont.)
Trislot®
has designed and manufactured radial flow reactor internals to many customers worldwide.
Scallops and Centrepipe in position
Centrepipe (length 10m) in Inconel 600
Centrepipe for revamp in 4 sections
Set of Scallop with perforated liners in AISI 321
Segment of Outer Screen
Outer Screen mock-up assembly
9
Feedstock Filtration
	 Wedge wire screen elements are employed in this
filtration system to remove contaminants such as
coke particles and scale rust from sour water,
reactor feeds and hydrocracker feeds.
	 These contaminants from process equipment and
pipelines lead to fouling of the catalyst beds.
	Screen elements will require backwashing to re-
move the buildup of filter cake.
Other applications in your plant
	Wedge wire screens are used in Ion Exchange,
Water Demineralisers & Softeners, Condensate
Polishers, Sand Filters for media retention and
thus eliminating the migration of expensive resin
out of the vessel.
Filter cycle
During the filter cycle, the solids are deposited
on the smooth surface. This ‘cake’ acts as an
extra filter for finer particles. The fines that slip
through do not get stuck in the conical slots.
Backwash cycle
By reversing the flow, the cake and dirt are re-
moved from the filter surface.
Filtering
Backwashing
Nozzle Screen
Distributor and collector laterals
Resin trap
Candle
filter
Nozzle
3
4
Picture with the courtesy of Asco Filtration
10
Technical Information
The tables below list the most commonly used Trislot®
surface and support profiles used in the refining and
petrochemical industry.
The open area, Fo, is expressed in % and can be calculated
using this formula:
SCREEN
HEIGHT
WIRE
HEIGHT
SUPPORT ROD
HEIGHT
WIRE
WIDTH
RELIEF
ANGLE
WELD PENETRATION
SLOT
Example:
Surface profile 22S : b = 1.8 mm and Slot width : s = 0.5 mm
Trislot®
surface profiles
Figure Name Width (mm) Height (mm)
12S 1 2
12SL 1 2
15S 1.2 2.5
18S 1.5 2.5
18SC 1.5 2.8
22S 1.8 3.7
28S 2.2 4.5
28SC 2.2 4.5
28ST 2.28 3.55
34S 2.8 5.5
42S 3.4 6.8
Trislot®
support profiles
Figure Name Width (mm) Height (mm)
Q25 2 3
Q35 3 5
D45 3.8 5.6
D56 5 6.5
10 x 3 3 10
12 x 3 3 12
15 x 3 3 15
25 x 3 3 25
50 x 3 3 50
s = slot width (mm)
b = width of surface profile
Fo =
s
x 100 (%)
b + s
Fo =
0.5
x 100 % = 22 %
1.8 + 0.5
	 To ensure there are no sudden and unwanted issues during site instal-
lation, we perform an in-house mock-up test assembly of complicated
reactor internals to check for correct fitment of adjacent items. For
example, catalyst support grids with associated support beams and
the HD trays, as pictured below.
	In all other cases, support grids and outlet collectors are still trial
assembled prior to shipment.
	 We welcome our valued customers to visit our factory and carryout a
joint inspection of our reactor internals prior to shipment.
Mock-Up Test Assembly
Mock-up Test Assembly of Catalyst Support Grid, Support Beams and HD Tray
Quality Assurance
Documentation
	Drawing
for Approval
	 Design Calculations
•	Mechanical strength of
screen internals
•	Recommended quantity
and size of support beams
	 Mill Certificates
	 Slot Opening Reports
	 Final Inspection Reports
	 WPS and PQR
	 PMI Reports (at request)
	 Dye Penetrant
11
Trislot®
Quality Assurance
	 ISO 9001 Certified
	Trislot®
focuses on Total Quality Management
Conclusion
Trislot®
offers an extensive range
of screen retention and filtration
solutions, making us an ideal
partner.
References
Trislot®
has supplied screen
internals to end users worldwide
and cooperates with engineering
and vessel fabrication companies
active in this market. Trislot®
is
also a qualified screen vendor of
Shell Global Solutions (SGS).
References can be submitted on
request after discussion with our
customers.
