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Position of NENALAB in
GLOSOLAN
SOPs to harmonize in 2020-2021
SOPs to harmonize in 2020-2021
- Texture and coarse fraction
(pipette method and
hydrometer)
- Bulk density
SOPs to harmonize in 2020-2021
2018 2019 (ongoing) 2020
• Sample pre-treatment
• Inorganic carbon (CaCO3
eq.)
• OC Walkley and Black
• Total carbon (Dumas – dry
combustion)
Planned:
• pH in water 1:2.5
• pH in CaCl2 and KCl
• EC saturated paste
• EC 1:5
• Moisture content (NO)
Harmonized:
• Organic carbon by Tyurin*
• Bray I and II
• Mehlich I
• Mehlich III
• Olsen (global leader Gina)
• Total Nitrogen by Kjedhal
and Dumas
• Mineral Nitrogen (KCl 1 or
2 M)
• Soil particle-size
distribution (pipette
method and hydrometer)
• Texture and coarse
fraction (pipette method
and hydrometer)
• Bulk density
Identification of regional leaders
regional leaders should be confident using the methods they take the
leadership for
What shall a regional leader do?
- Contribute to prepare the SOP matrix
Identification of regional leaders
regional leaders should be confident using the methods they take the
leadership for
What shall a regional leader do?
- Contribute to prepare the SOP matrix
- Harmonize the information in the matrix from your region
Identification of regional leaders
regional leaders should be confident using the methods they take the
leadership for
What shall a regional leader do?
- Contribute to prepare the SOP matrix
- Harmonize the information in the matrix from your region
- Contribute to the global harmonization of information
- Contribute to draft/review/finalize the GLOSOLAN SOP
Each SOP has a regional leader serving as global leader too. The global
leader takes the overall responsibility for the writing of the SOP
Identification of regional leaders
regional leaders should be confident using the methods they take the
leadership for
2020 Regional leader 2021
• Texture and coarse fraction
(pipette method and
hydrometer)
• Dry bulk density
• Total heavy metals –
digestion using aqua ragia
method
• CEC by ammonium acetate
• Exchangeable bases
(calcium and magnesium) -
titration by EDTA
• Exchangeable bases
(Sodium and potassium) by
flamephotometer and AAS
• Available micronutrients
(Fe Zn Cu Mn Mo) –
extraction using DTPA
• Lebanon Sandra Yanni + Jordan
Nabeel (Hydrometer)
• Morocco Jamal Hallam, Morocco
Hana Nabil + Tunisia Rafla
(Pipette method)
• TBC (dry bulk density)
• NENALAB Chair and UAE Ayeda +
Tunisia Rafla (total HM)
• Yemen Hezam + Iran Karim +
Sudan Nuha (CEC)
• Morocco Karima+ Tunisia Rafla +
Syria Solaf (exch. Bases Ca and
Mg)
• Yemen Hezam + Morocco Karima
(exch. Bases Na and K)
• Jordan Nabeel + Iran Karim +
Syria Alaa + Yemen Hezam + (av.
Micronutrients)
• Boron in soil extract by
chloromin method
• total Boron- hot water
extract
• Chloride and Sulfate in soil
extract
• Soil water retention curve
(SWRC)
• Soil aggregates stability
GLOSOLAN SOPs
• All laboratories sending information and all authors
are acknowledged in the GLOSOLAN SOPs
GLOSOLAN SOPs
• All laboratories sending information and all authors
are acknowledged in the GLOSOLAN SOPs
Next NENALAB meetings
• How was your experience? How can we improve?
• Do you want to have it online again? (Poll)
For in person meetings laboratories should look for self-
financing their participation. RESOLAN meetings usually
take place in different countries every year – we need of
volunteering hosting countries.
Having online meetings will allow us to involve more
laboratories and to allocate to budget to other activities
(purchasing lab equipment, training, organization of PTs,
etc.)
FAO Soils Bulletin 74 – “Guidelines for
Quality Management in Soil and Plant
Laboratories” (Poll)
http://www.fao.org/3/W7295E/W7295
E00.htm
We received a request for
updating/reviewing this document,
what do you think? (Poll)
Very few people knew about this
document. Those that know about it
think that it needs revision.
GLOSOLAN PT
Is there any lab/country that would like to
become a GLOSOLAN PT sample provider?
