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ALESSANDRO FIORESE
TRATTAMENTI
TERMICI IN VUOTO
TECNOLOGIE
ADDITIVE
MANUFACTURING
TAV VACUUM FURNACES
R&D Chief Engineer
Master’s Degree: Materials Engineering and
Nanotechnology
Politecnico Milan
OUR
VACUUM
FURNACES
Meeting Your needs
Uncompromising research for quality and customer
orientation are the basis of all TAV VACUUM
FURNACES solutions. Each furnace is designed
according to the specifications and meets the most strict
criteria and procedures to ensure compliance with the
most stringent industry specifications.
AT FIRST SIGHT
50 countries
5 Continents
Started in
1984
ISO 9001
+ AEROSPACE
+ COMMERCIAL HEAT TREATERS
+ IGT - INDUSTRIAL GAS TURBINES
+ HEAT EXCHANGERS INDUSTRY
+ SINTERING INDUSTRY
+ ADDITIVE MANUFACTURING
+ R&D AND LABORATORIES
Close collaboration
with customers
and partners.
OUR CORE VALUES
Flexibility, technology and quality. These three core values have been
driving us since 1984 make our company as market leader for vacuum
furnaces. This is because of the trust obtained from small and large-sized
companies on the international scene. Thanks to its top grade
specialization in vacuum engineering, TAV VACUUM FURNACES
can design and manufacture top quality vacuum furnaces for a wide range
of industries and applications worldwide focusing on constant innovation.
R&D department in TAV VACUUM FURNACES is constantly working to
ensure a tailor-made product according to customer needs, with regard to
innovative technologies.
Thanks to our wide know-how in vacuum engineering, we provide
customers with a team of professionals who can manage and solve all
issues, ranging from design to manufacture, to project management,
installation, technical assistance and training.
+
APPLICATIONS
VACUUM
HEAT TREATMENT
VACUUM
BRAZING
VACUUM
SINTERING
ADDITIVE
MANUFACTURING
APPLICATIONS
ADVANCED
CERAMICS
DIFFUSION
BONDING
ALUMINIZING UHV
(Ultra High Vacuum)
Alumina
+
+
+
It can be translucent and transparent
High mechanical properties
+
+
+
Orthodontic advice
Biomedical advice
Airborne optics
Complex shape
Opaque
Light scatterring
can be minimized
when ceramics
heterogeneities are limited
Porosity
Grain size
+
+
+ Defect concentration
Sintering
We have to minimize porosity
and grain size in order to
maximize translucence.
VACUUM THERMAL
PROCES
Debinding & Sintering
Powder
99,99% pure
Pressure
150 mbar
Thermal debinding
800 °C for 24 h
Sintering
From 1350°C to 1500 °C
For 2 h and 50 h
Air vs Vacuum Sintering
+
+
G. Mata-Osoro et al. / Journal of the European Ceramic Society 32 (2012) 2925–2933
RESULTS
DENSITY
SHRINKAGE
MICROSTRUCTURE MECHANICAL
PROPERTIES
OPTICAL
PROPERTIES
G. Mata-Osoro et al. / Journal of the European Ceramic Society 32 (2012) 2925–2933
MICROSTRUCTURE
50 h in vacuum
50 h in air
2 h in air
2 h in vacuum
Sintered 2h
at 1400 °C
In air
Sintered 2h
at 1400 °C
In vacuum
SEM
METHOD
G. Mata-Osoro et al. / Journal of the European Ceramic Society 32 (2012) 2925–2933
DENSITY
50 h in vacuum 50 h in air
2 h in air 2 h in vacuum
Archimede
METHOD
in vacuum in air
and SHRINKAGE
Dilatometer
G. Mata-Osoro et al. / Journal of the European Ceramic Society 32 (2012) 2925–2933
MECHANICAL PROPERTIES
Vickers
1350°C 2h
Vacuum
1350°C 2h
Air
1350°C 50h Vacuum
1500°C 2h Vacuum
1350°C 50h Air
1450°C 50h Vacuum
1450°C 50h
Air
METHOD
G. Mata-Osoro et al. / Journal of the European Ceramic Society 32 (2012) 2925–2933
OPTICAL PROPERTIES
FTIR
METHOD
Sintered 1350 °C for 50 h
Vacuum
Air
G. Mata-Osoro et al. / Journal of the European Ceramic Society 32 (2012) 2925–2933
CONCLUSIONS
+ Best sintering condition: 1350 °C for 50 h in vacuum
+ Vacuum sintering guarantee the quasi total absence of porosity
and the high stability of grain boundaries.
+ The same ceramics properties that make transparent samples,
are the ones required for high hardness and mechanical properties
G. Mata-Osoro et al. / Journal of the European Ceramic Society 32 (2012) 2925–2933
W O R L D W I DE
P R E S E N C E
CO N TAC T U S
info@tav-vacuumfurnaces.com
TEL: +39 0363 355711
Via dell'Industria, 11
24043 Caravaggio (BG) - ITALY
info@furna.care
TEL: 1 864 599 9955
TEL: 1 864 906 4457
100 Corporate Dr Ste A
Spartanburg – South Carolina 29303 - USA
www.furnacare.com
+

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Advanced Ceramics at ICACC19

  • 1.