Roterijstraat 134 - B-8970 Waregem - Belgium - T +32 56 62 72 22 - F +32 56 62 72 62 - info@trislot.be
www.trislot.be
From left to right : Mike Verduyn, Marie Cheyns, Corey Brightwell, Yannic Lievrouw, Glenn
Vercruyce, Sandra Van Slambrouck, Yves Struyve, Nurit Galling, Geert Follet
Trislot®
dedicated Sales team
12

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FolderTrislotPetrochemie2015_Lowres

  • 1. Reactor Internals and solid/liquid filtration for the Refining & Petrochemical Industry 1
  • 2. Wedge wire screens Trislot® manufactures reactor internals using wedge wire screens (V-wire screens). Such a screen consists of surface wires that are welded onto support profiles. The distance between the surface profiles is controlled very accurately, as it forms the continuous slot opening (aperture) through which the process liquid or gas flows and by which the media (catalyst or resin) is retained in its position. Strong Self-Supporting Construction In many applications the wedge wire screen is selfsupporting due to a strong weld at each surface wire to support profile intersection. Mesh tends to tear, especially when changing the catalyst. Non-Clogging The continuous slot opening formed by the triangularshaped (‘V’) sur- face wires ensures a two-point contact between particles and the slot, which minimises clogging. High-Precision Slot Sizes Precise slot sizes are available to meet customer’s requirements. Slot openings down to 25μm. Low Pressure Drop and High Open Area To optimise your process output. Smooth Screen Interface The low friction between the screen and expensive medium is a result of the smooth continuous slot openings, which run in one direction allowing the media to move in that direction with a low friction force. All these advantages result in a low maintenance cost and a minimal operational cost for the petrochemical and refining plants. Trislot® has many different profiles available in most stainless steel alloys, Duplex and Super Duplex alloys, Inconel 600, Titanium, Hastelloy C-276, AISI 310, 348, etc. For available profiles and materials, please refer to the end of this brochure or our website www.trislot.be Compared with conventional wire mesh internals, the wedge wire reactor internals have the following advantages: 2
  • 3. The refining process feedstock filtration axial flow internals radial flow internals To Black Oil Hydrocracking Light Naphtha Gasoline Treating Heavy Naphtha Atmospheric Gas Oil Kerosene Middle Distillate Desalted Crude Oil Vacuum Distillation Crude Distillation Light Naphtha Isomerization Kero/Jet Fuel Sweetening Catalytic Condensation Gasoline Treating Selective Hydrotreating Lube Base Oil Upgrading Lube Base Oils Diesel Kerosene & Jet Fuel Gasoline C4 Isomerization Hydrotreating Hydrotreating Hydrotreating Hydrotreating SHP Alkylation LPG Treating FCC Hydrocracking Reforming RF RF AF AF AF AF AF AF AF AF AF AF AF F F F F F F F 3
  • 4. Typical Applications in the refining and petrochemical process Trislot® has a wide range of wedge wire reactor internals available for your media retention and solid-liquid separation processes that have been used in many types of vessels and reactors. The wedge wire reactor internals are mainly used in two types of reactor processes. Axial flow (down or up) reactors, whereby the flow of the process liquid/gas through the catalyst is from top to bottom. Radial flow reactors, whereby the flow of the process liquid/gas through the catalyst is from outside to the centre of the reactor and vice versa. Bubble column reactors, where the catalyst freely moves in the reac- tor. Catalyst is retained by means of slot tubes. Refining Hydrotreating Hydrocracking Hydrodesulphurisation (HDS) Molecular Sieve Sulphur Recovery Units Alkylation Continuous Catalyst Regeneration (CCR) Petrochemical Purified Terephthalic Acid (PTA) Styrene Monomer Dehydrogenation Ammonia Conversion Mercury Removal Sulphur Recovery Ethylene Merox Gas Dehydration Natural Gas Molecular Sieves (Hydrogen) Activated Carbon Silica Gel Amine Mercury Removal Trislot® wedge wire reactor internals are commonly found in the following processes: 4