All information and material on QA/QC is available at http://www.fao.org/global-soil-
partnership/pillars-action/5-harmonization/glosolan/qaqc/en/
And send me an email at
lucrezia.caon@fao.org
GLOSOLAN PT – Additional information
GLOSOLAN PT – Additional information
GLOSOLAN PT – Additional information
GLOSOLAN PT – Additional information
We are currently testing an online GLOSOLAN PT
submission system.
Laboratories participating in future GLOSOLAN PTs will use
this online platform to submit their results.
All laboratories and countries will be given the opportunity
to participate in the GLOSOLAN PT. At least 1 lab per
country will participate.
However, we encourage countries and regions to organize
national and regional PTs. Highly qualified labs should take
the leadership on this.
Additional information
• SOPs on the GLOSOLAN webpage
http://www.fao.org/global-soil-partnership/pillars-action/5-
harmonization/glosolan/sops/en/
• Equipment: bartering/donation system
Please send me an email (lucrezia.caon@fao.org) if you have
any equipment you would like to barter/donate
Register in GLOSOLAN and invite more
labs to register in the network
Some laboratories attending the meeting are note
registered in GLOSOLAN. You are registered once
you receive the GLOSOLAN registration letter and
certificate. If you did not receive it, you are not
registered.
Only registered laboratories receive GLOSOLAN and
NENALAB related emails. Registration is important,
please.
Global assessment
We sent you all an email with the assessment to
complete. Can you please revert to us by
Wednesday next week (17 June)?
These information will be used for awareness
raising and fund raising. As agreed, once ready, we
will send you the draft version of the report so
that you will have a further chance to review the
profile of your country.
National Soil Laboratory Networks
- All National Reference Laboratories to complete
the assessment we are sending you. Your inputs
will be used to create the webpage of your
National Soil Laboratory Network.
- Countries that already established National Soil
Laboratory Networks are being asked to share
their experience. We are preparing guidelines on
how to establish National Soil Laboratory
Networks, which will include these case studies
International Network on
Fertilizers Analysis
• Please let us know if you are analysis fertilizers and
if your lab would like to be involved in this sub-
network and the related discussion.
• Complete the questionnaire at
https://forms.gle/Z5kYUpH5f6rpn6zUA (these inputs will
be used to open the discussion at the launch
meeting of the network)
Thanks for attending the meeting
and workshop, we hope that you
enjoyed it.
All participants will receive a certificate of
participation by email
All presentations and video recording will be
made available on the NENALAB webpage

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NENALAB's Position and SOP Harmonization Plans in GLOSOLAN

  • 1. Position of NENALAB in GLOSOLAN
  • 2. SOPs to harmonize in 2020-2021
  • 3. SOPs to harmonize in 2020-2021 - Texture and coarse fraction (pipette method and hydrometer) - Bulk density
  • 4. SOPs to harmonize in 2020-2021 2018 2019 (ongoing) 2020 • Sample pre-treatment • Inorganic carbon (CaCO3 eq.) • OC Walkley and Black • Total carbon (Dumas – dry combustion) Planned: • pH in water 1:2.5 • pH in CaCl2 and KCl • EC saturated paste • EC 1:5 • Moisture content (NO) Harmonized: • Organic carbon by Tyurin* • Bray I and II • Mehlich I • Mehlich III • Olsen (global leader Gina) • Total Nitrogen by Kjedhal and Dumas • Mineral Nitrogen (KCl 1 or 2 M) • Soil particle-size distribution (pipette method and hydrometer) • Texture and coarse fraction (pipette method and hydrometer) • Bulk density
  • 5. Identification of regional leaders regional leaders should be confident using the methods they take the leadership for What shall a regional leader do? - Contribute to prepare the SOP matrix
  • 6. Identification of regional leaders regional leaders should be confident using the methods they take the leadership for What shall a regional leader do? - Contribute to prepare the SOP matrix - Harmonize the information in the matrix from your region
  • 7. Identification of regional leaders regional leaders should be confident using the methods they take the leadership for What shall a regional leader do? - Contribute to prepare the SOP matrix - Harmonize the information in the matrix from your region - Contribute to the global harmonization of information - Contribute to draft/review/finalize the GLOSOLAN SOP Each SOP has a regional leader serving as global leader too. The global leader takes the overall responsibility for the writing of the SOP
