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IJSRD - International Journal for Scientific Research & Development| Vol. 2, Issue 07, 2014 | ISSN (online): 2321-0613
All rights reserved by www.ijsrd.com 165
Microhardness of Friction Stir Processed Aluminium Alloy-6063
Mr. Virender1
Mr. Rajesh Kumar2
Deepak Dhankhar3
1,2,3
Department of Mechanical engineering
1,2,3
U.I.E.T, MDU, Rohtak
Abstract— Aluminum alloy are in great demand in the field
of defense, automobile, and aerospace industries. These
alloys are known for its light weight, high thermal
conductivity, and low coefficient of thermal expansion, high
wear resistance, and high strength. Composites materials are
the multi-functional materials that are having better
properties. They can be utilized for the requirements of any
application. In this study, Aluminum oxide were united by
using Friction Stir Processing(FSP) into the commercially
aluminum alloy-6063. Samples were subjected to the
various tool rotating with aluminum oxide powder.
Microhardness observations were carried out. The result
showed that increasing rotating speed more uniform
distribution of Aluminum oxide particles. The
microhardness of produced alloy was improved as compared
to that of base aluminum alloy.
Keywords: thermal expansion, high wears resistance, high
strength, FSP
I. INTRODUCTION
Friction stir processing (FSP) is a modification of friction
stir welding (FSW) process. In 1991, a joining process
invented by Wayne Thomas at TWI is known as the Friction
stir welding process. It is a widely used technique for
joining of Al alloys because; Al alloys are very poor to
fusion weld. The main difference between those processes
that FSP does not join materials, but can locally enhances
the mechanical and tribological properties of materials like
eliminates casting defects, improve ductility and strength,
refine microstructure, superior wear resistance and improve
fatigue and resistance to corrosion . The basic principle of
FSP is similar to FSW. Friction stir processing technique is
widely used as solid state processing process and a surface-
engineering technology. Furthermore, the FSP technique has
been utilized as surface composite fabrication on Al alloy
substrate, MMC’s, and cast Al alloys . A schematic of FSP
is shown in Figure 1.1. The tool plays critical role during
FSP, because the selection and the designing of tool material
is critically important to process.
Fig. 1: Schematic of Friction stir processing
A rotating piece is defined as the tool, which designed and
manufactured to plastically deforming the processed zone
and produce heat due to stirring action between work piece
and the tool pin. The tool consists mainly three parts such as
tool pin, shoulder and the shank. The angle of the tool as
compare to the vertical direction is known as tilt angle. The
trailing and leading edge will be used to differentiate
between the rear and front limb of the tool as the front is
described as the direction of travel. Hence to enhance the
mechanical and tribological properties locally, Friction stir
processing shows the great route to get desired properties.
Friction stir processing can be applied variably up to the
depth of in the range of 0.5 to 50 mm. Principle of FSP
In Fiction stir processing, a non-consumable,
rapidly rotating tool containing pin and shoulder. The tool
pin is plunged in a work piece of material, and then moving
the tool across the surface. The tool pin causes upward metal
flow and a forging force provides by the shoulder. In the
narrow processed zone a continual hot working action is
provided by the rotating tool. As there is no liquid in narrow
processed zone, it cools without solidification, with fine
grain microstructure. The objective of this paper to
investigate the microhardness of aluminium alloy-6063 to
form metal composites by means of FSP technique.
Microhardness of Friction Stir Processed Aluminium Alloy-6063
(IJSRD/Vol. 2/Issue 07/2014/039)
All rights reserved by www.ijsrd.com 166
Fig. 2:Schematic illustration of FSP tool
II. EXPERIMENTAL PROCEDURE
The objective was achieved through a selection of the
experimental matrix including all material selection, friction
stir processing parameters, conducting a thorough analysis
and performing representative mechanical tests. Based on
the demand in the field of automobile, aerospace and other
application we can say that the study of microhardness
behaviour is almost necessary. In this present study, Al
based alloy processed by FSP to enhance mechanical
performance.The starting materials were plates of
aluminium-6063 with a nominal composition of si-0.20-.6,
iron-.35, copper-.10, mangnese-.10, zinc-.10, titanium-.10,
aluminium balanced. The dimensions of work piece were
50mm×100mm×6mm. After making drilled holes in
samples , the nano particles of aluminium oxide were added
in the holes and surface. Fig.2 showed a schematic
illustration tool designed for FSP. The tool was made up
from mild steel. The tool was rotated clockwise at rotation
speed of 930,1190,1480,1800 rpm. The travelling speed
were constant. All FSP studies were carried out at room
temperature with only a single pass. Vickers microhardness
test were performed on the treated plates. Four test samples
for each condition were tested.