  • 5. Shell Global Solutions (SGS) UOP IFP / Axens Haldor Topsoe (HTAS) ABB Lummus Uhde Linde Snamprogretti Air Products Chevron BOC Sasol Trislot® has been working with worldwide Process Licensors including the following: Wedge wire advantages Needless to say that the maintenance cost and risk of defects need to be minimised in refining & petrochemical applications. Wedge wire holds the advantages that have a larger return on invest- ment than any other filter medium: Strong mechanical construction Non-clogging surface No maintenance or replacement costs 5
  • 6. Axial Flow Reactor Internals These reactor internals are employed for their high ability to safely retain your expensive catalyst media from migration. Wedge wire screens allow the collection of process flow across the entire reactor/vessel diameter or length. Employing the advantages of wedge wire, Trislot® offers a wide range of reactor internals designed by our engi- neers to your specific requirements. All screen internals are designed to fit through the reactor manway and are commonly manufactured from Stainless Steel AISI 304 / 304L / 316L / 321 / 348 / 310. 1 Inlet Distributors (Feed Diffusers) Manufactured from either wedge wire screen or from plate. Used to evenly distribute the process flow over the top surface of the catalyst bed or onto the adjacent reactor internal (e.g. distribution tray). Designs vary depending on the Process Licensor. Support Grids A welded flat screen with or without additional support bars. Used for supporting and directly retaining media. Made in several sections to pass through the vessel manway. Designed to a calculated design load, which includes the bed weight and pressure drop through a catalyst/ resin bed. Can be easily accommodated with vessel support beams. Common slot openings: 0.25 – 1.0 mm. Filter Elements (Scale Traps) A series of cylindrical screens arrayed at the top of the upper catalyst bed. Used to collect metallic contaminants or scale from plugging the top surface of the upper catalyst bed. Will also increase the total surface area of the upper catalyst bed to extend the bed’s useful life. Common slot openings: 0.5 – 1.5 mm. Outlet Collectors (Bottom Baskets) A cylindrical screen with or without a screen top section. Used for direct media retention and as a safety screen to prevent migration of catalyst through the outlet nozzle. Designed to a calculated design load, which includes the bed weight and pressure drop through a catalyst/ resin bed. Fixed to the reactor/vessel bottom head via bolts; lugs with wedge-pins; or fully welded. Common slot openings: 0.25 – 4.0 mm. 6
  • 7. Axial Flow Reactor Internals (cont.) Trislot® has designed and manufactured axial flow reactor internals to many customers worldwide. Catalyst Support Grid with Support Beams 4 sets of Scale Trap Baskets Molecular Sieve Bed Support Grid for a horizontal vessel Large Catalyst Support Grid (4000 mm dia.) with Beams and Anti-Buckling Combs Outlet Collectors Scale Trap Baskets 7
  • 8. Radial Flow Reactor Internals These reactor internals are employed for their high-volume flow capacity with minimal pressure drop. Normally ar- ranged with two types of concentric-positioned screens, which create an annulus filled with either static or flowing catalyst media. Also employing the advantages of wedge wire, Trislot® offers a wide range of screen internals designed by our engineers to your specific requirements. All screen internals are designed to fit through the reactor manway and are commonly manufactured from Stainless Steel AISI 316L and 321/321H / Inconel. Cover Plates and Riser Plates Trislot® also offers the centrepipe cover plates and scallop riser seal plates. Other types of internals can also be supplied. Centrepipes A large cylindrical screen wrapped around a strong perforated tube. The slot openings run in the axial direction (up to down) to provide a smooth interface to eliminate the abrasion of expensive catalyst and thus minimising fines. Centrepipes or centre screens are designed to a calculated design load, which includes the bed load and pressure drop through the catalyst bed. Slot openings vary depending on the Process Licensor. Commonly 0.61 mm. Scallops ’D’-shaped screens manufactured from either wedge wire screen or perforated plate. Scallops are located around the reactor wall and held into position by expander rings. Provides a higher surface area than a traditional outer basket. Installation and repair can be much faster and simpler with these individual screens. Slot openings/perforation openings vary depending on the Process Licensor. Commonly 1.02 x 12.57 mm perforated slots. Spare Scallops are generally held in stock by many refiners for emergency shutdowns. 2 8
