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Santanu 06-26-2020 corrected by Dr S Dey.pdf

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Tamralipta Mahavidyalaya
Tamralipta Mahavidyalaya

Solved problems of Synthesis 2

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FGI DIS (or Discon.)
DIS
DIS DIS DIS
DIS DIS
DIS (1,5-Dicarbonyl) Avoid Cr(VI) reagent because it provides cyclohexenone as side pdt. Allylic C-H oxidation pdt.
DIS (1,5-Dicarbonyl) Better this route DIS DIS
PhCHO + MeCOMe DIS DIS Retro-Aldol Retro- Michael
DIS Retro- Aldol DIS Retro- Michael (1,3-Dicarbonyl) DIS Retro- Claisen N CO2Et DIS Retro- Michael MeNH2 +
DIS DIS Retro- Aldol Retro-Michael
1st introduce methylvinyl ketone, then methyl iodide and then aldol reaction to cyclize 1.Base 2. 1. Base (1 eq.) 2. Me-I
DIS
Reconnection DIS Retro- Diels-Alder DIS Retro- Aldol Reconnection FGI
Santanu 06-26-2020 corrected by Dr S Dey.pdf

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Santanu 06-26-2020 corrected by Dr S Dey.pdf