Processed zone
Fig. 3: Friction stir processed zone
III. RESULTS AND DISCUSSION
The effect of processing on the microhardness of plain and
aluminium oxide particles added specimens was shown in
graphs. Increased rpm caused significant increment in the
microhardness values. The microhardness of processed Al-
6063 has an average of 70.94. The highest microhrdness
value was 73.5 and the lowest was 69.1 for processed
specimens. The microhardness of plain Al has an average of
61.6. the highest value was 61.9. and lowest value was 60.4
for plain specimens. The highest hardness values were
obtained from high rpm for aluminium oxide added
specimens. With high rpm shoulder supplied more heat and
aluminium oxide particles were disperesed well in base
metal. As a result microhardness was increased with
uniformly added aluminium oxide.
Speed=930rpm
Speed=1190rpm
Speed=1480rpm
Speed=1800rpm
IV. CONCLUSION
Inthe present study the plain Al and aluminium oxide
composites were successfully united by FSP. The
Microhardness of Friction Stir Processed Aluminium Alloy-6063
(IJSRD/Vol. 2/Issue 07/2014/039)
All rights reserved by www.ijsrd.com 167
microhardness were evaluated obseving the reinforcement
particles. The following results were obtained :
(1) It has been demonstrated that FSP was better
method to modify the mehanical properties of Al-
6063. FSP increased the microhardness of
processed material.
(2) Increased rpm affects the reinforcing particles. A
good dispersion of aluminium oxide can be
obtained by ω= 1800 rpm.
(3) Good interfacial conditions between particles and
base metal can be formed during this solid-state
process which avoids the chemical reactions on the
interface.
(4) The depth of the surface layer can be penetrated by
welding parameters or probe design which could be
used with pin or without pin.
(5) FSP treatments improve the formability of plain
samples; hence they could be used for super plastic
applications.
(6) The microhardness of the plain surface of
Aluminium increased significantly with increasing
rotation. The highest microhardness value was
obtained 61.9Hv for the plain specimen.
(7) The microhardness of the aluminium oxide added
composites increases significantly with increasing
rotation speed. The highest microhardness value
was obtained 73.5Hv for the processed specimen.
(8) The high microhardness of aluminium oxide
composite can be attributed to the presence of
reinforcement particles.
(9) With further research efforts and increased
understanding, FSP could be conducted for
mechanical behaviour of these composites, like
fatigue and creep response and new tool design for
uniform distribution of reinforcement particles into
the matrix.
REFERENCES
[1] Mishra, R.S., Mahoney, M.W., 2002. Superplastic
deformation behaviour of friction stir processed
7075Al alloy. Acta Mater. 50, 4419–4430.
[2] W.M. Thomas, E.D. Nicholas, J.C. Needham, M.G.
Murch, P. Templesmith, C.J. Dawes, G.B. Patent
Application No. 9125978.8 (December 1991).
[3] C. Dawes, W. Thomas, TWI Bulletin 6,
November/December 1995, p. 124.
[4] B. London, M. Mahoney, B. Bingel, M. Calabrese,
D.Waldron, in: Proceedings of the Third International
Symposium on Friction Stir Welding, Kobe, Japan,
27–28 September, 2001.
[5] C.G. Rhodes, M.W. Mahoney, W.H. Bingel, R.A.
Spurling, C.C. Bampton, Scripta Mater. 36 (1997) 69.
[6] G. Liu, L.E. Murr, C.S. Niou, J.C. McClure, F.R.
Vega, Scripta Mater. 37 (1997) 355.
[7] Colligan, K., 1999. Material flow behavior during
friction stir welding of aluminium. Weld. J. 78, 229–
237.
[8] Kurt, A., Uygur, I., Ates, H., 2007. Effect of porosity
content on the weldability of powder metal parts
produced by friction stir welding. Mater. Sci. Forum.
534–536, 789–792.
[9] Kurt, A., Gulenc, B., Uygur, I., Ates, H., 2006. The
effect of rotation speed on mechanical properties of
commercially pure Aluminium joined by friction stir
welding. In: Materials and Technology Conference,
15–19 October., Fundamentals and Characterisation
vol. 1, Ohio, USA, pp. 565–570.
[10]R.S. Mishra, M.W. Mahoney, Mater. Sci. Forum
357–359 (2001) 507.
[11] K.N. Krishnan, Mater. Sci. Eng. A 327 (2002) 246.
[12]J.Q. Su, T.W. Nelson, R.S. Mishra, M.W. Mahoney,
Acta Mater. 51 (2003) 713.
[13]Z.Y. Ma, R.S. Mishra, M.W. Manohey, R. Grimes,
Mater. Sci. Eng. A 351 (2003) 148.