  • 9. Radial Flow Reactor Internals (cont.) Trislot® has designed and manufactured radial flow reactor internals to many customers worldwide. Scallops and Centrepipe in position Centrepipe (length 10m) in Inconel 600 Centrepipe for revamp in 4 sections Set of Scallop with perforated liners in AISI 321 Segment of Outer Screen Outer Screen mock-up assembly 9
  • 10. Feedstock Filtration Wedge wire screen elements are employed in this filtration system to remove contaminants such as coke particles and scale rust from sour water, reactor feeds and hydrocracker feeds. These contaminants from process equipment and pipelines lead to fouling of the catalyst beds. Screen elements will require backwashing to re- move the buildup of filter cake. Other applications in your plant Wedge wire screens are used in Ion Exchange, Water Demineralisers & Softeners, Condensate Polishers, Sand Filters for media retention and thus eliminating the migration of expensive resin out of the vessel. Filter cycle During the filter cycle, the solids are deposited on the smooth surface. This ‘cake’ acts as an extra filter for finer particles. The fines that slip through do not get stuck in the conical slots. Backwash cycle By reversing the flow, the cake and dirt are re- moved from the filter surface. Filtering Backwashing Nozzle Screen Distributor and collector laterals Resin trap Candle filter Nozzle 3 4 Picture with the courtesy of Asco Filtration 10
  • 11. Technical Information The tables below list the most commonly used Trislot® surface and support profiles used in the refining and petrochemical industry. The open area, Fo, is expressed in % and can be calculated using this formula: SCREEN HEIGHT WIRE HEIGHT SUPPORT ROD HEIGHT WIRE WIDTH RELIEF ANGLE WELD PENETRATION SLOT Example: Surface profile 22S : b = 1.8 mm and Slot width : s = 0.5 mm Trislot® surface profiles Figure Name Width (mm) Height (mm) 12S 1 2 12SL 1 2 15S 1.2 2.5 18S 1.5 2.5 18SC 1.5 2.8 22S 1.8 3.7 28S 2.2 4.5 28SC 2.2 4.5 28ST 2.28 3.55 34S 2.8 5.5 42S 3.4 6.8 Trislot® support profiles Figure Name Width (mm) Height (mm) Q25 2 3 Q35 3 5 D45 3.8 5.6 D56 5 6.5 10 x 3 3 10 12 x 3 3 12 15 x 3 3 15 25 x 3 3 25 50 x 3 3 50 s = slot width (mm) b = width of surface profile Fo = s x 100 (%) b + s Fo = 0.5 x 100 % = 22 % 1.8 + 0.5 To ensure there are no sudden and unwanted issues during site instal- lation, we perform an in-house mock-up test assembly of complicated reactor internals to check for correct fitment of adjacent items. For example, catalyst support grids with associated support beams and the HD trays, as pictured below. In all other cases, support grids and outlet collectors are still trial assembled prior to shipment. We welcome our valued customers to visit our factory and carryout a joint inspection of our reactor internals prior to shipment. Mock-Up Test Assembly Mock-up Test Assembly of Catalyst Support Grid, Support Beams and HD Tray Quality Assurance Documentation Drawing for Approval Design Calculations • Mechanical strength of screen internals • Recommended quantity and size of support beams Mill Certificates Slot Opening Reports Final Inspection Reports WPS and PQR PMI Reports (at request) Dye Penetrant 11
  • 12. Trislot® Quality Assurance ISO 9001 Certified Trislot® focuses on Total Quality Management Conclusion Trislot® offers an extensive range of screen retention and filtration solutions, making us an ideal partner. References Trislot® has supplied screen internals to end users worldwide and cooperates with engineering and vessel fabrication companies active in this market. Trislot® is also a qualified screen vendor of Shell Global Solutions (SGS). References can be submitted on request after discussion with our customers. Roterijstraat 134 - B-8970 Waregem - Belgium - T +32 56 62 72 22 - F +32 56 62 72 62 - info@trislot.be www.trislot.be From left to right : Mike Verduyn, Marie Cheyns, Corey Brightwell, Yannic Lievrouw, Glenn Vercruyce, Sandra Van Slambrouck, Yves Struyve, Nurit Galling, Geert Follet Trislot® dedicated Sales team 12