  • 8. Identification of regional leaders regional leaders should be confident using the methods they take the leadership for 2020 Regional leader 2021 • Texture and coarse fraction (pipette method and hydrometer) • Dry bulk density • Total heavy metals – digestion using aqua ragia method • CEC by ammonium acetate • Exchangeable bases (calcium and magnesium) - titration by EDTA • Exchangeable bases (Sodium and potassium) by flamephotometer and AAS • Available micronutrients (Fe Zn Cu Mn Mo) – extraction using DTPA • Lebanon Sandra Yanni + Jordan Nabeel (Hydrometer) • Morocco Jamal Hallam, Morocco Hana Nabil + Tunisia Rafla (Pipette method) • TBC (dry bulk density) • NENALAB Chair and UAE Ayeda + Tunisia Rafla (total HM) • Yemen Hezam + Iran Karim + Sudan Nuha (CEC) • Morocco Karima+ Tunisia Rafla + Syria Solaf (exch. Bases Ca and Mg) • Yemen Hezam + Morocco Karima (exch. Bases Na and K) • Jordan Nabeel + Iran Karim + Syria Alaa + Yemen Hezam + (av. Micronutrients) • Boron in soil extract by chloromin method • total Boron- hot water extract • Chloride and Sulfate in soil extract • Soil water retention curve (SWRC) • Soil aggregates stability
  • 9. GLOSOLAN SOPs • All laboratories sending information and all authors are acknowledged in the GLOSOLAN SOPs
  • 10. GLOSOLAN SOPs • All laboratories sending information and all authors are acknowledged in the GLOSOLAN SOPs
  • 11. Next NENALAB meetings • How was your experience? How can we improve? • Do you want to have it online again? (Poll) For in person meetings laboratories should look for self- financing their participation. RESOLAN meetings usually take place in different countries every year – we need of volunteering hosting countries. Having online meetings will allow us to involve more laboratories and to allocate to budget to other activities (purchasing lab equipment, training, organization of PTs, etc.)
  • 12. FAO Soils Bulletin 74 – “Guidelines for Quality Management in Soil and Plant Laboratories” (Poll) http://www.fao.org/3/W7295E/W7295 E00.htm We received a request for updating/reviewing this document, what do you think? (Poll) Very few people knew about this document. Those that know about it think that it needs revision.
  • 13. GLOSOLAN PT Is there any lab/country that would like to become a GLOSOLAN PT sample provider? All information and material on QA/QC is available at http://www.fao.org/global-soil- partnership/pillars-action/5-harmonization/glosolan/qaqc/en/ And send me an email at lucrezia.caon@fao.org
  • 14. GLOSOLAN PT – Additional information
  • 15. GLOSOLAN PT – Additional information
  • 16. GLOSOLAN PT – Additional information
  • 17. GLOSOLAN PT – Additional information We are currently testing an online GLOSOLAN PT submission system. Laboratories participating in future GLOSOLAN PTs will use this online platform to submit their results. All laboratories and countries will be given the opportunity to participate in the GLOSOLAN PT. At least 1 lab per country will participate. However, we encourage countries and regions to organize national and regional PTs. Highly qualified labs should take the leadership on this.
  • 18. Additional information • SOPs on the GLOSOLAN webpage http://www.fao.org/global-soil-partnership/pillars-action/5- harmonization/glosolan/sops/en/ • Equipment: bartering/donation system Please send me an email (lucrezia.caon@fao.org) if you have any equipment you would like to barter/donate
  • 19. Register in GLOSOLAN and invite more labs to register in the network Some laboratories attending the meeting are note registered in GLOSOLAN. You are registered once you receive the GLOSOLAN registration letter and certificate. If you did not receive it, you are not registered. Only registered laboratories receive GLOSOLAN and NENALAB related emails. Registration is important, please.
  • 20. Global assessment We sent you all an email with the assessment to complete. Can you please revert to us by Wednesday next week (17 June)? These information will be used for awareness raising and fund raising. As agreed, once ready, we will send you the draft version of the report so that you will have a further chance to review the profile of your country.
  • 21. National Soil Laboratory Networks - All National Reference Laboratories to complete the assessment we are sending you. Your inputs will be used to create the webpage of your National Soil Laboratory Network. - Countries that already established National Soil Laboratory Networks are being asked to share their experience. We are preparing guidelines on how to establish National Soil Laboratory Networks, which will include these case studies
  • 22. International Network on Fertilizers Analysis • Please let us know if you are analysis fertilizers and if your lab would like to be involved in this sub- network and the related discussion. • Complete the questionnaire at https://forms.gle/Z5kYUpH5f6rpn6zUA (these inputs will be used to open the discussion at the launch meeting of the network)
  • 23. Thanks for attending the meeting and workshop, we hope that you enjoyed it. All participants will receive a certificate of participation by email All presentations and video recording will be made available on the NENALAB webpage