[14]Z.Y. Ma, S.R. Sharma, R.S. Mishra, M.W. Manohey,
Mater. Sci. Forum 426–432(2003) 2891.

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Microhardness of Friction Stir Processed Aluminium-6063

  • 1. IJSRD - International Journal for Scientific Research & Development| Vol. 2, Issue 07, 2014 | ISSN (online): 2321-0613 All rights reserved by www.ijsrd.com 165 Microhardness of Friction Stir Processed Aluminium Alloy-6063 Mr. Virender1 Mr. Rajesh Kumar2 Deepak Dhankhar3 1,2,3 Department of Mechanical engineering 1,2,3 U.I.E.T, MDU, Rohtak Abstract— Aluminum alloy are in great demand in the field of defense, automobile, and aerospace industries. These alloys are known for its light weight, high thermal conductivity, and low coefficient of thermal expansion, high wear resistance, and high strength. Composites materials are the multi-functional materials that are having better properties. They can be utilized for the requirements of any application. In this study, Aluminum oxide were united by using Friction Stir Processing(FSP) into the commercially aluminum alloy-6063. Samples were subjected to the various tool rotating with aluminum oxide powder. Microhardness observations were carried out. The result showed that increasing rotating speed more uniform distribution of Aluminum oxide particles. The microhardness of produced alloy was improved as compared to that of base aluminum alloy. Keywords: thermal expansion, high wears resistance, high strength, FSP I. INTRODUCTION Friction stir processing (FSP) is a modification of friction stir welding (FSW) process. In 1991, a joining process invented by Wayne Thomas at TWI is known as the Friction stir welding process. It is a widely used technique for joining of Al alloys because; Al alloys are very poor to fusion weld. The main difference between those processes that FSP does not join materials, but can locally enhances the mechanical and tribological properties of materials like eliminates casting defects, improve ductility and strength, refine microstructure, superior wear resistance and improve fatigue and resistance to corrosion . The basic principle of FSP is similar to FSW. Friction stir processing technique is widely used as solid state processing process and a surface- engineering technology. Furthermore, the FSP technique has been utilized as surface composite fabrication on Al alloy substrate, MMC’s, and cast Al alloys . A schematic of FSP is shown in Figure 1.1. The tool plays critical role during FSP, because the selection and the designing of tool material is critically important to process. Fig. 1: Schematic of Friction stir processing A rotating piece is defined as the tool, which designed and manufactured to plastically deforming the processed zone and produce heat due to stirring action between work piece and the tool pin. The tool consists mainly three parts such as tool pin, shoulder and the shank. The angle of the tool as compare to the vertical direction is known as tilt angle. The trailing and leading edge will be used to differentiate between the rear and front limb of the tool as the front is described as the direction of travel. Hence to enhance the mechanical and tribological properties locally, Friction stir processing shows the great route to get desired properties. Friction stir processing can be applied variably up to the depth of in the range of 0.5 to 50 mm. Principle of FSP In Fiction stir processing, a non-consumable, rapidly rotating tool containing pin and shoulder. The tool pin is plunged in a work piece of material, and then moving the tool across the surface. The tool pin causes upward metal flow and a forging force provides by the shoulder. In the narrow processed zone a continual hot working action is provided by the rotating tool. As there is no liquid in narrow processed zone, it cools without solidification, with fine grain microstructure. The objective of this paper to investigate the microhardness of aluminium alloy-6063 to form metal composites by means of FSP technique.
