Pensky Martens Closed Cup (PMCC) Apparatus is a technique to detect the flash points of distillate fuels as well as residual fuel according to ASTM D93.
2. The lowest temperature
corrected to a barometric
pressure of 101.3 kPa (760 mm
Hg) of a volatile sample, at which
application of an ignition source
causes the vapors of a specimen
of the sample to ignite under
specified conditions of test.
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3. Temperature range 40 °C to 250 °C (Precisely).
A brass test cup of specified dimensions with a cover of
specified dimensions.
75 mL of sample is required for each test (Remove excess
specimen).
The temperature of the test cup and test specimen shall be at
least 18°C or 32°F below the expected flash point.
Test flame diameter range from 3.2 – 4.8 mm
Gas pressure should be less than 3 kPa.
Follow two standard operating procedures based on specimen.
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4. 4
SoP - A SoP - B
Used for distillate fuels Used for Residual fuels
Temp Changes 5-6 °C/min Temp changes 1 – 1.6 °C/min
Stirring at 90-120 rpm Stirring at 250 ± 5 rpm
Apply Ignition source before
23 ± 5 °C of expected flash
point
e.g. residual fuel oils, used
lubricating oils, mixtures of
petroleum liquids with solids,
Dipping at each 1 °C for 1s only petroleum liquids that tend to
form a surface film under test
conditions
Discontinue stirring during
dipping.
5. 5
ASTM IP Range Uses
9C 15C -5 to 110 °C Low
88C 101C 10 to 200 °C Medium
10C 16C 90 to 370 °C High
6. ●》The correction factor is applicable as following-
Corrected Fash point = C + 0.25 (101.3 – K)
Corrected Fash point = F + 0.06 (760 - P)
Corrected Fash point = C + 0.033 (760 - P)
●》where: C = observed Fash point, °C,
F = observed Fash point, °F,
P = ambient barometric pressure, mm Hg, and
K = ambient barometric pressure, kPa.
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7. Handling and transportation risk assessment.
Storage risk assessment.
used as elements of fire safety risk assessment.
assessing the overall flammability hazard of a material.
detection of contamination of relatively nonvolatile or
nonflammable materials with volatile or flammable
materials.
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8. Avoid spillage of fuel samples around instrument vicininty.
75 mL of sample is required for each test (Remove excess
specimen).
The temperature of the test cup and test specimen shall be at
least 18°C or 32°F below the expected flash point.
Test flame diameter range from 3.2 – 4.8 mm
Gas pressure should be less than 3 kPa.
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