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Dielectric constant study of polyaniline magnesium stanate mg sno3 composites
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INTERNATIONAL JOURNAL OF
MECHANICAL ENGINEERING AND International Journal of Mechanical Engineering and Technology (IJMET), ISSN 0976 – 6340(Print), ISSN 0976 – 6359(Online), Volume 5, Issue 11, November (2014), pp. 13-16 © IAEME TECHNOLOGY (IJMET) ISSN 0976 – 6340 (Print) ISSN 0976 – 6359 (Online) Volume 5, Issue 11, November (2014), pp. 13-16 © IAEME: www.iaeme.com/IJMET.asp Journal Impact Factor (2014): 7.5377 (Calculated by GISI) www.jifactor.com 13 IJMET © I A E M E DIELECTRIC CONSTANT STUDY OF POLYANILINE - MAGNESIUM STANATE (MgSnO3) COMPOSITES Venkatesh B. P1, Sangshetty Kalyane2 1Department of Physics, Singhania University, Pacheri Bari Jhunjhunu, Rajastan, India 2Department of Physics, BKIT, Bhalki, Karnataka, India ABSTRACT Chemical route for the synthesis of polymer composites with oxide materials enhances the composite technology. Polyaniline (PANI) and Polyaniline-magnesium stanate (PANI-MgSnO3) composite material was prepared by insitu polymerization of aniline with Magnesium stanate (MgSnO3) as composite material. Variation in the oxide composition with polymer matrix is maintained to know its detailed changes. The dielectric behavior is also investigated in the frequency range 102–107 Hz at room temperature. The dimensions of MgSnO3 particles in the matrix have a greater influence on the observed dielectric values. Keywords: Synthesis, Composites, Dielectric Constant, Polyaniline, MgSnO3. 1. INTRODUCTION The technological importance of basic research and its development on conducting polymer has been carried for new properties and applications [1]. Magnesium stagnate (MgSnO3) is a materials shows good electrical and optical properties [2-3]. Various techniques have been used for the preparation of Magnesium stanate materials [4-6]. More recently, there has been considerable attention on the synthesis of MgSnO3 with additional properties for potential applications [7-8] However, new approach on conducting polymer composite materials integrates the technology of conducting polymeric materials. Metal oxide inserted Polymers constitute polymer composites, which are well studied for its properties [9-11]. Conducting polymers have a variety of applications in various fields, such as in Industry, Scientific and in medical (ISM) fields. Applications like anticorrosion, static coating electromagnetic shielding etc., comes under first generation. Second Generation of electric polymers have applications such as transistors, LEDs, solar cells, batteries etc. Controlled conductivity, high temperature resistance, low cost and ease of bulk preparation make
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International Journal of
Mechanical Engineering and Technology (IJMET), ISSN 0976 – 6340(Print), ISSN 0976 – 6359(Online), Volume 5, Issue 11, November (2014), pp. 13-16 © IAEME these materials attractive in the engineering and scientific world. Among conducting polymers, polyaniline is the most extensively studied polymer obtained by simple chemical or electrochemical route. Polymeric materials have become an area of increasing interest in research because of the fact that these materials have great potential for solid state devices [12-13]. This polyaniline has received much attention because of its high electrical conductivity and ease of preparation at low cost. The demand of high quality materials for electromagnetic compatibility is alarmingly increasing [14]. Metal oxides dispersed polymer composites have attracted a great deal of interest from researchers, because they frequently exhibit unexpected hybrid properties synergistically derived from both components. Magnesium stanate (MgSnO3) is one of the examples of oxide material, which is known for progressive properties and applications [15]. Composite of Magnesium stagnate (MgSnO3) dispersed PANI with variable compositions my lead to desirable properties and new applications. These materials are especially important owing to their bridging role between the worlds of conducting polymers [16-18]. In this paper, we describe the synthesis of PANI and Magnesium stanate (MgSnO3) dispersed PANI composite materials through insitu polymerization method. Dielectric study of the as prepared PANI composite material is also well studied for its dielectric behavior. 14 2. EXPERIMENTAL Materials and Methods Ammonium persulphate (NH4)2S2O8, Hydrochloric acid (HCl) and Magnesium stanate (MgSnO3) used were of AR grade. Doubly distilled water and aniline is used as a solvent and a monomer. Polyaniline is prepared by oxidative method and Polyaniline composites were prepared by insitu polymerization method with dispersion of Magnesium stanate in polyaniline. Synthesis of Polyaniline/Magnesium stanate (MgSnO3) Composites Aniline was dissolved in 1m HCl to form polyaniline (PANI). Magnesium stanate (MgSnO3) was added to PANI solution with vigorous stirring to keep the Magnesium stanate (MgSnO3) suspended in the solution. To this reaction mixture, 0.1M of ammonium persulphate [(NH4)2S2O8], which acts as an oxidant, was added slowly with continuous stirring for 4-6 hours at 0-5OC. The precipitated powder recover was vacuum-filtered and washed with deionizer water. Finally, the resultant precipitate was dried in an oven for 24 hours to achieve a constant weight. In the similar manner pure PANI is prepared without adding Magnesium stanate PANI/ Magnesium stanate (MgSnO3) composites were prepared in weight percent ratio in which the concentration of Magnesium stanate (10, 30, and 50wt %) was varied. The test samples to be used were prepared in pellet form of diameter 10mm and thickness 3mm by applying pressure of 7t using Pye-Unicam dye. The contacts for these composites were made using silver paste as electrodes on both sides. AC conductivity measurements were carried out at room temperature over the frequency range 102-107Hz using the Hiokie LCR Q meter. 3. RESULTS AND DISCUSSION 3.1. Polyaniline – Magnesium stanate (MgSnO3) composites Figure 1 shows the variation of ' as a function of frequency for polyaniline – MgSnO3 composites (different wt %). it is observed that, the dielectric constant is quite high at low frequency and decreases with increase in applied frequency but 30wt% of composite shows maximum value. The observed behavior may be due to Debye like relaxation mechanism taking place in all these materials.