  • 2. ALESSANDRO FIORESE TRATTAMENTI TERMICI IN VUOTO TECNOLOGIE ADDITIVE MANUFACTURING TAV VACUUM FURNACES R&D Chief Engineer Master’s Degree: Materials Engineering and Nanotechnology Politecnico Milan
  • 3. OUR VACUUM FURNACES Meeting Your needs Uncompromising research for quality and customer orientation are the basis of all TAV VACUUM FURNACES solutions. Each furnace is designed according to the specifications and meets the most strict criteria and procedures to ensure compliance with the most stringent industry specifications.
  • 4. AT FIRST SIGHT 50 countries 5 Continents Started in 1984 ISO 9001 + AEROSPACE + COMMERCIAL HEAT TREATERS + IGT - INDUSTRIAL GAS TURBINES + HEAT EXCHANGERS INDUSTRY + SINTERING INDUSTRY + ADDITIVE MANUFACTURING + R&D AND LABORATORIES Close collaboration with customers and partners.
  • 5. OUR CORE VALUES Flexibility, technology and quality. These three core values have been driving us since 1984 make our company as market leader for vacuum furnaces. This is because of the trust obtained from small and large-sized companies on the international scene. Thanks to its top grade specialization in vacuum engineering, TAV VACUUM FURNACES can design and manufacture top quality vacuum furnaces for a wide range of industries and applications worldwide focusing on constant innovation. R&D department in TAV VACUUM FURNACES is constantly working to ensure a tailor-made product according to customer needs, with regard to innovative technologies. Thanks to our wide know-how in vacuum engineering, we provide customers with a team of professionals who can manage and solve all issues, ranging from design to manufacture, to project management, installation, technical assistance and training. +
  • 8. Alumina + + + It can be translucent and transparent High mechanical properties + + + Orthodontic advice Biomedical advice Airborne optics Complex shape
  • 9. Opaque Light scatterring can be minimized when ceramics heterogeneities are limited Porosity Grain size + + + Defect concentration
  • 10. Sintering We have to minimize porosity and grain size in order to maximize translucence. VACUUM THERMAL PROCES Debinding & Sintering Powder 99,99% pure Pressure 150 mbar Thermal debinding 800 °C for 24 h Sintering From 1350°C to 1500 °C For 2 h and 50 h Air vs Vacuum Sintering + + G. Mata-Osoro et al. / Journal of the European Ceramic Society 32 (2012) 2925–2933
  • 11. RESULTS DENSITY SHRINKAGE MICROSTRUCTURE MECHANICAL PROPERTIES OPTICAL PROPERTIES G. Mata-Osoro et al. / Journal of the European Ceramic Society 32 (2012) 2925–2933
  • 12. MICROSTRUCTURE 50 h in vacuum 50 h in air 2 h in air 2 h in vacuum Sintered 2h at 1400 °C In air Sintered 2h at 1400 °C In vacuum SEM METHOD G. Mata-Osoro et al. / Journal of the European Ceramic Society 32 (2012) 2925–2933
  • 13. DENSITY 50 h in vacuum 50 h in air 2 h in air 2 h in vacuum Archimede METHOD in vacuum in air and SHRINKAGE Dilatometer G. Mata-Osoro et al. / Journal of the European Ceramic Society 32 (2012) 2925–2933
  • 14. MECHANICAL PROPERTIES Vickers 1350°C 2h Vacuum 1350°C 2h Air 1350°C 50h Vacuum 1500°C 2h Vacuum 1350°C 50h Air 1450°C 50h Vacuum 1450°C 50h Air METHOD G. Mata-Osoro et al. / Journal of the European Ceramic Society 32 (2012) 2925–2933
  • 15. OPTICAL PROPERTIES FTIR METHOD Sintered 1350 °C for 50 h Vacuum Air G. Mata-Osoro et al. / Journal of the European Ceramic Society 32 (2012) 2925–2933
  • 16. CONCLUSIONS + Best sintering condition: 1350 °C for 50 h in vacuum + Vacuum sintering guarantee the quasi total absence of porosity and the high stability of grain boundaries. + The same ceramics properties that make transparent samples, are the ones required for high hardness and mechanical properties G. Mata-Osoro et al. / Journal of the European Ceramic Society 32 (2012) 2925–2933
  • 17. W O R L D W I DE P R E S E N C E
  • 18. CO N TAC T U S info@tav-vacuumfurnaces.com TEL: +39 0363 355711 Via dell'Industria, 11 24043 Caravaggio (BG) - ITALY info@furna.care TEL: 1 864 599 9955 TEL: 1 864 906 4457 100 Corporate Dr Ste A Spartanburg – South Carolina 29303 - USA www.furnacare.com
  • 19. +