  • 2. Microhardness of Friction Stir Processed Aluminium Alloy-6063 (IJSRD/Vol. 2/Issue 07/2014/039) All rights reserved by www.ijsrd.com 166 Fig. 2:Schematic illustration of FSP tool II. EXPERIMENTAL PROCEDURE The objective was achieved through a selection of the experimental matrix including all material selection, friction stir processing parameters, conducting a thorough analysis and performing representative mechanical tests. Based on the demand in the field of automobile, aerospace and other application we can say that the study of microhardness behaviour is almost necessary. In this present study, Al based alloy processed by FSP to enhance mechanical performance.The starting materials were plates of aluminium-6063 with a nominal composition of si-0.20-.6, iron-.35, copper-.10, mangnese-.10, zinc-.10, titanium-.10, aluminium balanced. The dimensions of work piece were 50mm×100mm×6mm. After making drilled holes in samples , the nano particles of aluminium oxide were added in the holes and surface. Fig.2 showed a schematic illustration tool designed for FSP. The tool was made up from mild steel. The tool was rotated clockwise at rotation speed of 930,1190,1480,1800 rpm. The travelling speed were constant. All FSP studies were carried out at room temperature with only a single pass. Vickers microhardness test were performed on the treated plates. Four test samples for each condition were tested. Processed zone Fig. 3: Friction stir processed zone III. RESULTS AND DISCUSSION The effect of processing on the microhardness of plain and aluminium oxide particles added specimens was shown in graphs. Increased rpm caused significant increment in the microhardness values. The microhardness of processed Al- 6063 has an average of 70.94. The highest microhrdness value was 73.5 and the lowest was 69.1 for processed specimens. The microhardness of plain Al has an average of 61.6. the highest value was 61.9. and lowest value was 60.4 for plain specimens. The highest hardness values were obtained from high rpm for aluminium oxide added specimens. With high rpm shoulder supplied more heat and aluminium oxide particles were disperesed well in base metal. As a result microhardness was increased with uniformly added aluminium oxide. Speed=930rpm Speed=1190rpm Speed=1480rpm Speed=1800rpm IV. CONCLUSION Inthe present study the plain Al and aluminium oxide composites were successfully united by FSP. The
  • 3. Microhardness of Friction Stir Processed Aluminium Alloy-6063 (IJSRD/Vol. 2/Issue 07/2014/039) All rights reserved by www.ijsrd.com 167 microhardness were evaluated obseving the reinforcement particles. The following results were obtained : (1) It has been demonstrated that FSP was better method to modify the mehanical properties of Al- 6063. FSP increased the microhardness of processed material. (2) Increased rpm affects the reinforcing particles. A good dispersion of aluminium oxide can be obtained by ω= 1800 rpm. (3) Good interfacial conditions between particles and base metal can be formed during this solid-state process which avoids the chemical reactions on the interface. (4) The depth of the surface layer can be penetrated by welding parameters or probe design which could be used with pin or without pin. (5) FSP treatments improve the formability of plain samples; hence they could be used for super plastic applications. (6) The microhardness of the plain surface of Aluminium increased significantly with increasing rotation. The highest microhardness value was obtained 61.9Hv for the plain specimen. (7) The microhardness of the aluminium oxide added composites increases significantly with increasing rotation speed. The highest microhardness value was obtained 73.5Hv for the processed specimen. (8) The high microhardness of aluminium oxide composite can be attributed to the presence of reinforcement particles. (9) With further research efforts and increased understanding, FSP could be conducted for mechanical behaviour of these composites, like fatigue and creep response and new tool design for uniform distribution of reinforcement particles into the matrix. REFERENCES [1] Mishra, R.S., Mahoney, M.W., 2002. Superplastic deformation behaviour of friction stir processed 7075Al alloy. Acta Mater. 50, 4419–4430. [2] W.M. Thomas, E.D. Nicholas, J.C. Needham, M.G. Murch, P. Templesmith, C.J. Dawes, G.B. Patent Application No. 9125978.8 (December 1991). [3] C. Dawes, W. Thomas, TWI Bulletin 6, November/December 1995, p. 124. [4] B. London, M. Mahoney, B. Bingel, M. Calabrese, D.Waldron, in: Proceedings of the Third International Symposium on Friction Stir Welding, Kobe, Japan, 27–28 September, 2001. [5] C.G. Rhodes, M.W. Mahoney, W.H. Bingel, R.A. Spurling, C.C. Bampton, Scripta Mater. 36 (1997) 69. [6] G. Liu, L.E. Murr, C.S. Niou, J.C. McClure, F.R. Vega, Scripta Mater. 37 (1997) 355. [7] Colligan, K., 1999. Material flow behavior during friction stir welding of aluminium. Weld. J. 78, 229– 237. [8] Kurt, A., Uygur, I., Ates, H., 2007. Effect of porosity content on the weldability of powder metal parts produced by friction stir welding. Mater. Sci. Forum. 534–536, 789–792. [9] Kurt, A., Gulenc, B., Uygur, I., Ates, H., 2006. The effect of rotation speed on mechanical properties of commercially pure Aluminium joined by friction stir welding. In: Materials and Technology Conference, 15–19 October., Fundamentals and Characterisation vol. 1, Ohio, USA, pp. 565–570. [10]R.S. Mishra, M.W. Mahoney, Mater. Sci. Forum 357–359 (2001) 507. [11] K.N. Krishnan, Mater. Sci. Eng. A 327 (2002) 246. [12]J.Q. Su, T.W. Nelson, R.S. Mishra, M.W. Mahoney, Acta Mater. 51 (2003) 713. [13]Z.Y. Ma, R.S. Mishra, M.W. Manohey, R. Grimes, Mater. Sci. Eng. A 351 (2003) 148. [14]Z.Y. Ma, S.R. Sharma, R.S. Mishra, M.W. Manohey, Mater. Sci. Forum 426–432(2003) 2891.