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International Journal of
Mechanical Engineering and Technology (IJMET), ISSN 0976 – 6340(Print), ISSN 0976 – 6359(Online), Volume 5, Issue 11, November (2014), pp. 13-16 © IAEME 1 0 % P M S 3 0% P M S 5 0% P M S 15 0 .0 5 .0 x 1 0 6 1 .0 x 1 0 7 1 .5 x 1 0 7 2 .0 x 1 0 7 2 .5 x 1 0 7 4 .0 x 1 0 3 .5 x 1 0 3 .0 x 1 0 2 .5 x 1 0 2 .0 x 1 0 1 .5 x 1 0 1 .0 x 1 0 5 .0 x 1 0 6 6 6 6 6 6 6 5 0 .0 e' F e rq u e n c y Figure 1: Variation of Dielectric constant as a function of frequency for Polyaniline – magnesium stanate composites 4. CONCLUSION Polyaniline composites with different weight percentages of Magnesium stanate (MgSnO3) in PANI were synthesized by chemical oxidative polymerization of monomer aniline. The results of Dielectric constant show a strong dependence on the weight percent of Magnesium stagnate (MgSnO3) in polyaniline. REFERENCES [1] V.R.Gowrikar, N.V. Vishwnathan, S.Jayadev, Polymer Science, Wiley Eastern Ltd., New Delhi, 1986. [2] M.D. Ingram, H. Staesche, K.S. Ryder, J. Power Sources 129(1)(2004)107 [3] A.F. Diaz, B. Hall, J. Rev. Dev. 27(1983) 342 [4] ST Wellinghoff, T. Kedrowski, S. Jenekhe and H. Ishida, J. Phys. Colloq. (France), 44, (1983) C3-677. [5] D.C.Trivedi, Handbook of Organic Conductive Molecules and Polymers, vol.11, John Wiley and Sons Ltd, 1997 [6] G.B. Street, T.C. Clarke, R.H. Geiss, V.Y. Lee, A. Nazzal,.P. Pfluger. . J.C. Scott, J. Phys. (Paris) Colloque, C3(6)(1983), 599. [7] S. Holta, T. Hosaka, W. Shimotsuma, Synth. Met.6 (1985) 317. [8] S.E. Lindsey, G.B. Street, Synth.Met.10 (1988) 67. [9] M. Salmon, A.F. Diaz, M. Krounbi, J.Bargon, Mol. Cryst. Liq. Cryst. 83 (1982)265. [10] M. Raghu, S.V. Subramanyam, Phys. Rev. B 43 (1991) 4236. [11] W. Schumann. Synth.Met.41-43 (1991) 429. [12] F. Selampinar, U. Akbulut, M.Y. Ozden, L. Toppare, Biomaterials(1997) 64, [13] R. Singh, R.P. Tandon V.S. Panwar, S. Chandra, J. Appl, Phys. 64 (4)(1991) 2504. [14] S. Kivelson, Phys. Rev. Lett 46 (1981) 1344.
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International Journal of
Mechanical Engineering and Technology (IJMET), ISSN 0976 – 6340(Print), ISSN 0976 – 6359(Online), Volume 5, Issue 11, November (2014), pp. 13-16 © IAEME 16 [15] S.C. Raghavendra, S. Khasim, M. Revanasiddappa, M.V.N. AmbikaPrasad, A.B. Kulkarni, Bull. Mater.Sci 26 (7) (2003) 733. [16] K.C. Patil, S.S. Manoharan, D. Gajapathy, in: P. Nicholas (Ed.), Hand Book of Ceramics and Composites, Synthesis and Properties, Vol. 1, Chereminision off Marcel and Pecker, Inc., New York and Basel.1990, p. 461. [17] SangshettyKalyane, Magnetic properties study of polyaniline-CeO2 composites at X-Band frequency. Deccan Journal of Chemistry.Vol.1, Issue-2, July 2014, p. 29-31 [18] SangshettyKalyane, Permeability study of Pani-Dy2O3 Composites in X-Band Frequency. Deccan Journal of Chemistry. Vol.1, Issue-2, July 2014, p. 33-35. [19] K C Sajjan, Muhammad Faisal, Khened B.S and Syed Khasim, “Humidity Sensing Properties of Polyaniline/Potassium Molybdate Composites”, International Journal of Electrical Engineering Technology (IJEET), Volume 4, Issue 2, 2013, pp. 179 - 186, ISSN Print: 0976-6545, ISSN Online: 0976-6553. [20] T. K. Vishnuvardhan, V. R. Kulkarni, C. Basavaraja, S C Raghavendra, M Revanasiddappa, Ambika Prasad Mvn and Do Sung Hu, “Synthesis Characterization and Study of Dielectric Properties of Conducting Co-Polymer of Panippy-Y2o3 Nanocomposites”, International Journal of Advanced Research in Engineering Technology (IJARET), Volume 4, Issue 6, 2013, pp. 278 - 287, ISSN Print: 0976-6480, ISSN Online: 0976-6499. [21] A.M.Bhavikatti, Dr.Subhash Kulkarni and Dr. Arunkumar, “Electromagnetic Studies on Nano-Sized Magnesium Ferrite”, International Journal of Electronics and Communication Engineering Technology (IJECET), Volume 2, Issue 2, 2011, pp. 8 - 15, ISSN Print: 0976- 6464, ISSN Online: 0976 –6472.
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